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Cas:563-43-9
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Cas:563-43-9
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Cas:563-43-9
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inquiryNo. Test item Index 1 performance transparent liquid 2 aluminum (Wt%) 20.2
Cas:563-43-9
Min.Order:1600 Kilogram
FOB Price: $1.0
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inquiryEthylaluminum dichloride solution 563-43-9 Appearance:Colorless liquid Assay(TiTration by EDTA):1.03M Appearance:Colorless liquid Package:drum Application:industral Transportation:by sea Port:Shanghai, Ningbo
Cas:563-43-9
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Cas:563-43-9
Min.Order:1 Kilogram
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Min.Order:10 Milligram
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Cas:563-43-9
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Ethylaluminum dichloride CAS#563-43-9 Storage:Keep container tightly closed in a dry, cool and well-ventilated place. Package:25Kg/drum, 150Kg/drum, 200kg/drum, According to request. Transportation:By sea, by air.
Good Price, prompt shipment Application:Catalytic agent; Petrochemical additive; Used in organic synthesis
Cas:563-43-9
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inquiryConditions | Yield |
---|---|
With aluminium und anschliessend mit AlCl3; | |
With aluminium trichloride; aluminium |
Conditions | Yield |
---|---|
at 180 - 190℃; |
Conditions | Yield |
---|---|
With iodine bei Ausschluss von Feuchtigkeit und Sauerstoff; | |
With aluminium trichloride bei Ausschluss von Feuchtigkeit und Sauerstoff; |
Conditions | Yield |
---|---|
With iodine bei Ausschluss von Feuchtigkeit und Sauerstoff; | |
With aluminium trichloride bei Ausschluss von Feuchtigkeit und Sauerstoff; |
gem-1,1-bis(dichloroalumino)ethane
ethene
aluminium
A
ethylaluminum dichloride
B
diethylaluminium chloride
Conditions | Yield |
---|---|
In n-heptane byproducts: (CH2CHCHCH2CH(CH3))x; High Pressure; (Ar); to a soln. of Al-compound and Al added ethylene (20 bar pressure) under stirring at 100-150°C for 16 h; distd. in vacuo at 50°C; elem. anal.; |
Conditions | Yield |
---|---|
In n-heptane byproducts: (CH2CHCHCH2CH(CH3))x; High Pressure; (Ar); to a soln. of Al-compound added ethylene (20 bar pressure) under stirring at 100°C for 24 h; distd. in vacuo at 50°C; elem. anal.; |
aluminium trichloride
triisobutylaluminum
A
ethylaluminum dichloride
B
diisobutylaluminum chloride
Conditions | Yield |
---|---|
In diethyl ether; toluene all manipulations under dry, O2 free N2 atm.; AlCl3 dissolved in Et2O, soln. of iso-Bu3Al in toluene added at -78°C, allowed to warm to room temp., stirred and refluxed for for 3, stirred at room temp. for 48 h h; |
Conditions | Yield |
---|---|
In benzene Addn. of Et2AlCl to benzene soln. of Ti-compd. at 50°C.; Electronic absorption spectroscopy.; |
Conditions | Yield |
---|---|
In toluene byproducts: C2H6; (Ar); using Schlenk techniques; addn. of HCl saturated toluene to react. mixt. with Et2AlCl; |
Conditions | Yield |
---|---|
In benzene Decompn. of Ti-compd.; Slow pptn. of TiCl2 from the soln. on a time scale of days-to-months obsd. by elecronic absorption spectroscopy.; |
Conditions | Yield |
---|---|
In benzene Addn. of Et3Al to benzene soln. of Ti-compd. at 50°C.; Electronic absorption spectroscopy.; |
Conditions | Yield |
---|---|
In toluene Kinetics; 25°C; UV/VIS monitoring; |
gem-1,1-bis(dichloroalumino)ethane
A
aluminium trichloride
B
ethylaluminum dichloride
Conditions | Yield |
---|---|
With HCl In methyl cyclohexane byproducts: ethane; passing of dry HCl into stirred soln. of Al-compnd. (1 h); solvent removal, anal.; |
1-(chloroethylaluminum)-2-(dichloroaluminum)ethane
ethene
ethylaluminum dichloride
Conditions | Yield |
---|---|
In further solvent(s) (Ar); ethylene bubbled through a soln. of Al-compound in a mixture of hydrocarbons (C10-C14) at 150°C for 48 h; distd.; elem. anal.; |
1-(chloroethylaluminum)-2-(dichloroaluminum)ethane
A
AlCl2CH2CH2Al(Cl)C2H4Al(Cl)C2H5
B
ethylaluminum dichloride
C
diethylaluminium chloride
Conditions | Yield |
---|---|
heated to 100°C; |
diethylaluminium chloride
A
ethylaluminum dichloride
B
ethylgallium dichloride
Conditions | Yield |
---|---|
Heating; | A 50 %Spectr. B 50 %Spectr. |
Conditions | Yield |
---|---|
Heating; | A 33 %Spectr. B 66 %Spectr. |
Conditions | Yield |
---|---|
In benzene at 25°C, after 4 days were warmed to 70°C for 20h; evapn.; | 100% |
Conditions | Yield |
---|---|
In benzene react. at room temp. for 4 days, warmed to 70°C for 20h; evapn.; | 100% |
Conditions | Yield |
---|---|
With triphenylphosphine In benzene mixing of Ti-compd. in benzene with cyclopentadiene, then addn. of Al-compd. and phosphine (molar ratio of Ti/Al/PPh3 = 1/2/2); monitored by ESR; | 100% |
With triphenylphosphine In benzene mixing of Ti-compd. in benzene with cyclopentadiene, then addn. of Al-compd. and phosphine (molar ratio of Ti/Al/PPh3 = 1/3/2); monitored by ESR; | 100% |
Conditions | Yield |
---|---|
With triphenylphosphine In benzene mixing of Ti-compd. in benzene with cyclopentadiene, then addn. of Al-compd. (molar ratio of Ti/Al/PPh3 = 1/4/4); monitored by ESR; | 100% |
methanol
ethylaluminum dichloride
succinoyl dichloride
methyl 4-oxohexanoate
Conditions | Yield |
---|---|
In dichloromethane at -40℃; for 3.5h; | 99% |
Stage #1: ethylaluminum dichloride; succinoyl dichloride In dichloromethane at -40℃; for 3.5h; Stage #2: methanol In dichloromethane at -40℃; | 99% |
ethylaluminum dichloride
Conditions | Yield |
---|---|
In toluene at 100℃; for 16h; Schlenk technique; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
In pentane Ar-atmosphere; addn. of equimolar amt. of EtAlCl2 in pentane to P(SiMe3)3 in pentane; stirring (room temp., 24 h); decantation, evapn. of residual solvent from the solid; elem. anal.; | 97.6% |
Conditions | Yield |
---|---|
In neat (no solvent) anhyd. BaCl2 and C2H5AlCl2 heated at 50°C for 5 h with stirring,soln. cooled to 0°C, (C2H5)2AlCl added under N2 atm.; mixt. cooled to 0°C, n-heptane added, ppt. filtered off, washed with n-hexane and dried in vacuo; elem. anal.; | 97% |
Conditions | Yield |
---|---|
In neat (no solvent) anhyd. CaCl2 added to C2H5AlCl2 and mixt. heated with stirring at 110°C for 5 h under N2 atm.; soln. cooled to room temp., n-heptane added, ppt. filtered off, washed with n-hexane and dried in vacuo; elem. anal.; | 96.7% |
ethylaluminum dichloride
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane at -35 - 20℃; Inert atmosphere; Glovebox; | 96% |
Conditions | Yield |
---|---|
In neat (no solvent) anhyd. CaCl2 added to C2H5AlCl2 and mixt. heated with stirring at 110°C for 5 h under N2 atm.; soln. cooled to -10°C, n-heptane added, ppt. filtered off, washed with n-hexane and dried in vacuo; elem. anal.; | 95.8% |
Conditions | Yield |
---|---|
In neat (no solvent) anhyd. SrCl2 and C2H5AlCl2 heated at 100°C for 18 h with stirring, (C2H5)2AlCl added to soln. under N2 atm.; mixt. cooled to 0°C, n-heptane added, ppt. filtered off, washed with n-hexane and dried in vacuo; elem. anal.; | 95.7% |
allyl 2-(4-methoxyphenylimino)-2-(4-methoxyphenyl)acetate
ethylaluminum dichloride
diethylaluminium chloride
4-methoxy-N-ethylaniline
Conditions | Yield |
---|---|
Stage #1: allyl 2-(4-methoxyphenylimino)-2-(4-methoxyphenyl)acetate; ethylaluminum dichloride; diethylaluminium chloride In 1,2-dimethoxyethane; hexane at 40℃; Inert atmosphere; Stage #2: With water; Rochelle's salt In 1,2-dimethoxyethane; hexane at 20℃; for 0.5h; | 95% |
ethylaluminum dichloride
N-phenyl-S-(4-methylphenyl)sulfoximidoyl chloride
S-ethyl-S-(4-methylphenyl)-N-phenylsulfoximine
Conditions | Yield |
---|---|
In dichloromethane at -78℃; for 1h; | 94% |
ethylaluminum dichloride
Conditions | Yield |
---|---|
In toluene inert atmosphere; cooling soln. of Ti-compd. in toluene (-78°C)addn. of AlCl2Et in toluene, stirring (-78°C, 30 min); not isolated, quenched with HCl isolation of org. compds.; | 94% |
1-tert-butoxy-2-propanol
ethylaluminum dichloride
[Cl2Al(OCH(CH3)CH2OC(CH3)3)]2
Conditions | Yield |
---|---|
In hexane (Ar); addn. of a soln. of alcohol in hexane to a soln. of aluminium compd. in hexane at 0°C; evapn., drying in vac., recrystn. (hexane); elem. anal.; | 94% |
ethylaluminum dichloride
Conditions | Yield |
---|---|
In toluene inert atmosphere; cooling soln. of Ti-compd. in toluene (-78°C)addn. of AlCl2Et in toluene, stirring (-78°C, 30 min); not isolated, quenched with HCl isolation of org. compds.; | 93% |
ethylaluminum dichloride
Conditions | Yield |
---|---|
In toluene byproducts: 1,2-dimethylcyclopentane; inert atmosphere; cooling soln. of Ti-compd. in toluene (-78°C)addn. of AlCl2Et in toluene, stirring (-78°C, 30 min); not isolated, quenched with HCl isolation of org. compds.; | 93% |
Conditions | Yield |
---|---|
In tetrahydrofuran byproducts: KCl; (N2 or Ar); pptn. of carbonyl dianion in situ, cooling (-78°C), addn. of CH3CH2AlCl2 (-78°C), warming (room temp.), stirring (1 h), addn. of Lewis base ligand, stirring (30 min, 25°C); solvent removing (vac.), extn. (CH2Cl2), graphite sedimentation, filtn. (cannula), concn., storing (-30°C), decantation, concn.; | 92% |
In tetrahydrofuran; dichloromethane byproducts: KCl; molar ratio Cr complex:AlCl2R:TMEDA 2:2:1, cooling (-78°C), stirring (3 h, 25°C); solvent exchange, filtn., concn., crystn. (-30°C); | 90% |
Conditions | Yield |
---|---|
In tetrahydrofuran byproducts: KCl; (N2 or Ar); pptn. of carbonyl dianion in situ, cooling (-78°C), addn. of CH3CH2AlCl2 (-78°C), warming (room temp.), stirring (1 h), addn. of Lewis base ligand, stirring (30 min, 25°C); solvent removing (vac.), extn. (CH2Cl2), graphite sedimentation, filtn. (cannula), concn., storing (-30°C), decantation, concn.; | 92% |
Conditions | Yield |
---|---|
In tetrahydrofuran byproducts: KCl; (N2 or Ar); pptn. of carbonyl dianion in situ, cooling (-78°C), addn. of CH3CH2AlCl2 (-78°C), warming (room temp.), stirring (1 h), addn. of Lewis base ligand, stirring (30 min, 25°C); solvent removing (vac.), extn. (CH2Cl2), graphite sedimentation, filtn. (cannula), concn., storing (-30°C), decantation, concn.; | 92% |
ethylaluminum dichloride
3,6-endomethylene-1,2,3,6-tetrahydrophthalic anhydride
(+/-)-(2,3-endo)-3-(1-oxopropyl)bicyclo<2.2.1>hept-5-ene-2-carboxylic acid
Conditions | Yield |
---|---|
In hexane; dichloromethane at -10℃; for 1h; | 91% |
Conditions | Yield |
---|---|
In hexane (Ar); slow addn. of a soln. of alcohol in hexane to a soln. of aluminiumcompd. in hexane at 0°C, stirring for 0.5 h, slow warming to roo m temp.; evapn., drying in vac. crystn. (toluene, 5°C, 3 d); elem. anal.; | 91% |
Conditions | Yield |
---|---|
With triphenylphosphine In benzene mixing of Ti-compd. in benzene with cyclopentadiene, then addn. of Al-compd. and phosphine (molar ratio of Ti/Al/PPh3 = 1/5/5); monitored by ESR; | 90% |
ethylaluminum dichloride
Conditions | Yield |
---|---|
In diethyl ether dropping of ethereal soln. of Al compd. into suspn. of Co complex at 20°C; elem. anal.; | 90% |
Conditions | Yield |
---|---|
In dichloromethane added at -70 deg C, then 7-13 h at room temperature; | 89% |
Conditions | Yield |
---|---|
In dichloromethane -70 deg C, then 20 deg C, 8 h; | 88% |
In dichloromethane added at -70 deg C, then 7-13 h at room temperature; | 88% |
ethylaluminum dichloride
E-4-hexen-3-one
Conditions | Yield |
---|---|
In dichloromethane added at -70 deg C, then 7-13 h at at room temperature. AlCl3 can be added as well.; | 87% |
ethylaluminum dichloride
1-cyclohex-3-enyl-propan-1-one
Conditions | Yield |
---|---|
In dichloromethane added at -70 deg C, then 7-13 h at at room temperature.; | 87% |
ethylaluminum dichloride
(S)-3-butyl-2-methanesulfonyloxy-3-heptanol
(S)-6-methyl-5-decanone
Conditions | Yield |
---|---|
In hexane; dichloromethane | 87% |
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