As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:613-32-1
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:613-32-1
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Type:Manufacturers
inquiryProduct Name: 5,10-DIHYDRO-PHENAZINE Synonyms: AURORA KA-4601;5,10-DIHYDRO-PHENAZINE;Phenazine,5,10-dihydro- CAS: 613-32-1 MF: C12H10N2 MW: 182.22 Mol File: 613-32-1.mol Appearance:white powder Storage:room tempu
Cas:613-32-1
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:613-32-1
Min.Order:1 Kilogram
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiry1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
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inquiry5,10-DIHYDRO-PHENAZINE CAS:613-32-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inte
Cas:613-32-1
Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:613-32-1
Min.Order:1 Kilogram
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:613-32-1
Min.Order:0 Metric Ton
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inquiryWhy Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:613-32-1
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryWe Huarong Pharm can provide Customized Synthesis & Process R&D & APIs and intermediates Production & Quality Research & Registration Application, especially our GMP validation service which complies with SFDA, FDA, WHO and EU EMPA. O
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:613-32-1
Min.Order:0
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inquiryAcmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
Cas:613-32-1
Min.Order:1 bottle
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inquiryJ&H CHEM is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other Value-added customer services, for diversified range products of chemicals
bulk productiongoods in stockswe have the best competitive price in the marketmeantime,we are committed to service to our every customer Chemsigma International Co.,Ltd. is a chemical manufacturer, specialize in custom synthesis and organic chemical
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
"HANGZHOU TIANYE CHEMICALS Co.LTD , Located in Eastern Science and Innovation Park Hangzhou .We are a high-tech enterprise specialized in technical research and development, production, development and trade of chemical products. We supply Multiple s
Phenazine,5,10-dihydro- cas 613-32-1Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home an
Cas:613-32-1
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquirylow price and high purityAppearance:solid or liquid Storage:in sealed air resistant place Package:As customer require Application:Pharma;Industry;Agricultural Transportation:by sea or by airplane Port:any port in China
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen
Conditions | Yield |
---|---|
With sodium dithionite; water In ethanol for 2.5h; Ambient temperature; | 98% |
With sodium dithionite In ethanol; water at 20℃; for 4h; Inert atmosphere; | 98% |
With sodium dithionite In ethanol; water at 85℃; for 0.5h; Inert atmosphere; | 97.5% |
Conditions | Yield |
---|---|
With 18-crown-6 ether; copper; caesium carbonate In 1,2-dichloro-benzene for 24h; Reflux; | 72.1% |
With copper(l) iodide; 2,2'-biimidazole; caesium carbonate In N,N-dimethyl-formamide at 120℃; for 24h; Ullmann reaction; Inert atmosphere; | 63% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); acetophenone p-toluenesulfonylhydrazone; lithium tert-butoxide In 1,4-dioxane at 100℃; for 6h; Inert atmosphere; | 70% |
Conditions | Yield |
---|---|
With Cp*Rh(2-(2-pyridyl)phenyl)H; hydrogen In tetrahydrofuran at 80℃; under 3040.2 Torr; for 48h; Catalytic behavior; Glovebox; | A 19% B 54% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); lithium tert-butoxide; XPhos In 1,4-dioxane at 110℃; Inert atmosphere; | A 30% B 35% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); lithium tert-butoxide; XPhos In 1,4-dioxane at 110℃; Inert atmosphere; | A 35% B 15% |
N'‑(1‑phenylethylidene)benzenesulfonohydrazide
2-bromoaniline
A
5,10-dihydrophenazine
B
2-(1-phenylvinyl)aniline
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); lithium tert-butoxide; XPhos In 1,4-dioxane at 110℃; Inert atmosphere; | A 11% B 30% |
acetophenone p-toluenesulfonylhydrazone
2-bromoaniline
A
5,10-dihydrophenazine
B
2-(1-phenylvinyl)aniline
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); lithium tert-butoxide; XPhos In 1,4-dioxane at 110℃; Inert atmosphere; | A 22% B 28% |
bis(2-nitrophenyl)amine
5,10-dihydrophenazine
Conditions | Yield |
---|---|
With methanol; sodium |
benzene-1,2-diol
1,2-diamino-benzene
A
Phenazin
B
5,10-dihydrophenazine
Conditions | Yield |
---|---|
at 200 - 210℃; im Rohr; |
Conditions | Yield |
---|---|
Hydrogenation; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: K2CO3 2: sodium; methanol View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: K2CO3 2: sodium; methanol View Scheme |
5,10-dihydrophenazine
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; caesium carbonate In toluene at 110℃; Inert atmosphere; |
N1-(2-chlorophenyl)benzene-1,2-diamine
5,10-dihydrophenazine
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; caesium carbonate In toluene at 110℃; Inert atmosphere; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: caesium carbonate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate / toluene / 110 °C / Inert atmosphere 2: caesium carbonate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate / toluene / 110 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
Stage #1: 5,10-dihydrophenazine; 4-bromo-1,1'-biphenyl With tris-(dibenzylideneacetone)dipalladium(0); palladium diacetate In toluene for 8h; Reflux; Stage #2: 1-Bromo-2-iodobenzene In toluene for 8h; Reflux; | 97% |
Conditions | Yield |
---|---|
With oxygen; silver carbonate at 100℃; under 517.162 Torr; for 0.0833333h; Reagent/catalyst; Time; | 96% |
durch Sublimieren; | |
With ethanol |
Conditions | Yield |
---|---|
Stage #1: 5,10-dihydrophenazine With potassium tert-butylate In tetrahydrofuran at 20℃; for 1h; Stage #2: methyl iodide With phosphorus In tetrahydrofuran at 66℃; for 4h; | 92% |
With n-butyllithium In 1,2-dimethoxyethane; hexane for 0.5h; Ambient temperature; Yield given; |
Conditions | Yield |
---|---|
With chloro-(2-dicyclohexylphosphino-2′,6′-diisopropoxy-1,1′-biphenyl)[2-(2-aminoethyl)phenyl]palladium(II) methyl-tert-butyl ether adduct; sodium t-butanolate; ruphos In 1,4-dioxane at 110℃; for 10h; Sealed tube; Inert atmosphere; | 90% |
5,10-dihydrophenazine
2-bromo-5,10-dihydrophenazine
Conditions | Yield |
---|---|
With N-Bromosuccinimide In N,N-dimethyl-formamide at 0 - 20℃; Inert atmosphere; | 89.5% |
5,10-dihydrophenazine
terephthaloyl chloride
Terephthaloyl-5',5''-bis(5,10-dihydrophenazin)
Conditions | Yield |
---|---|
With dmap In tetrahydrofuran; pyridine at 80℃; for 5h; | 85% |
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate In toluene at 80℃; | 85% |
With chloro(2-dicyclohexylphosphino-2′,6′-di-i-propoxy-1,1′-biphenyl)(2′-amino-1,1′-biphenyl-2-yl)-palladium(II); sodium t-butanolate; ruphos In 1,4-dioxane at 100℃; for 10h; Buchwald-Hartwig Coupling; Inert atmosphere; | 0.75 g |
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate In toluene Reflux; | 85% |
Conditions | Yield |
---|---|
With palladium diacetate; caesium carbonate; XPhos In o-xylene at 130℃; for 12h; | 85% |
5,10-dihydrophenazine
4-N,N-diphenylamino-1-bromobenzene
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In o-xylene at 20℃; for 3h; | 83% |
With chloro-(2-dicyclohexylphosphino-2′,6′-diisopropoxy-1,1′-biphenyl)[2-(2-aminoethyl)phenyl]palladium(II) methyl-tert-butyl ether adduct; sodium t-butanolate; ruphos In 1,4-dioxane at 110℃; for 12h; Inert atmosphere; | 20% |
5,10-dihydrophenazine
bis(trichloromethyl) carbonate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; Reagent/catalyst; Inert atmosphere; | 83% |
5,10-dihydrophenazine
2-chloro-5-bromonitrobenzene
Conditions | Yield |
---|---|
With copper; potassium carbonate In 5,5-dimethyl-1,3-cyclohexadiene at 180℃; for 5h; Inert atmosphere; | 82% |
Conditions | Yield |
---|---|
With sodium t-butanolate; ruphos In 1,4-dioxane at 110℃; for 12h; Buchwald-Hartwig Coupling; Schlenk technique; | 82% |
Conditions | Yield |
---|---|
With copper; potassium carbonate In 5,5-dimethyl-1,3-cyclohexadiene at 180℃; for 5h; Inert atmosphere; | 81% |
Conditions | Yield |
---|---|
at 80℃; for 5h; | 79% |
Conditions | Yield |
---|---|
Stage #1: 5,10-dihydrophenazine With n-butyllithium In tetrahydrofuran; hexane at 20℃; for 0.5h; Inert atmosphere; Stage #2: 2-chloroethyl methyl ether In tetrahydrofuran; hexane at 20℃; Inert atmosphere; | 78.2% |
5,10-dihydrophenazine
1-bromo-4-phenylethynylbenzene
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate In toluene Reflux; | 78% |
5,10-dihydrophenazine
Conditions | Yield |
---|---|
Stage #1: 5,10-dihydrophenazine; 7-bromo-5,9-dioxa-13b-boranaphtho[3,2,1-de]anthracene With potassium carbonate In toluene for 0.166667h; Buchwald-Hartwig Coupling; Inert atmosphere; Stage #2: With tri-tert-butyl phosphine; palladium diacetate In toluene Buchwald-Hartwig Coupling; Reflux; Inert atmosphere; | 78% |
5,10-dihydrophenazine
methyl chloroformate
5,10-Dihydrophenazin-5,10-dicarbonsaeure-dimethylester
Conditions | Yield |
---|---|
at 80℃; for 5h; | 77% |
5,10-dihydrophenazine
benzene-1,3-dicarbonyl dichloride
Isophthaloyl-5',5''-bis(5,10-dihydrophenazin)
Conditions | Yield |
---|---|
With dmap In tetrahydrofuran; pyridine at 80℃; for 5h; | 77% |
5,10-dihydrophenazine
Conditions | Yield |
---|---|
Stage #1: 5,10-dihydrophenazine; 7-bromo-2,12-di-tert-butyl-5,9-dioxa-13b-boranaphtho[3,2,1-de]anthracene With potassium carbonate In toluene for 0.166667h; Buchwald-Hartwig Coupling; Inert atmosphere; Stage #2: With tri-tert-butyl phosphine; palladium diacetate In toluene for 20h; Buchwald-Hartwig Coupling; Reflux; Inert atmosphere; | 75% |
5,10-dihydrophenazine
phenyl chloroformate
5,10-Dihydrophenazin-5,10-dicarbonsaeure-diphenylester
Conditions | Yield |
---|---|
With dmap In pyridine for 3h; Heating; | 74% |
Conditions | Yield |
---|---|
With sodium t-butanolate; ruphos In 1,4-dioxane at 110℃; for 12h; Buchwald-Hartwig Coupling; Schlenk technique; | 73% |
With chloro(2-dicyclohexylphosphino-2′,6′-di-i-propoxy-1,1′-biphenyl)(2′-amino-1,1′-biphenyl-2-yl)-palladium(II); sodium t-butanolate; ruphos In 1,4-dioxane at 100℃; for 10h; Buchwald-Hartwig Coupling; Inert atmosphere; | 0.96 g |
With chloro-(2-dicyclohexylphosphino-2′,6′-diisopropoxy-1,1′-biphenyl)[2-(2-aminoethyl)phenyl]palladium(II) methyl-tert-butyl ether adduct; sodium t-butanolate; ruphos In 1,4-dioxane at 110℃; for 10h; Inert atmosphere; Sealed tube; |
Conditions | Yield |
---|---|
With chloro-(2-dicyclohexylphosphino-2’,6’-diisopropoxy-1,1‘-biphenyl)[2-(2-aminoethyl)phenyl] palladium(ll) methyl-tert-butyl ether adduct; sodium t-butanolate; ruphos In 1,4-dioxane at 110℃; for 16h; Buchwald-Hartwig Coupling; Schlenk technique; Inert atmosphere; | 73% |
With chloro-(2-dicyclohexylphosphino-2’,6’-diisopropoxy-1,1‘-biphenyl)[2-(2-aminoethyl)phenyl] palladium(ll) methyl-tert-butyl ether adduct; sodium t-butanolate; ruphos In 1,4-dioxane at 110℃; for 10h; Inert atmosphere; Sealed tube; | 46% |
5,10-dihydrophenazine
2-bromo-4,6-diphenyl-1,3,5-triazabenzene
Conditions | Yield |
---|---|
With copper; sodium t-butanolate In toluene for 24h; Inert atmosphere; Reflux; | 71% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 115℃; for 12h; Inert atmosphere; | 70.9% |
Conditions | Yield |
---|---|
With chloro-(2-dicyclohexylphosphino-2′,6′-diisopropoxy-1,1′-biphenyl)[2-(2-aminoethyl)phenyl]palladium(II) methyl-tert-butyl ether adduct; sodium t-butanolate; ruphos In 1,4-dioxane at 110℃; for 10h; Inert atmosphere; Sealed tube; | 69% |
With sodium t-butanolate; ruphos In 1,4-dioxane at 110℃; for 12h; Buchwald-Hartwig Coupling; Schlenk technique; | 25% |
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