CAS No.573-56-8,2,6-DINITROPHENOL Suppliers

: 69-72-7
salicylic acid

A: 51-28-5
2,4-Dinitrophenol

B: 573-56-8
2,6-dinitrophenol

Conditions

Conditions	Yield
With ammonium cerium(IV) nitrate In acetonitrile at 20℃; for 12h;	A 95% B 3%

: 3535-67-9
2,6-dinitroanisole

: 573-56-8
2,6-dinitrophenol

Conditions

Conditions	Yield
With aluminum (III) chloride In dichloromethane at -5 - 25℃;	92%

: 18710-65-1
N-(2,6-dinitrophenyl)-α-alanine

A: 2-methyl-7-nitro-1H-benzimidazole 3-oxide

B: 573-56-8
2,6-dinitrophenol

Conditions

Conditions	Yield
With sodium hydroxide In 1,4-dioxane; water for 0.25h; Heating;	A 90% B n/a

: 4-[(2,6-dinitrophenyl)amino]butyric acid

A: 3-(7-nitro-3-oxido-1H-benzimidazol-2-yl)propionic acid

B: 573-56-8
2,6-dinitrophenol

Conditions

Conditions	Yield
With sodium hydroxide In 1,4-dioxane; water for 0.333333h; Heating;	A 83% B 7%

: N-(2,6-dinitrophenyl)-β-alanine

A: 2-methyl-7-nitro-1H-benzimidazole 3-oxide

B: 573-56-8
2,6-dinitrophenol

Conditions

Conditions	Yield
With sodium hydroxide In 1,4-dioxane; water for 0.166667h; Heating;	A 79% B 10%

: 88-75-5
2-hydroxynitrobenzene

A: 51-28-5
2,4-Dinitrophenol

B: 573-56-8
2,6-dinitrophenol

Conditions

Conditions	Yield
With perchloric acid; montmorillonite K10 supported ammonium nitrate at 50℃; for 1.5h;	A 73% B 23%
durch Nitrieren; Trennung durch fraktionierte Faellung des Gemisches der Kaliumsalze mit BaCl2;
With tetrachloromethane; nitrosylsulfuric acid at 30℃;
With nitric acid

: 108-95-2
phenol

A: 51-28-5
2,4-Dinitrophenol

B: 573-56-8
2,6-dinitrophenol

Conditions

Conditions	Yield
With thionyl chloride; bismuth subnitrate In dichloromethane at 20℃; for 2h;	A 72% B 14%

: 71-43-2
benzene

A: 51-28-5
2,4-Dinitrophenol

B: 100-02-7
4-nitro-phenol

C: 573-56-8
2,6-dinitrophenol

D: 98-95-3
nitrobenzene

E: 88-75-5
2-hydroxynitrobenzene

Conditions

Conditions	Yield
With nitric acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone at 30 - 35℃; for 24h; Irradiation;	A n/a B n/a C 62% D n/a E n/a

...Expand

: 88-75-5
2-hydroxynitrobenzene

: 573-56-8
2,6-dinitrophenol

Conditions

Conditions	Yield
With uronium nitrate In water; acetonitrile at 80℃; for 1h; Microwave irradiation; regioselective reaction;	60%
With sulfuric acid; nitric acid; acetic acid
durch Nitrierung;

: 71-43-2
benzene

: 573-56-8
2,6-dinitrophenol

Conditions

Conditions	Yield
With oxygen; nitric acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone In water at 30℃; for 24h; Irradiation; Large scale;	56%

: 108-95-2
phenol

A: 51-28-5
2,4-Dinitrophenol

B: 100-02-7
4-nitro-phenol

C: 573-56-8
2,6-dinitrophenol

D: 88-75-5
2-hydroxynitrobenzene

Conditions

Conditions	Yield
With trinitratooxovanadium(V) In dichloromethane for 0.00833333h; Ambient temperature; Further byproducts given;	A 51% B 9% C 1% D 32%

...Expand

: 626-23-3
Di-sec-butylamin

: 573-55-7
2-fluoro-1,3-dinitrobenzene

: 584-08-7
potassium carbonate

A: 573-56-8
2,6-dinitrophenol

B: 2,6-dinitrophenyl N,N-di-s-butylcarbamate

Conditions

Conditions	Yield
In dimethyl sulfoxide for 3h; Heating;	A 45% B 48%

...Expand

: 573-55-7
2-fluoro-1,3-dinitrobenzene

: 584-08-7
potassium carbonate

: 108-18-9
diisopropylamine

A: 573-56-8
2,6-dinitrophenol

B: 2,6-dinitrophenyl N,N-diisopropylcarbamate

Conditions

Conditions	Yield
In dimethyl sulfoxide for 3h; Heating;	A 29% B 42%

...Expand

: 69-72-7
salicylic acid

A: 51-28-5
2,4-Dinitrophenol

B: 573-56-8
2,6-dinitrophenol

C: 96-97-9
5-nitrosalicylic acid

D: 88-75-5
2-hydroxynitrobenzene

Conditions

Conditions	Yield
With ammonium cerium(IV) nitrate In acetonitrile at 50 - 60℃; for 0.25h; Further byproducts given;	A 24% B 13% C 37% D 5%

...Expand

: 69-72-7
salicylic acid

A: 51-28-5
2,4-Dinitrophenol

B: 573-56-8
2,6-dinitrophenol

C: 85-38-1
3-nitrosalicylic acid

D: 88-75-5
2-hydroxynitrobenzene

Conditions

Conditions	Yield
With ammonium cerium(IV) nitrate In acetonitrile at 50 - 60℃; for 0.25h; Further byproducts given;	A 24% B 13% C 31% D 5%
With ammonium cerium(IV) nitrate In acetonitrile at 50 - 60℃; for 0.25h; Further byproducts given;	A 24% B 13% C 24% D 5%

...Expand

: 50-78-2
aspirin

A: 51-28-5
2,4-Dinitrophenol

B: 573-56-8
2,6-dinitrophenol

C: 85-38-1
3-nitrosalicylic acid

D: 88-75-5
2-hydroxynitrobenzene

Conditions

Conditions	Yield
With ammonium cerium(IV) nitrate In acetonitrile at 60 - 70℃; for 0.25h; Further byproducts given;	A 24% B 13% C 31% D 5%

...Expand

: 50-78-2
aspirin

A: 51-28-5
2,4-Dinitrophenol

B: 573-56-8
2,6-dinitrophenol

C: 96-97-9
5-nitrosalicylic acid

D: 88-75-5
2-hydroxynitrobenzene

Conditions

Conditions	Yield
With ammonium cerium(IV) nitrate In acetonitrile at 60 - 70℃; for 0.25h; Further byproducts given;	A 24% B 13% C 31% D 5%

...Expand

: 509-14-8
tetranitromethane

: 71-43-2
benzene

A: 573-56-8
2,6-dinitrophenol

B: 71156-15-5
1-nitro-4-trinitromethylbenzene

C: 67483-29-8
phenyltrinitromethane

D: 88-89-1
2,4,6-Trinitrophenol

Conditions

Conditions	Yield
In dichloromethane at 20℃; for 48h; Irradiation; Further byproducts given. Title compound not separated from byproducts;	A 0.6% B 3% C 3.3% D 0.3%

...Expand

: 509-14-8
tetranitromethane

: 71-43-2
benzene

A: 573-56-8
2,6-dinitrophenol

B: 67483-29-8
phenyltrinitromethane

C: 88-89-1
2,4,6-Trinitrophenol

D: 157096-63-4
1,3-dinitro-5-trinitromethylbenzene

Conditions

Conditions	Yield
In dichloromethane at 20℃; for 48h; Irradiation; Further byproducts given. Title compound not separated from byproducts;	A 0.6% B 3.3% C 0.3% D 0.4%

...Expand

: 99-65-0
meta-dinitrobenzene

A: 51-28-5
2,4-Dinitrophenol

B: 573-56-8
2,6-dinitrophenol

Conditions

Conditions	Yield
With sulfuric acid at 140 - 150℃;

: 603-13-4
1,2,3-trinitrobenzene

: furan-2,3,5(4H)-trione pyridine (1:1)

: 573-56-8
2,6-dinitrophenol

: 3535-67-9
2,6-dinitroanisole

: 124-41-4
sodium methylate

: 573-56-8
2,6-dinitrophenol

: 85-38-1
3-nitrosalicylic acid

A: 573-56-8
2,6-dinitrophenol

B: 609-99-4
3,5-dinitrosalicylic acid

: 85365-92-0
3,5-dinitro-4-methoxybenzoic acid

: 573-56-8
2,6-dinitrophenol

Conditions

Conditions	Yield
With water at 170℃;

: 17973-92-1
isopicramic acid

: 573-56-8
2,6-dinitrophenol

Conditions

Conditions	Yield
Kochen der Diazoniumverbindung mit absol. Alkohol;
laesst sich in ein sehr explosives Diazoniumsalz ueberfuehren,das beim Kochen mit absol.Alkohol;

: 67329-16-2
4-hydroxy-3,5-dinitro-benzenesulfonic acid

: 573-56-8
2,6-dinitrophenol

Conditions

Conditions	Yield
With hydrogenchloride at 180 - 200℃; im Rohr;

: 64-17-5
ethanol

: 124-41-4
sodium methylate

: 606-21-3
1-chloro-2,6-dinitrobenzene

: 573-56-8
2,6-dinitrophenol

...Expand

: 606-21-3
1-chloro-2,6-dinitrobenzene

: 573-56-8
2,6-dinitrophenol

Conditions

Conditions	Yield
With sodium hydroxide
With methanol; ethanol; sodium methylate
With acetamide; sodium acetate at 170℃;
Stage #1: 1-chloro-2,6-dinitrobenzene With water at 50 - 85℃; Alkaline conditions; Large scale; Stage #2: With hydrogenchloride pH=1; Large scale;

: 108-95-2
phenol

A: 573-56-8
2,6-dinitrophenol

B: 67329-16-2
4-hydroxy-3,5-dinitro-benzenesulfonic acid

Conditions

Conditions	Yield
With sulfuric acid Eintragen des Reaktionsgemisches in Natriumnitrat-Loesung und Zufuegen von weiterer Natriumnitrat-Loesung und konz. Schwefelsaeure unter Erwaermen auf 102-105grad;

: 110-89-4
piperidine

: 3535-67-9
2,6-dinitroanisole

A: 573-56-8
2,6-dinitrophenol

B: 10156-50-0
1-piperidino-2,6-dinitrobenzene

C: 20650-73-1
2,6-dinitrophenoxide ion

Conditions

Conditions	Yield
In benzene

...Expand

: 573-56-8
2,6-dinitrophenol

: 22440-82-0
2,6-diaminophenol

Conditions

Conditions	Yield
With hydrogen; palladium 10% on activated carbon In ethanol	100%
With palladium 10% on activated carbon; hydrogen In methanol at 25℃; under 1050.11 Torr; for 3h;	100%
With hydrogen; palladium 10% on activated carbon In methanol	89%

: 573-56-8
2,6-dinitrophenol

: 603-87-2
2-amino-6-nitrophenol

Conditions

Conditions	Yield
With hydrogen; palladium 10% on activated carbon In ethyl acetate for 5h;	95%
With palladium 10% on activated carbon; hydrogen In methanol for 1h;	92%
With cyclohexene; palladium on activated charcoal In ethanol at 25℃; for 16h;	81%

: 573-56-8
2,6-dinitrophenol

: 65-85-0
benzoic acid

: 1523-16-6
2,6-dinitrophenyl benzoate

Conditions

Conditions	Yield
With iodine; triethylamine; triphenylphosphine In dichloromethane at 0 - 20℃; for 0.333333h;	89%
With pyridine; thionyl chloride at 0℃;

: 573-56-8
2,6-dinitrophenol

: 108-24-7
acetic anhydride

: 1523-09-7
2,6-dinitrophenyl acetate

Conditions

Conditions	Yield
With 2,3,4,5,7,8,9,10-octahydropyrimido[1,2-a]azepin-1-ium acetate In neat (no solvent) at 50℃; for 1h; Green chemistry;	89%

: 573-56-8
2,6-dinitrophenol

: 98-59-9
p-toluenesulfonyl chloride

: 88791-50-8
toluene-4-sulfonic acid 2,6-dinitro-phenyl ester

Conditions

Conditions	Yield
With N-ethyl-N,N-diisopropylamine In dichloromethane; water	86%
With triethylamine In dichloromethane	80%
With sodium carbonate

: 61941-89-7
5-(2-chlorophenyl)-2-furoyl chloride

: 573-56-8
2,6-dinitrophenol

: 2,6-dinitrophenyl 5-(2-chlorophenyl)-2-furoate

Conditions

Conditions	Yield
With PEG-400; sodium hydroxide In dichloromethane; water at 20℃; for 1h;	82%

: 573-56-8
2,6-dinitrophenol

: 1889-01-6
(1,4-phenylenedioxy)di(acetyl chloride)

: [4-(2,6-Dinitro-phenoxycarbonylmethoxy)-phenoxy]-acetic acid 2,6-dinitro-phenyl ester

Conditions

Conditions	Yield
With polyethylene glycol-400; sodium hydroxide In dichloromethane; water for 1h; Ambient temperature;	81%

: copper(II) perchlorate hexahydrate

: 573-56-8
2,6-dinitrophenol

: 149-73-5
trimethyl orthoformate

: 105744-50-1
di-[μ-methoxo-(2,6-dinitrophenolato)(pyridine)copper(II)]

Conditions

Conditions	Yield
With pyridine; piperidine In methanol dissolving Cu-salt and ester in abs. MeOH; keeping for 1 d at room temp.; addn. of dinitrophenol, pyridine and piperidine in MeOH; complete crystn. within 1 d; washing (MeOH); drying (vac. desiccator); elem. anal.;	78%

...Expand

: 573-56-8
2,6-dinitrophenol

: 88-10-8
N,N-diethylcarbamyl chloride

: 2,6-dinitrophenyl N,N-diethylcarbamate

Conditions

Conditions	Yield
With pyridine for 3h; Heating;	76%

: 573-56-8
2,6-dinitrophenol

: 605-65-2
5-(dimethylamino)naphth-1-ylsulfonyl chloride

: C18H15N3O7S

Conditions

Conditions	Yield
In dichloromethane at 0 - 20℃; for 4h; Inert atmosphere;	76%

: 573-56-8
2,6-dinitrophenol

: 51822-12-9
4-chloroformylphenoxyacetyl chloride

: 4-(2,6-dinitro-phenoxycarbonylmethoxy)-benzoic acid 2,6-dinitro-phenyl ester

Conditions

Conditions	Yield
With polyethylene glycol-400; sodium hydroxide In dichloromethane; water at 20℃; for 1h; Acylation;	75%

: 573-56-8
2,6-dinitrophenol

: 40466-95-3
4-bromo-2,6-dinitrophenol

Conditions

Conditions	Yield
With sulfuric acid; bromine at 100℃; for 3.5h;	74%
With acetic acid beim Bromieren;
With ethanol; bromine

: 66-71-7
1,10-Phenanthroline

: europium(III) chloride hexahydrate

: 573-56-8
2,6-dinitrophenol

: 1310-73-2
sodium hydroxide

: [europium(III)(2,6-dinitrophenol(-H))3(hydroxy)(1,10-phenanthroline)](1,10-phenanthroline(+H))

Conditions

Conditions	Yield
In methanol NaOH soln. added to soln. of 2,6-DNP (0.25 mmol) (pH=4-5), soln. of phen(1.0 mmol) and EuCl3*6H2O (0.5 mmol) added dropwise, stirred for 8 h; ppt. filtered off, washed with MeOH, crystd.; elem. anal.;	72.8%

...Expand

: 366-18-7
[2,2]bipyridinyl

: europium(III) chloride hexahydrate

: 573-56-8
2,6-dinitrophenol

: 1310-73-2
sodium hydroxide

: [europium(III)(2,6-dinitrophenol(-H))3(OH)(2,2'-bipyridine)](2,2-bipyridine(+H))

Conditions

Conditions	Yield
In methanol NaOH soln. added to soln. of 2,6-DNP (0.25 mmol) (pH=6-7), soln. of bipy(0.25 mmol) and EuCl3*6H2O (0.5 mmol) added dropwise, stirred for 8 h; ppt. filtered off, washed with MeOH, crystd.; elem. anal.;	72.3%

...Expand

: 366-18-7
[2,2]bipyridinyl

: gadolinium(III) oxide

: 573-56-8
2,6-dinitrophenol

: 1310-73-2
sodium hydroxide

: [gadolinium(III)(2,6-dinitrophenol(-H))3(OH)(2,2'-bipyridine)](2,2-bipyridine(+H))

Conditions

Conditions	Yield
In methanol NaOH soln. added to soln. of 2,6-DNP (0.25 mmol) (pH=4-5), soln. of bipy(0.25 mmol) and GdCl3*6H2O (0.5 mmol) added dropwise, stirred for 8 h; ppt. filtered off, washed with MeOH, crystd.; elem. anal.;	71.6%

...Expand

: 66-71-7
1,10-Phenanthroline

: 573-56-8
2,6-dinitrophenol

: terbium(III) chloride hexahydrate

: 7732-18-5
water

: {[Tb(2,6-dinitrophenol)3(1,10-phenanthroline)OH2]*1,10-phenanthroline}

Conditions

Conditions	Yield
	69.9%

...Expand

: 366-18-7
[2,2]bipyridinyl

: gadolinium(III) oxide

: 573-56-8
2,6-dinitrophenol

: [gadolinium(III)(2,6-dinitrophenol(-H))3(H2O)(2,2'-bipyridine)]

Conditions

Conditions	Yield
With NaOH In methanol NaOH soln. added to soln. of 2,6-DNP (0.25 mmoL) (pH=6-7), soln. of bipy(0.25 mmol) and GdCl3*6H2O (0.5 mmol) added dropwise, stirred for 8 h; ppt. filtered off, washed with MeOH, crystd.; elem. anal.;	69.8%

...Expand

: 67-56-1
methanol

: gadolinium(III) oxide

: 66-71-7
1,10-Phenanthroline

: 573-56-8
2,6-dinitrophenol

: [gadolinium(III)(2,6-dinitrophenol(-H))3(methanol)(1,10-phenanthroline)]

Conditions

Conditions	Yield
With NaOH In methanol NaOH soln. added to soln. of 2,6-DNP (0.25 mmol) (pH=6-7), soln. of phen(1.0 mmol) and GdCl3*6H2O (0.5 mmol) added dropwise, stirred for 8 h; ppt. filtered off, washed with MeOH, crystd.; elem. anal.;	69.4%

...Expand

: 573-56-8
2,6-dinitrophenol

: 7205-98-3
chloromethyl phenyl sulfone

: 92241-31-1
3-Benzenesulfonylmethyl-2,6-dinitro-phenol

Conditions

Conditions	Yield
With sodium hydroxide In dimethyl sulfoxide at 20℃;	69%

: 366-18-7
[2,2]bipyridinyl

: europium(III) chloride hexahydrate

: 573-56-8
2,6-dinitrophenol

: [europium(III)(2,6-dinitrophenol(-H))3(H2O)(2,2'-bipyridine)]

Conditions

Conditions	Yield
With NaOH In methanol NaOH soln. added to soln. of 2,6-DNP (0.25 mmol) (pH=6-7), soln. of bipy(0.25 mmol) and EuCl3*6H2O (0.5 mmol) added dropwise, stirred for 8 h; ppt. filtered off, washed with MeOH, crystd.; elem. anal.;	68.3%

...Expand

: 67-56-1
methanol

: 66-71-7
1,10-Phenanthroline

: europium(III) chloride hexahydrate

: 573-56-8
2,6-dinitrophenol

: [europium(III)(2,6-dinitrophenol(-H))3(methanol)(1,10-phenanthroline)]

Conditions

Conditions	Yield
With NaOH In methanol NaOH soln. added to soln. of 2,6-DNP (0.25 mmol) (pH=6-7), soln. of phen(1.0 mmol) and EuCl3*6H2O (0.5 mmol) added dropwise, stirred for 8 h; ppt. filtered off, washed with MeOH, crystd.; elem. anal.;	67.3%

...Expand

: gadolinium(III) oxide

: 66-71-7
1,10-Phenanthroline

: 573-56-8
2,6-dinitrophenol

: 1310-73-2
sodium hydroxide

: [gadolinium(III)(2,6-dinitrophenol(-H))3(hydroxy)3(1,10-phenanthroline)]2(1,10-phenanthroline(+H))2

Conditions

Conditions	Yield
In methanol NaOH soln. added to soln. of 2,6-DNP (0.25 mmol) (pH=4-5), soln. of phen(1.0 mmol) and GdCl3*6H2O (0.5 mmol) added dropwise, stirred for 8 h; ppt. filtered off, washed with MeOH, crystd.; elem. anal.;	66.8%

...Expand

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