DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:36809-26-4
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inquiryUnique advantages for 4-Bromotriphenylamine Cas 36809-26-4 Guaranteed the purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Powder Storage:Store at RT Package:25kg/drum Application:Intermedia
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inquiryhigh quality Appearance:white crystalline powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Intermediates Transportation:by air or by sea Port:shanghai
4-Bromotriphenylamine CAS No.:36809-26-4 Name: 4-Bromotriphenylamine Synonyms: 4-Bromo-N,N-diphenylaniline Molecular Structure Molecular Formula: C18H14BrN
Cas:36809-26-4
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
ISO9001 Exporting Japan, Korea regularly. Appearance:white crystal Package:25kg/ fibre drum Application:OLED intermediate Port:Chinese port
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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/1452.html Product Name 4-Bromotriphenylamine CAS No.
Cas:36809-26-4
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inquiry4-Bromotriphenylamine Basic information Product Name: 4-Bromotriphenylamine Synonyms: 4-BROMO-N,N-DIPHENYLANILINE;4-BROMOTRIPHENYLAMINE;(4-BROMO-PHENYL)-DIPHENYL-AMINE;4-BROOTRIPHENYLAMI
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu
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Cas:36809-26-4
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inquiryProduct Name: 4-Bromotriphenylamine Synonyms: 4-BROMO-N,N-DIPHENYLANILINE;4-BROMOTRIPHENYLAMINE;(4-BROMO-PHENYL)-DIPHENYL-AMINE;4-BROOTRIPHENYLAMINE;4-BROMOTRIPHENYLAMINE 95%;4-Bromotriphenylamine (BTPA
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Cas:36809-26-4
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inquiryBeluga chemical professional supply High quality 4-BROMOTRIPHENYLAMINE CAS 36809-26-4 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and research capabilities. 2. Made in
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Cas:36809-26-4
Min.Order:10 Gram
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
4-Bromotriphenylamine CAS: 36809-26-4 Specificati Item Standard Identification A.H-NMR:Comply with the structure B.LC-MS:Comply with the structure C.The IR spect
Cas:36809-26-4
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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Cas:36809-26-4
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inquirySuperior quality, moderate price & quick delivery. Appearance:white crystalline powder Storage:Well-sealed and put in dry and cool conditions. Package:25kg/plastic drum; or as per your request Application:Used as OLED material intermediates Tr
Cas:36809-26-4
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Cas:36809-26-4
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
1,4-bromoiodobenzene
diphenylamine
A
N,N,N',N'-tetraphenyl-p-phenylenediamine
B
4-N,N-diphenylamino-1-bromobenzene
Conditions | Yield |
---|---|
With copper(l) iodide; sodium t-butanolate In tetrahydrofuran at 60℃; for 12h; Catalytic behavior; Reagent/catalyst; Temperature; Ullmann Condensation; Inert atmosphere; chemoselective reaction; | A n/a B 98% |
With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; tri-tert-butyl phosphine; sodium t-butanolate; triethylamine In hexane; toluene at 20℃; for 4h; | A 25% B 45% |
N,N-diphenylaminobenzene
4-N,N-diphenylamino-1-bromobenzene
Conditions | Yield |
---|---|
With N-Bromosuccinimide In tetrachloromethane for 4h; Reflux; | 94% |
With N-Bromosuccinimide In tetrachloromethane for 4h; Heating; | 93% |
With N-Bromosuccinimide In tetrachloromethane for 4h; Inert atmosphere; Reflux; | 93% |
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate In toluene at 115℃; for 10h; Inert atmosphere; | 91% |
With (2-chloro-(5-trifluoromethylphenyl)pyridin-2-ylethylamine)(triphenylphosphine)copper(I) perchlorate; potassium tert-butylate In toluene at 90℃; for 12h; Inert atmosphere; | 65% |
With C39H33CuF3N2P2(1+)*ClO4(1-); potassium tert-butylate In toluene at 90℃; for 12h; Inert atmosphere; | 64% |
Conditions | Yield |
---|---|
With copper chromium oxide; potassium hydroxide In toluene for 10h; Ullmann Condensation; Inert atmosphere; Reflux; Green chemistry; | 84% |
With 1,10-Phenanthroline; copper(I) iodide; potassium hydroxide In toluene for 12h; Ullmann Condensation; Inert atmosphere; Reflux; Green chemistry; | 77% |
With 1,10-Phenanthroline; copper(l) chloride; potassium hydroxide In toluene Ullmann Condensation; Inert atmosphere; Dean-Stark; Reflux; | 74% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 70℃; | 80% |
With palladium diacetate; sodium t-butanolate In toluene Reflux; Inert atmosphere; | 79% |
With palladium diacetate; sodium t-butanolate In toluene Inert atmosphere; | 78% |
Conditions | Yield |
---|---|
With 1,1'-bis(diphenylphosphino)ferrocene; palladium diacetate; sodium t-butanolate In toluene at 90℃; for 15h; Buchwald-Hartwig coupling; Inert atmosphere; | 65% |
With 1,10-Phenanthroline; potassium hydroxide; copper(I) bromide In o-xylene for 72h; Ullmann reaction; Inert atmosphere; Reflux; | 63.5% |
Stage #1: 1.4-dibromobenzene With tris-(dibenzylideneacetone)dipalladium(0); 1,1'-bis(diphenylphosphino)ferrocene; sodium t-butanolate In toluene at 25℃; for 0.25h; Stage #2: diphenylamine In toluene at 90℃; for 15h; | 59% |
iodobenzene
Phenanthroline
4-bromo-aniline
4-N,N-diphenylamino-1-bromobenzene
Conditions | Yield |
---|---|
With potassium hydroxide | 65% |
1,4-bromoiodobenzene
1,2-dichloro-benzene
4-N,N-diphenylamino-1-bromobenzene
Conditions | Yield |
---|---|
With copper; potassium carbonate; diphenylamine | 35% |
iodobenzene
para-nitrophenyl bromide
4-N,N-diphenylamino-1-bromobenzene
Conditions | Yield |
---|---|
(i) Cu, (heating), (ii) Zn, AcOH; Multistep reaction; |
1,4-bromoiodobenzene
copper
diphenylamine
4-N,N-diphenylamino-1-bromobenzene
Conditions | Yield |
---|---|
With potassium carbonate In methanol; hexane; toluene; decalin |
iodobenzene
4-N,N-diphenylamino-1-bromobenzene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 75 percent / cesium carbonate; Cu(PPh3)3Br / toluene / 24 h / 110 °C 2: 54 percent / cesium carbonate; Cu(PPh3)3Br / toluene / 24 h / 120 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 75 percent / cesium carbonate; Cu(PPh3)3Br / toluene / 24 h / 110 °C 2: 54 percent / cesium carbonate; Cu(PPh3)3Br / toluene / 24 h / 120 °C View Scheme |
bromobenzene
4-N,N-diphenylamino-1-bromobenzene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine / toluene / 40 °C 2: sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine / toluene / 70 °C View Scheme | |
Multi-step reaction with 2 steps 1: triphenylphosphine; tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate / toluene / 24 h / 100 °C 2: triphenylphosphine; tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate / toluene / 24 h / 100 °C View Scheme |
aniline
4-N,N-diphenylamino-1-bromobenzene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine / toluene / 40 °C 2: sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine / toluene / 70 °C View Scheme | |
Multi-step reaction with 2 steps 1: triphenylphosphine; tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate / toluene / 24 h / 100 °C 2: triphenylphosphine; tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate / toluene / 24 h / 100 °C View Scheme |
4-N,N-diphenylamino-1-bromobenzene
tributyl(thien-2-yl)stannane
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0) In toluene at 110℃; for 24h; Stille Cross Coupling; Inert atmosphere; | 100% |
With bis-triphenylphosphine-palladium(II) chloride In N,N-dimethyl-formamide at 90℃; for 24h; Stille coupling; Inert atmosphere; | 80% |
With bis-triphenylphosphine-palladium(II) chloride In N,N-dimethyl-formamide at 100℃; for 20h; Inert atmosphere; | 78% |
4-N,N-diphenylamino-1-bromobenzene
N,N-dimethyl-formamide
4-[N-(4-bromophenyl)-N-phenylamine]benzaldehyde
Conditions | Yield |
---|---|
Stage #1: 4-N,N-diphenylamino-1-bromobenzene; N,N-dimethyl-formamide With trichlorophosphate at 0 - 50℃; Vilsmeier-Haack reaction; Inert atmosphere; Stage #2: With water; sodium hydroxide In N,N-dimethyl-formamide at 70℃; Vilsmeier-Haack reaction; Inert atmosphere; Cooling; | 99.4% |
With trichlorophosphate In N,N-dimethyl-formamide at 60℃; for 2h; Vilsmeier-Haack Formylation; | 93% |
Stage #1: N,N-dimethyl-formamide With trichlorophosphate for 0.333333h; Vilsmeier-Haack Formylation; Cooling with ice; Stage #2: 4-N,N-diphenylamino-1-bromobenzene at 0 - 110℃; for 7h; | 93% |
4-N,N-diphenylamino-1-bromobenzene
1-Naphthylboronic acid
1-(4'-(N,N-diphenylamino)phenyl)naphthalene
Conditions | Yield |
---|---|
With potassium carbonate; palladium diacetate; tris-(o-tolyl)phosphine In ethanol; water; toluene at 90℃; for 2h; Suzuki Coupling; | 99% |
With potassium carbonate; tris-(o-tolyl)phosphine; palladium diacetate In ethanol; toluene at 90℃; for 2h; Inert atmosphere; | 99% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 70℃; for 24h; Suzuki-Miyaura Coupling; Inert atmosphere; | 85% |
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate In 1,2-dimethoxyethane; water at 90℃; for 12h; Inert atmosphere; |
4-N,N-diphenylamino-1-bromobenzene
N-(trimethylsilyl)-diphenylamine
N,N,N',N'-tetraphenyl-p-phenylenediamine
Conditions | Yield |
---|---|
With cesium fluoride; bis(dibenzylideneacetone)-palladium(0); XPhos at 100℃; for 3h; Inert atmosphere; | 99% |
With cesium fluoride; bis(dibenzylideneacetone)-palladium(0); XPhos at 100℃; for 3h; Inert atmosphere; | 99% |
4-N,N-diphenylamino-1-bromobenzene
N4,N4’-bis(4-bromophenyl)-N4,N4’-diphenyl-[1,1'-biphenyl]-4,4'-diamine
Conditions | Yield |
---|---|
Stage #1: 4-N,N-diphenylamino-1-bromobenzene With methanesulfonic acid In dichloromethane at 0℃; Stage #2: With chloranil In dichloromethane at 0 - 20℃; for 0.0166667h; | 99% |
Stage #1: 4-N,N-diphenylamino-1-bromobenzene With methanesulfonic acid In dichloromethane at 0℃; Stage #2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone In dichloromethane | 99% |
With tungsten(VI) chloride In dichloromethane Inert atmosphere; | 50% |
Triisopropyl borate
4-N,N-diphenylamino-1-bromobenzene
water
4-(diphenylamino)phenyl boronic acid
Conditions | Yield |
---|---|
Stage #1: 4-N,N-diphenylamino-1-bromobenzene With n-butyllithium In tetrahydrofuran; hexane at -60℃; for 3h; Stage #2: Triisopropyl borate In tetrahydrofuran; hexane for 0.5h; Stage #3: water In tetrahydrofuran; hexane for 1h; | 99% |
Stage #1: 4-N,N-diphenylamino-1-bromobenzene With n-butyllithium In diethyl ether; hexane at -78℃; for 0.5h; Stage #2: Triisopropyl borate In diethyl ether; hexane at -78 - 20℃; Stage #3: water With hydrogenchloride | 80% |
Stage #1: 4-N,N-diphenylamino-1-bromobenzene With n-butyllithium In tetrahydrofuran; hexane at -60℃; for 3.5h; Inert atmosphere; Stage #2: Triisopropyl borate In tetrahydrofuran; hexane at -60℃; Inert atmosphere; Stage #3: water In toluene | 160 g |
Stage #1: 4-N,N-diphenylamino-1-bromobenzene With n-butyllithium In tetrahydrofuran; hexane for 3h; Inert atmosphere; Stage #2: Triisopropyl borate In tetrahydrofuran; hexane for 1h; Inert atmosphere; Stage #3: water In tetrahydrofuran; hexane | 160 g |
4-N,N-diphenylamino-1-bromobenzene
N-(trimethylsilyl)-9H-carbazole
4-(9H-carbazol-9-yl)-N,N-diphenylaniline
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel (0); 1,3-bis(2,6-diisopropylphenyl)imidazolidin-2-ylidene hydrochloride; potassium tert-butylate; sodium acetate at 100℃; for 18h; Inert atmosphere; | 99% |
4-N,N-diphenylamino-1-bromobenzene
silver(I) trifluoromethanethiolate
N,N-diphenyl-4-((trifluoromethyl)thio)aniline
Conditions | Yield |
---|---|
Stage #1: 4-N,N-diphenylamino-1-bromobenzene With bis[(trimethylsilyl)methyl](1,5-cyclooctadiene)palladium(II); dicyclohexyl-(2′,4′,6′-triisopropyl-3,6-dimethoxy-[1,1′-biphenyl]-2-yl)phosphine In toluene at 80℃; for 0.0166667h; Inert atmosphere; Stage #2: silver(I) trifluoromethanethiolate With N,N,N-triethylbenzenaminium iodide In toluene at 80℃; for 2h; Inert atmosphere; | 98% |
4-N,N-diphenylamino-1-bromobenzene
trimethylsilylacetylene
N,N-diphenyl-4-[(trimethylsilyl)ethynyl]benzenamine
Conditions | Yield |
---|---|
Stage #1: 4-N,N-diphenylamino-1-bromobenzene With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; triphenylphosphine for 0.25h; Microwave irradiation; Inert atmosphere; Stage #2: trimethylsilylacetylene With triethylamine at 80℃; Microwave irradiation; Inert atmosphere; | 97.3% |
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); diisopropylamine In toluene at 80℃; Sonogashira coupling; Inert atmosphere; | 95.4% |
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene In toluene at 70℃; for 3h; Sonogashira Cross-Coupling; Sealed tube; Inert atmosphere; | 94% |
4-N,N-diphenylamino-1-bromobenzene
aniline
N,N,N'-triphenyl-p-phenylenediamine
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0) In toluene at 80℃; for 6h; Molecular sieve; Heating / reflux; | 97% |
With caesium carbonate; triphenylphosphine; sodium t-butanolate In toluene at 80℃; for 8h; Inert atmosphere; | 91% |
With sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine In toluene for 12h; Heating / reflux; | 85% |
4-N,N-diphenylamino-1-bromobenzene
bis(pinacol)diborane
4-(diphenylamino)phenylboronic pinacol ester
Conditions | Yield |
---|---|
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate In 1,4-dioxane for 24h; Inert atmosphere; Reflux; | 97% |
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate In 1,4-dioxane at 85℃; for 16h; Miyaura Borylation Reaction; | 95% |
With potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In dimethyl sulfoxide at 80℃; for 6h; | 89% |
2-triethylsilylacetylene
4-N,N-diphenylamino-1-bromobenzene
N,N-diphenyl-4-((triethylsilyl)ethynyl)aniline
Conditions | Yield |
---|---|
With piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triphenylphosphine In toluene at 90℃; Sonogashira Cross-Coupling; Schlenk technique; Inert atmosphere; | 97% |
N1,N1'-((1,4-phenylenebis(azanediyl))bis(4,1-phenylene))bis(N4,N4-diphenylbenzene-1,4-diamine)
4-N,N-diphenylamino-1-bromobenzene
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In toluene at 40 - 50℃; for 13h; Inert atmosphere; | 97% |
4-N,N-diphenylamino-1-bromobenzene
N-(4-bromophenyl)-4-iodo-N-(4-iodophenyl)benzenamine
Conditions | Yield |
---|---|
With potassium iodate; acetic acid; potassium iodide at 85℃; for 12h; | 96% |
With iodine; periodic acid In ethanol for 2h; Reflux; Inert atmosphere; | 92% |
With potassium iodate; acetic acid; potassium iodide at 85℃; for 12h; | 80% |
With N-iodo-succinimide In N,N-dimethyl-formamide at 0 - 20℃; Inert atmosphere; | 71% |
4-N,N-diphenylamino-1-bromobenzene
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In toluene at 50℃; for 15h; Inert atmosphere; | 96% |
4-N,N-diphenylamino-1-bromobenzene
1,1-dimethyl-1,3-dihydrobenzo[c][1,2]oxasilole
[4-(diphenylamino)phenyl][2-(hydroxymethyl)phenyl]dimethylsilane
Conditions | Yield |
---|---|
Stage #1: 4-N,N-diphenylamino-1-bromobenzene With magnesium In tetrahydrofuran; diethyl ether at 60℃; for 4h; Stage #2: 1,1-dimethyl-1,3-dihydrobenzo[c][1,2]oxasilole In tetrahydrofuran; diethyl ether at 20℃; Further stages.; | 95% |
4-N,N-diphenylamino-1-bromobenzene
tributyltin chloride
Conditions | Yield |
---|---|
Stage #1: 4-N,N-diphenylamino-1-bromobenzene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Stage #2: tributyltin chloride In tetrahydrofuran; hexane at -78℃; | 95% |
Stage #1: 4-N,N-diphenylamino-1-bromobenzene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.75h; Stage #2: tributyltin chloride In tetrahydrofuran; hexane at 20℃; for 4.5h; Inert atmosphere; | 50% |
Stage #1: 4-N,N-diphenylamino-1-bromobenzene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Stage #2: tributyltin chloride In tetrahydrofuran; hexane at -78 - 20℃; |
2,5-bis(2-ethylhexyl)-3,6-di(thiophen-2-yl)pyrrolo[3,4-c]pyrrole-1,4-dione
4-N,N-diphenylamino-1-bromobenzene
3,6-bis(5-(4-(diphenylamino)phenyl)thiophen-2-yl)-2,5-bis(2-ethyl hexyl)pyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione
Conditions | Yield |
---|---|
With palladium diacetate; potassium carbonate; Trimethylacetic acid In N,N-dimethyl acetamide at 110℃; for 4h; Inert atmosphere; Schlenk technique; | 95% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene for 12h; Reflux; | 95% |
4-N,N-diphenylamino-1-bromobenzene
bis(2,6-bis(trifluoromethyl)phenyl)fluoroborane
Conditions | Yield |
---|---|
Stage #1: 4-N,N-diphenylamino-1-bromobenzene With n-butyllithium In hexane at -78 - 60℃; for 22h; Inert atmosphere; Schlenk technique; Glovebox; Stage #2: bis(2,6-bis(trifluoromethyl)phenyl)fluoroborane In hexane; tert-butyl methyl ether at -78 - 20℃; for 12h; Inert atmosphere; Sealed tube; Glovebox; | 95% |
4-N,N-diphenylamino-1-bromobenzene
5-[4-(diphenylamino)phenyl]thiophene-2-carbaldehyde
Conditions | Yield |
---|---|
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate In methanol; toluene at 75℃; for 16h; Suzuki-Miyaura Coupling; | 94% |
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate In methanol; toluene at 75℃; for 16h; Inert atmosphere; | 91.3% |
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate In methanol; toluene for 16h; Inert atmosphere; Reflux; | 89% |
N1,N1'-([1,1'-biphenyl]-4,4'-diyl)bis(N4-phenylbenzene-1,4-diamine)
4-N,N-diphenylamino-1-bromobenzene
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In toluene at 40 - 50℃; for 13h; Inert atmosphere; | 94% |
4-N,N-diphenylamino-1-bromobenzene
Conditions | Yield |
---|---|
With copper (II)-fluoride; tris-(dibenzylideneacetone)dipalladium(0); tris(2,4,6-trimethoxyphenyl)phosphine; cesium fluoride at 100℃; for 17h; Inert atmosphere; Glovebox; | 94% |
4-N,N-diphenylamino-1-bromobenzene
4-formylphenylboronic acid,
4′-(diphenylamino)-[1,1′-biphenyl]-4-carbaldehyde
Conditions | Yield |
---|---|
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate In methanol; toluene at 75℃; for 16h; Inert atmosphere; | 93.2% |
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate In water; isopropyl alcohol at 100℃; for 2h; Inert atmosphere; | 92% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In water; toluene Suzuki Coupling; Reflux; Inert atmosphere; | 85% |
Conditions | Yield |
---|---|
With bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate In toluene for 7h; Reflux; | 93.1% |
4-N,N-diphenylamino-1-bromobenzene
2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-5,5-dimethyl-1,3,2-dioxaborinane
[4-(5,5-dimethyl[1,3,2]dioxaborinan-2-yl)phenyl]diphenylamine
Conditions | Yield |
---|---|
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate In dimethyl sulfoxide at 80℃; for 5.5h; | 93% |
4-N,N-diphenylamino-1-bromobenzene
Conditions | Yield |
---|---|
With palladium hydroxide, 20 wt% on carbon; potassium acetate In N,N-dimethyl acetamide at 150℃; for 16h; Reagent/catalyst; Solvent; Temperature; Inert atmosphere; | 93% |
2-formylthiophene-3-carbonitrile
4-N,N-diphenylamino-1-bromobenzene
Conditions | Yield |
---|---|
With palladium diacetate; potassium carbonate; tricyclohexylphosphine tetrafluoroborate; Trimethylacetic acid In toluene at 100℃; for 16.3h; Inert atmosphere; | 93% |
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