As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:5581-75-9
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inquiryWe are leading fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Orga
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Min.Order:1 Gram
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Min.Order:1 Gram
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6-PHENYLHEXANOIC ACID Basic information Product Name: 6-PHENYLHEXANOIC ACID Synonyms: 6-Phenylhexanoic acid,99%;NSC 66179;RARECHEM AH CK 0156;BENZENEHEXANOIC ACID;6-PHENYLHEXANOIC ACID;6-Phenylhexanoic acid 98%;6-Phenylhexanoic acid, 98+%;6-Phe
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Min.Order:1 Kilogram
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Min.Order:1 Metric Ton
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Type:Trading Company
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Min.Order:0
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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Min.Order:1 bottle
Negotiable
Type:Lab/Research institutions
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Min.Order:0
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HANGZHOU TIANYE CHEMICALS Co.LTD , Located in Eastern Science and Innovation Park Hangzhou .We are a high-tech enterprise specialized in technical research and development, production, development and trade of chemical products. We supply Multiple so
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Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquiryChangzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa
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Type:Lab/Research institutions
inquirytrans 6-phenyl-5-hexenoic acid
6-phenylhexanic acid
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethyl acetate at 25℃; under 1551.4 Torr; for 1h; | 95% |
With platinum(IV) oxide; hydrogen In tetrahydrofuran at 20℃; for 1h; |
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; water; sodium hydrogencarbonate at 80℃; under 600.06 Torr; for 9h; Reagent/catalyst; Time; | 95% |
1-Diazo-6-phenylhexan-2-one
6-phenylhexanic acid
Conditions | Yield |
---|---|
With lithium perchlorate In acetonitrile at 26.85℃; Wolff rearrangement; Electrochemical reaction; | 94% |
With silver nanocluster In 1,4-dioxane; water at 60℃; | 92% |
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; bis(1,5-cyclooctadiene)nickel (0); zinc In N,N-dimethyl acetamide at 80℃; for 12h; | 90% |
Conditions | Yield |
---|---|
With oxygen; vanadium(V) oxychloride In acetic acid at 65℃; for 52h; | 81% |
With potassium hydroxide In 5,5-dimethyl-1,3-cyclohexadiene Reflux; | 78% |
Conditions | Yield |
---|---|
With 10% rhodium on carbon; water; sodium hydroxide at 100℃; under 675.068 Torr; for 6h; Pressure; | A 11% B 80% |
Conditions | Yield |
---|---|
With indium; ammonium chloride In tetrahydrofuran for 24h; Heating; | A 60% B 27% |
6-oxo-6-phenyl-hexanoic acid methyl ester
6-phenylhexanic acid
Conditions | Yield |
---|---|
With hydrazine hydrate | 56% |
Multi-step reaction with 2 steps 1: aq. NaOH / acetone / 25 °C / other temp., ΔΔH excit., ΔΔS excit. View Scheme |
carbon dioxide
2-bromo-5-phenylpentane
6-phenylhexanic acid
Conditions | Yield |
---|---|
With rubidium carbonate; diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; (6,6’-dimethyl-2,2'-bipyridine)nickel(II) dibromide In N,N-dimethyl-formamide at 10℃; under 750.075 Torr; for 20h; Schlenk technique; Sealed tube; Irradiation; | 52% |
6-phenyl-1-hexanol
A
pentylbenzene
B
6-phenylhexanic acid
C
1-pentenylbenzene
Conditions | Yield |
---|---|
With 10% rhodium on carbon; sodium hydroxide In water at 100℃; for 24h; Inert atmosphere; | A n/a B 50% C n/a |
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; water; sodium hydrogencarbonate at 80℃; under 600.06 Torr; for 6h; | A 19% B 7% |
sodium diethylmalonate
1-Bromo-4-phenylbutane
6-phenylhexanic acid
5-benzylthiophene-2-carboxylic acid
6-phenylhexanic acid
Conditions | Yield |
---|---|
With alkaline solution; nickel |
6-phenylhexanenitrile
6-phenylhexanic acid
Conditions | Yield |
---|---|
With potassium hydroxide |
Conditions | Yield |
---|---|
With hydrogenchloride; amalgamated zinc Verseifung und Behandlung des Reaktionsprodukts mit Wasserstoff in Alkohol bei Gegenwart von kolloidalem Palladium; | |
With hydrogenchloride; mercury; zinc | |
With triethylsilane; trifluoroacetic acid |
rac-(2-phenylbutyl)propanedioic acid
6-phenylhexanic acid
Conditions | Yield |
---|---|
at 160℃; |
4-oxo-6-phenylhexanoic acid
6-phenylhexanic acid
Conditions | Yield |
---|---|
With hydrogenchloride; amalgamated zinc |
Conditions | Yield |
---|---|
With potassium hydroxide; hydrazine hydrate; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol |
Conditions | Yield |
---|---|
With sodium hydroxide In acetone at 25℃; Kinetics; Thermodynamic data; other temp., ΔH excit., ΔS excit.; | |
With sodium hydroxide In tetrahydrofuran; water at 20℃; | 541 mg |
peracide phenyl-6 hexanoique
A
phenyl butyl ketone
B
1-Phenyl-1-pentanol
C
5-phenylpentan-1-ol
D
6-phenylhexanic acid
Conditions | Yield |
---|---|
In n-heptane at 98℃; Further byproducts given; | A 0.01 mol B 0.19 mol C 0.20 mol D 0.18 mol |
peracide phenyl-6 hexanoique
A
phenyl butyl ketone
B
1-Phenyl-1-pentanol
C
5-phenylpentan-1-ol
D
6-phenylhexanic acid
E
5-Phenylpentanoic acid
Conditions | Yield |
---|---|
In n-heptane at 98℃; Mechanism; Product distribution; | A 0.01 mol B 0.19 mol C 0.20 mol D 0.18 mol E 0.01 mol |
peracide phenyl-6 hexanoique
A
1-Phenyl-1-pentanol
B
5-phenylpentan-1-ol
C
6-phenylhexanic acid
D
5-Phenylpentanoic acid
Conditions | Yield |
---|---|
In n-heptane at 98℃; Further byproducts given; | A 0.19 mol B 0.20 mol C 0.18 mol D 0.01 mol |
peracide phenyl-7 heptanoique
A
6-phenyl-1-hexanol
B
6-phenylhexanic acid
C
7-phenylheptanoic acid
D
1-phenyl-2-hexanone
E
1-phenylhexan-1-ol
F
(+/-)-1-phenylhexan-2-ol
Conditions | Yield |
---|---|
In hexane at 69℃; Mechanism; Product distribution; | A 0.38 mol B 0.02 mol C 0.27 mol D n/a E 0.13 mol F 0.04 mol |
peracide phenyl-7 heptanoique
A
6-phenyl-1-hexanol
B
6-phenylhexanic acid
C
7-phenylheptanoic acid
D
1-phenylhexan-1-ol
Conditions | Yield |
---|---|
In hexane at 69℃; Further byproducts given; | A 0.38 mol B 0.02 mol C 0.27 mol D 0.13 mol |
6-chlorohexanoic acid
benzene
A
6-phenylhexanic acid
B
4-phenylhexanoic acid
C
5-phenylhexanoic acid
Conditions | Yield |
---|---|
With aluminium trichloride Product distribution; degree of isomerization of the alkyl chain; | A 42 % Chromat. B 1 % Chromat. C 57 % Chromat. |
5-oxo-6-phenylhexanoic acid
6-phenylhexanic acid
Conditions | Yield |
---|---|
With hydrazine Heating; |
6-phenylhexanic acid
Conditions | Yield |
---|---|
With sodium ethanolate; hydrazine hydrate at 180℃; |
Conditions | Yield |
---|---|
Verseifen des Reaktionsprodukts; |
methyl adipoyl chloride
6-phenylhexanic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 53 percent 2: 56 percent / hydrazine hydrate, base View Scheme | |
Multi-step reaction with 3 steps 1: 77 percent / AlCl3 2: aq. NaOH / acetone / 25 °C / other temp., ΔΔH excit., ΔΔS excit. View Scheme |
Conditions | Yield |
---|---|
With chloro-trimethyl-silane at 0 - 20℃; for 4h; Inert atmosphere; | 100% |
trioctyl(propyl-3-sulfonic acid)ammonium bis(trifluoromethylsulfonyl)imide In water at 90℃; for 24h; | 80% |
With chloro-trimethyl-silane at 0℃; | 2.88 g |
With hydrogenchloride In methanol for 24h; Heating / reflux; | |
With sulfuric acid for 3h; Reflux; |
Conditions | Yield |
---|---|
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 15h; Inert atmosphere; | 99% |
diazomethane
6-phenylhexanic acid
6-phenyl-hexanoic acid methyl ester
Conditions | Yield |
---|---|
In diethyl ether at 20℃; for 1h; Inert atmosphere; | 96% |
6-phenylhexanic acid
6-phenylhexanoyl chloride
Conditions | Yield |
---|---|
With thionyl chloride | 94% |
With phosphorus pentachloride | |
With thionyl chloride; benzene |
Conditions | Yield |
---|---|
With triethylsilane; tris(pentafluorophenyl)borate In dichloromethane at 20℃; | 93% |
With triethylsilane; tris(pentafluorophenyl)borate In dichloromethane at 20℃; for 20h; | 93% |
6-phenylhexanic acid
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; | 91.6% |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In diethyl ether at 25℃; for 4h; | 91% |
Multi-step reaction with 2 steps 1: 2.88 g / TMSCl / 0 °C 2: 76 percent / DIBAL-H / tetrahydrofuran; toluene / 2 h / 0 °C View Scheme | |
With diborane In tetrahydrofuran |
6-phenylhexanic acid
Conditions | Yield |
---|---|
With sulfuric acid at 100℃; for 2h; | 85% |
6-phenylhexanic acid
(2S,3S,4R)-2-amino-3,4-di-O-benzyl-1-O-(2,3-di-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)octadec-6-ene-1,3,4-triol
(2S,3S,4R)-3,4-di-O-benzyl-1-O-(2,3-di-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-2-(6-phenylhexanoylamino)octadec-6-ene-1,3,4-triol
Conditions | Yield |
---|---|
Stage #1: 6-phenylhexanic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide for 0.5h; Stage #2: (2S,3S,4R)-2-amino-3,4-di-O-benzyl-1-O-(2,3-di-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)octadec-6-ene-1,3,4-triol With N-ethyl-N,N-diisopropylamine In dichloromethane; N,N-dimethyl-formamide for 18h; | 85% |
6-phenylhexanic acid
Conditions | Yield |
---|---|
With thionyl chloride In dichloromethane at 20℃; for 5h; Inert atmosphere; | 85% |
Conditions | Yield |
---|---|
Stage #1: 6-phenylhexanic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0℃; for 0.166667h; Inert atmosphere; Stage #2: C28H44N4O8*C2HF3O2 With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 12h; Inert atmosphere; | 84% |
6-phenylhexanic acid
2-hydroxymethyl-18-crown-6
Conditions | Yield |
---|---|
With dmap; silica gel; dicyclohexyl-carbodiimide at 20℃; for 24h; Steglich Esterification; Inert atmosphere; | 79% |
6-phenylhexanic acid
trans-4-hydroxycyclohexylamine
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 25℃; for 16h; | 77.8% |
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 10℃; for 10h; | 15.3% |
tert-butyl (4-aminocyclohexyl)carbamate
6-phenylhexanic acid
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 25℃; for 12h; | 77.4% |
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide at 0 - 20℃; for 8.5h; | 76% |
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane Reflux; |
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 25℃; for 12h; | 76% |
Conditions | Yield |
---|---|
Stage #1: 6-phenylhexanic acid With oxalyl dichloride In dichloromethane at 0 - 20℃; for 14h; Stage #2: With aluminum (III) chloride In dichloromethane for 20.5h; Inert atmosphere; | 75% |
With PPA | |
Multi-step reaction with 2 steps 1: SOCl2 2: AlCl3 / CS2 View Scheme | |
With oxalyl dichloride In dichloromethane at 0 - 20℃; for 1h; |
6-(8-oxo-5,6,7,8-tetrahydro-naphthalen-2-yl)-pyridine-2-sulfonamide
6-phenylhexanic acid
N-(6-phenyl-hexanoyl)-6-(8-oxo-5,6,7,8-tetrahydro-naphthalen-2-yl)-pyridine-2-sulfonamide
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 16h; | 75% |
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 25℃; for 20h; | 75% |
6-phenylhexanic acid
1-[(R)-1-(tert-butyldimethylsilyloxy)-4-(6-aminoindol-1-yl)-2-butyl]imidazole-4-carboxamide
1-[(R)-1-(tert-butyldimethylsilyloxy)-4-(6-(6-phenylhexanoylamino)indol-1-yl)-2-butyl]imidazole-4-carboxamide
Conditions | Yield |
---|---|
Stage #1: 6-phenylhexanic acid With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide In dichloromethane at 20℃; for 0.666667h; Stage #2: 1-[(R)-1-(tert-butyldimethylsilyloxy)-4-(6-aminoindol-1-yl)-2-butyl]imidazole-4-carboxamide In dichloromethane at 20℃; for 4h; | 74.8% |
phenyl sulfamate
6-phenylhexanic acid
phenyl (6-phenylhexanoyl)sulfamate
Conditions | Yield |
---|---|
Stage #1: 6-phenylhexanic acid With oxalyl dichloride In dichloromethane; N,N-dimethyl-formamide at 0 - 20℃; for 0.75h; Inert atmosphere; Stage #2: phenyl sulfamate With dmap; triethylamine In dichloromethane; N,N-dimethyl-formamide Inert atmosphere; | 74% |
(3,5-dichloropyridin-4-yl)hydrazine
6-phenylhexanic acid
N'-(3,5-dichloropyridin-4-yl)-6-phenylhexanehydrazide
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; | 71% |
6-phenylhexanic acid
(E)-6-phenyl-2-hexenoic acid
Conditions | Yield |
---|---|
Stage #1: 6-phenylhexanic acid With Zn(2,2,6,6-tetramethylpiperidine)2*2LiCl In tetrahydrofuran at -40℃; for 1.5h; Inert atmosphere; Sealed tube; Stage #2: With bis(η3-allyl-μ-chloropalladium(II)); Allyl acetate In tetrahydrofuran at -40 - 60℃; for 3h; Inert atmosphere; Sealed tube; diastereoselective reaction; | 69% |
6-phenylhexanic acid
cis-4-aminocyclohexanol
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 25℃; for 16h; | 67.4% |
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 10℃; for 10h; | 15.3% |
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