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Silver acetate Basic information Product Name: Silver acetate Synonyms: SILVER ACETATE;SILVER(I) ACETATE;ACETIC ACID SILVER SALT;Aceticacid,silver(1+)salt;aceticaci
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inquirySilver acetate CAS 563-63-3 Description Purity: 99% Min Application: Intermediates Appearance: Powder Package: Bag Delivery: 3-5days Our Advantage & Service 1.Top quality: Using high quality material and establishing a strict quali
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inquirySuperior quality, moderate price & quick delivery. Appearance:Off-white/brown crystalline powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Applicati
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inquirySilver acetate Chemical Properties Melting point decomposes [STR93] density 3.25 storage temp. Store below +30°C. solubility 10.2g/l form Powder/Solid Specific Gravity 3.259 color White to gray Water Solubility 10.2
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inquiryConditions | Yield |
---|---|
at 50℃; for 0.0833333h; | 99% |
In acetic acid react. of freshly prepared Ag2O (by electrolysis) with stoichiometric amounts of concd. acid, evapn. until begin of crystn., removal of remaining H2O under diminished pressure; apparatus described;; | |
In acetic acid crystn. on evapn. of the soln.;; | |
In acetic acid react. of freshly prepared Ag2O (by electrolysis) with stoichiometric amounts of concd. acid, evapn. until begin of crystn., removal of remaining H2O under diminished pressure; apparatus described;; |
Conditions | Yield |
---|---|
With acetic acid In water at 23℃; | 91% |
With acetic acid In water addn. of satd. aq. soln. of sodium acetate to satd. aq. soln. of AgNO3 contg. few drops of acetic acid in the dark; filtration, washing the residue with water, methanol, hexane, drying in vac.; | 90% |
In water soln. of AgNO3 in water was added to soln. of NaCH3CO2 in water; filtered in air, washed with water, EtOH, Et2O, dried in vacuo; elem. anal.; | 64% |
Pd[(μ-O2CMe)2Ag(HO2CMe)2]2
1,10-phenanthroline hydrate
(1,10-phenanthroline)-palladium(II) acetate
B
silver(I) acetate
Conditions | Yield |
---|---|
In benzene benzene soln. of ligand added with stirring to benzene soln. of Pd compd. (1:1 molar ratio), mixt. stirred at room temp. for 30 min; ppt. filtered off, concd., pptd. (heptane), dried, elem. anal.; | A 75% B n/a |
Conditions | Yield |
---|---|
In benzene benzene soln. of ligand added with stirring to benzene soln. of Pd compd. (3:1 molar ratio), mixt. stirred at room temp. for 1.5 h; ppt. filtered off, concd., crystd., dried, elem. anal.; | A 70% B n/a |
2,4,6-trimethyl-[1,3,5]dioxathiane
A
silver(I) acetate
Conditions | Yield |
---|---|
bei der Oxydation; |
Conditions | Yield |
---|---|
at 100℃; |
Conditions | Yield |
---|---|
In acetic anhydride boiling, pptn.;; recrystn. from glacial acetic acid;; |
silver(I) acetate
Conditions | Yield |
---|---|
With aldehyde In water | |
With aldehyde In water |
Conditions | Yield |
---|---|
In water in the air; | |
In water in the air; |
silver(I) acetate
Conditions | Yield |
---|---|
With trimethylamine acetate triacetatesolvate In not given addition of AgClO4 to a solution of the triacetatesolvate of trimethylamine acetate;; |
Conditions | Yield |
---|---|
In acetic acid in the light within several days;; |
Conditions | Yield |
---|---|
slow react.; |
Conditions | Yield |
---|---|
In water aq. soln. of Ag complex dried at 23°C for 24 h; detd. by X-ray diffraction; |
Conditions | Yield |
---|---|
In water at 20℃; | 3.1 g |
silver(I) acetate
2-<(N-cyclohexyl-N-methylamino)methyl>benzeneselenyl bromide
Conditions | Yield |
---|---|
In dichloromethane for 2h; | 100% |
silver(I) acetate
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 100℃; for 3h; | 100% |
silver(I) acetate
4,6-bis(chloromethyl)-2,5-dimethoxytropone
4-acetoxymethyl-6-chloromethyl-2,5-dimethoxytropone
Conditions | Yield |
---|---|
In acetic acid at 80℃; for 2h; | 100% |
1-chloro-1,3-dihydro-3,3-dimethyl-1,2-benziodoxole
silver(I) acetate
3,3-dimethyl-1λ3-benzo[d][1,2]iodoxol-1(3H)-yl acetate
Conditions | Yield |
---|---|
In acetonitrile at 20℃; for 15h; | 100% |
In acetonitrile Darkness; | 98% |
97% |
silver(I) acetate
11-{[(1R,3aS,5aR,5bR,7aR,9S,11aR,11bR,13aR,13bS)-9-Acetoxy-1-(1-bromomethyl-vinyl)-5a,5b,8,8,11a-pentamethyl-icosahydro-cyclopenta[a]chrysene-3a-carbonyl]-amino}-undecanoic acid methyl ester
11-{[(1R,3aS,5aR,5bR,7aR,9S,11aR,11bR,13aR,13bS)-9-Acetoxy-1-(1-acetoxymethyl-vinyl)-5a,5b,8,8,11a-pentamethyl-icosahydro-cyclopenta[a]chrysene-3a-carbonyl]-amino}-undecanoic acid methyl ester
Conditions | Yield |
---|---|
With tetrabutylammomium bromide In toluene for 2h; Heating; | 100% |
silver(I) acetate
2-<(N-cyclohexyl-N-methylamino)methyl>benzeneselenyl bromide
Conditions | Yield |
---|---|
In dichloromethane | 100% |
silver(I) acetate
1-chloro-3,3-bis(trifluoromethyl)-1,3-dihydro-1λ3-benzo[d][1,2]iodaoxole
Conditions | Yield |
---|---|
In acetonitrile Inert atmosphere; Darkness; | 100% |
In acetonitrile at 20℃; for 14.5h; | 98% |
In acetonitrile at 20℃; Darkness; | 92% |
In acetonitrile at 20℃; for 12h; Darkness; | 90% |
Conditions | Yield |
---|---|
In water at 40℃; for 24h; | 100% |
silver(I) acetate
Conditions | Yield |
---|---|
In methanol; dichloromethane silver acetate added to soln. of Pd-compd. at room temp., stirred for 30 min.; filtered, evapd.; | 100% |
silver(I) acetate
Conditions | Yield |
---|---|
In methanol Sonication; mixt. was ultrasonicated for 10 min at room temp.; soln. was filtered and aq. NH4PF6 was added, pptn. was filtered off, washed with water, dried over P2O5; elem. anal.; | 100% |
silver(I) acetate
Conditions | Yield |
---|---|
In methanol Sonication; mixt. was ultrasonicated for 10 min at room temp.; soln. was filtered and aq. NH4PF6 was added, pptn. was filtered off, washed with water, dried over P2O5; elem. anal.; | 100% |
silver(I) acetate
Conditions | Yield |
---|---|
In methanol Sonication; mixt. was ultrasonicated for 10 min at room temp.; soln. was filtered and aq. NH4PF6 was added, pptn. was filtered off, washed with water, dried over P2O5; elem. anal.; | 100% |
Conditions | Yield |
---|---|
In dichloromethane (N2); using of Schlenk techniques; combining of 1 equiv. of (((C6H4NC10H15)2C)PdCl2)2 with 4.1 equiv. of AgOAc in wet CH2Cl2; stirring under ambient conditions for 1.5 h; filtration, removal of volatiles in vac.; | 100% |
7,7-dichlorobicyclo<4.1.0>hept-3-ene
silver(I) acetate
Conditions | Yield |
---|---|
Stage #1: 7,7-dichlorobicyclo<4.1.0>hept-3-ene; silver(I) acetate With iodine; acetic acid Inert atmosphere; Stage #2: With water at 20℃; for 48h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
In diethyl ether (Ar), Ag acetate suspnd. in Et2O, reacted with 3 equiv. of (n-Bu)3P at 25°C for 1 h under stirring; evapd., elem. anal.; | 100% |
tributylphosphine
silver(I) acetate
tetra(tri-n-butyl phosphine)silver(I) acetate
Conditions | Yield |
---|---|
In diethyl ether (Ar), Ag acetate suspnd. in Et2O, reacted with 4 equiv. of (n-Bu)3P at 25°C for 1 h under stirring; evapd., elem. anal.; | 100% |
silver(I) acetate
Nevirapine
11-cyclopropyl-4-methyl-6-oxo-6,11-dihydro-5H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-2-yl acetate
Conditions | Yield |
---|---|
With iodine In dichloromethane at 104℃; for 0.0833333h; | 100% |
1-(iodomethyl)-3-(2,2,2-trifluoroacetyl)-2,3-dihydro-1H-benzo[e]indole-7-carbonitrile
silver(I) acetate
(7-cyano-3-(2,2,2-trifluoroacetyl)-2,3-dihydro-1H-benzo[e]indol-1-yl)methyl acetate
Conditions | Yield |
---|---|
In acetic acid for 48h; Reflux; | 100% |
silver(I) acetate
Conditions | Yield |
---|---|
In chloroform; acetonitrile | 100% |
silver(I) acetate
Conditions | Yield |
---|---|
In dichloromethane; acetonitrile at 20℃; for 1h; | 100% |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 0.333333h; Inert atmosphere; Optical yield = 54.545 %de; | 100% |
trans-1,2-dimethylcyclopentane
silver(I) acetate
cobalt(II) acetate
Conditions | Yield |
---|---|
Stage #1: trans-1,2-dimethylcyclopentane; C40H76N2O2(2+)*2NO3(1-) In dichloromethane at 20℃; Stage #2: cobalt(II) acetate In dichloromethane at 20℃; for 12h; Stage #3: silver(I) acetate In dichloromethane for 12h; | 100% |
2,2-Dimethyl-1,3-diaminopropane
silver(I) acetate
cobalt(II) acetate
Conditions | Yield |
---|---|
Stage #1: 2,2-Dimethyl-1,3-diaminopropane; C40H76N2O2(2+)*2NO3(1-) In dichloromethane at 20℃; Stage #2: cobalt(II) acetate In dichloromethane at 20℃; for 12h; Stage #3: silver(I) acetate In dichloromethane for 12h; | 100% |
Conditions | Yield |
---|---|
In toluene at 25℃; for 2h; Glovebox; | 100% |
silver(I) acetate
cobalt(II) acetate
Conditions | Yield |
---|---|
Stage #1: trans-1,2-diaminocyclohexane monohydrochloride; {3-methyl-5-[{Bu3N+(CH2)3}2CMe]salicylaldehyde}(I-)2 With sodium t-butanolate In methanol for 4h; Inert atmosphere; Stage #2: silver nitrate In dichloromethane for 5h; Darkness; Stage #3: silver(I) acetate; cobalt(II) acetate Further stages; | 100% |
Conditions | Yield |
---|---|
In methanol for 0.333333h; | 100% |
Conditions | Yield |
---|---|
In methanol for 0.333333h; | 100% |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 1h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
Stage #1: C48H46N4; silver(I) acetate In methanol Stage #2: sodium hexaflorophosphate | 100% |
Conditions | Yield |
---|---|
With nickel(II) triflate In chlorobenzene at 140℃; for 24h; | 100% |
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