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Wuhan Fortuna Chemical Co.,Ltd

1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; ...... Appearance:Colorless Transparent Liquid Package:25kg/drum;100kg/drum App

Stock 3-Methyl-3-methoxybutanol CAS 56539-66-3 with best price and fast delivery

Cas:56539-66-3

Min.Order:5 Liter

FOB Price: $50.0

Type:Trading Company

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 3-methoxy-3-methylbutan-1-ol

Cas:56539-66-3

Min.Order:1

Negotiable

Type:Other

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Factory price Cosmetic METHOXYMETHYLBUTANOL 56539-66-3 Manufacturer

Cas:56539-66-3

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for t

High purity 3-Methyl-3-methoxybutanol 98% TOP1 supplier in China

Cas:56539-66-3

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

3-Methoxy-3-methylbutanol

Cas:56539-66-3

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

3-Methyl-3-methoxybutanol

Cas:56539-66-3

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Wholesale price CAS 56539-66-3 with best price

Cas:56539-66-3

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W

3-Methyl-3-methoxybutanol:cas;56539-66-3

Cas:56539-66-3

Min.Order:1 Metric Ton

FOB Price: $20.0 / 30.0

Type:Trading Company

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Hebei yanxi chemical co.,LTD.

1. Best quality in your requirement 2. Competitive price in China market 3. mature Technical support 4. Professional logistic support 5 . Full experience of large numbers containers loading in Chinese sea port 6 Fast shipment by reputed shipping

3-Methyl-3-methoxybutanol

Cas:56539-66-3

Min.Order:1 Kilogram

FOB Price: $9.5 / 10.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

3-Methyl-3-methoxybutanol CAS No.: 56539-66-3 Formula: C6H14O2 Molecular Weight: 118.17 Melting Point: -50ºC

3-Methoxy-3-methyl-1-butanol CAS: 56539-66-3

Cas:56539-66-3

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

1-Butanol,3-methoxy-3-methyl- 56539-66-3

Cas:56539-66-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Qingdao Beluga Import and Export Co., LTD

3-Methyl-3-methoxybutanol CAS:56539-66-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organi

3-Methyl-3-methoxybutanol CAS:56539-66-3

Cas:56539-66-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

1-Butanol,3-methoxy-3-methyl-

Cas:56539-66-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

1-Butanol,3-methoxy-3-methyl-

Cas:56539-66-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanxi Ankesi Biotechnology Co., Ltd

Our Advantage 1. Rich experience We specialize in this filed for many years, our APIs exported to all over the world and and we established long friendly relations of cooperation with our clients. 2. Great quality,purity and favorable Good qual

High quality CAS 56539-66-3 3-Methyl-3-methoxybutanol

Cas:56539-66-3

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Changchun Artel lmport and Export trade company

Price, service, company and transport advantage: 1.place of origin china with super quality by reasonable price. 2. it's customers' right to choose the package (ems, dhl, fedex, ups); 3. it's custo

BEST PRICE/methyl hydroperoxide

Cas:56539-66-3

Min.Order:10 Gram

Negotiable

Type:Trading Company

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Hebei Miheng Trading Co., Ltd.

3-Methyl-3-methoxybutanol CAS 56539-66-3 Our advantage 1.Top quality: Using high quality material and establishing a strict quality control system,assigning specific persons in charge of each part of production,from raw material purchase to a

3-Methyl-3-methoxybutanol CAS 56539-66-3

Cas:56539-66-3

Min.Order:1 Kilogram

FOB Price: $10.0 / 50.0

Type:Trading Company

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Triumph International Development Limilted

Appearance:off-white to white solid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for Synthesis API and Research Transportation:By Sea/Air/Courier Port:Qingdao

3-Methyl-3-methoxybutanol 56539-66-3

Cas:56539-66-3

Min.Order:1 Kilogram

FOB Price: $16.0 / 20.0

Type:Lab/Research institutions

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

methyl hydroperoxide CAS NO.56539-66-3

Cas:56539-66-3

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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Hefei Zhaobo Technology Co., Ltd.

3-Methyl-3-methoxybutanol CAS 56539-66-3 Description Purity: 99% Min Application: Intermediates Appearance: Powder Package: Bag Delivery: 3-5days Our Advantage & Service 1.Top quality: Using high quality material and establishing a

3-Methyl-3-methoxybutanol CAS 56539-66-3

Cas:56539-66-3

Min.Order:1 Kilogram

FOB Price: $10.0 / 50.0

Type:Trading Company

inquiry

SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

3-Methyl-3-methoxybutanol

Cas:56539-66-3

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

1-Butanol,3-methoxy-3-methyl-

Cas:56539-66-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High purity 3-Methyl-3-methoxybutanol

Cas:56539-66-3

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:colourless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediat

1-Butanol,3-methoxy-3-methyl-

Cas:56539-66-3

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

3-methoxy-3-methyl-1-butano

Cas:56539-66-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

Factory Supplier3-Methyl-3-methoxybutanol

Cas:56539-66-3

Min.Order:0

Negotiable

Type:Trading Company

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EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

methyl hydroperoxide CAS NO.56539-66-3

Cas:56539-66-3

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

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TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

3-Methyl-3-methoxybutanol

Cas:56539-66-3

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

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Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

methyl hydroperoxide CAS NO.56539-66-3

Cas:56539-66-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

methyl hydroperoxide CAS NO.56539-66-3

Cas:56539-66-3

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

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Synthetic route

4,4-dimethyl-1,3-dioxane
766-15-4

4,4-dimethyl-1,3-dioxane

solfit
56539-66-3

solfit

Conditions
ConditionsYield
With diisobutylaluminium hydride In benzene for 2h; Heating;90%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

methanol
67-56-1

methanol

solfit
56539-66-3

solfit

Conditions
ConditionsYield
With sodium iodide at 40 - 50℃; Green chemistry;51%
With Na34[{MoVI6O21(H2O)6}12{(MoV2O4)30(OAc)22(H2O)16}] In water-d2 at 65℃; for 65h;
4,4-dimethyl-1,3-dioxane
766-15-4

4,4-dimethyl-1,3-dioxane

methanol
67-56-1

methanol

solfit
56539-66-3

solfit

Conditions
ConditionsYield
With sulfuric acid
With sulfuric acid at 40 - 90℃;
4,4-dimethyl-1,3-dioxane
766-15-4

4,4-dimethyl-1,3-dioxane

A

3-methyl-butane-1,3-diol
2568-33-4

3-methyl-butane-1,3-diol

B

solfit
56539-66-3

solfit

Conditions
ConditionsYield
With porous sulfonic acid type strongly acidic ion exchange resin In methanol at 55℃; for 1h;
solfit
56539-66-3

solfit

p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

3-methoxy-3-methylbutyl 4-methylbenzenesulfonate
869370-01-4

3-methoxy-3-methylbutyl 4-methylbenzenesulfonate

Conditions
ConditionsYield
With dmap; triethylamine In dichloromethane at 20℃; for 16h;95.5%
With pyridine at 0 - 20℃; for 16h; Inert atmosphere;78%
With triethylamine In dichloromethane at 20℃; for 3h;49%
With pyridine at 0 - 20℃;
With triethylamine In dichloromethane at 20℃; for 21h;
solfit
56539-66-3

solfit

ethylaluminum dichloride
563-43-9

ethylaluminum dichloride

[Cl2Al(OCH2CH2C(CH3)2OCH3)]2
463966-53-2

[Cl2Al(OCH2CH2C(CH3)2OCH3)]2

Conditions
ConditionsYield
In hexane (Ar); slow addn. of a soln. of alcohol in hexane to a soln. of aluminiumcompd. in hexane at 0°C, stirring for 0.5 h, slow warming to roo m temp.; evapn., drying in vac. crystn. (toluene, 5°C, 3 d); elem. anal.;91%
trimethylaluminium dimer

trimethylaluminium dimer

solfit
56539-66-3

solfit

[(CH3)2Al(μ-O-CH2CH2C(CH3)2-OCH3)]2

[(CH3)2Al(μ-O-CH2CH2C(CH3)2-OCH3)]2

Conditions
ConditionsYield
In pentane byproducts: CH4; Ar-atmosphere; dropwise addn. of ligand to AlMe3 at -78°C, stirring for 2 h, then at room temp. for 12 h; solvent removal (vac.), dissoln. in PhMe, crystn. (-30°C); elem. anal.;91%
solfit
56539-66-3

solfit

p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

methoxy-3-methylbutyl 4-methylbenzenesulfonate

methoxy-3-methylbutyl 4-methylbenzenesulfonate

Conditions
ConditionsYield
With dmap; triethylamine In dichloromethane at 20℃;91%
solfit
56539-66-3

solfit

3-methoxy-3-methylbutanal
181134-54-3

3-methoxy-3-methylbutanal

Conditions
ConditionsYield
Swern oxidation;89%
With pyridine; oxalyl dichloride; dimethyl sulfoxide; triethylamine In dichloromethane at -78 - 4℃; for 1.25h; Swern oxidation;89%
With oxalyl dichloride; dimethyl sulfoxide; triethylamine In dichloromethane at -60 - 20℃; Swern oxidation;41%
Swern oxidation;
With Dess-Martin periodane In chloroform at 20℃; for 5h; Cooling with ice;
solfit
56539-66-3

solfit

trimethyl gallium
1445-79-0

trimethyl gallium

[(CH3)2Ga(μ-O-CH2CH2C(CH3)2-OCH3)]2

[(CH3)2Ga(μ-O-CH2CH2C(CH3)2-OCH3)]2

Conditions
ConditionsYield
In pentane byproducts: CH4; Ar-atmosphere; dropwise addn. of ligand to GaMe3 at room temp., stirringovernight; distn. off of solvent, sublimation (74°C/0.1 mbar), then distn. (67°C/0.1 mbar) and crystn. on standing at -30°C for 1 h; elem. anal.;89%
solfit
56539-66-3

solfit

triethylsilyl formate
18296-01-0

triethylsilyl formate

3-methoxy-3-methyl-1-(triethylsiloxy)butane
80920-24-7

3-methoxy-3-methyl-1-(triethylsiloxy)butane

Conditions
ConditionsYield
With [Ru(κ1-OAc)(κ2-OAc)(κ3-1,1,1-tris(diphenylphosphinomethyl)ethane)] In acetonitrile at 70℃; for 1h; Inert atmosphere; Schlenk technique;88%
With tris(2-diphenylphosphinoethyl)phosphine; iron(II) acetate In dichloromethane Glovebox; Inert atmosphere; Heating;87%
solfit
56539-66-3

solfit

1-chloro-4-(trifluoromethyl)-2-vinylbenzene

1-chloro-4-(trifluoromethyl)-2-vinylbenzene

1-chloro-2-(2-(3-methoxy-3-methylbutoxy)ethyl)-4-(trifluoromethyl)benzene

1-chloro-2-(2-(3-methoxy-3-methylbutoxy)ethyl)-4-(trifluoromethyl)benzene

Conditions
ConditionsYield
With phosphazene base-P4-tert-butyl In hexane; m-xylene at 70℃; for 24h; Inert atmosphere;82%
solfit
56539-66-3

solfit

2-trifluoromethylbenzenesulfonyl chloride
776-04-5

2-trifluoromethylbenzenesulfonyl chloride

3-methoxy-3-methylbutyl 2-(trifluoromethyl)benzenesulfonate

3-methoxy-3-methylbutyl 2-(trifluoromethyl)benzenesulfonate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 4h;81%
solfit
56539-66-3

solfit

2,6-dichlorostyrene
28469-92-3

2,6-dichlorostyrene

1,3-dichloro-2-(2-(3-methoxy-3-methylbutoxy)ethyl)benzene

1,3-dichloro-2-(2-(3-methoxy-3-methylbutoxy)ethyl)benzene

Conditions
ConditionsYield
With phosphazene base-P4-tert-butyl In hexane; m-xylene at 100℃; for 24h; Inert atmosphere;81%
solfit
56539-66-3

solfit

propionyl chloride
79-03-8

propionyl chloride

3-methoxy-3-methylbutyl propanoate
1080673-42-2

3-methoxy-3-methylbutyl propanoate

Conditions
ConditionsYield
In tetrahydrofuran for 2.25h; Inert atmosphere;80.1%
solfit
56539-66-3

solfit

methyl chloroformate
79-22-1

methyl chloroformate

3-methoxy-3-methylbutyl methoxyformate
1203544-43-7

3-methoxy-3-methylbutyl methoxyformate

Conditions
ConditionsYield
With pyridine In tetrahydrofuran Inert atmosphere;80%
solfit
56539-66-3

solfit

4-((6-chloro-1-ethyl-1H-pyrazolo[3,4-d]pyrimidin-4-yl)aminomethyl)benzenesulfonamide

4-((6-chloro-1-ethyl-1H-pyrazolo[3,4-d]pyrimidin-4-yl)aminomethyl)benzenesulfonamide

4-((1-ethyl-6-(3-methoxy-3-methylbutoxy)-1H-pyrazolo[3,4-d]pyrimidin-4-yl)aminomethyl)benzenesulfonamide

4-((1-ethyl-6-(3-methoxy-3-methylbutoxy)-1H-pyrazolo[3,4-d]pyrimidin-4-yl)aminomethyl)benzenesulfonamide

Conditions
ConditionsYield
Stage #1: solfit With potassium tert-butylate at 20℃; for 0.333333h;
Stage #2: 4-((6-chloro-1-ethyl-1H-pyrazolo[3,4-d]pyrimidin-4-yl)aminomethyl)benzenesulfonamide at 70℃; for 10h;
76%
oxalyl dichloride
79-37-8

oxalyl dichloride

solfit
56539-66-3

solfit

bis(3-methoxy-3-methylbutylethane)-1,2-dioate
1203544-56-2

bis(3-methoxy-3-methylbutylethane)-1,2-dioate

Conditions
ConditionsYield
In dichloromethane at 0℃;73.3%
solfit
56539-66-3

solfit

3-methoxy-3-methylbutyl 4-methylbenzenesulfonate
869370-01-4

3-methoxy-3-methylbutyl 4-methylbenzenesulfonate

1-methoxy-3-(3-methoxy-3-methylbutoxy)-1,1-dimethylpropane
1203544-39-1

1-methoxy-3-(3-methoxy-3-methylbutoxy)-1,1-dimethylpropane

Conditions
ConditionsYield
Stage #1: solfit With sodium hydride In tetrahydrofuran at 40 - 70℃; Inert atmosphere;
Stage #2: 3-methoxy-3-methylbutyl 4-methylbenzenesulfonate In tetrahydrofuran
71.7%
solfit
56539-66-3

solfit

3-oxapentanoic acid
627-03-2

3-oxapentanoic acid

3-methoxy-3-methylbutyl 2-ethoxyacetate
1203544-47-1

3-methoxy-3-methylbutyl 2-ethoxyacetate

Conditions
ConditionsYield
With toluene-4-sulfonic acid at 40℃; for 5h;71.2%
solfit
56539-66-3

solfit

3-chloro-isonicotinonitrile
68325-15-5

3-chloro-isonicotinonitrile

3-(3-methoxy-3-methylbutoxy)pyridine-4-carbonitrile

3-(3-methoxy-3-methylbutoxy)pyridine-4-carbonitrile

Conditions
ConditionsYield
Stage #1: solfit With sodium hydride In tetrahydrofuran; mineral oil at 0 - 20℃; for 1h; Inert atmosphere;
Stage #2: 3-chloro-isonicotinonitrile In tetrahydrofuran; mineral oil at 20℃; Inert atmosphere;
67%
Stage #1: solfit With sodium hydride In tetrahydrofuran at 0 - 20℃; for 0.65h;
Stage #2: 3-chloro-isonicotinonitrile In tetrahydrofuran at 20℃;
67%
1-bromo-2,2-dimethoxyethane
7252-83-7

1-bromo-2,2-dimethoxyethane

solfit
56539-66-3

solfit

3-(2,2-dimethoxyethoxy)-1-methoxy-1,1-dimethylpropane
1203544-32-4

3-(2,2-dimethoxyethoxy)-1-methoxy-1,1-dimethylpropane

Conditions
ConditionsYield
Stage #1: solfit With sodium hydride In tetrahydrofuran at 40 - 70℃; Inert atmosphere;
Stage #2: 1-bromo-2,2-dimethoxyethane In tetrahydrofuran at 70℃; for 16.5h; Inert atmosphere;
65.5%
carbon disulfide
75-15-0

carbon disulfide

solfit
56539-66-3

solfit

potassium 3-methoxy-3-methyl-1-butylxanthate

potassium 3-methoxy-3-methyl-1-butylxanthate

Conditions
ConditionsYield
Stage #1: solfit With potassium hydroxide at 20℃; for 2h;
Stage #2: carbon disulfide
62.8%
solfit
56539-66-3

solfit

2-methoxyacetic acid
625-45-6

2-methoxyacetic acid

3-methoxy-3-methylbutyl 2-methoxyacetate
1203544-46-0

3-methoxy-3-methylbutyl 2-methoxyacetate

Conditions
ConditionsYield
Stage #1: 2-methoxyacetic acid With oxalyl dichloride In dichloromethane; N,N-dimethyl-formamide at 20 - 40℃;
Stage #2: solfit With pyridine In dichloromethane; N,N-dimethyl-formamide at 0℃; Inert atmosphere;
61.1%
solfit
56539-66-3

solfit

3-Chloro-2-methylpropene
563-47-3

3-Chloro-2-methylpropene

1-methoxy-1,1-dimethyl-3-(2-methylprop-2-enyloxy)propane
1093653-61-2

1-methoxy-1,1-dimethyl-3-(2-methylprop-2-enyloxy)propane

Conditions
ConditionsYield
With sodium hydroxide; tetra(n-butyl)ammonium hydroxide In water at 70℃; for 10h;61%
solfit
56539-66-3

solfit

2-methyl-8-(6-(naphthalen-1-yl)pyridin-2-yl)-1,2,3,4-tetrahydroquinoline

2-methyl-8-(6-(naphthalen-1-yl)pyridin-2-yl)-1,2,3,4-tetrahydroquinoline

hafnium tetrachloride
13499-05-3

hafnium tetrachloride

C27H26HfN2

C27H26HfN2

Conditions
ConditionsYield
In toluene at 20℃; for 4h; Glovebox; Cooling with ice;57.1%
formic acid
64-18-6

formic acid

solfit
56539-66-3

solfit

3-methoxy-3-methylbutyl formate
1203544-40-4

3-methoxy-3-methylbutyl formate

Conditions
ConditionsYield
at 20℃; for 6h;56.3%
solfit
56539-66-3

solfit

acrolein
107-02-8

acrolein

3-(3-methoxy-3-methylbutoxy)propanal
1203544-54-0

3-(3-methoxy-3-methylbutoxy)propanal

Conditions
ConditionsYield
With hydrogenchloride In water at 40℃; for 72h; Subdued light;55.9%
solfit
56539-66-3

solfit

pentafluorobenzenesulonyl chloride
832-53-1

pentafluorobenzenesulonyl chloride

3-methoxy-3-methylbutyl 2,3,4,5,6-pentafluorobenzenesulfonate

3-methoxy-3-methylbutyl 2,3,4,5,6-pentafluorobenzenesulfonate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 2h;51%
solfit
56539-66-3

solfit

N-[5-chloro-2-(3-methoxy-3-methylbutoxy)phenyl]-N'-(5-cyano-2-pyrazinyl)urea
660851-16-1

N-[5-chloro-2-(3-methoxy-3-methylbutoxy)phenyl]-N'-(5-cyano-2-pyrazinyl)urea

Conditions
ConditionsYield
46%
solfit
56539-66-3

solfit

N-{(3E)-5-tert-butyl-1-methyl-2-[(2R)-tetrahydrofuran-2-ylmethyl]-1,2-dihydro-3H-pyrazol-3-ylidene}-2-fluoro-5-(trifluoromethyl)benzamide
1140917-51-6

N-{(3E)-5-tert-butyl-1-methyl-2-[(2R)-tetrahydrofuran-2-ylmethyl]-1,2-dihydro-3H-pyrazol-3-ylidene}-2-fluoro-5-(trifluoromethyl)benzamide

N-{(3E)-5-tert-butyl-1-methyl-2-[(2R)-tetrahydrofuran-2-ylmethyl]-1,2-dihydro-3H-pyrazol-3-ylidene}-2-(3-methoxy-3-methylbutoxy)-5-(trifluoromethyl)benzamide
1140917-56-1

N-{(3E)-5-tert-butyl-1-methyl-2-[(2R)-tetrahydrofuran-2-ylmethyl]-1,2-dihydro-3H-pyrazol-3-ylidene}-2-(3-methoxy-3-methylbutoxy)-5-(trifluoromethyl)benzamide

Conditions
ConditionsYield
Stage #1: solfit With potassium tert-butylate In tetrahydrofuran for 0.166667h;
Stage #2: N-{(3E)-5-tert-butyl-1-methyl-2-[(2R)-tetrahydrofuran-2-ylmethyl]-1,2-dihydro-3H-pyrazol-3-ylidene}-2-fluoro-5-(trifluoromethyl)benzamide In tetrahydrofuran for 3h;
41%
Stage #1: solfit With potassium tert-butylate In tetrahydrofuran for 0.166667h;
Stage #2: N-{(3E)-5-tert-butyl-1-methyl-2-[(2R)-tetrahydrofuran-2-ylmethyl]-1,2-dihydro-3H-pyrazol-3-ylidene}-2-fluoro-5-(trifluoromethyl)benzamide In tetrahydrofuran for 3h;
41%

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