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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 2,9-Dicarboxy-1,10-Phenanthroline with high purity

Cas:57709-61-2

Min.Order:1 Kilogram

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Type:Manufacturers

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Factory Price OLED 99% 57709-61-2 2,9-dicarboxy-1,10-phenanthroline Manufacturer

Cas:57709-61-2

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine c

1,10-Phenanthroline-2,9-dicarboxylic acid

Cas:57709-61-2

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

1,10-Phenanthroline-2,9-dicarboxylic acid

Cas:57709-61-2

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

1,10-PHENANTHROLINE-2,9-DICARBOXYLIC ACID Basic information Product Name: 1,10-PHENANTHROLINE-2,9-DICARBOXYLIC ACID Synonyms: 1,10-PHENANTHROLINE-2,9-DICARBOXYLIC ACID;1,10-PHENANTHROLIN

1,10-PHENANTHROLINE-2,9-DICARBOXYLIC ACID

Cas:57709-61-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 57709-61-2 with best quality

Cas:57709-61-2

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Product name 1,10-Phenanthroline-2,9-dicarboxylic acid CAS 57709-61-2 Molecular Formula C14H8N2O4 Molecular Weight 268.22 App

1,10-Phenanthroline-2,9-dicarboxylic acid

Cas:57709-61-2

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

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Shanghai Minstar Chemical Co., Ltd

Product Name: 1,10-PHENANTHROLINE-2,9-DICARBOXYLIC ACID CAS: 57709-61-2 MF: C14H8N2O4 MW: 268.22 EINECS: Mol File: 57709-61-2.mol 1,10-PHENANTHROLINE-2,9-DICARBOXYLIC ACID Structure 1,10-PHENANTHROLINE-2,9-DICARBOXYLIC ACID Chemi

1,10-PHENANTHROLINE-2,9-DICARBOXYLIC ACID

Cas:57709-61-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

1,10-Phenanthroline-2,9-dicarboxylic acid

Cas:57709-61-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

1,10-Phenanthroline-2,9-dicarboxylic acid

Cas:57709-61-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

2,9-Dicarboxy-1,10-Phenanthroline

Cas:57709-61-2

Min.Order:0

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 1,10-Phenanthroline-2,9-dicarboxylic acid

Cas:57709-61-2

Min.Order:0 Metric Ton

Negotiable

Type:Other

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

1,10-Phenanthroline-2,9-dicarboxylic acid

Cas:57709-61-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

1,10-PHENANTHROLINE-2,9-DICARBOXYLIC ACID

Cas:57709-61-2

Min.Order:1 Milligram

Negotiable

Type:Trading Company

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Hangzhou Huarong Pharm Co., Ltd.

Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu

2,9-Dicarboxylicacid-1,10-phenanthroline

Cas:57709-61-2

Min.Order:0

Negotiable

Type:Trading Company

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KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

57709-61-2 CAS NO.57709-61-2

Cas:57709-61-2

Min.Order:1 Metric Ton

FOB Price: $7.0 / 8.0

Type:Trading Company

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SAGECHEM LIMITED

SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe

1,10-Phenanthroline-2,9-dicarboxylic acid hydrate

Cas:57709-61-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

1,10-Phenanthroline-2,9-dicarboxylic acid

Cas:57709-61-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

1,10-Phenanthroline-2,9-dicarboxylic acid hydrate cas no. 57709-61-2 98%

Cas:57709-61-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

1,10-Phenanthroline-2,9-dicarboxylic acid

Cas:57709-61-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

1,10-Phenanthroline-2,9-dicarboxylic acid

Cas:57709-61-2

Min.Order:0

Negotiable

Type:Other

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JINHUA HUAYI CHEMICAL CO., LTD.

Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands

2,9-Dicarboxy-1,10-Phenanthroline

Cas:57709-61-2

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Acmec Biochemical Technology Co., Ltd.

Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea

Acmec 1,10-Phenanthroline-2,9-dicarboxylic acid hydrate 25g

Cas:57709-61-2

Min.Order:1 bottle

Negotiable

Type:Lab/Research institutions

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

2,9-Dicarboxy-1,10-Phenanthroline

Cas:57709-61-2

Min.Order:0

Negotiable

Type:Manufacturers

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Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

1,10-Phenanthroline-2,9-dicarboxylic acid

Cas:57709-61-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Circle Star Chem-medical Technology co.,Ltd.

good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:25kg,50kg,180kg,200kg,250kg,1000kg,customization Application:Pharma;Industry;Agricultural;chemical reaserch Tran

1,10-PHENANTHROLINE-2,9-DICARBOXYLIC ACID

Cas:57709-61-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Changchun Artel lmport and Export trade company

Supply top quality products with a reasonable price Application:api

57709-61-2

Cas:57709-61-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Fandachem Co.,Ltd

1,10-Phenanthroline-2,9-dicarboxylic acid cas 57709-61-2Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

1,10-Phenanthroline-2,9-dicarboxylic acid cas 57709-61-2

Cas:57709-61-2

Min.Order:0

Negotiable

Type:Other

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Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

1,10-Phenanthroline-2,9-dicarboxylic acid

Cas:57709-61-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Sartort Biopharma Co., Ltd

Best quality with low price Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai

1,10-phenanthroline-2,9-dicarboxylic acid

Cas:57709-61-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

2,9-Bis(trichloromethyl)-1,10-phenanthroline
78831-41-1

2,9-Bis(trichloromethyl)-1,10-phenanthroline

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

Conditions
ConditionsYield
With sulfuric acid In water at 85℃; for 7h;100%
With sulfuric acid at 80 - 90℃; for 6h;91%
With nitric acid for 3h; Heating;
1,10-phenanthroline-2,9-dicarboxaldehyde
57709-62-3

1,10-phenanthroline-2,9-dicarboxaldehyde

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

Conditions
ConditionsYield
With nitric acid for 4h; Heating;96%
With nitric acid for 24h; Reflux;90%
With nitric acid for 6h; Reflux;83.15%
2,9-bis(tribromomethyl)-1,10-phenanthroline
78831-40-0

2,9-bis(tribromomethyl)-1,10-phenanthroline

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

Conditions
ConditionsYield
With nitric acid for 3h; Heating;
2.9-dimethyl-1,10-phenanthroline
484-11-7

2.9-dimethyl-1,10-phenanthroline

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: SeO2 / dioxane / 2 h / Heating
2: 430 mg / aq. HNO3 / 2 h / Heating
View Scheme
Multi-step reaction with 2 steps
1: 86 percent / NCS, 3-chloroperbenzoic acid / CCl4 / 12 h / Heating
2: 91 percent / 98percent H2SO4 / 6 h / 80 - 90 °C
View Scheme
Multi-step reaction with 2 steps
1: SeO2 / dioxane
2: 96 percent / 60percent nitric acid / 4 h / Heating
View Scheme
1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

1,10‐phenanthroline‐2,9‐dicarbonyl dichloride
84670-37-1

1,10‐phenanthroline‐2,9‐dicarbonyl dichloride

Conditions
ConditionsYield
With thionyl chloride at 120℃; for 1h; Inert atmosphere;100%
With thionyl chloride for 2h; Heating;76%
With thionyl chloride In toluene
pentafluorophenyl trifloroacetate
14533-84-7

pentafluorophenyl trifloroacetate

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

bis(pentafluorophenyl)-1,10-phenanthroline-2,9-dicarboxylate
516462-64-9

bis(pentafluorophenyl)-1,10-phenanthroline-2,9-dicarboxylate

Conditions
ConditionsYield
In pyridine; N,N-dimethyl-formamide at 20℃; for 12h;98%
1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

4,4',4-tri-tert-butyl-2,2':6',2-terpyridine

4,4',4-tri-tert-butyl-2,2':6',2-terpyridine

C41H41N5O4Ru
1452388-81-6

C41H41N5O4Ru

Conditions
ConditionsYield
With triethylamine In ethanol; water for 2h; Reflux;97%
3-aminoquinoline
580-17-6

3-aminoquinoline

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

N2,N9-di(quinolin-3-yl)-1,10-phenanthroline-2,9-dicarboxamide
929895-49-8

N2,N9-di(quinolin-3-yl)-1,10-phenanthroline-2,9-dicarboxamide

Conditions
ConditionsYield
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole In N,N-dimethyl-formamide at 20℃; for 1h;89%
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 48h; Reagent/catalyst; Solvent; Inert atmosphere;85%
Ru(2,2′;6,2″-terpyridine)Cl3

Ru(2,2′;6,2″-terpyridine)Cl3

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

C29H17N5O4Ru
1452388-79-2

C29H17N5O4Ru

Conditions
ConditionsYield
With triethylamine In ethanol; water for 2h; Reflux;89%
methanol
67-56-1

methanol

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

2,9-dimethyl 1,10-phenanthroline-2,9-dicarboxylate
78831-35-3

2,9-dimethyl 1,10-phenanthroline-2,9-dicarboxylate

Conditions
ConditionsYield
With sulfuric acid Reflux;86%
With sulfuric acid at 70℃; for 10h;78%
With hydrogenchloride for 2.5h; Heating;67%
With hydrogenchloride for 2.5h; Reflux;65%
With sulfuric acid
2,6-Diaminopyridine
141-86-6

2,6-Diaminopyridine

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

N,N'-bis(2-amino-6-pyridyl)-1,10-phenanthroline-2,9-dicarboxamide

N,N'-bis(2-amino-6-pyridyl)-1,10-phenanthroline-2,9-dicarboxamide

Conditions
ConditionsYield
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 3h;85%
4-(trimethylsilyloxy)aniline
36309-42-9

4-(trimethylsilyloxy)aniline

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

N,N'-bis(4-aminophenol)-1,10-phenanthroline-2,9-carboxamide
1266331-36-5

N,N'-bis(4-aminophenol)-1,10-phenanthroline-2,9-carboxamide

Conditions
ConditionsYield
With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 2h;78%
ethanol
64-17-5

ethanol

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

1,10-phenanthroline-2,9-dicarboxylic acid diethyl ester
1172621-51-0

1,10-phenanthroline-2,9-dicarboxylic acid diethyl ester

Conditions
ConditionsYield
With sulfuric acid for 11h; Reflux;78%
With sulfuric acid for 12h; Reflux;73%
1,10-Phenanthroline
66-71-7

1,10-Phenanthroline

iron(III) chloride hexahydrate

iron(III) chloride hexahydrate

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

[FeCl(1,10-phenanthroline)(1,10-phenanthroline-2,9-dicarboxylate)]*H2O

[FeCl(1,10-phenanthroline)(1,10-phenanthroline-2,9-dicarboxylate)]*H2O

Conditions
ConditionsYield
In methanol at 130℃; for 72h; High pressure; Autoclave;75%
methanol
67-56-1

methanol

iron(II) perchlorate hexahydrate

iron(II) perchlorate hexahydrate

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

[FeII(2,9-bis(carbomethoxy)-1,10-phenanthroline)2](ClO4)2

[FeII(2,9-bis(carbomethoxy)-1,10-phenanthroline)2](ClO4)2

Conditions
ConditionsYield
for 5h; Reflux;74%
1-iodo-10-undecene
7766-49-6

1-iodo-10-undecene

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

C36H48N2O4

C36H48N2O4

Conditions
ConditionsYield
Stage #1: 1,10-phenanthroline-2,9-dicarboxylic acid With tetrabutyl ammonium fluoride In tetrahydrofuran at 20℃; for 3h; Inert atmosphere;
Stage #2: 1-iodo-10-undecene In tetrahydrofuran at 20℃; for 48h; Inert atmosphere;
74%
2-(aminoethyl)pyridine
2706-56-1

2-(aminoethyl)pyridine

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

2,9-bis{[2-(2-pyridyl)ethylamino]carbonyl}-1,10-phenanthroline

2,9-bis{[2-(2-pyridyl)ethylamino]carbonyl}-1,10-phenanthroline

Conditions
ConditionsYield
Stage #1: 1,10-phenanthroline-2,9-dicarboxylic acid With 1,1'-carbonyldiimidazole In N,N-dimethyl-formamide at 40 - 50℃;
Stage #2: 2-(aminoethyl)pyridine In N,N-dimethyl-formamide at 20℃; for 108h;
73%
iron(III) chloride hexahydrate

iron(III) chloride hexahydrate

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

acetonitrile
75-05-8

acetonitrile

NH4[Fe(1,10-phenanthroline-2,9-dicarboxylate)2]*2(acetonitrile)

NH4[Fe(1,10-phenanthroline-2,9-dicarboxylate)2]*2(acetonitrile)

Conditions
ConditionsYield
With 1,10-Phenanthroline In water at 130℃; for 72h; High pressure; Autoclave;73%
methanol
67-56-1

methanol

dysprosium(III) nitrate hexahydrate

dysprosium(III) nitrate hexahydrate

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

C28H12DyN4O8(1-)*4CH4O

C28H12DyN4O8(1-)*4CH4O

Conditions
ConditionsYield
With triethylamine at 120℃; for 48h; pH=8.2; pH-value; Sealed tube;72%
C24H24Br2O4

C24H24Br2O4

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

C38H30N2O8

C38H30N2O8

Conditions
ConditionsYield
Stage #1: 1,10-phenanthroline-2,9-dicarboxylic acid With tetrabutyl ammonium fluoride In tetrahydrofuran at 20℃; for 3h; Inert atmosphere;
Stage #2: C24H24Br2O4 In tetrahydrofuran at 20℃; for 48h; Inert atmosphere;
66%
methyl 3-methoxy-4-aminobenzoate
41608-64-4

methyl 3-methoxy-4-aminobenzoate

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

C32H26N4O8

C32H26N4O8

Conditions
ConditionsYield
Stage #1: 1,10-phenanthroline-2,9-dicarboxylic acid With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide In dichloromethane
Stage #2: methyl 3-methoxy-4-aminobenzoate In dichloromethane
65%
histamine
51-45-6

histamine

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

2,9-bis-{[2-(4-imidazolyl)ethylamino]carbonyl}-1,10-phenanthroline

2,9-bis-{[2-(4-imidazolyl)ethylamino]carbonyl}-1,10-phenanthroline

Conditions
ConditionsYield
Stage #1: 1,10-phenanthroline-2,9-dicarboxylic acid With 1,1'-carbonyldiimidazole In N,N-dimethyl-formamide
Stage #2: histamine In N,N-dimethyl-formamide
63%
2-(1H-benzimidazol-2-yl)ethylamine
29518-68-1

2-(1H-benzimidazol-2-yl)ethylamine

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

2,9-bis-{[2-(2-benzimidazolyl)ethylamino]carbonyl}-1,10-phenanthroline

2,9-bis-{[2-(2-benzimidazolyl)ethylamino]carbonyl}-1,10-phenanthroline

Conditions
ConditionsYield
Stage #1: 1,10-phenanthroline-2,9-dicarboxylic acid With 1,1'-carbonyldiimidazole In N,N-dimethyl-formamide
Stage #2: 2-(1H-benzimidazol-2-yl)ethylamine In N,N-dimethyl-formamide
61%
nickel(II) perchlorate hexahydrate

nickel(II) perchlorate hexahydrate

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

[Ni(1,10-phenanthroline-2,9-dicarboxylate)(H2O)3]*H2O
854933-76-9

[Ni(1,10-phenanthroline-2,9-dicarboxylate)(H2O)3]*H2O

Conditions
ConditionsYield
With KOH In methanol; water Ni(ClO4)2*6H2O mixed with 1,10-phenanthroline-2,9-dicarboxylic acid; pH adjusted to about 7 (aq. KOH); filtered; allowed to stand at room temp.; solvent was slowly evapd.; elem. anal.;60%
3-(1H-imidazol-1-yl)propan-1-amine
5036-48-6

3-(1H-imidazol-1-yl)propan-1-amine

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

2,9-bis(N-(1-imidazolyl)propylaminocarbonyl)-1,10-phenanthroline

2,9-bis(N-(1-imidazolyl)propylaminocarbonyl)-1,10-phenanthroline

Conditions
ConditionsYield
Stage #1: 1,10-phenanthroline-2,9-dicarboxylic acid With 1,1'-carbonyldiimidazole In N,N-dimethyl-formamide at 45℃; for 2h;
Stage #2: 3-(1H-imidazol-1-yl)propan-1-amine In N,N-dimethyl-formamide at 20℃; for 96h;
59%
n-dioctylamine
1120-48-5

n-dioctylamine

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

N,N′-dioctyl-N,N′-dioctyl-2,9-diamide-1,10-phenanthroline

N,N′-dioctyl-N,N′-dioctyl-2,9-diamide-1,10-phenanthroline

Conditions
ConditionsYield
Stage #1: 1,10-phenanthroline-2,9-dicarboxylic acid With thionyl chloride for 6h; Reflux;
Stage #2: n-dioctylamine With N-ethyl-N,N-diisopropylamine In dichloromethane for 6h; Reflux;
59%
dysprosium(III) nitrate hexahydrate

dysprosium(III) nitrate hexahydrate

silicotungstic acid hydrate

silicotungstic acid hydrate

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

4C14H6N2O4(2-)*O40SiW12(4-)*18H2O*4Dy(3+)

4C14H6N2O4(2-)*O40SiW12(4-)*18H2O*4Dy(3+)

Conditions
ConditionsYield
Stage #1: dysprosium(III) nitrate hexahydrate; silicotungstic acid hydrate; 1,10-phenanthroline-2,9-dicarboxylic acid In water for 0.5h;
Stage #2: In water for 0.5h;
Stage #3: With ammonium metavanadate; sodium hydroxide In water at 130℃; for 72h; pH=2.5; Autoclave;
55%
ZnCl2*5H2O

ZnCl2*5H2O

water
7732-18-5

water

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

acetonitrile
75-05-8

acetonitrile

C28H12N4O8Zn(2-)*2CH3NO2*2H2O*2H3O(1+)

C28H12N4O8Zn(2-)*2CH3NO2*2H2O*2H3O(1+)

Conditions
ConditionsYield
Stage #1: ZnCl2*5H2O; water; 1,10-phenanthroline-2,9-dicarboxylic acid; acetonitrile for 0.5h; High pressure;
Stage #2: at 130℃; for 72h; Autoclave;
53%
dysprosium(III) nitrate hexahydrate

dysprosium(III) nitrate hexahydrate

α-H4SiMo12O40*xH2O

α-H4SiMo12O40*xH2O

water
7732-18-5

water

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

2[Dy4(PDA)4(H2O)11(SiMo12O40)]*7H2O

2[Dy4(PDA)4(H2O)11(SiMo12O40)]*7H2O

Conditions
ConditionsYield
Stage #1: dysprosium(III) nitrate hexahydrate; α-H4SiMo12O40*xH2O; water; 1,10-phenanthroline-2,9-dicarboxylic acid for 0.5h;
Stage #2: With sodium hydroxide at 130℃; for 72h; pH=1.8; Autoclave; High pressure;
51.44%
cerium(III) chloride heptahydrate

cerium(III) chloride heptahydrate

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

3Ce(3+)*3C14H6N2O4(2-)*3C14H7N2O4(1-)

3Ce(3+)*3C14H6N2O4(2-)*3C14H7N2O4(1-)

Conditions
ConditionsYield
In water at 180℃; for 24h; Autoclave;47%
n-Octylamine
111-86-4

n-Octylamine

1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

2,9-bis(N-octylaminocarbonyl)-1,10-phenanthroline

2,9-bis(N-octylaminocarbonyl)-1,10-phenanthroline

Conditions
ConditionsYield
Stage #1: 1,10-phenanthroline-2,9-dicarboxylic acid With thionyl chloride for 6h; Reflux;
Stage #2: n-Octylamine With N-ethyl-N,N-diisopropylamine In dichloromethane for 6h; Reflux;
46%
1,10-phenanthroline-2,9-dicarboxylic acid
57709-61-2

1,10-phenanthroline-2,9-dicarboxylic acid

3-(2-methyl-1H-imidazol-1-yl)propan-1-amine
2258-21-1

3-(2-methyl-1H-imidazol-1-yl)propan-1-amine

2,9-bis(N-(1-(2-methylimidazolyl))propylaminocarbonyl)-1,10-phenanthrolin

2,9-bis(N-(1-(2-methylimidazolyl))propylaminocarbonyl)-1,10-phenanthrolin

Conditions
ConditionsYield
Stage #1: 1,10-phenanthroline-2,9-dicarboxylic acid With 1,1'-carbonyldiimidazole In N,N-dimethyl-formamide at 45℃; for 2h;
Stage #2: 3-(2-methyl-1H-imidazol-1-yl)propan-1-amine In N,N-dimethyl-formamide at 20℃; for 96h;
46%

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