Items Standard Result Appearance White crystalline powder Confirm Assay ≥ 99.0%min
Cas:5144-89-8
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for th
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inquiryHigh quality 1,10-Phenanthroline hydrate CAS 5144-89-8 with factory price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/
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inquiryProduct Name: 1,10-Phenanthroline hydrate Synonyms: 1,10-PHENANTHROLINE H2O;1,10-PHENANTHROLINE HYDRATE;1,10-PHENANTHROLINE MONOHYDRATE;1,10-PHENANTHROLINE MONOHYDRATE (O-);ORTHO-PHENANTHROLINE;ORTHOPHENANTHROLINE MONOHYDRATE;O-PHENANT
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryPhenanthroline SeriesCurrent page:Home > Products 1,10-phenathroline(monohydrate) Product Name 1,10-phenathroline(monohydrate) Structural formula CAS No. 5144-89-8 Alias name:Monohydrated phe
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inquiry1,10-Phenanthroline hydrateCAS: 5144-89-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organi
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inquiryMinimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,
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inquiry1,10-phenathroline(monohydrate) CAS: 5144-89-8 Specification Item Standard Test Results Identification A.H-NMR:Comply with the structure Complies B.LC-MS:C
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inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
1,10- PhenanthrolineCAS No: 5144-89-8Formula: C12H8N2?H2OAssay: 99.0% min. Iron coordination compound molar absorption coefficient: 1.15×104≥ L/cm·molResidue on ignition: 0.1% max Application:Used in Synthesis, Pharmaceuticals and other fields Transp
Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryProName: 1,10-Phenanthroline hydrate CasNo: 5144-89-8 Molecular Formula: C12H8N2.H2O Appearance: white crystals or powder Application: It is an important raw material and in... DeliveryTime: prompt PackAge: according to the clients requiremen
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inquiryPacking: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Transportation:Express/Sea/Air Port:Ningbo/Shanghai/Qingd
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide stirred for 10 min; filtered, washed with DMF, acetone and diethyl ether, dried in vac.; elem. anal.; | 99% |
1,10-phenanthroline hydrate
1,2-bis-(diphenylphosphino)ethane
(1,10-phenanthroline)(1,2-bis(diphenylphosphino)ethane)copper(I) tetrafluoroborate
Conditions | Yield |
---|---|
In dichloromethane (N2); Cu complex was reacted with P ligand in CH2Cl2; phenanthroline wasadded after dissolution; mixt. was stirred for 1 h; solvent removed (vac.); Et2O added; pptd.; washed (Et2O); | 99% |
hydrogenchloride
1,10-phenanthroline hydrate
[palladium(II)dichloride(1,10-phenanthroline)]
Conditions | Yield |
---|---|
In water stirring Na2PdCl4 with 1 equiv. ligand and excess HCl (80°C, 30 min); standing at room temp. for several h, collection (filtration), washing (water, MeOH); elem. anal.; | 99% |
1,10-phenanthroline hydrate
copper
1,2-bis-(diphenylphosphino)ethane
[Cu(1,2-bis(diphenylphosphino)ethane)(1,10-phenanthroline)]NO3
Conditions | Yield |
---|---|
In acetonitrile (N2); mixt. of Cu(NO3)2 and Cu in CH3CN was stirred for 2 h; filtered under N2; P ligand and phenanthroline were subsequently added to filtrate;soln. was stirred for 15 min; solvent removed (vac.); extd. (CH2Cl2); CH2Cl2 removed (vac.); Et2O added; washed (Et2O); | 99% |
tetrakis(acetonitrile)copper(I) perchlorate
1,10-phenanthroline hydrate
1,2-bis-(diphenylphosphino)ethane
[Cu(1,2-bis(diphenylphosphino)ethane)(1,10-phenanthroline)]ClO4
Conditions | Yield |
---|---|
In dichloromethane (N2); Cu complex was reacted with P ligand in CH2Cl2; phenanthroline wasadded after dissolution; mixt. was stirred for 1 h; solvent removed (vac.); Et2O added; pptd.; washed (Et2O); | 99% |
1,10-phenanthroline hydrate
5,6-epoxy-5,6-dihydro-[1,10]phenanthroline
Conditions | Yield |
---|---|
With industrial bleach (pH 8.2-8.3 with conc. HCl); tetra(n-butyl)ammonium hydrogensulfate In chloroform; water | 98% |
Conditions | Yield |
---|---|
In ethanol addn. of a soln. of 1,10-phenanthroline*H2O in ethanol to a filtered soln. of Cu(OAc)2*H2O in ethanol; stirring the soln. for 1 h, evapn. of the solvent, washing the residue with benzene and drying in vacuo, elem. anal.; | 98% |
1,10-phenanthroline hydrate
Conditions | Yield |
---|---|
In ethanol; water addn. of a soln. of organic compound in boiling ethanol to a soln. of Ni-salt and B-compound in water with stirring; filtn., washing (warm water, hot ethanol, absolute ether), drying over P2O5, elem. anal.; | 98% |
1,10-phenanthroline hydrate
Conditions | Yield |
---|---|
With CH3COOH; CH3COONa; Na2SO3 In hydrogenchloride; water soln. of MnCl2*4H2O in acetate buffer (pH 4.56) mixed with phen*H2O soln. in aq. HCl (H2O:HCl=1:4), Na2SO3 added, heated at 70°C, hot soln. Cs-Ni-complex in H2O added, stored for 12 h; ppt. filtered off, washed with H2O and C6H6, dried under vac. at 70°C; elem. anal.; | 98% |
1,10-phenanthroline hydrate
Conditions | Yield |
---|---|
With acetate buffer In water Mn salt dissolved in acetate buffer (pH 4.56); 1,10-phenanthroline monohydrate dissolved with stirring in acetate buffer soln.; solns. combined with stirring; soln. heated to 70°C; hot soln. of Cs2B20H18 in H2O added with stirring; ppt. formed; suspn. allowed to coagulate for 12 h; ppt. filtered off on glass frit; washed (H2O); dried (vac., 70°C); | 98% |
1,10-phenanthroline hydrate
Conditions | Yield |
---|---|
With HCl In water Mn compd. dissolved (acetate buffer), mixed with a soln. of ligand (water, dilute HCl (drops)) under stirring, heated to 70°C, a hot soln. of borate added, kept for 12 h at 70°C; ppt. filtered, washed (water), dried (vac., 70°C); elem. anal.; | 98% |
hydrogenchloride
potassium tetrachloroplatinate(II)
1,10-phenanthroline hydrate
dichloro(1,10-phenanthroline)platinum(II)
Conditions | Yield |
---|---|
In water elem. anal.; | 97.7% |
1,10-phenanthroline hydrate
thiourea
Conditions | Yield |
---|---|
In ethanol Co-compound, PHA and Tu were suspended in EtOH; the product was stirred in its mother soln. for many h; washed (EtOH, Et2O); elem.anal.; | 97% |
nitric acid
1,10-phenanthroline hydrate
palladium
Pd(phen)(ONO2)2
Conditions | Yield |
---|---|
With water In ethanol; nitric acid addn. of a soln. of 1,10-phenanthroline*H2O in ethanol to the aq. HNO3 soln. obtained after dissolution of Pd black in concd. HNO3 and dilutionwith water; stirring the soln. at room temp. for 2 h, filtration of the yellow ppt., washing with ethanol and drying in vacuo, elem. anal.; | 97% |
1,10-phenanthroline hydrate
(PdBr2(phen))
Conditions | Yield |
---|---|
In dichloromethane byproducts: IC6H4CH2CH(CO2CH3)NH2; ligand added to a soln. of Pd complex, stirred for 3 h at room temp.; filtered, washed (Et2O), air-dried; | 97% |
1,10-phenanthroline hydrate
[palladium(II)dichloride(1,10-phenanthroline)]
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol; water addn. of concd. HCl to an aq. PdCl2 soln., filtration of the soln. and addn. of a soln of 1,10-phenanthroloine*H2O in ethanol to the filtered soln.; stirring for 2 h, filtering the ppt., washing with ethanol and drying in vacuo, elem. anal.; | 96% |
1,10-phenanthroline hydrate
(1,10-phenanthroline)cadmium(II) bis(tri-tert-butoxysilanethiolate)
Conditions | Yield |
---|---|
In benzene mixing solns. of Cd-complex and ligand in benzene gives instantaneously a white voluminous ppt., addn. of more benzene, refluxing under Ar until a clear soln. is obtained; slow cooling to room temp., pptn., washing with benzene, drying in vacuo, elem. anal.; | 96% |
chloro{2-(dimethylamino)-1-methylpropyl-C,N}(dimethylamine)palladium(II)
1,10-phenanthroline hydrate
Conditions | Yield |
---|---|
In acetone added at 0°C, stirred for 10 min; evaporated to dryness; elem. anal.; | 96% |
1,10-phenanthroline hydrate
Conditions | Yield |
---|---|
In hexane; dichloromethane to a suspn. of (AuAg(C6Cl5)2)n in dichloromethane added 1,10-phenantroline in hexane and stirred at room temp. for 24 h; solid filtered off and washed with diethylether; elem. anal.; | 96% |
1,10-phenanthroline hydrate
chlorobis(triphenylphosphine)(1,10-phenanthroline)palladium(II) hexafluorophosphate
Conditions | Yield |
---|---|
In acetone to suspn. of Pd complex ligand was added, standing for 30 min; soln. was reduced in vac., pptd. with ether, elem. anal.; | 96% |
1,10-phenanthroline hydrate
Conditions | Yield |
---|---|
With HCl In water Mn compd. dissolved (acetate buffer), mixed with a soln. of ligand (water, dilute HCl (drops)) under stirring, heated to 70°C, a hot soln. of borate added, kept for 12 h; ppt. filtered, washed (water), dried (vac., 70°C); elem. anal.; | 96% |
oxalic acid dihydrate
copper(II) acetate monohydrate
1,10-phenanthroline hydrate
[Cu(1,10'-phenanthroline)3][tris(oxalate-O,O')germanate]
Conditions | Yield |
---|---|
In water addn. of distld. water to 1:3:1:3 mixt. of germanium dioxide, oxalic acid, copper acetate and phenanthroline, stirring for 30 min at room temp.,heating at 100°C for 72 h; isolation of crystals, washing with distld. water, filtration, air drying, elem. anal.; | 95.6% |
Ir(OClO3)(C6F4C6H6)2
1,10-phenanthroline hydrate
{Ir(tetrafluorobenzobarrelene)(1,10-phenanthroline)}ClO4
Conditions | Yield |
---|---|
In dichloromethane (N2); complex suspn. treated for 30 min with stoich. amt. of ligand; concd. (vac.), pptd. (ether), filtered off, washed (ether), dried in vac.; elem. anal.; | 95% |
silver tetrafluoroborate
{IrCl(tetrafluorobenzobarrelene)2}
1,10-phenanthroline hydrate
[Ir(C6F4C6H6)(C12H8N2)](1+)*BF4(1-)=[Ir(C6F4C6H6)(C12H8N2)]BF4
Conditions | Yield |
---|---|
In acetone byproducts: AgCl; under N2 and protected from daylight complex suspn. in acetone or CH2Cl2 treated for 30 min with ligand and with AgBF4 in acetone; AgCl filtered off, filtrate concd. (vac.), pptd. (ether), filtered off,washed with ether, dried in vac.; elem. anal.; | 95% |
Conditions | Yield |
---|---|
In ethanol mixt. of ZnCO3, α-hydroxycarboxylic acid, and diamine in EtOH refluxed for 4 h, allowed to cool to room temp., stirred for 1 wk; recrystd. from nethanol/isopropanol (1/1), dried under vac.; elem. anal.; | 95% |
1,10-phenanthroline hydrate
Conditions | Yield |
---|---|
With HCl In water; N,N-dimethyl-formamide High Pressure; solvothermal synthesis; mixt. of Pb(NO3)2, phen*H2O, CuCl2*2H2O (0.5:1:0.5 mmol) in DMF with 36 % aq. HCl (1 ml) heated in Teflon-lined stainless steel vessel at 120°C for 3 d; cooled to room temp. (rate 3°C/h); elem. anal.; | 95% |
1,10-phenanthroline hydrate
Conditions | Yield |
---|---|
In benzene addn. of phen*H2O to anhyd. benzene, refluxing (until a clear soln. was obtained), addn. of soln. of ((t-BuO)3SiSCu)4 (colour change to deep red), left to stand, 1 day, room temp., pptn.; filtered, washed (hexane), vac. dried, elem. anal.; | 94% |
1,10-phenanthroline hydrate
Conditions | Yield |
---|---|
In isopropyl alcohol soln. of Er-comp. in isopropanol treated with isopropanol-soln. of 2,2'-1,10-phenantroline monohydrate, mixt.allowed to stay for 24 h; filtered, crystals dried over P4O10, elem. anal.; | 94% |
bis(dimethylphenylphosphine)bis(monothiobenzoato)ruthenium(II)
1,10-phenanthroline hydrate
bis(dimethylphenylphosphine)bis(monothiobenzoato)(1,10-phenanthroline)ruthenium(II)
Conditions | Yield |
---|---|
In ethanol reflux for 2 h under N2; the volume of the soln. reduced, after standing for some h the product filtered; elem. anal.; | 94% |
potassium tetrachloroplatinate(II)
1,10-phenanthroline hydrate
Conditions | Yield |
---|---|
In ethanol; water addn. of a soln. of organic compound in ethanol to a soln. of B-compound in water, addn. of a soln. of Pt-complex in water, keeping the mixtureat 35°C. for 24 h; filtn., washing (warm water, ethanol, absolute ether), drying in vac. over P2O5, elem. anal.; | 94% |
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