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Hangzhou Dingyan Chem Co., Ltd

Items Standard Result Appearance White crystalline powder Confirm Assay ≥ 99.0%min

High purity 1-10 phenanthroline monohydrate with high quality and best price cas:5144-89-8

Cas:5144-89-8

Min.Order:1 Kilogram

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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for th

1,10-Phenanthroline hydrate

Cas:5144-89-8

Min.Order:100 Gram

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Hangzhou Ocean Chemical Co., Ltd.

★.Best quality according to requirement ★.Competitive price in China market ★.Mature Technical support ★.Professional logistic support ★.Shortest delivery time . There are several standard production bases in Zhejiang, Jiangsu and Sha

1,10-Phenanthroline hydrate

Cas:5144-89-8

Min.Order:1 Kilogram

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Wuhan Kemi-Works Chemical Co., Ltd

Superiority : 1.ISO certificate 2..Powerful R & D team 3.The ability of quantized production,from grams to tons; 4.Various kinds of advanced equipment in the laboratory and plant; 5.Strict QC standard to meet the demand of customers,a

1,10-Phenanthroline hydrate CAS NO.5144-89-8

Cas:5144-89-8

Min.Order:1 Kilogram

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 1,10-Phenathroline(Monohydrate)

Cas:5144-89-8

Min.Order:1 Kilogram

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Wuhan Fortuna Chemical Co.,Ltd

High quality 1,10-Phenanthroline hydrate CAS 5144-89-8 with factory price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/

High quality 1,10-Phenanthroline hydrate CAS 5144-89-8 with factory price

Cas:5144-89-8

Min.Order:10 Kilogram

FOB Price: $10.0

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Henan Allgreen Chemical Co.,Ltd

T he company has advanced technology, as well as a large number of excellent R & D team, to provide customers from the grams to one hundred kilograms and tons of high-quality products, competitive prices and quality service Appearance:white

1,10-Phenanthroline

Cas:5144-89-8

Min.Order:1 Kilogram

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 1,10-Phenanthroline hydrate

Cas:5144-89-8

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Hebei yanxi chemical co.,LTD.

chengdu and import and export trade co., LTD., who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do res

1,10-Phenanthroline hydrate

Cas:5144-89-8

Min.Order:10 Kilogram

FOB Price: $90.0

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Henan Tianfu Chemical Co., Ltd.

Product Name: 1,10-Phenanthroline hydrate Synonyms: 1,10-PHENANTHROLINE H2O;1,10-PHENANTHROLINE HYDRATE;1,10-PHENANTHROLINE MONOHYDRATE;1,10-PHENANTHROLINE MONOHYDRATE (O-);ORTHO-PHENANTHROLINE;ORTHOPHENANTHROLINE MONOHYDRATE;O-PHENANT

5144-89-8 1,10-Phenanthroline hydrate

Cas:5144-89-8

Min.Order:1 Gram

FOB Price: $8900.0

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Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

1,10-Phenanthroline hydrate

Cas:5144-89-8

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

High Purity CAS 5144-89-8 with high quality products

Cas:5144-89-8

Min.Order:10 Gram

FOB Price: $146.0 / 176.0

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Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages ♦ High purity, all above 98.5%, no impurities after the dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available &diam

o-Phenanthroline monohydrate CAS5144-89-8

Cas:5144-89-8

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Factory Supply High Quality CAS 5144-89-8 ,1,10-Phenanthroline hydrate

Cas:5144-89-8

Min.Order:10 Kilogram

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Henan Sinotech Import&Export Corporation

Phenanthroline SeriesCurrent page:Home > Products 1,10-phenathroline(monohydrate) Product Name 1,10-phenathroline(monohydrate) Structural formula CAS No. 5144-89-8 Alias name:Monohydrated phe

1,10-phenathroline(monohydrate)

Cas:5144-89-8

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

1,10-Phenanthroline hydrate 5144-89-8

Cas:5144-89-8

Min.Order:1 Kilogram

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Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present

1,10-Phenanthroline hydrate/CAS:5144-89-8

Cas:5144-89-8

Min.Order:1 Kilogram

FOB Price: $245.0 / 300.0

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Qingdao Beluga Import and Export Co., LTD

1,10-Phenanthroline hydrateCAS: 5144-89-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organi

1,10-Phenanthroline hydrateCAS: 5144-89-8

Cas:5144-89-8

Min.Order:1 Gram

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Changchun Artel lmport and Export trade company

Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,

1,10-Phenanthroline hydrate supplier in China CAS NO.5144-89-8

Cas:5144-89-8

Min.Order:10 Gram

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Lonwin Chemical Group Limited

1,10-phenathroline(monohydrate) CAS: 5144-89-8 Specification Item Standard Test Results Identification A.H-NMR:Comply with the structure Complies B.LC-MS:C

Factory supply 1,10-phenathroline(monohydrate)

Cas:5144-89-8

Min.Order:1 Kilogram

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Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

1,10-Phenanthroline monohydrate

Cas:5144-89-8

Min.Order:1 Kilogram

FOB Price: $40.0 / 50.0

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

1,10-Phenanthroline hydrate

Cas:5144-89-8

Min.Order:0

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

1,10-Phenanthroline Hydrate

Cas:5144-89-8

Min.Order:0

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HUBEI RISON CHEMICAL CO.,LTD.

1,10- PhenanthrolineCAS No: 5144-89-8Formula: C12H8N2?H2OAssay: 99.0% min. Iron coordination compound molar absorption coefficient: 1.15×104≥ L/cm·molResidue on ignition: 0.1% max Application:Used in Synthesis, Pharmaceuticals and other fields Transp

1,10- Phenanthroline

Cas:5144-89-8

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Afine Chemicals Limited

Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter

1,10-Phenanthroline hydrate

Cas:5144-89-8

Min.Order:1 Kilogram

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

1,10-Phenanthroline hydrate

Cas:5144-89-8

Min.Order:0 Metric Ton

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

1,10-Phenanthroline hydrate

Cas:5144-89-8

Min.Order:0

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SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

4-bromo-2-fluorotoluene

Cas:5144-89-8

Min.Order:4 Kilogram

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Saiwante (shanghai) New Material Technology Co., Ltd.

ProName: 1,10-Phenanthroline hydrate CasNo: 5144-89-8 Molecular Formula: C12H8N2.H2O Appearance: white crystals or powder Application: It is an important raw material and in... DeliveryTime: prompt PackAge: according to the clients requiremen

1,10-Phenanthroline hydrate

Cas:5144-89-8

Min.Order:1 Gram

FOB Price: $6.0 / 9.0

Type:Trading Company

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Hangzhou Fonlynn Health Technology Co., Ltd.

Packing: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Transportation:Express/Sea/Air Port:Ningbo/Shanghai/Qingd

1,10-Phenanthroline hydrate

Cas:5144-89-8

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Synthetic route

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

{Mn3(O2CCH3)6(1,10-phenanthroline)2}

{Mn3(O2CCH3)6(1,10-phenanthroline)2}

Conditions
ConditionsYield
In N,N-dimethyl-formamide stirred for 10 min; filtered, washed with DMF, acetone and diethyl ether, dried in vac.; elem. anal.;99%
tetrakis(acetonitrile)copper(I)tetrafluoroborate

tetrakis(acetonitrile)copper(I)tetrafluoroborate

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

1,2-bis-(diphenylphosphino)ethane
1663-45-2

1,2-bis-(diphenylphosphino)ethane

(1,10-phenanthroline)(1,2-bis(diphenylphosphino)ethane)copper(I) tetrafluoroborate
498584-34-2

(1,10-phenanthroline)(1,2-bis(diphenylphosphino)ethane)copper(I) tetrafluoroborate

Conditions
ConditionsYield
In dichloromethane (N2); Cu complex was reacted with P ligand in CH2Cl2; phenanthroline wasadded after dissolution; mixt. was stirred for 1 h; solvent removed (vac.); Et2O added; pptd.; washed (Et2O);99%
hydrogenchloride
7647-01-0

hydrogenchloride

sodium tetrachloropalladate(II)

sodium tetrachloropalladate(II)

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

[palladium(II)dichloride(1,10-phenanthroline)]
14783-10-9

[palladium(II)dichloride(1,10-phenanthroline)]

Conditions
ConditionsYield
In water stirring Na2PdCl4 with 1 equiv. ligand and excess HCl (80°C, 30 min); standing at room temp. for several h, collection (filtration), washing (water, MeOH); elem. anal.;99%
Conditions
ConditionsYield
In acetonitrile (N2); mixt. of Cu(NO3)2 and Cu in CH3CN was stirred for 2 h; filtered under N2; P ligand and phenanthroline were subsequently added to filtrate;soln. was stirred for 15 min; solvent removed (vac.); extd. (CH2Cl2); CH2Cl2 removed (vac.); Et2O added; washed (Et2O);99%
tetrakis(acetonitrile)copper(I) perchlorate
14057-91-1

tetrakis(acetonitrile)copper(I) perchlorate

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

1,2-bis-(diphenylphosphino)ethane
1663-45-2

1,2-bis-(diphenylphosphino)ethane

[Cu(1,2-bis(diphenylphosphino)ethane)(1,10-phenanthroline)]ClO4
498584-33-1

[Cu(1,2-bis(diphenylphosphino)ethane)(1,10-phenanthroline)]ClO4

Conditions
ConditionsYield
In dichloromethane (N2); Cu complex was reacted with P ligand in CH2Cl2; phenanthroline wasadded after dissolution; mixt. was stirred for 1 h; solvent removed (vac.); Et2O added; pptd.; washed (Et2O);99%
1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

5,6-epoxy-5,6-dihydro-[1,10]phenanthroline
65115-91-5

5,6-epoxy-5,6-dihydro-[1,10]phenanthroline

Conditions
ConditionsYield
With industrial bleach (pH 8.2-8.3 with conc. HCl); tetra(n-butyl)ammonium hydrogensulfate In chloroform; water98%
copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

(1,10-Phen)Cu(OAc)2

(1,10-Phen)Cu(OAc)2

Conditions
ConditionsYield
In ethanol addn. of a soln. of 1,10-phenanthroline*H2O in ethanol to a filtered soln. of Cu(OAc)2*H2O in ethanol; stirring the soln. for 1 h, evapn. of the solvent, washing the residue with benzene and drying in vacuo, elem. anal.;98%
nickel(II) chloride hexahydrate

nickel(II) chloride hexahydrate

dicesium dodecachloro-closo-dodecaborate

dicesium dodecachloro-closo-dodecaborate

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

[nickel(II)(1,10-phenanthroline)3]B12Cl12

[nickel(II)(1,10-phenanthroline)3]B12Cl12

Conditions
ConditionsYield
In ethanol; water addn. of a soln. of organic compound in boiling ethanol to a soln. of Ni-salt and B-compound in water with stirring; filtn., washing (warm water, hot ethanol, absolute ether), drying over P2O5, elem. anal.;98%
manganese(II) chloride tetrahydrate

manganese(II) chloride tetrahydrate

caesium [3,3'-commo-bis(η5-nonahydro-1,2-dicarba-3-nickel-closo-decarborate)]

caesium [3,3'-commo-bis(η5-nonahydro-1,2-dicarba-3-nickel-closo-decarborate)]

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

[Mn(II)(1,10-phenantroline)3][bis(η5-1,2-B9C2H11)nickeliate(III)]2

[Mn(II)(1,10-phenantroline)3][bis(η5-1,2-B9C2H11)nickeliate(III)]2

Conditions
ConditionsYield
With CH3COOH; CH3COONa; Na2SO3 In hydrogenchloride; water soln. of MnCl2*4H2O in acetate buffer (pH 4.56) mixed with phen*H2O soln. in aq. HCl (H2O:HCl=1:4), Na2SO3 added, heated at 70°C, hot soln. Cs-Ni-complex in H2O added, stored for 12 h; ppt. filtered off, washed with H2O and C6H6, dried under vac. at 70°C; elem. anal.;98%
manganese(II) chloride tetrahydrate

manganese(II) chloride tetrahydrate

cesium 1,2;1',2'-trans-bis[nonahydro-closo-decaborate]

cesium 1,2;1',2'-trans-bis[nonahydro-closo-decaborate]

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

[tris(1,10-phenanthroline)manganese(II)] 1,2;1',2'-trans-bis[nonahydro-closo-decaborate]

[tris(1,10-phenanthroline)manganese(II)] 1,2;1',2'-trans-bis[nonahydro-closo-decaborate]

Conditions
ConditionsYield
With acetate buffer In water Mn salt dissolved in acetate buffer (pH 4.56); 1,10-phenanthroline monohydrate dissolved with stirring in acetate buffer soln.; solns. combined with stirring; soln. heated to 70°C; hot soln. of Cs2B20H18 in H2O added with stirring; ppt. formed; suspn. allowed to coagulate for 12 h; ppt. filtered off on glass frit; washed (H2O); dried (vac., 70°C);98%
manganese(II) chloride tetrahydrate

manganese(II) chloride tetrahydrate

cesium nido-1,2-dicarbaundecaborate

cesium nido-1,2-dicarbaundecaborate

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

tris-(1,10-phenanthroline)manganese(II) nido-1,2-dicarbaundecaborate

tris-(1,10-phenanthroline)manganese(II) nido-1,2-dicarbaundecaborate

Conditions
ConditionsYield
With HCl In water Mn compd. dissolved (acetate buffer), mixed with a soln. of ligand (water, dilute HCl (drops)) under stirring, heated to 70°C, a hot soln. of borate added, kept for 12 h at 70°C; ppt. filtered, washed (water), dried (vac., 70°C); elem. anal.;98%
hydrogenchloride
7647-01-0

hydrogenchloride

potassium tetrachloroplatinate(II)
10025-99-7

potassium tetrachloroplatinate(II)

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

dichloro(1,10-phenanthroline)platinum(II)
18432-95-6

dichloro(1,10-phenanthroline)platinum(II)

Conditions
ConditionsYield
In water elem. anal.;97.7%
1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

cobalt(II) perchlorate hexahydrate

cobalt(II) perchlorate hexahydrate

thiourea
17356-08-0

thiourea

{Co(C12H8N2)3(SC(NH2)2)}(2+)*2(ClO4)(1-) = Co(ClO4)2(C12H8N2)3(SC(NH2)2)

{Co(C12H8N2)3(SC(NH2)2)}(2+)*2(ClO4)(1-) = Co(ClO4)2(C12H8N2)3(SC(NH2)2)

Conditions
ConditionsYield
In ethanol Co-compound, PHA and Tu were suspended in EtOH; the product was stirred in its mother soln. for many h; washed (EtOH, Et2O); elem.anal.;97%
nitric acid
7697-37-2

nitric acid

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

palladium
7440-05-3

palladium

Pd(phen)(ONO2)2
31476-92-3

Pd(phen)(ONO2)2

Conditions
ConditionsYield
With water In ethanol; nitric acid addn. of a soln. of 1,10-phenanthroline*H2O in ethanol to the aq. HNO3 soln. obtained after dissolution of Pd black in concd. HNO3 and dilutionwith water; stirring the soln. at room temp. for 2 h, filtration of the yellow ppt., washing with ethanol and drying in vacuo, elem. anal.;97%
trans-(S,S)-[PdBr2(NH2CH(CO2Me)CH2C6H4-I-2)2]

trans-(S,S)-[PdBr2(NH2CH(CO2Me)CH2C6H4-I-2)2]

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

(PdBr2(phen))
41876-11-3

(PdBr2(phen))

Conditions
ConditionsYield
In dichloromethane byproducts: IC6H4CH2CH(CO2CH3)NH2; ligand added to a soln. of Pd complex, stirred for 3 h at room temp.; filtered, washed (Et2O), air-dried;97%
1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

palladium dichloride

palladium dichloride

[palladium(II)dichloride(1,10-phenanthroline)]
14783-10-9

[palladium(II)dichloride(1,10-phenanthroline)]

Conditions
ConditionsYield
With hydrogenchloride In ethanol; water addn. of concd. HCl to an aq. PdCl2 soln., filtration of the soln. and addn. of a soln of 1,10-phenanthroloine*H2O in ethanol to the filtered soln.; stirring for 2 h, filtering the ppt., washing with ethanol and drying in vacuo, elem. anal.;96%
cadmium(II) bis(tri-tert-butoxysilanethiolate)

cadmium(II) bis(tri-tert-butoxysilanethiolate)

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

(1,10-phenanthroline)cadmium(II) bis(tri-tert-butoxysilanethiolate)
142372-83-6

(1,10-phenanthroline)cadmium(II) bis(tri-tert-butoxysilanethiolate)

Conditions
ConditionsYield
In benzene mixing solns. of Cd-complex and ligand in benzene gives instantaneously a white voluminous ppt., addn. of more benzene, refluxing under Ar until a clear soln. is obtained; slow cooling to room temp., pptn., washing with benzene, drying in vacuo, elem. anal.;96%
chloro{2-(dimethylamino)-1-methylpropyl-C,N}(dimethylamine)palladium(II)
91409-21-1

chloro{2-(dimethylamino)-1-methylpropyl-C,N}(dimethylamine)palladium(II)

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

{2-(dimethylamino)-1-methylpropyl-C,N}(phenanthroline)palladium(II) chloride

{2-(dimethylamino)-1-methylpropyl-C,N}(phenanthroline)palladium(II) chloride

Conditions
ConditionsYield
In acetone added at 0°C, stirred for 10 min; evaporated to dryness; elem. anal.;96%
[{Au(C6Cl5)2}Ag]n

[{Au(C6Cl5)2}Ag]n

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

Au(1+)*Ag(1+)*2C6Cl5(1-)*N2C12H8=(AuAg(C6Cl5)2(N2C12H8))

Au(1+)*Ag(1+)*2C6Cl5(1-)*N2C12H8=(AuAg(C6Cl5)2(N2C12H8))

Conditions
ConditionsYield
In hexane; dichloromethane to a suspn. of (AuAg(C6Cl5)2)n in dichloromethane added 1,10-phenantroline in hexane and stirred at room temp. for 24 h; solid filtered off and washed with diethylether; elem. anal.;96%
chlorotris(triphenylphosphine)palladium(II) hexafluorophosphate * acetone

chlorotris(triphenylphosphine)palladium(II) hexafluorophosphate * acetone

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

chlorobis(triphenylphosphine)(1,10-phenanthroline)palladium(II) hexafluorophosphate
101019-70-9

chlorobis(triphenylphosphine)(1,10-phenanthroline)palladium(II) hexafluorophosphate

Conditions
ConditionsYield
In acetone to suspn. of Pd complex ligand was added, standing for 30 min; soln. was reduced in vac., pptd. with ether, elem. anal.;96%
caesium cobalt(III)bis(1,2-dicarboilide)

caesium cobalt(III)bis(1,2-dicarboilide)

manganese(II) chloride tetrahydrate

manganese(II) chloride tetrahydrate

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

tris-(1,10-phenanthroline)manganese(II) 3,3-commo-bis[η5-1,2-dicarba-(3)-cobalt(III)-closo-dodecaborate]

tris-(1,10-phenanthroline)manganese(II) 3,3-commo-bis[η5-1,2-dicarba-(3)-cobalt(III)-closo-dodecaborate]

Conditions
ConditionsYield
With HCl In water Mn compd. dissolved (acetate buffer), mixed with a soln. of ligand (water, dilute HCl (drops)) under stirring, heated to 70°C, a hot soln. of borate added, kept for 12 h; ppt. filtered, washed (water), dried (vac., 70°C); elem. anal.;96%
oxalic acid dihydrate
6153-56-6

oxalic acid dihydrate

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

germanium dioxide

germanium dioxide

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

[Cu(1,10'-phenanthroline)3][tris(oxalate-O,O')germanate]
947503-45-9

[Cu(1,10'-phenanthroline)3][tris(oxalate-O,O')germanate]

Conditions
ConditionsYield
In water addn. of distld. water to 1:3:1:3 mixt. of germanium dioxide, oxalic acid, copper acetate and phenanthroline, stirring for 30 min at room temp.,heating at 100°C for 72 h; isolation of crystals, washing with distld. water, filtration, air drying, elem. anal.;95.6%
Ir(OClO3)(C6F4C6H6)2
90634-69-8

Ir(OClO3)(C6F4C6H6)2

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

{Ir(tetrafluorobenzobarrelene)(1,10-phenanthroline)}ClO4
90634-76-7

{Ir(tetrafluorobenzobarrelene)(1,10-phenanthroline)}ClO4

Conditions
ConditionsYield
In dichloromethane (N2); complex suspn. treated for 30 min with stoich. amt. of ligand; concd. (vac.), pptd. (ether), filtered off, washed (ether), dried in vac.; elem. anal.;95%
silver tetrafluoroborate
14104-20-2

silver tetrafluoroborate

{IrCl(tetrafluorobenzobarrelene)2}
88478-63-1

{IrCl(tetrafluorobenzobarrelene)2}

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

[Ir(C6F4C6H6)(C12H8N2)](1+)*BF4(1-)=[Ir(C6F4C6H6)(C12H8N2)]BF4
90634-85-8

[Ir(C6F4C6H6)(C12H8N2)](1+)*BF4(1-)=[Ir(C6F4C6H6)(C12H8N2)]BF4

Conditions
ConditionsYield
In acetone byproducts: AgCl; under N2 and protected from daylight complex suspn. in acetone or CH2Cl2 treated for 30 min with ligand and with AgBF4 in acetone; AgCl filtered off, filtrate concd. (vac.), pptd. (ether), filtered off,washed with ether, dried in vac.; elem. anal.;95%
2-methyllactic acid
594-61-6

2-methyllactic acid

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

zinc(II) carbonate
743369-26-8

zinc(II) carbonate

[Zn(2-methyllactate)(1,10-phenanthroline)2](2-methyllactate)*4H2O

[Zn(2-methyllactate)(1,10-phenanthroline)2](2-methyllactate)*4H2O

Conditions
ConditionsYield
In ethanol mixt. of ZnCO3, α-hydroxycarboxylic acid, and diamine in EtOH refluxed for 4 h, allowed to cool to room temp., stirred for 1 wk; recrystd. from nethanol/isopropanol (1/1), dried under vac.; elem. anal.;95%
lead(II) nitrate

lead(II) nitrate

copper(II) choride dihydrate

copper(II) choride dihydrate

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

poly[chlorobis(1,10-phenanthroline)copper(II) trichloroplumbate(II)]

poly[chlorobis(1,10-phenanthroline)copper(II) trichloroplumbate(II)]

Conditions
ConditionsYield
With HCl In water; N,N-dimethyl-formamide High Pressure; solvothermal synthesis; mixt. of Pb(NO3)2, phen*H2O, CuCl2*2H2O (0.5:1:0.5 mmol) in DMF with 36 % aq. HCl (1 ml) heated in Teflon-lined stainless steel vessel at 120°C for 3 d; cooled to room temp. (rate 3°C/h); elem. anal.;95%
cyclo-tetrakis-{tri-tert-butoxysilanethiolatocopper(I)}

cyclo-tetrakis-{tri-tert-butoxysilanethiolatocopper(I)}

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

((CH3)3CO)3SiS(1-)*Cu(1+)*C12H8N2=((CH3)3CO)3SiSCu*C12H8N2

((CH3)3CO)3SiS(1-)*Cu(1+)*C12H8N2=((CH3)3CO)3SiSCu*C12H8N2

Conditions
ConditionsYield
In benzene addn. of phen*H2O to anhyd. benzene, refluxing (until a clear soln. was obtained), addn. of soln. of ((t-BuO)3SiSCu)4 (colour change to deep red), left to stand, 1 day, room temp., pptn.; filtered, washed (hexane), vac. dried, elem. anal.;94%
erbium(III) nitrate pentahydrate

erbium(III) nitrate pentahydrate

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

trinitrato-bis-(1,10-phenantroline)erbium(III)

trinitrato-bis-(1,10-phenantroline)erbium(III)

Conditions
ConditionsYield
In isopropyl alcohol soln. of Er-comp. in isopropanol treated with isopropanol-soln. of 2,2'-1,10-phenantroline monohydrate, mixt.allowed to stay for 24 h; filtered, crystals dried over P4O10, elem. anal.;94%
bis(dimethylphenylphosphine)bis(monothiobenzoato)ruthenium(II)
81704-56-5, 68249-87-6

bis(dimethylphenylphosphine)bis(monothiobenzoato)ruthenium(II)

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

bis(dimethylphenylphosphine)bis(monothiobenzoato)(1,10-phenanthroline)ruthenium(II)
74244-05-6, 74215-94-4

bis(dimethylphenylphosphine)bis(monothiobenzoato)(1,10-phenanthroline)ruthenium(II)

Conditions
ConditionsYield
In ethanol reflux for 2 h under N2; the volume of the soln. reduced, after standing for some h the product filtered; elem. anal.;94%
potassium tetrachloroplatinate(II)
10025-99-7

potassium tetrachloroplatinate(II)

dicesium dodecachloro-closo-dodecaborate

dicesium dodecachloro-closo-dodecaborate

1,10-phenanthroline hydrate
5144-89-8

1,10-phenanthroline hydrate

[platinum(II)(1,10-phenanthroline)2]B12Cl12

[platinum(II)(1,10-phenanthroline)2]B12Cl12

Conditions
ConditionsYield
In ethanol; water addn. of a soln. of organic compound in ethanol to a soln. of B-compound in water, addn. of a soln. of Pt-complex in water, keeping the mixtureat 35°C. for 24 h; filtn., washing (warm water, ethanol, absolute ether), drying in vac. over P2O5, elem. anal.;94%
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