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inquiryItems Standard Result Appearance An odorless almost white or buffcolored powder Conform Specific rotation
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inquiryFounded in 2014, Kono Chem Co., Ltd is an export-oriented production enterprise supported by the State Department of Commerce. Kono Chem covers an area of 312,000 square meters, with scientific and technological personnel accounting for more than 35%
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inquiryProduct Name: L-Thyroxine CAS No.: 51-48-9 Molecular formula: C15H11I4NO4 Molecular weight: 776 Appearance: beige powder Appearance: white powder Storage:Store in cool and dry place,
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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Product Name: L-Thyroxine Synonyms: 3,5,3’,5’-tetraiodothyronine;beta-[(3,5-diiodo-4-hydroxyphenoxy)-3,5-diiodophenyl]alanine;l-3,5,3’,5’-tetraiodothyronine;l-t4;o-(4-hydroxy-3,5-diiodophenyl)-3,5-diiod
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inquiryOur Advantage & Service 1.Top quality: Using high quality material and establishing a strict quality control system,assigning specific persons in charge of each part of production,from raw material purchase to assembly. 2 Professional R&D
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inquiry3,5-diiodo-L-thyronine
L-thyroxine
Conditions | Yield |
---|---|
With sodium hypochlorite; tert-butylamine; sodium iodide In methanol at 20 - 30℃; Reagent/catalyst; Solvent; | 100% |
With iodine; methylamine; potassium iodide In water at 0 - 5℃; for 2h; | 95% |
With iodine; potassium iodide; sodium hydroxide In water at -10 - 10℃; Reagent/catalyst; Temperature; | 76.7% |
With water; iodine; ethylamine; potassium iodide | |
With ammonia; iodine; potassium iodide |
L-thyroxine
Conditions | Yield |
---|---|
With hydrogenchloride In methanol; dimethyl sulfoxide | 96% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 24℃; for 16h; 0.2 M borate buffer, pH 8.0 (add. of 0.1 M NaOH); | 94% |
Conditions | Yield |
---|---|
Stage #1: 3,3′-diiodothyronine With methylamine In methanol at 25 - 30℃; Stage #2: With iodine In methanol at -8 - 0℃; Stage #3: With potassium dihydrogenphosphate; sodium hydrogensulfite In methanol at 15 - 20℃; | 91.2% |
Conditions | Yield |
---|---|
With sodium hydroxide; dihydrogen peroxide; butan-1-ol | |
Multi-step reaction with 4 steps 1.1: sodium hydroxide / water / 1 h 1.2: 2 h / 20 - 40 °C 2.1: diisopropylamine / water; butan-1-ol / 2 h / 20 - 90 °C 2.2: 2 h / 20 - 30 °C 3.1: acetic acid; hydrogen iodide / 5 h / 100 °C 4.1: methylamine / methanol / 25 - 30 °C 4.2: -8 - 0 °C 4.3: 15 - 20 °C View Scheme |
Conditions | Yield |
---|---|
With air; water at 37℃; Erhitzen des Reaktionsprodukts mit wss. Salzsaeure und Essigsaeure; |
Conditions | Yield |
---|---|
at 0℃; for 0.75h; Yield given; |
Conditions | Yield |
---|---|
With methanol; triethylamine |
1-methyl-4-nitrosobenzene
3,5-diiodo-l-tyrosine
dihydrogen peroxide
butan-1-ol
L-thyroxine
L-thyroxine
Conditions | Yield |
---|---|
Jodierung und anschliessende Hydrolyse; |
L-thyroxine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 37 percent / NaBiO3 / ethyl acetate; acetic acid; H2O / 4 h 2: 94 percent / dimethylformamide / 16 h / 24 °C / 0.2 M borate buffer, pH 8.0 (add. of 0.1 M NaOH) View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 2: (-)-α-phenethylamine; water 3: hydrobromic acid 4: concentrated ammonia; potassium iodide; iodine View Scheme |
3.5-diiodo-N.O-diacetyl-L-tyrosine
L-thyroxine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. NaOH solution 2: water; air / 37 °C / Erhitzen des Reaktionsprodukts mit wss. Salzsaeure und Essigsaeure View Scheme |
N-formyl-3,5-diiodo-DL-thyronine
L-thyroxine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: (-)-α-phenethylamine; water 2: hydrobromic acid 3: concentrated ammonia; potassium iodide; iodine View Scheme |
N-formyl-3,5-diiodo-L-thyronine
L-thyroxine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrobromic acid 2: concentrated ammonia; potassium iodide; iodine View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: acetic acid; iodine monochloride 2: aq. NaOH solution; butanol-(1); aqueous hydrogen peroxide View Scheme | |
Multi-step reaction with 8 steps 1: hydrogenchloride / water / 24 h / 20 °C 2: sodium hydrogencarbonate / water; tetrahydrofuran / 24 h / 20 °C 3: N-iodo-succinimide / dichloromethane / 0.67 h / 0 °C 4: N-ethyl-N,N-diisopropylamine; pyridine; copper diacetate / dichloromethane / 48 h / 20 °C / Molecular sieve 5: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / 0 - 20 °C 6: Iodine monochloride; N-butylamine / dichloromethane; N,N-dimethyl-formamide / 0.33 h / 0 °C 7: lithium hydroxide / water; methanol / 1.5 h / 4 °C 8: hydrogenchloride / 1,4-dioxane / 20 °C / Inert atmosphere View Scheme |
L-thyroxine
Conditions | Yield |
---|---|
With hydrogenchloride In water at 20℃; for 1h; pH=~ 4 - 5; |
Conditions | Yield |
---|---|
With chiral stationary phase including isopropyl-functionalized CF6 In methanol; acetic acid; triethylamine; acetonitrile at 20℃; Purification / work up; |
methyl (S)-2-((tert-butoxycarbonyl)amino)-3-(4-(4-hydroxy-3,5-diaiodophenoxy)-3,5-diaiodophenyl)propanoate
L-thyroxine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: lithium hydroxide / water; methanol / 1.5 h / 4 °C 2: hydrogenchloride / 1,4-dioxane / 20 °C / Inert atmosphere View Scheme |
L-thyroxine
Conditions | Yield |
---|---|
With hydrogenchloride In 1,4-dioxane at 20℃; Inert atmosphere; |
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: sodium hydrogencarbonate / water; tetrahydrofuran / 24 h / 20 °C 2: N-iodo-succinimide / dichloromethane / 0.67 h / 0 °C 3: N-ethyl-N,N-diisopropylamine; pyridine; copper diacetate / dichloromethane / 48 h / 20 °C / Molecular sieve 4: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / 0 - 20 °C 5: Iodine monochloride; N-butylamine / dichloromethane; N,N-dimethyl-formamide / 0.33 h / 0 °C 6: lithium hydroxide / water; methanol / 1.5 h / 4 °C 7: hydrogenchloride / 1,4-dioxane / 20 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: N-iodo-succinimide / dichloromethane / 0.67 h / 0 °C 2: N-ethyl-N,N-diisopropylamine; pyridine; copper diacetate / dichloromethane / 48 h / 20 °C / Molecular sieve 3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / 0 - 20 °C 4: Iodine monochloride; N-butylamine / dichloromethane; N,N-dimethyl-formamide / 0.33 h / 0 °C 5: lithium hydroxide / water; methanol / 1.5 h / 4 °C 6: hydrogenchloride / 1,4-dioxane / 20 °C / Inert atmosphere View Scheme |
(S)-methyl 2-((tert-butoxycarbonyl)amino)-3-(4-hydroxy-3,5-diiodophenyl)propanoate
L-thyroxine
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: N-ethyl-N,N-diisopropylamine; pyridine; copper diacetate / dichloromethane / 48 h / 20 °C / Molecular sieve 2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / 0 - 20 °C 3: Iodine monochloride; N-butylamine / dichloromethane; N,N-dimethyl-formamide / 0.33 h / 0 °C 4: lithium hydroxide / water; methanol / 1.5 h / 4 °C 5: hydrogenchloride / 1,4-dioxane / 20 °C / Inert atmosphere View Scheme |
C30H43I2NO6Si
L-thyroxine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / 0 - 20 °C 2: Iodine monochloride; N-butylamine / dichloromethane; N,N-dimethyl-formamide / 0.33 h / 0 °C 3: lithium hydroxide / water; methanol / 1.5 h / 4 °C 4: hydrogenchloride / 1,4-dioxane / 20 °C / Inert atmosphere View Scheme |
C21H23I2NO6
L-thyroxine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: Iodine monochloride; N-butylamine / dichloromethane; N,N-dimethyl-formamide / 0.33 h / 0 °C 2: lithium hydroxide / water; methanol / 1.5 h / 4 °C 3: hydrogenchloride / 1,4-dioxane / 20 °C / Inert atmosphere View Scheme |
L-thyroxine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: diisopropylamine / water; butan-1-ol / 2 h / 20 - 90 °C 1.2: 2 h / 20 - 30 °C 2.1: acetic acid; hydrogen iodide / 5 h / 100 °C 3.1: methylamine / methanol / 25 - 30 °C 3.2: -8 - 0 °C 3.3: 15 - 20 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: diisopropylamine / water; butan-1-ol / 2 h / 20 - 90 °C 1.2: 2 h / 20 - 30 °C 2.1: acetic acid; hydrogen iodide / 5 h / 100 °C 3.1: methylamine / methanol / 25 - 30 °C 3.2: -8 - 0 °C 3.3: 15 - 20 °C View Scheme |
2-amino-3-(3,5-diiodo-4-(4-methoxyphenoxy)phenyl)propanoic acid
L-thyroxine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: acetic acid; hydrogen iodide / 5 h / 100 °C 2.1: methylamine / methanol / 25 - 30 °C 2.2: -8 - 0 °C 2.3: 15 - 20 °C View Scheme |
Conditions | Yield |
---|---|
at 10 - 20℃; for 168h; | 99.5% |
Conditions | Yield |
---|---|
With sodium carbonate In water Reflux; | 98% |
Stage #1: L-thyroxine With sulfuric acid; ammonia In butan-1-ol at 5 - 65℃; for 1h; pH=8; Stage #2: With sodium hydroxide In propan-1-ol; butan-1-ol at 25 - 50℃; pH=10; | 83% |
With sodium carbonate Reflux; | 79.2% |
With sodium carbonate In propan-1-ol; water at 80 - 90℃; for 1h; | 68% |
Conditions | Yield |
---|---|
In ethanol for 72h; | 96% |
L-thyroxine
3,5-diiodo-L-thyronine
Conditions | Yield |
---|---|
With sodium sulfite In water at 130℃; for 2h; Sealed tube; Microwave irradiation; Green chemistry; | 92% |
L-thyroxine
Conditions | Yield |
---|---|
With sodium hydroxide In propan-1-ol; water at 80 - 90℃; | 91% |
With sodium hydroxide In ethanol for 0.25h; Reflux; |
di-tert-butyl dicarbonate
L-thyroxine
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 2h; | 90% |
In N,N-dimethyl-formamide at 20℃; for 2h; | 90% |
With triethylamine In N,N-dimethyl-formamide at 20℃; for 1h; | 50% |
With sodium carbonate In dimethyl sulfoxide | |
With hydrogenchloride; sodium hydrogencarbonate In N-methyl-acetamide; methanol; water | 4.2 g (4.8 mmol, 83%) |
Conditions | Yield |
---|---|
With hydrogenchloride In methanol; water | 87% |
With hydrogenchloride In methanol; water | 87% |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran; water at 20℃; Condensation; | 85% |
Conditions | Yield |
---|---|
In ethanol at 10 - 20℃; for 120h; | 82.5% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 50℃; for 1h; | 80% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 50℃; for 1h; Inert atmosphere; | 80% |
L-thyroxine
α-(N-Trifluoroacetyl)amino-β-[3,5-diiodo-4-(3',5'-diiodo-4'-hydroxyphenoxy)phenyl] propanoic acid
Conditions | Yield |
---|---|
With sodium hydrogencarbonate; trifluoroacetic acid; trifluoroacetic anhydride In water; ethyl acetate | 70.5% |
With sodium hydrogencarbonate; trifluoroacetic acid; trifluoroacetic anhydride In water; ethyl acetate | 70.5% |
L-thyroxine
ethyl iodide
2-(ethylamino)-3-[4-(4-hydroxy-3,5-diiodophenoxy)-3,5-diiodophenyl]propanoic acid
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 2h; | 62% |
In N,N-dimethyl-formamide at 20℃; for 2h; | 62% |
butanoic acid anhydride
L-thyroxine
2-(butyrylamino)-3-[4-(4-hydroxy-3,5-diiodophenoxy)-3,5-diiodophenyl]propanoic acid
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide at 20℃; for 0.0833333h; | 50% |
Stage #1: L-thyroxine With triethylamine In N,N-dimethyl-formamide at 20℃; for 0.0833333h; Stage #2: butanoic acid anhydride In N,N-dimethyl-formamide at 20℃; | 45% |
Stage #1: L-thyroxine With triethylamine In N,N-dimethyl-formamide at 20℃; for 0.0833333h; Stage #2: butanoic acid anhydride In N,N-dimethyl-formamide at 20℃; for 0.75h; | 45% |
L-thyroxine
acetic anhydride
2-acetamido-3-[4-(4-acetoxy-3,5-diiodophenoxy)-3,5-diiodophenyl]propanoic acid
Conditions | Yield |
---|---|
Stage #1: L-thyroxine With triethylamine In N,N-dimethyl-formamide at 20℃; for 0.0833333h; Stage #2: acetic anhydride In N,N-dimethyl-formamide at 20℃; | 50% |
With pyridine at 0 - 23℃; for 12h; Inert atmosphere; |
L-thyroxine
ethyl iodide
ethyl 2-(ethylamino)-3-[4-(4-hydroxy-3,5-diiodophenoxy)-3,5-diiodophenyl]propanoate
Conditions | Yield |
---|---|
Stage #1: L-thyroxine With caesium carbonate In N,N-dimethyl-formamide at 20℃; for 0.0833333h; Stage #2: ethyl iodide In N,N-dimethyl-formamide at 20℃; for 1h; | 50% |
Stage #1: L-thyroxine With caesium carbonate In N,N-dimethyl-formamide at 20℃; for 0.0833333h; Stage #2: ethyl iodide In N,N-dimethyl-formamide at 20℃; | 10% |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; dimethyl sulfoxide at 20℃; Cooling with ice; | 42% |
L-thyroxine
Conditions | Yield |
---|---|
With chlorosulfonic acid; trifluoroacetic acid at 0℃; for 0.166667h; | 40% |
L-thyroxine
methyl iodide
potassium 3-[4-(4-hydroxy-3,5-diiodophenoxy)-3,5-diiodophenyl]-2-(methylamino)propanoate dihydrate
Conditions | Yield |
---|---|
Stage #1: L-thyroxine; methyl iodide In N,N-dimethyl-formamide at 20℃; for 2h; Stage #2: With potassium carbonate In N,N-dimethyl-formamide | 24% |
Stage #1: L-thyroxine; methyl iodide With triiodothyronine In N,N-dimethyl-formamide at 20℃; for 2h; Stage #2: With potassium carbonate In water; N,N-dimethyl-formamide | 24% |
L-thyroxine
Conditions | Yield |
---|---|
Stage #1: L-thyroxine With chlorosulfonic acid In N,N-dimethyl acetamide at 0 - 20℃; for 5h; Inert atmosphere; Stage #2: With sodium hydrogencarbonate; sodium carbonate In N,N-dimethyl acetamide; water for 1.5h; | 18% |
Conditions | Yield |
---|---|
With potassium hydroxide; palladium Hydrogenation; | |
With sodium tetrahydroborate; C10H8STe; D,L-dithiothreitol In aq. phosphate buffer at 37℃; for 0.5h; pH=7.5; Reagent/catalyst; |
L-thyroxine
chloroacetyl chloride
N-chloroacetyl-3,5,3',5'-tetraiodo-L-thyronine
Conditions | Yield |
---|---|
With ethyl acetate |
Conditions | Yield |
---|---|
With sodium hydroxide |
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