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(4-Methoxyphenyl)acetaldehyde cas 5703-26-4Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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4-[(E)-2-(4-Methoxy-phenyl)-vinyl]-morpholine
4-Methoxyphenylacetaldehyde
Conditions | Yield |
---|---|
With aq. acid for 1h; Ambient temperature; | 100% |
4-methoxy-phenyl acetic acid methyl ester
4-Methoxyphenylacetaldehyde
Conditions | Yield |
---|---|
With diisobutylaluminium hydride In toluene at -78℃; for 1.16667 - 1.25h; | 100% |
With diisobutylaluminium hydride In toluene at -70℃; for 0.5h; | 81% |
With diisobutylaluminium hydride In dichloromethane; toluene at -78℃; for 1.5h; Inert atmosphere; | 80% |
Conditions | Yield |
---|---|
With Dess-Martin periodane In dichloromethane at 0 - 20℃; for 1h; | 100% |
With Dess-Martin periodane In dichloromethane at 0 - 20℃; for 1h; | 100% |
With Dess-Martin periodane In dichloromethane at 0 - 20℃; for 1h; | 100% |
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine; osmium(VIII) oxide; [bis(acetoxy)iodo]benzene; water In tetrahydrofuran at 25℃; for 8h; Inert atmosphere; | 97% |
Stage #1: Estragole With ozone In dichloromethane at -78℃; Stage #2: With (Z,Z,Z)-4,4'-bis[4-(diphenylphosphino)styryl]stilbene In dichloromethane at -78 - 23℃; for 0.5h; Stage #3: With erythrosine B In tetrahydrofuran for 1h; Irradiation; | 91% |
bei der Ozonspaltung; |
4-Methoxyphenylacetaldehyde
Conditions | Yield |
---|---|
With bis[dicarbonylcyclopentadienylruthenium(I)] In tetrahydrofuran-d8 at 20℃; Inert atmosphere; Irradiation; | 97% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate In benzene at 45℃; for 2.5h; | 96% |
With indium(III) chloride In tetrahydrofuran at 25℃; for 0.166667h; Rearrangement; | 90% |
With oxovanadium(V) ethoxydichloride In ethanol at 20℃; for 4h; Rearrangement; | 90% |
Conditions | Yield |
---|---|
With Halomonas elongata/Co imm pyridoxal phosphate In toluene at 37℃; for 0.25h; pH=7.5; Flow reactor; Enzymatic reaction; | 95% |
4-Methoxyphenylacetaldehyde
Conditions | Yield |
---|---|
With triethylsilane; palladium on activated charcoal In tetrahydrofuran at 20℃; for 2h; Fukuyama reduction; | 93% |
(E/Z)-1-methoxy-4-(2-methoxyvinyl)benzene
4-Methoxyphenylacetaldehyde
Conditions | Yield |
---|---|
With oxalyl dichloride In ethanol; chloroform; water at 20℃; for 1h; | 93% |
With formic acid In dichloromethane for 16h; Reflux; | 85% |
With trifluoroacetic acid In dichloromethane at 0 - 20℃; for 16h; Inert atmosphere; | 66% |
Conditions | Yield |
---|---|
With C48H36Cl4N8Zn2(2+)*2Cl(1-); oxygen at 20℃; for 4h; Reagent/catalyst; Irradiation; | 90.7% |
Conditions | Yield |
---|---|
With Pyridine-2,6-dicarboxylic acid; iron(II) tetrafluoroborate hexahydrate; iodosylbenzene In chloroform at 20℃; for 20h; Molecular sieve; regioselective reaction; | 90% |
With ammonium persulfate; Pd(E-2-(benzylthio)-N-{(2-methoxynaphthalene-1-yl)methylene}benzenamine)Cl; 1-butyl-3-methylimidazolium Tetrafluoroborate In water at 70℃; for 0.25h; Wacker Oxidation; Microwave irradiation; regioselective reaction; | 85% |
With iodosylbenzene; 5,5'-dinitro-N,N'-ethylenebis(salicylideneaminato) manganese(III)(hexafluorophosphate) In acetonitrile at 25℃; | 48% |
diethyl ether
4-methoxy-phenyl acetic acid methyl ester
4-Methoxyphenylacetaldehyde
Conditions | Yield |
---|---|
With diisobutylaluminium hydride; sodium hydrogencarbonate In toluene | 90% |
(methoxymethyl)triphenylphosphonium chloride
4-methoxy-benzaldehyde
4-Methoxyphenylacetaldehyde
Conditions | Yield |
---|---|
Stage #1: (methoxymethyl)triphenylphosphonium chloride; 4-methoxy-benzaldehyde With lithium hexamethyldisilazane In tetrahydrofuran Wittig Olefination; Stage #2: With hydrogenchloride In tetrahydrofuran; water Reflux; | 90% |
Stage #1: (methoxymethyl)triphenylphosphonium chloride With sodium hexamethyldisilazane In tetrahydrofuran at 0℃; for 0.5h; Stage #2: 4-methoxy-benzaldehyde In tetrahydrofuran at 0 - 20℃; for 2h; Stage #3: With water; toluene-4-sulfonic acid In acetonitrile at 0 - 20℃; for 6h; | 53% |
4-Methoxystyrene
bis-[(trifluoroacetoxy)iodo]benzene
4-Methoxyphenylacetaldehyde
Conditions | Yield |
---|---|
Stage #1: 4-Methoxystyrene; bis-[(trifluoroacetoxy)iodo]benzene In dichloromethane for 0.25h; Stage #2: With silica gel In dichloromethane Further stages.; | 85% |
Conditions | Yield |
---|---|
With cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate; 5,5′-bis(trifluoromethyl)-2,2′-bipyridine In 1-methyl-pyrrolidin-2-one; water at 25℃; for 8h; Inert atmosphere; Autoclave; | 84% |
With [CpRu(6-Ph2P-Py-2-yl)(MeCN)][PF6(1-)]; water In acetone at 70℃; for 24h; | 99.8 % Spectr. |
Conditions | Yield |
---|---|
Stage #1: Chloroiodomethane With TurboGrignard In tetrahydrofuran at -20℃; for 0.000277778h; Flow reactor; Stage #2: 4-methoxy-benzaldehyde In tetrahydrofuran at -20℃; for 0.000444444h; Flow reactor; Stage #3: With sodium hydroxide In tetrahydrofuran; water | 84% |
(p-methoxybenzyl)pentacarbonylmanganese(I)
HMn(CO)4(P(CH3)2C6H5)
A
4-Methoxyphenylacetaldehyde
nonacarbonyl(dimethylphenylphosphine)dimanganese
Conditions | Yield |
---|---|
With carbon monoxide; Triphenylphosphine oxide In benzene-d6 Kinetics; High Pressure; in C6D6 at 45°C, initial concn. ranges were 3.8E-3 to 2.4E-2 M p-MeOC6H4CH2Mn(CO)5, 3.3E-2 to 0.16 M HMn(CO)4(PMe2Ph) (typically 10-fold excess), 0.040 to 0.30 M OPPh3, and 1.1 to 2.3 atm (8.1E-3 to 1.7E-2 M) of CO; followed by NMR and FTIR; | A 80% B >99 |
vinylene carbonate
4-methoxyphenylboronic acid
4-Methoxyphenylacetaldehyde
Conditions | Yield |
---|---|
Stage #1: 4-methoxyphenylboronic acid With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; tetrahydroxydiboron; 1,3-bis(bis(4-methoxyphenyl)phosphino)propane; Hexamethylbenzene In 1,2-dichloro-ethane at 25℃; for 0.0166667h; Schlenk technique; Inert atmosphere; Stage #2: vinylene carbonate In water at 90℃; for 1h; Sealed tube; | 72% |
4-Methoxystyrene
A
2-(4-methoxyphenyl)oxirane
B
4-Methoxyphenylacetaldehyde
C
4-methoxy-benzaldehyde
Conditions | Yield |
---|---|
With dihydrogen peroxide for 5h; Catalytic behavior; | A 69% B 9% C 22% |
With 2,6-dichloropyridine N-oxide; carbonyl(1,4,8,11,15,18,22,25-octaisopentylphthalocyaninato)ruthenium(II) In toluene at 90℃; for 24h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; | A 64 %Chromat. B 13 %Chromat. C 21 %Chromat. |
Conditions | Yield |
---|---|
With 4-methylpyridine-1-oxide; oxochromium(V) complex of dichloro tetramethylsalen IIf In acetonitrile at 25℃; | A 19% B 65% |
With pyridine N-oxide; oxochromium(V) complex of dichloro tetramethylsalen IIf In acetonitrile at 23℃; Rate constant; Product distribution; Mechanism; effect of donor ligands on the rate of further olefins; ligand-induced cleavage of olefins by oxochromium(V); (18)O-labeling studies of oxochromium(V); | |
With 5C16H36N(1+)*(x)H2O*MnO39SiW11(5-); dihydrogen peroxide In water; acetonitrile at 80℃; for 6h; |
(E)-4-methoxyphenylacetaldehyde O-methyloxime
4-Methoxyphenylacetaldehyde
Conditions | Yield |
---|---|
With formaldehyd; Amberlyst 15 In water; acetone for 29h; Ambient temperature; | 65% |
(E)-2-(4-methoxyphenyl)acetaldehyde oxime
4-Methoxyphenylacetaldehyde
Conditions | Yield |
---|---|
With ozone In dichloromethane at -78℃; for 0.166667h; Inert atmosphere; | 65% |
A
4-Methoxyphenylacetaldehyde
B
4-methoxy-benzaldehyde
C
syringic aldehyde
Conditions | Yield |
---|---|
With oxygen; vanadium(V) oxytriisopropoxide In acetonitrile at 25 - 40℃; under 760.051 Torr; for 12h; Irradiation; Sealed tube; | A 6% B 38% C 61% |
Conditions | Yield |
---|---|
With sodium hypophosphite; nickel In ethanol; water at 40 - 60℃; for 2h; | 53% |
methyl 2-(p-methoxyphenyl)-1-methylthioethyl sulfoxide
4-Methoxyphenylacetaldehyde
Conditions | Yield |
---|---|
With sulfuric acid; sodium hydrogencarbonate In methanol | 53% |
With sulfuric acid In ethanol |
Conditions | Yield |
---|---|
Stage #1: 4-methoxy-aniline With hydrogenchloride; sodium nitrite In water Stage #2: 4-tolyl vinyl ether With sodium hydrogencarbonate; calcium carbonate; copper dichloride In water; acetone at 25 - 30℃; pH=3 - 4; | 49% |
Conditions | Yield |
---|---|
With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; cadmium(II) chloride In acetonitrile at -5℃; for 0.05h; | 48% |
Stage #1: 4-methoxyphenyl-acetic chloride With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; N,N-dimethyl-formamide; cadmium(II) chloride In acetonitrile at -5 - 0℃; for 0.666667h; Stage #2: With hydrogenchloride; water In acetonitrile pH=3; Product distribution / selectivity; | 48% |
Rusenmund reduction; |
dicobalt octacarbonyl
Trifluoro-methanesulfonic acid 4-methoxy-benzyl ester
4-Methoxyphenylacetaldehyde
Conditions | Yield |
---|---|
With triethylsilane; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sodium acetate In acetonitrile at 25℃; for 16h; Schlenk technique; Inert atmosphere; | 47% |
3-(4′-methoxyphenyl)-prop-1,2-diol
4-Methoxyphenylacetaldehyde
Conditions | Yield |
---|---|
With lead(IV) acetate In benzene Ambient temperature; | 45% |
Conditions | Yield |
---|---|
With sodium ethanolate In diethyl ether at -35℃; for 0.166667h; | 99% |
4-Methoxyphenylacetaldehyde
1-(isocyanomethyl)-4-methoxybenzene
acetic acid
C20H23NO5
Conditions | Yield |
---|---|
In dichloromethane at 20℃; Passerini Condensation; | 99% |
4-Methoxyphenylacetaldehyde
Glyoxilic acid
5-hydroxy-4-(4-methoxy-phenyl)-5H-furan-2-one
Conditions | Yield |
---|---|
With morpholin hydrochloride In 1,4-dioxane; water for 24h; Heating / reflux; | 98% |
With water; morpholin hydrochloride In 1,4-dioxane for 24h; Reflux; | 98% |
morpholine
4-Methoxyphenylacetaldehyde
4-[(E)-2-(4-Methoxy-phenyl)-vinyl]-morpholine
Conditions | Yield |
---|---|
In chloroform at 20℃; for 3h; Molecular sieve; | 96% |
In benzene Heating; | 86% |
In chloroform at 20℃; for 5h; Molecular sieve; Schlenk technique; |
4-Methoxyphenylacetaldehyde
1-bromo-3,5-dimethoxybenzene
(+/-)-1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)ethanol
Conditions | Yield |
---|---|
Stage #1: 1-bromo-3,5-dimethoxybenzene With iodine; magnesium In tetrahydrofuran for 0.5h; Heating; Stage #2: 4-Methoxyphenylacetaldehyde In tetrahydrofuran for 0.5h; Grignard reaction; Heating; | 96% |
With n-butyllithium In tetrahydrofuran at -78℃; for 0.5h; Inert atmosphere; | 75% |
4-Methoxyphenylacetaldehyde
(2-cyclohex-1-enyl-ethyl)-methyl-amine
(2-cyclohex-1-enyl-ethyl)-(4-methoxy-styryl)-methyl-amine
Conditions | Yield |
---|---|
In toluene | 95.3% |
With diethyl ether |
4-Methoxyphenylacetaldehyde
benzamidrazone
3-phenyl-5-(p-methoxybenzene)-1,2,4-triazine
Conditions | Yield |
---|---|
Stage #1: 4-Methoxyphenylacetaldehyde With iodine; dimethyl sulfoxide at 100℃; for 2h; Green chemistry; Stage #2: benzamidrazone at 100℃; for 1h; Green chemistry; | 95% |
Conditions | Yield |
---|---|
With methanol; aluminum (III) chloride In acetonitrile at 80℃; for 6h; | 94% |
1.3-propanedithiol
4-Methoxyphenylacetaldehyde
2-(4-methoxyphenyl)methyl-1,3-dithiane
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In dichloromethane at 0 - 20℃; Molecular sieve; | 93% |
With boron trifluoride diethyl etherate In dichloromethane; water at 0 - 20℃; for 14h; Molecular sieve; Inert atmosphere; | 91% |
4-Methoxyphenylacetaldehyde
Phenyl azide
4-(4-methoxyphenyl)-1-phenyl-1H-[1,2,3]triazole
Conditions | Yield |
---|---|
With 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate; potassium hydroxide at 20℃; for 0.666667h; Green chemistry; regioselective reaction; | 92% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dimethyl sulfoxide at 25℃; for 0.5h; regioselective reaction; | 90% |
In dimethyl sulfoxide at 20℃; for 1h; | 80% |
4-Methoxyphenylacetaldehyde
(2S)-(-)-3,4-dimethyl-2-<(p-methoxyphenyl)methyl>-1-<(1R)-1-phenylethyl>-1,2,5,6-tetrahydropyridine
Conditions | Yield |
---|---|
With polyphosphoric acid at 45℃; for 18h; Inert atmosphere; | 91% |
4-Methoxyphenylacetaldehyde
3,6-dimethylthio-1,2,4,5-tetrazine
5-(p-methoxyphenyl)-3-methylsulfanyl-1,2,4-triazine
Conditions | Yield |
---|---|
With pyrrolidine; 1,1,1,3',3',3'-hexafluoro-propanol at 25℃; | 91% |
4-Methoxyphenylacetaldehyde
formamide
N-[2-(4-methoxyphenyl)ethyl]formamide
Conditions | Yield |
---|---|
With formic acid at 180℃; for 2h; Leukardt-Wallach Amination; | 90% |
4-Methoxyphenylacetaldehyde
2,2-difluoro-2-(4-methoxyphenyl)ethanol
Conditions | Yield |
---|---|
Stage #1: 4-Methoxyphenylacetaldehyde With L-proline In N,N-dimethyl acetamide at 20℃; for 0.5h; Stage #2: With N-fluorobis(benzenesulfon)imide In N,N-dimethyl acetamide at 20℃; for 4h; | 90% |
Conditions | Yield |
---|---|
With phosphoric acid at 30℃; for 8h; | 90% |
4-Methoxyphenylacetaldehyde
2-(3,4-dimethoxyphenyl)-ethylamine
7,12-O,O'-dimethylcoclaurine
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid at 20 - 70℃; for 5h; Reagent/catalyst; | 89.01% |
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