img _fcksaAppearance:Colorless crystal Storage:Store in dry, dark and ventilated place. Package:according to the clients requirement Application:It is an important raw material and intermediate used in Organic Synthesis, Pharmaceuticals, Agrochemi
Cas:5949-29-1
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inquiryOther Names: citric acid, citric acid monohydra... MF: C6H5O7.2H2O EINECS No.: 201-069-1 Place of Origin: China (Mainland) Type: Acidity Regulat… Appearance:white crystal powder Storage:cool and dry place Package:25kg/bag Application:food ad
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inquiryItem Standard Result Appearance White or colorless crystalline granule or powder Conform Assay
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Cas:5949-29-1
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CAS RN.: 5949-29-1 EINECS: 221-095-7 Molecular Weight:
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inquiryName:Citric acid monohydrate CAS NO: 5949-29-1 Grade:Medical scientific research and export Molecular formula: C6H10O8 Molecular weight:210.1388 Product Quality 12 years of chemical raw materials Mature operation of the industry System
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inquiryCitric acid monohydrate Basic information Product Name: Citric acid monohydrate Synonyms: 1,2,3-Propanetricarboxylic acid, 2-hydroxy-, monohydrate;1,2,3-Propanetricarboxylicacid,2-hydrox
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inquiryDescription: Citric Acid Monohydrate is colorless translucent crystal or white coarse to fine powder crystal. Odorless, but has a taste of strong acidity. It’s easy weathering in dry air, the relative density of 1.542 and the melting
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inquiryConditions | Yield |
---|---|
With sodium hydroxide |
citric acid monohydrate
Conditions | Yield |
---|---|
In methanol at 20℃; for 0.166667h; | 98.8% |
citric acid monohydrate
Conditions | Yield |
---|---|
In methanol at 20℃; for 0.166667h; | 97.8% |
Conditions | Yield |
---|---|
Stage #1: citric acid monohydrate With calcium oxide In water at 20℃; Stage #2: L-lysine In water at 70 - 80℃; for 4h; | 97.1% |
Conditions | Yield |
---|---|
Stage #1: citric acid monohydrate With calcium hydroxide In water at 20℃; Stage #2: L-arginine In water at 70 - 80℃; for 4h; | 96% |
Conditions | Yield |
---|---|
Stage #1: citric acid monohydrate With calcium carbonate In water at 20℃; Stage #2: Acetyl-L-carnitine In water at 70 - 80℃; for 4h; | 95.8% |
citric acid monohydrate
propionyl-L-carnitine
Conditions | Yield |
---|---|
Stage #1: citric acid monohydrate With calcium hydroxide In water at 20℃; Stage #2: propionyl-L-carnitine In water at 70 - 80℃; for 4h; | 95.3% |
ammonia
dihydrogen peroxide
titanium tetrachloride
citric acid monohydrate
zinc(II) carbonate
Conditions | Yield |
---|---|
In water TiCl4 added dropwise to a water on ice bath, H2O2 and acid added, allowed to warm to room temp., carbonate added, pH adjusted to 2 (aq. ammonia); crystd. (THF/water) for several d at 4°C; elem. anal.; | 94.6% |
water
titanium tetrachloride
citric acid monohydrate
lithium hydroxide
Conditions | Yield |
---|---|
In water TiCl4 added dropwise to a water on ice bath, acid added at room temp., pH adjusted to 2 (LiOH); stored for several d at room temp.; elem. anal.; | 93.7% |
citric acid monohydrate
Conditions | Yield |
---|---|
In ethyl acetate at 70℃; for 2h; | 89.5% |
ammonia
dihydrogen peroxide
titanium tetrachloride
citric acid monohydrate
Conditions | Yield |
---|---|
In water addn. of titanium chloride to water at 0°C, addn. of hydrogen peroxide and citric acid, warming to room temp., addn. of gold compd., adjusting pH to 2 by aq. ammonia; crystn. at 4°C from aq. THF, elem. anal.; | 89% |
Conditions | Yield |
---|---|
In water byproducts: H2O; dissolving of Al(NO3)3*9H2O and citric acid monohydrate with 1:2 molar ratio in nano-pure water; stirring at 50°C overnight, rotary evapn. to dryness, redissolving in min. amt. of H2O, adjusting of pH to 4.5 with aq. ammonia; crystn. at 4°C in abs. ethanol, filtration; elem. anal.; | 88.4% |
ammonia
dihydrogen peroxide
titanium tetrachloride
citric acid monohydrate
caesium carbonate
Conditions | Yield |
---|---|
In water TiCl4 added dropwise to H2O, cooled in an ice bath, H2O2 soln. and citric acid monohydrate added, warmed to room temp., treated with Cs2CO3, pH adjusted to 2 using NH3 soln.; crystd. from H2O/THF at 4°C for days; elem. anal.; | 87.4% |
ammonia
dihydrogen peroxide
titanium tetrachloride
lithium carbonate
citric acid monohydrate
Conditions | Yield |
---|---|
In water TiCl4 added dropwise to a water on ice bath, H2O2 and acid added, allowed to warm to room temp., carbonate added, pH adjusted to 2 (aq. ammonia); crystd. (THF/water) for several d at 4°C; elem. anal.; | 86.4% |
water
citric acid monohydrate
[La(citric acis(-3H))(H2O)]
Conditions | Yield |
---|---|
In water High Pressure; under hydrothermal conditions; equimolar mixt. of La2O3 and citric acid in water (pH 2.2-2.5) heated at 120°C for 5 d; ppt. sepd. from hot mixt.; washed with cold water; dried under vac.; elem. anal.; | 85% |
citric acid monohydrate
p-nitrobenzyl (4R,5S,6S)-3-<(3S,5S)-5-dimethylaminocarbonyl-1-(p-nitrobenzyloxycarbonyl)pyrrolidin-3-ylthio>-4-methyl-7-oxo-6-<(1R)-1-trimethylsilyloxoethyl>-1-azabicyclo<3.2.0>hept-2-en-2-carboxylate
p-nitrobenzyl (4R,5S,6S)-3-<(3S,5S)-5-dimethylaminocarbonyl-1-(p-nitrobenzyloxycarbonyl)pyrrolidin-3-ylthio>-6-<(1R)-1-hydroxyethyl>-4-methyl-7-oxo-1-azabicyclo<3.2.0>hept-2-en-2-carboxylate
Conditions | Yield |
---|---|
In methanol | 84% |
In methanol | 84% |
Conditions | Yield |
---|---|
In water High Pressure; under aerobic conditions; citric acid hydrate (2 mmol) and MnCO3 (1 mmol) dissolved in H2O, mixt. heated at 160°C in sealed teflon tube for 3 d; elem. anal.; | 84% |
With Ca(NO3)2 In water High Pressure; under aerobic conditions; citric acid hydrate, Ca(NO3)2, and MnCO3 (molar ratio = 8:1:4-5) dissolved in H2O, mixt. heated at 160°C in sealed teflon tube for 3 d; elem. anal.; |
ethanol
silver(I) citrate
citric acid monohydrate
triphenylphosphine
[(Ph3P)2Ag(H2cit)]*EtOH
Conditions | Yield |
---|---|
In ethanol mixt. Ag3cit, citric acid monohydrate, PPh3 and EtOH was heated with stirring; soln. was filtered hot and allowed to cool slowly, ppt. was colledcted and washed with ice-cold EtOH; elem. anal.; | 84% |
citric acid monohydrate
Conditions | Yield |
---|---|
In ethyl acetate at 70℃; for 1.5h; | 83.1% |
citric acid monohydrate
Conditions | Yield |
---|---|
In ethyl acetate at 70℃; for 1.5h; | 82% |
Conditions | Yield |
---|---|
With KOH In ethanol; water V2O5 dissolved in KOH soln., mixed with an aq. soln. of citric acid monohydrate, 1,10-phenanthroline monohydrate in EtOH added, brought to pH 4.0 with a KOH soln.; crystd. for 2 wk, sepd., washed with EtOH; elem. anal.; | 81% |
citric acid monohydrate
2,2-difluoroethyl triflate
1-(2,2-difluoroethyl)-7-methyl-2-oxo-1,2,3,4-tetrahydroquinoline-6-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide | 81% |
[(1R)-1-{2-[(2,5-difluorophenyl)formamido]acetamido}-3-methylbutyl]boronic acid
citric acid monohydrate
Conditions | Yield |
---|---|
In ethyl acetate at 70℃; for 2h; | 80.5% |
Conditions | Yield |
---|---|
In water aq. KOH was added to an aq. soln. to pH about 2; recrystd. from hot water; elem. anal.; | 80% |
Conditions | Yield |
---|---|
In water pH of aq. soln. of TiCl4 and citric acid monohydrate adjusted to 2.0 by addn. aq. ammonia, stirred for 30 min; ppt. collected and recrystd. from hot water; elem. anal.; | 80% |
Conditions | Yield |
---|---|
In water ZnO (5 mmol) added to aq. soln. of TiCl4 (10 mmol) and citric acid monohydrate (30 mmol); pH adjusted to 2.0 by addn. of NH4OH; elem. anal.; | 80% |
Conditions | Yield |
---|---|
In water Fe (5 mmol) added to aq. soln. of TiCl4 (10 mmol) and citric acid monohydrate (30 mmol); pH adjusted to 2.0 by addn. of NH4OH; elem. anal.; | 80% |
citric acid monohydrate
Conditions | Yield |
---|---|
In ethyl acetate at 70℃; for 0.5h; | 80% |
Conditions | Yield |
---|---|
Stage #1: (5-((2,5-difluorobenzyl)oxy)-1-(3,3-dimethylbutyl)-1H-pyrazol-3-yl)methylmethanesulfonate; methylamine In methanol; toluene at 5℃; for 1.25h; Stage #2: citric acid monohydrate In isopropyl alcohol | 76.3% |
manganese (II) acetate tetrahydrate
tripotassium citrate monohydrate
citric acid monohydrate
KMn(citrate)(H2O)
Conditions | Yield |
---|---|
In ethanol; water High Pressure; 2 equiv. of Mn-salt, 1.5 equiv. of K-citrate and 1.0 equiv. of citric acid were heated in alcohol/H2O at 160 °C for 3 d in a teflon-linedstainless steel autoclave; cooling, crystals were air-dried, elem. anal.; | 76% |
citric acid monohydrate
Conditions | Yield |
---|---|
With ammonium hydroxide In water a soln. of Ce-complex and citric acid in water was stirred for 0.5 h, pHwas adjusted to 5.5 by 5% NH4OH, heated at 70°C for 2 days; evapd., washed with cold water and ethanol, dried in air; elem. anal.; | 76% |
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