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Shandong Xingshun New Material Co., Ltd.

The company is committed to research, develop, produce and sale fine chemicals and pharmaceutical intermediates. The company is the leading producer of 1-Chloromethyl Naphthalene in China,The company has a professional production, strict quality mana

6-Bromo-2-naphthoic acid 99% best price factory

Cas:5773-80-8

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

6-Bromo-2-naphthoic acid

Cas:5773-80-8

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 6-Bromo-2-Naphthoic Acid supplier in China

Cas:5773-80-8

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Wuhan Fortuna Chemical Co.,Ltd

Unique advantages for 6-Bromo-2-naphthoic acid Cas 5773-80-8 Guaranteed the purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White Powder Package:1kg/foil bag, 25kg/drum or as you r

Factory low price 6-Bromo-2-naphthoic acid Cas 5773-80-8 with high quality

Cas:5773-80-8

Min.Order:1 Kilogram

FOB Price: $90.0

Type:Trading Company

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 6-Bromo-2-Naphthoic Acid

Cas:5773-80-8

Min.Order:1

Negotiable

Type:Other

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

6-Bromo-2-naphthoic acid

Cas:5773-80-8

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Leader Biochemical Group

About Product Details Item Specification Test Results Appearance White crystalline powder Conform

China Biggest factory Supply High Quality 6-Bromo-2-naphthoic acid CAS 5773-80-8

Cas:5773-80-8

Min.Order:1 Kilogram

FOB Price: $1.0 / 5.0

Type:Lab/Research institutions

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Henan Tianfu Chemical Co., Ltd.

6-Bromo-2-naphthoic acid Basic information Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relations

6-Bromo-2-naphthoic acid CAS:5773-80-8

Cas:5773-80-8

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Jinan Finer Chemical Co., Ltd

Product Description Product website: http://www.finerchem.com Product Name 6-Bromo-2-naphthoic acid CAS No. 5773-80-8

6-Bromo-2-naphthoic acid

Cas:5773-80-8

Min.Order:1 Gram

FOB Price: $12.0

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. High quality and competitive price: 1) Standard: BP/USP/EP/ enterprise standard 2) All purity ≥99% 3) We are manufacturers and can provide high quality products at factory prices. 2. Fast and safe delivery 1) The package c

6-Bromo-2-naphthoic acid CAS:5773-80-8

Cas:5773-80-8

Min.Order:1 Gram

FOB Price: $2.0 / 5.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

New production CAS 5773-80-8 with best quality

Cas:5773-80-8

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W

6-Bromo-2-naphthoic acid CAS5773-80-8

Cas:5773-80-8

Min.Order:1 Kilogram

FOB Price: $289.0 / 499.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Product name 6-bromo-2-naphthoic acid Product category Naphthalene series CAS NO. 5773-80-8 Structural formula Appearance:Light brown solid Storage:Store in cool and dry place, away from sun ligh

6-bromo-2-naphthoic acid

Cas:5773-80-8

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

6-Bromo-2-naphthoic acid 5773-80-8

Cas:5773-80-8

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At presen

6-Bromo-2-naphthoic acid

Cas:5773-80-8

Min.Order:5 Gram

FOB Price: $524.0

Type:Trading Company

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

6-Bromo-2-naphthoic acid

Cas:5773-80-8

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

6-Bromo-2-naphthoic acid

Cas:5773-80-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

6-Bromo-2-Naphthoic Acid

Cas:5773-80-8

Min.Order:0

Negotiable

Type:Manufacturers

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

6-Bromo-2-naphthoic acid

Cas:5773-80-8

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

6-Bromo-2-naphthoic acid

Cas:5773-80-8

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

6-BROMO-2-NAPHTHOIC ACID

Cas:5773-80-8

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

6-Bromo-2-naphthoic acid

Cas:5773-80-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

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SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

6-Bromo-2-naphthoic acid

Cas:5773-80-8

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

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Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

6-Bromo-naphthalene-2-carboxylic acid?/High quality/Best price

Cas:5773-80-8

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 6-Bromo-2-Naphthoic Acid

Cas:5773-80-8

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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Hangzhou Lingrui Chemical Co.,Ltd.

6-Bromo-2-naphthoic acidAppearance:Colorless transparent liquid Storage:Keep away of light, cool place Package:according to customers' requirements Application:pharmaceutical intermediates Transportation:By air(EMS or EUB or FedEx or TNT ect...) or b

6-Bromo-2-naphthoic acid

Cas:5773-80-8

Min.Order:1 Gram

Negotiable

Type:Other

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SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

6-Bromo-2-naphthoic acid

Cas:5773-80-8

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

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Siwei Development Group Ltd.

Product name: 6-Bromo-2-Naphthonic Acid CAS No.: 5773-80-8 Molecule Formula:C11H7BrO2 Molecule Weight:251.08 Purity: 99.0% Package: 25kg/drum Description:Pale yellow to white powder Manufacture Standards:Enterprise Standard

Lower Price 6-Bromo-2-Naphthonic Acid

Cas:5773-80-8

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

High quality 6-Bromo-2-Naphthoic Acid supplier in China

Cas:5773-80-8

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

Best Offer6-Bromo-2-naphthoic acid

Cas:5773-80-8

Min.Order:0

Negotiable

Type:Trading Company

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Synthetic route

methyl 6-bromo-2-naphthoate
33626-98-1

methyl 6-bromo-2-naphthoate

6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

Conditions
ConditionsYield
With water; lithium hydroxide In tetrahydrofuran at 20℃; for 5h;96%
With lithium hydroxide In tetrahydrofuran; water at 20℃; for 5h;96%
Stage #1: methyl 6-bromo-2-naphthoate With lithium hydroxide monohydrate In tetrahydrofuran; water
Stage #2: With hydrogenchloride In tetrahydrofuran; water pH=3;
92%
6-bromo-naphthalen-2-ol
15231-91-1

6-bromo-naphthalen-2-ol

acetic acid
64-19-7

acetic acid

6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

Conditions
ConditionsYield
for 1.5h; Large scale;96%
Sodium; 6-bromo-naphthalene-2-carboxylate

Sodium; 6-bromo-naphthalene-2-carboxylate

6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

Conditions
ConditionsYield
With hydrogenchloride In water at 50℃; for 1h; Concentration; Inert atmosphere;95.5%
methyl 6-bromo-2-naphthoate
33626-98-1

methyl 6-bromo-2-naphthoate

A

2-Naphthalenemethanol
1592-38-7

2-Naphthalenemethanol

B

6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

C

(6-bromo-2-naphthy)methanol
100751-63-1

(6-bromo-2-naphthy)methanol

Conditions
ConditionsYield
With [RuCl2(N-heterocyclic carbene)(bis[2-(diphenylphosphino)ethyl]amine)]; potassium tert-butylate; hydrogen In 2-methyltetrahydrofuran at 45℃; under 3000.3 Torr; for 4h; Catalytic behavior; Pressure; Temperature; Autoclave;A n/a
B n/a
C 82%
1-(6-bromonaphthalen-2-yl)ethanone
1590-25-6

1-(6-bromonaphthalen-2-yl)ethanone

6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

Conditions
ConditionsYield
With sodium hypochlorite; sodium hydroxide In 1,4-dioxane; water at 70℃; for 4h;70%
With sodium hydroxide; sodium hypochlorite In 1,4-dioxane; water3.54 g (88%)
With sodium hydroxide; sodium hypochlorite In 1,4-dioxane; sulfuric acid; water3.54 g (88%)
carbon dioxide
124-38-9

carbon dioxide

6-bromo-2-naphthalenyl trifluoromethanesulfonate
151600-02-1

6-bromo-2-naphthalenyl trifluoromethanesulfonate

6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

Conditions
ConditionsYield
With (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; palladium diacetate; caesium carbonate; N-ethyl-N,N-diisopropylamine; DavePhos In dimethyl sulfoxide at 20℃; for 36h; Irradiation; Green chemistry; chemoselective reaction;65%
1-(6-bromonaphthalen-2-yl)ethanone
1590-25-6

1-(6-bromonaphthalen-2-yl)ethanone

A

6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

B

1,1-bis(pyridinium)methane diiodide
32405-50-8

1,1-bis(pyridinium)methane diiodide

Conditions
ConditionsYield
With pyridine; water; iodine In methanol at 30℃; Kinetics; Mechanism; Thermodynamic data; other temperatures; ΔH(excit.);
1-<6-bromo-naphthyl-(2)>-ethanone-(1)

1-<6-bromo-naphthyl-(2)>-ethanone-(1)

6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

Conditions
ConditionsYield
With alkaline aqueous sodium hypochlorite solution
With nitric acid
6-bromo-naphthonitrile-(2)

6-bromo-naphthonitrile-(2)

6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

2-bromonaphthalene
580-13-2

2-bromonaphthalene

1-(6-bromonaphthalen-2-yl)ethanone
1590-25-6

1-(6-bromonaphthalen-2-yl)ethanone

acetyl chloride
75-36-5

acetyl chloride

6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

Conditions
ConditionsYield
With hydrogenchloride; AlCl3 In hexane; nitrobenzene
sodium metabisulfite

sodium metabisulfite

1-(6-bromonaphthalen-2-yl)ethanone
1590-25-6

1-(6-bromonaphthalen-2-yl)ethanone

6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

Conditions
ConditionsYield
With sodium hydroxide; sodium hypochlorite In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; water
2-bromo-6-methylnaphthalene
37796-78-4

2-bromo-6-methylnaphthalene

6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

Conditions
ConditionsYield
With oxygen; manganese (II) acetate tetrahydrate; cobalt(II) diacetate tetrahydrate; acetic anhydride; acetic acid; potassium bromide at 110℃; for 4.5h; Concentration; Reagent/catalyst; Time; Temperature; Pressure;8.29 g
β-naphthol
135-19-3

β-naphthol

6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: iron(II) bromide; acetic acid; dihydrogen peroxide / water / 8 h / 87 °C / 760.05 Torr / Large scale
2: / 0.58 h / 87 °C / 760.05 Torr / Inert atmosphere; Large scale
3: 1.5 h / Large scale
View Scheme
2-bromonaphthalene
580-13-2

2-bromonaphthalene

6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: aluminum (III) chloride / nitrobenzene / 4 h / 100 °C
2: sodium hypochlorite; sodium hydroxide / water; 1,4-dioxane / 4 h / 70 °C
View Scheme
6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

6-bromonaphthalene-2-carbonyl chloride
87700-60-5

6-bromonaphthalene-2-carbonyl chloride

Conditions
ConditionsYield
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane100%
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane for 3h;
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 0 - 20℃; for 18h;
6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

6-Bromonaphthalen-2-amine
7499-66-3

6-Bromonaphthalen-2-amine

Conditions
ConditionsYield
Stage #1: 6-bromo-2-naphthoic acid With diphenyl phosphoryl azide; triethylamine In N,N-dimethyl-formamide at 20℃; for 3h;
Stage #2: With water In N,N-dimethyl-formamide at 100℃; for 1h;
100%
Stage #1: 6-bromo-2-naphthoic acid With diphenyl phosphoryl azide; triethylamine In N,N-dimethyl-formamide at 20℃; for 3h;
Stage #2: With water In N,N-dimethyl-formamide at 100℃; for 1h;
100%
Stage #1: 6-bromo-2-naphthoic acid With diphenyl phosphoryl azide; triethylamine In N,N-dimethyl-formamide at 20℃; for 3h;
Stage #2: With water In N,N-dimethyl-formamide at 100℃; for 1h;
100%
methanol
67-56-1

methanol

6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

methyl 6-bromo-2-naphthoate
33626-98-1

methyl 6-bromo-2-naphthoate

Conditions
ConditionsYield
With sulfuric acid; trimethyl orthoformate for 48h; Reflux;100%
With sulfuric acid for 36h; Reflux;100%
With sulfuric acid Reflux;100%
4-aminotetrahydropyran
38041-19-9

4-aminotetrahydropyran

6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

6-bromonaphthalene-2-carboxylic acid (tetrahydropyran-4-yl)amide
1350411-39-0

6-bromonaphthalene-2-carboxylic acid (tetrahydropyran-4-yl)amide

Conditions
ConditionsYield
With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide at 20℃; Cooling with ice;100%
With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide at 20℃; for 16h; Cooling with ice;100%
Chloro-oxo-acetic acid
4732-69-8

Chloro-oxo-acetic acid

6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

6-bromonaphthalene-2-carbonyl chloride
87700-60-5

6-bromonaphthalene-2-carbonyl chloride

Conditions
ConditionsYield
In dichloromethane; N,N-dimethyl-formamide100%
3-(1-adamantyl)-4-methoxyphenylboronic acid
459423-32-6

3-(1-adamantyl)-4-methoxyphenylboronic acid

6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

adapalene
106685-40-9

adapalene

Conditions
ConditionsYield
Stage #1: 3-(1-adamantyl)-4-methoxyphenylboronic acid; 6-bromo-2-naphthoic acid With potassium carbonate; palladium 10% on activated carbon In tetrahydrofuran; water for 8h; Heating / reflux;
Stage #2: With hydrogenchloride; water In tetrahydrofuran for 1h; Product distribution / selectivity;
99%
Stage #1: 3-(1-adamantyl)-4-methoxyphenylboronic acid; 6-bromo-2-naphthoic acid With potassium hydroxide; 5%-palladium/activated carbon In tetrahydrofuran; water at 55℃; for 2h; Heating / reflux;
Stage #2: With hydrogenchloride; water In tetrahydrofuran at 20℃; pH=6 - 7; Product distribution / selectivity;
99%
Stage #1: 3-(1-adamantyl)-4-methoxyphenylboronic acid; 6-bromo-2-naphthoic acid With potassium carbonate; palladium diacetate; CyJohnPhos In tetrahydrofuran; water for 2 - 4h; Suzuki Coupling; Heating / reflux;
Stage #2: With hydrogenchloride; water In tetrahydrofuran for 1h; Product distribution / selectivity;
94.8%
6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

naphthalene-2-carboxylate
93-09-4

naphthalene-2-carboxylate

Conditions
ConditionsYield
With palladium 10% on activated carbon; potassium acetate; bis(pinacol)diborane In ethanol at 60℃; for 6h; Suzuki-Miyaura Coupling; Inert atmosphere;98.8%
6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

N,O-dimethylhydroxylamine*hydrochloride
6638-79-5

N,O-dimethylhydroxylamine*hydrochloride

6-bromo-N-methoxy-N-methyl-2-naphthamide
861880-64-0

6-bromo-N-methoxy-N-methyl-2-naphthamide

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 0 - 20℃; for 12.25h;98%
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 4h;90%
6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

ethyl iodide
75-03-6

ethyl iodide

ethyl 6-bromo-naphthalene-2-carboxylate
86471-14-9

ethyl 6-bromo-naphthalene-2-carboxylate

Conditions
ConditionsYield
With caesium carbonate In ethyl acetate; acetonitrile97%
6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

6-bromo-naphthalene-2-carboxylic acid amide
1255871-55-6

6-bromo-naphthalene-2-carboxylic acid amide

Conditions
ConditionsYield
Stage #1: 6-bromo-2-naphthoic acid With oxalyl dichloride In dichloromethane; N,N-dimethyl-formamide at 20℃; for 1h;
Stage #2: With ammonium hydroxide In tetrahydrofuran at -10 - 20℃;
96%
Multi-step reaction with 2 steps
1: thionyl chloride / 16 h / 70 °C
2: ammonia / dichloromethane; methanol / 3 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: thionyl chloride / 16 h / 70 °C
2: ammonia / methanol / 3 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: thionyl chloride; triethylamine / 1 h / Reflux
2: ammonium hydroxide / water; dichloromethane / 4 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Inert atmosphere
2: ammonium hydroxide / water / 0.5 h / 0 - 20 °C
View Scheme
6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

4-methoxyphenylboronic acid
5720-07-0

4-methoxyphenylboronic acid

6-(4-methoxyphenyl)-2-naphthoic acid

6-(4-methoxyphenyl)-2-naphthoic acid

Conditions
ConditionsYield
With palladium 10% on activated carbon; sodium carbonate In methanol; water at 78℃; Suzuki coupling; Inert atmosphere;94%
rac-(2-ethynylcyclopropyl)methanol

rac-(2-ethynylcyclopropyl)methanol

6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

6-(((trans)-2-(hydroxymethyl)cyclopropyl)ethynyl)-2-naphthoic acid

6-(((trans)-2-(hydroxymethyl)cyclopropyl)ethynyl)-2-naphthoic acid

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine In tetrahydrofuran for 168h; Inert atmosphere;94%
6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

6-chloronaphthalene-2-carboxylic acid
5042-97-7

6-chloronaphthalene-2-carboxylic acid

Conditions
ConditionsYield
With copper(l) iodide; copper(l) chloride In N,N-dimethyl-formamide for 4h; Inert atmosphere; Reflux;93%
With copper(l) iodide; copper(l) chloride In N,N-dimethyl-formamide for 4h; Inert atmosphere; Darkness; Reflux;93%
With copper(l) iodide; copper(l) chloride In N,N-dimethyl-formamide for 4h; Reflux; Inert atmosphere; Darkness;93%
6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

tert-butyl alcohol
75-65-0

tert-butyl alcohol

6-bromo-2-N-tert-butoxycarbonylaminonaphthalene
869114-68-1

6-bromo-2-N-tert-butoxycarbonylaminonaphthalene

Conditions
ConditionsYield
With diphenylphosphoranyl azide; triethylamine In toluene at 100℃; for 4h;93%
With diphenyl phosphoryl azide; triethylamine at 100℃;85%
With diphenyl phosphoryl azide; triethylamine at 80℃; for 16h;
6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

3-adamantyl-4-methoxyphenyltriethoxysilane

3-adamantyl-4-methoxyphenyltriethoxysilane

adapalene
106685-40-9

adapalene

Conditions
ConditionsYield
With potassium fluoride; propylene glycol; chloro-[2-(9-phenyl-1,10-phenanthrolin-2-yl)phenyl]palladium In dichloromethane at 100℃; for 12h; Inert atmosphere;93%
6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

6-bromo-2-aminonaphthalene hydrochloride
71590-31-3

6-bromo-2-aminonaphthalene hydrochloride

Conditions
ConditionsYield
Stage #1: 6-bromo-2-naphthoic acid With diphenyl phosphoryl azide; triethylamine In tert-butyl alcohol for 15h; Reflux;
Stage #2: With hydrogenchloride In methanol at -78 - 20℃; for 15h;
91%
Stage #1: 6-bromo-2-naphthoic acid With diphenyl phosphoryl azide; triethylamine In tert-butyl alcohol for 15h; Reflux;
Stage #2: With sodium hydrogencarbonate In tert-butyl methyl ether for 0.5h;
Stage #3: With hydrogenchloride In methanol at -78 - 20℃; for 15h;
91%
Stage #1: 6-bromo-2-naphthoic acid With diphenyl phosphoryl azide; triethylamine In tert-butyl alcohol for 15h; Reflux;
Stage #2: With hydrogenchloride In methanol at -78℃; for 15h;
6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

trimethylaluminum
75-24-1

trimethylaluminum

6-bromo-3-methyl-2-naphthoic acid

6-bromo-3-methyl-2-naphthoic acid

Conditions
ConditionsYield
Stage #1: 6-bromo-2-naphthoic acid; trimethylaluminum With iron(III)-acetylacetonate; 4-(bis(2-(diphenylphosphanyl)phenyl)phosphanyl)-N,N-dimethylaniline In tetrahydrofuran; 1,2-dimethoxyethane; toluene at 20℃; Inert atmosphere; Schlenk technique;
Stage #2: With 2,3-dichlorobutane In tetrahydrofuran; 1,2-dimethoxyethane; toluene at 70℃; for 24h; Inert atmosphere; Schlenk technique; Sealed tube;
91%
ethanol
64-17-5

ethanol

6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

ethyl 6-bromo-naphthalene-2-carboxylate
86471-14-9

ethyl 6-bromo-naphthalene-2-carboxylate

Conditions
ConditionsYield
With sulfuric acid at 90℃; for 16h;91%
6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

(6-bromo-2-naphthy)methanol
100751-63-1

(6-bromo-2-naphthy)methanol

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran for 1h; Heating;90%
With dimethylsulfide borane complex In tetrahydrofuran at 0 - 20℃;89%
With borane-THF In tetrahydrofuran at 0 - 25℃;85%
6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

methylamine
74-89-5

methylamine

6-bromo-N-methyl-2-naphthamide
426219-35-4

6-bromo-N-methyl-2-naphthamide

Conditions
ConditionsYield
Stage #1: 6-bromo-2-naphthoic acid With thionyl chloride; N,N-dimethyl-formamide In toluene at 45 - 50℃; for 1h;
Stage #2: methylamine With triethylamine In methanol; toluene at 10 - 25℃; for 1h;
89%
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; N,N-dimethyl-formamide at 0 - 20℃; for 18h; Inert atmosphere;82%
Stage #1: 6-bromo-2-naphthoic acid With thionyl chloride In DMF (N,N-dimethyl-formamide); ethyl acetate at 30 - 65℃; for 0.5h;
Stage #2: methylamine With triethylamine In methanol; DMF (N,N-dimethyl-formamide); water; ethyl acetate at 25℃; for 3h;
80%
6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

N-Boc-1,3-diaminopropane
75178-96-0

N-Boc-1,3-diaminopropane

tert-butyl 3-(6-bromo-2-naphthamido)propylcarbamate

tert-butyl 3-(6-bromo-2-naphthamido)propylcarbamate

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 4h;85%
6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

(trifluoromethyl)trimethylsilane
81290-20-2

(trifluoromethyl)trimethylsilane

1-(6-bromonaphthalen-2-yl)-2,2,2-trifluoroethan-1-one

1-(6-bromonaphthalen-2-yl)-2,2,2-trifluoroethan-1-one

Conditions
ConditionsYield
With dmap; cesium fluoride; trifluoroacetic anhydride at 120℃; for 15h; Schlenk technique; Inert atmosphere;84%
N-(2-phenylquinazolin-4-yl)-benzene-1,4-diamine

N-(2-phenylquinazolin-4-yl)-benzene-1,4-diamine

6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

6-bromo-N-(3-((2-phenylquinazolin-4-yl)amino)phenyl)-2-naphthamide

6-bromo-N-(3-((2-phenylquinazolin-4-yl)amino)phenyl)-2-naphthamide

Conditions
ConditionsYield
Stage #1: 6-bromo-2-naphthoic acid With HATU In N,N-dimethyl-formamide at 0℃; for 0.333333h; Inert atmosphere;
Stage #2: N-(2-phenylquinazolin-4-yl)-benzene-1,4-diamine With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 0.333333h; Inert atmosphere;
81%
6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

bis(pinacol)diborane
73183-34-3

bis(pinacol)diborane

6-(4,4,5,5-tetramethyl-[1,3,2]-dioxaborolan-2-yl)-naphthalen-2-carboxylic acid
1426082-97-4

6-(4,4,5,5-tetramethyl-[1,3,2]-dioxaborolan-2-yl)-naphthalen-2-carboxylic acid

Conditions
ConditionsYield
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate In N,N-dimethyl-formamide at 90℃;80%
6-bromo-2-naphthoic acid
5773-80-8

6-bromo-2-naphthoic acid

N-phenyl-1,2-benzenediamine
534-85-0

N-phenyl-1,2-benzenediamine

2-(6-bromonaphthalen-2-yl)-1-phenyl-1H-benzimidazole
935472-87-0

2-(6-bromonaphthalen-2-yl)-1-phenyl-1H-benzimidazole

Conditions
ConditionsYield
Stage #1: 6-bromo-2-naphthoic acid With thionyl chloride; N,N-dimethyl-formamide for 4h; Heating;
Stage #2: N-phenyl-1,2-benzenediamine In 1-methyl-pyrrolidin-2-one at 160℃; for 12h;
78%
Stage #1: 6-bromo-2-naphthoic acid With thionyl chloride In N,N-dimethyl-formamide for 4h; Reflux;
Stage #2: N-phenyl-1,2-benzenediamine In 1-Methylpyrrolidine; N,N-dimethyl-formamide at 160℃; for 12h;
78%
Stage #1: 6-bromo-2-naphthoic acid With thionyl chloride; N,N-dimethyl-formamide for 4h; Heating;
Stage #2: N-phenyl-1,2-benzenediamine In 1-methyl-pyrrolidin-2-one at 160℃; for 12h;
78%
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