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Name:1-Triacontanol The alias:myricyl;NSC402492;NSC405588;1-Triacontanol-90%min;WELL-BLOOM; CAS NO:593-50-0 EINECS NO:209-794-5 Molecular formula:C30H62O Molecular weight: 438.81 Product Quality 12 years of chemical raw materials Mature o
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inquiryProduct name Triacontanol CAS NO. 593-50-0 Molecular Formula C30H62O Classification Pl
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12-Triaconten-1-ol
melissyl alcohol
Conditions | Yield |
---|---|
With hydrogen; platinum(IV) oxide In methanol; toluene for 6h; | 98% |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran 1.) -10 deg C -> room temperature, 1 h, 2.) room temperature, 4 h; | 96% |
With lithium aluminium tetrahydride In tetrahydrofuran 1.) -10 deg C to room temperature, 1 h, 2.) room temperature, 4 h; | 95% |
With lithium aluminium tetrahydride In tetrahydrofuran | 95% |
triacont-11-yn-1-ol
melissyl alcohol
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In tetrahydrofuran for 4h; | 95% |
10-triacontyn-1-ol
melissyl alcohol
Conditions | Yield |
---|---|
With hydrogen; platinum(IV) oxide In ethanol for 2h; Heating; | 90% |
(Z)-12-Triacontan-1-ol
melissyl alcohol
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethyl acetate for 8h; Ambient temperature; | 90% |
melissyl alcohol
Conditions | Yield |
---|---|
Stage #1: C36H74OSi With palladium 10% on activated carbon; hydrogen In methanol at 20℃; Stage #2: With hydrogenchloride In water for 0.333333h; Solvent; Reagent/catalyst; Reflux; | 90% |
Conditions | Yield |
---|---|
With hydrogenchloride; thionyl chloride In diethyl ether; ethanol; chloroform; ethyl acetate; acetone; benzene | 86% |
Multi-step reaction with 2 steps 1: H2SO4 2: sodium; butyl alcohol View Scheme |
(9E,21E)-Triaconta-9,21-dienoic acid methyl ester
melissyl alcohol
Conditions | Yield |
---|---|
With hydrogen; Atkins' catalysator In diethylene glycol dimethyl ether at 250℃; under 152000 Torr; | 80% |
Multi-step reaction with 2 steps 1: H2 / PtO / 760 Torr 2: LiAlH4 / tetrahydrofuran / 3 h / Heating View Scheme |
Conditions | Yield |
---|---|
dilithium tetrachlorocuprate In tetrahydrofuran at -5 - 0℃; for 4h; | 68% |
icosane
n-docosane
n-hexacosane
Tridecane
octadecane
tetracosane
octacosane
n-triacontane
A
1-octadecanol
B
n-eicosanol
C
melissyl alcohol
D
1-docosanol
E
tetracosyl alcohol
F
hexacosyl alcohol
G
octacosyl alcohol
Conditions | Yield |
---|---|
Stage #1: icosane; n-docosane; n-hexacosane; octadecane; tetracosane; octacosane; n-triacontane With oxygen at 30 - 50℃; under 1575.16 Torr; for 0.5h; Stage #2: Tridecane With titanium(IV) isopropylate at 30 - 50℃; under 1575.16 - 3750.38 Torr; for 6.86667h; Stage #3: With sulfuric acid; water at 80℃; Product distribution / selectivity; | A 17.66% B 19.46% C 0.1% D 13.62% E 6.93% F 2.04% G 0.48% |
icosane
n-docosane
n-hexacosane
octadecane
tetracosane
octacosane
n-triacontane
A
1-octadecanol
B
n-eicosanol
C
melissyl alcohol
D
1-docosanol
E
tetracosyl alcohol
F
hexacosyl alcohol
G
octacosyl alcohol
Conditions | Yield |
---|---|
Stage #1: icosane; n-docosane; n-hexacosane; octadecane; tetracosane; octacosane; n-triacontane With oxygen at 30 - 50℃; under 1575.16 - 3675.37 Torr; for 3h; Stage #2: With sulfuric acid; water Product distribution / selectivity; | A 12.4% B 13.4% C 0.05% D 7.8% E 3.2% F 1% G 0.2% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; zirconocene dichloride; sodium bis(2-methoxyethoxy)aluminium dihydride 1.) THF, 96 h, 40 deg C, 2.) ClCH2CH2Cl, 1 h, room temp.; Yield given. Multistep reaction; | A n/a B 10% |
Conditions | Yield |
---|---|
With sodium; butan-1-ol | |
With lithium aluminium tetrahydride In tetrahydrofuran Yield given; |
1-triacontyne
melissyl alcohol
Conditions | Yield |
---|---|
With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide 1) THF, 10 h; Yield given. Multistep reaction; |
n-triacontyl acetate
melissyl alcohol
Conditions | Yield |
---|---|
saponification; | |
With potassium hydroxide In ethanol Yield given; |
1-triacosanal
melissyl alcohol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In diethyl ether Yield given; |
1-octadecylmagnesium bromide
2-[(12-bromododecyl)oxy]tetrahydro-2H-pyran
melissyl alcohol
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate; dilithium tetrachlorocuprate 1) 0 deg C 2) methanol, heating, 4 h; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With sodium hydroxide; borane; dihydrogen peroxide Yield given. Multistep reaction. Title compound not separated from byproducts; | |
With sodium hydroxide; borane; dihydrogen peroxide Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; | |
With sodium hydroxide; borane; dihydrogen peroxide In tetrahydrofuran; diethylene glycol dimethyl ether Product distribution; | A 36 % Chromat. B 15 % Chromat. |
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol |
trans-triacontyl-4-hydroxycinnamate
A
melissyl alcohol
B
p-Coumaric Acid
Conditions | Yield |
---|---|
With potassium hydroxide In methanol; chloroform for 2h; Heating; | A 5 mg B 10 mg |
triacont-13-yn-1-ol
melissyl alcohol
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In tetrahydrofuran for 4h; |
Sodium; triacontanoate
melissyl alcohol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran Heating; Yield given; |
13-(Z)-triacontene
melissyl alcohol
Conditions | Yield |
---|---|
With sodium hydroxide; bis(cyclohexanyl)borane; dihydrogen peroxide 1a) THF, RT, 2 h, 1b) diglyme, 48 h, reflux; Yield given. Multistep reaction; |
melissyl alcohol
Conditions | Yield |
---|---|
With trimethylsilyl iodide In chloroform at 25℃; for 1h; Yield given; |
melissyl alcohol
Conditions | Yield |
---|---|
With hydrogenchloride In ethyl acetate for 4h; Ambient temperature; Yield given; |
Conditions | Yield |
---|---|
With potassium hydroxide In methanol Hydrolysis; |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 90 percent / 50percent HBr / acetic acid / 5 h / Heating 2: EtONa / ethanol / 0.5 h / Heating 3: Li2CuCl4 / tetrahydrofuran / 4 h / -10 - -5 °C 4: LiAlH4 / tetrahydrofuran / Heating View Scheme |
12-bromododecanoic acid
melissyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: EtONa / ethanol / 0.5 h / Heating 2: Li2CuCl4 / tetrahydrofuran / 4 h / -10 - -5 °C 3: LiAlH4 / tetrahydrofuran / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 1.) butyllithium / 1.) THF, hexane, -70 deg C, 15 min, 2.) a) -70 deg C, 5 h, b) from -70 deg to RT, 1.5 h, c) RT, 15 h 2: 90 percent / H2 / 2percent Pd-C / hexane / 120 h / Ambient temperature 3: 69 percent / lithium aluminum hydride / diethyl ether / 1.) reflux, 5 h, 2.) from 20 deg C to 25 deg C, 15 h View Scheme |
Conditions | Yield |
---|---|
With stannous octoate In chloroform Reflux; Inert atmosphere; | 86.1% |
Conditions | Yield |
---|---|
With carbon tetrabromide; triphenylphosphine In acetonitrile for 2h; Heating; | 85.5% |
With bromine; triphenylphosphine In dichloromethane Ambient temperature; Yield given; |
Conditions | Yield |
---|---|
With stannous octoate In chloroform Reflux; Inert atmosphere; | 82.6% |
Conditions | Yield |
---|---|
With dmap; 2-chloro-1-methyl-pyridinium iodide In N,N-dimethyl acetamide at 20℃; for 12h; Inert atmosphere; | 72.6% |
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In dichloromethane at 25℃; for 1.5h; | 70% |
Conditions | Yield |
---|---|
With triethylamine In chloroform at 20℃; for 12h; Inert atmosphere; | 44% |
melissyl alcohol
1-iodotriacontane
Conditions | Yield |
---|---|
With phosphorus; water; iodine |
Conditions | Yield |
---|---|
With chromium; acetic acid | |
With nitric acid |
Conditions | Yield |
---|---|
With sodium acetate | |
In pyridine | |
With pyridine | |
With pyridine |
melissyl alcohol
1-chlorotriacontane
Conditions | Yield |
---|---|
With phosphorus pentachloride |
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