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inquiryDL-Alaninol CAS 6168-72-5 Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed additives, Fine chemicals in distributing t
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DL-Alaninol Basic information Product Name: DL-Alaninol Synonyms: (+)-2-Aminopropan-1-ol;2-AMINOPROPANOL;H-ALA-OL;H-ALANINOL;H-ALA-OL S-(+)-2 AMINO-PROPANOL;H-L-ALA-OL;L-ALANILOL;L-(+)-2
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J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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DL-Alaninol Chemical Properties Melting point 8°C Boiling point 72-73 °C11 mm Hg(lit.) density 0.943 g/mL at 25 °C(lit.) refractive index n20/D 1.450 Fp 145 °F storage temp. 2-8°C pka pK1: 9.469(+1) (25&
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inquiryConditions | Yield |
---|---|
With trichlorosilane; N-ethyl-N,N-diisopropylamine In acetonitrile at 15℃; for 30h; | 100% |
With trichlorosilane; N-ethyl-N,N-diisopropylamine In acetonitrile at 0 - 20℃; for 18h; Inert atmosphere; | 90% |
With ethanol; nickel Hydrogenation; | |
With methanol; nickel Hydrogenation; | |
With hydrogen; palladium on activated charcoal In ethanol under 2280 Torr; |
Conditions | Yield |
---|---|
Stage #1: formaldehyd; Nitroethane With triethanolamine In water at 50℃; for 105h; Stage #2: With Fe/Ni; hydrogen at 70℃; under 22502.3 Torr; for 4h; Reagent/catalyst; Temperature; Pressure; | 82.6% |
Conditions | Yield |
---|---|
Stage #1: hydroxy-2-propanone With ammonia In water at 0 - 20℃; for 1 - 1.5h; Stage #2: With hydrogen; nickel In water at 85℃; under 57647.8 Torr; Product distribution / selectivity; | 71.5% |
Stage #1: hydroxy-2-propanone With ammonia at 20℃; for 1h; Stage #2: With hydrogen; nickel at 85℃; under 57647.8 Torr; Product distribution / selectivity; | 33.4% |
Stage #1: hydroxy-2-propanone With ammonia In water at 20℃; for 1.5h; Stage #2: With hydrogen; Nickel Raney 5886 In water at 85℃; under 23252.3 Torr; for 0.166667 - 0.333333h; Product distribution / selectivity; | |
Stage #1: hydroxy-2-propanone With ammonia In water at 20℃; for 1.5h; Stage #2: With hydrogen; nickel oxide on kieselguhr In water at 85℃; under 25877.6 - 113786 Torr; Product distribution / selectivity; | |
With (S)-1-phenyl-ethylamine; pyridoxal 5'-phosphate; pQR1108 In aq. phosphate buffer; dimethyl sulfoxide at 30℃; for 18h; pH=8; Enzymatic reaction; |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; iodine In tetrahydrofuran for 15h; Heating; | 60% |
With dimethylsulfide borane complex; boron trifluoride diethyl etherate In tetrahydrofuran for 2.5h; Heating; | |
Stage #1: rac-Ala-OH With lithium aluminium tetrahydride In tetrahydrofuran for 12h; Reflux; Stage #2: With sodium hydroxide In tetrahydrofuran; water at 0 - 20℃; |
ethyl pyruvate oxime
2-Amino-1-propanol
Conditions | Yield |
---|---|
With sodium tetrahydroborate; iodine In tetrahydrofuran for 4h; Heating; | 60% |
AlaOEt
2-Amino-1-propanol
Conditions | Yield |
---|---|
With ethanol; nickel at 50 - 100℃; Hydrogenation; |
Conditions | Yield |
---|---|
With ethanol; sodium |
Conditions | Yield |
---|---|
With ethanol; sodium |
Conditions | Yield |
---|---|
With sodium amalgam; acetic acid |
Conditions | Yield |
---|---|
With alkaline aqueous sodium hypobromite |
hydroxy-2-propanone
A
2,5-dimethoxy-2,5-dimethyl-1,4-dioxane
B
2-Amino-1-propanol
Conditions | Yield |
---|---|
With methanol; ammonia; water; nickel at 90℃; under 11032.6 Torr; Hydrogenation; |
2-amino-2-[1,3]dithiolan-2-yl-ethanol
2-Amino-1-propanol
Conditions | Yield |
---|---|
With nickel |
methyl 2-aminopropanoate monohydrochloride
2-Amino-1-propanol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride |
propylamine
A
2-Amino-1-propanol
B
(RS)-isoserine
C
glycine
D
propan-1-ol-3-amine
E
3-amino propanoic acid
Conditions | Yield |
---|---|
In water at 10 - 20℃; Product distribution; pH=2.7 and pH=12.0, various reaction times, contact glow discharge electrolysis; |
propylamine
A
2-Amino-1-propanol
B
(RS)-isoserine
C
glycine
D
3-amino propanoic acid
Conditions | Yield |
---|---|
In water at 10 - 20℃; contact glow discharge electrolysis; Yield given. Further byproducts given. Yields of byproduct given; | |
In water at 10 - 20℃; contact glow discharge electrolysis, pH=2.7; Yield given. Further byproducts given. Yields of byproduct given; | |
In water at 10 - 20℃; contact glow discharge electrolysis, pH=2.7; Yield given. Further byproducts given; |
N-chloro-2-aminopropan-1-ol
2-Amino-1-propanol
Conditions | Yield |
---|---|
With disodium hydrogenphosphate; sodium dihydrogenphosphate; sodium perchlorate; sodium iodide Thermodynamic data; Kinetics; Rate constant; Ea, ΔH, ΔS, influence of pH on the rate constant, reaction mechanism; |
2-Amino-1-propanol
Conditions | Yield |
---|---|
With hydrogen S, Ram, L. D. Spicer Synth. Commun. 1987, 17, 415.; |
ammonia
hydroxy-2-propanone
A
2,5-dimethoxy-2,5-dimethyl-1,4-dioxane
B
2-Amino-1-propanol
Conditions | Yield |
---|---|
und anschliessenden Hydrierung an Raney-Nickel bei 80grad/15 at; |
tetrahydrofuran
N-(N-benzoyl-glycyl)-alanine ethyl ester
A
2-Amino-1-propanol
B
ethanolamine
Conditions | Yield |
---|---|
Stage #1: hydroxy-2-propanone With ammonia In water at 20℃; for 1.5h; Stage #2: With hydrogen; nickel In water at 85℃; under 113786 Torr; Product distribution / selectivity; | |
With ammonia; hydrogen; Nickel Raney 5886 at 85℃; under 23252.3 Torr; Product distribution / selectivity; |
Conditions | Yield |
---|---|
With trifluoroacetic acid polystyrene ((aminomethyl)polystyrene); Product distribution / selectivity; |
glycerol
A
piperazine
B
propylamine
C
2-Amino-1-propanol
D
N-(1-aminomethyl-2-hydroxyethyl)amine
E
(RS)-2-methylpiperazine
F
ethylamine
G
isopropylamine
H
1,2-diaminopropan
I
3-amino-2-propanol
J
methylamine
Conditions | Yield |
---|---|
With ammonia; hydrogen; catalyst obtained by prereduction from precursor whose catalytically active composition before the reduction with hydrogen comprised 13% by weight of Cu, calculated as CuO, 28% by weight of NI, calculated as NiO, 28% by weight of Co, calculated as CoO and 31% by weight of Zr, calculated as ZrO2 In water at 250℃; under 37503.8 - 225023 Torr; Product distribution / selectivity; Autoclave; |
glycerol
A
2-Amino-1-propanol
B
N-(1-aminomethyl-2-hydroxyethyl)amine
C
1,2,3-triaminopropane
D
(RS)-2-methylpiperazine
E
1,2-diaminopropan
F
2,6-dimethylpiperazine
G
2,5-dimethylpiperazine
Conditions | Yield |
---|---|
With ammonia; hydrogen; catalyst precursor whose active composition comprised 13% by weight of Cu, calculated as CuO, 28% by weight of Ni, calculated as NiO, 28% by weight of Co, calculated as CoO and 31% by weight of Zr, calculated as ZrO2 In water at 180℃; under 150015 Torr; for 53h; Product distribution / selectivity; |
glycerol
A
2-Amino-1-propanol
B
N-(1-aminomethyl-2-hydroxyethyl)amine
C
1,2,3-triaminopropane
D
2-aminomethyl-6-methylpiperazine
E
2,5-bis(aminomethyl)piperazine
F
2-aminomethylpiperazine
G
2-aminomethyl-5-methylpiperazine
H
(RS)-2-methylpiperazine
I
1,2-diaminopropan
J
2,6-dimethylpiperazine
K
2,5-dimethylpiperazine
Conditions | Yield |
---|---|
With ammonia; hydrogen; catalyst precursor whose active composition comprised 50% by weight of Ni, calculated as NiO, 18% by weight of Cu, calculated as CuO, 2% by weight of Mo, calculated as MoO3, and 30% by weight or Zr, calculated as ZrO2 In water at 192℃; under 150015 Torr; for 1076h; Product distribution / selectivity; |
glycerol
A
propan-1-ol
B
2-Amino-1-propanol
C
3-amino-2-propanol
D
isopropyl alcohol
Conditions | Yield |
---|---|
With ammonia; hydrogen In water at 20℃; under 37503.8 Torr; for 24h; |
2-Amino-1-propanol
N-methyl-N-tert-butyldimethylsilyl-1,1,1-trifluoroacetamide
(tert-Butyl-dimethyl-silanyl)-[2-(tert-butyl-dimethyl-silanyloxy)-1-methyl-ethyl]-amine
Conditions | Yield |
---|---|
With tert-butyldimethylsilyl chloride In acetonitrile for 0.0833333h; Ambient temperature; other silylating agent; | 100% |
phthalic anhydride
2-Amino-1-propanol
2-(2-hydroxy-1-methylethyl)-1H-isoindole-1,3(2H)-dione
Conditions | Yield |
---|---|
With triethylamine In toluene Reflux; | 100% |
In toluene | 100% |
With triethylamine In toluene for 3h; Condensation; Heating; | 95% |
Conditions | Yield |
---|---|
In acetonitrile | 100% |
Conditions | Yield |
---|---|
In methanol at 20℃; for 1h; | 100% |
2-Amino-1-propanol
2-fluoro-4-[4-(4-fluorophenyl)-1-(2-methoxyethyl)-2-(methylsulfanyl)-1H-imidazol-5-yl]pyridine
Conditions | Yield |
---|---|
at 155℃; for 19h; | 100% |
In ethyl acetate at 155℃; for 19h; | 99.7% |
2-Amino-1-propanol
tert-butyldimethylsilyl chloride
1-(tert-butyldimethylsilyloxy)propan-2-amine
Conditions | Yield |
---|---|
With 1H-imidazole In dichloromethane at 20℃; for 4h; | 100% |
2-Amino-1-propanol
3-nitro-benzeneacetic acid
N-(1-hydroxypropan-2-yl)-2-(3-nitrophenyl)acetamide
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide for 16h; | 100% |
Conditions | Yield |
---|---|
With sodium ethanolate at 125℃; for 5h; | 99% |
With potassium carbonate at 130℃; for 3h; | 73% |
With sodium methylate for 4h; | |
With sodium methylate | |
With sodium methylate In methanol at 20℃; Heating / reflux; |
Conditions | Yield |
---|---|
In acetonitrile | 99% |
2-Amino-1-propanol
methyl [6-(3-fluoro-4-methoxybenzyl)-1,2,4,7-tetrahydro-3H-indolo[2,3-c][1,7]naphthyridin-3-yl]acetate
2-[6-(3-fluoro-4-methoxybenzyl)-1,2,4,7-tetrahydro-3H-indolo[2,3-c][1,7]naphthyridin-3-yl]-N-(2-hydroxy-1-methylethyl)acetamide
Conditions | Yield |
---|---|
at 100℃; for 18h; | 99% |
2-Amino-1-propanol
cis-5-tert-butoxycarbonyltetrahydro-3aH-furo[3,4-c]pyrrole-1,3-dione
C14H22N2O5
Conditions | Yield |
---|---|
In toluene at 170℃; for 0.233333h; Microwave irradiation; | 99% |
Conditions | Yield |
---|---|
at 50℃; for 3h; | 98% |
2-Amino-1-propanol
phenyl isothiocyanate
1-(1-hydroxypropan-2-yl)-3-phenylthiourea
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 0.5h; Alkylation; | 98% |
In tetrahydrofuran at 20℃; |
Conditions | Yield |
---|---|
Stage #1: 2-Amino-1-propanol; 2-fluorobenzonitrile With potassium tert-butylate In tetrahydrofuran at 0 - 25℃; Stage #2: With hydrogenchloride In tetrahydrofuran; 2-methyltetrahydrofuran; 1,4-dioxane | 97% |
2-Amino-1-propanol
di-tert-butyl dicarbonate
tert-butyl (1-hydroxypropan-2-yl)carbamate
Conditions | Yield |
---|---|
With sodium hydroxide In tetrahydrofuran; water at 20℃; for 14h; | 96% |
In dichloromethane at 20℃; for 1h; | 93% |
With triethylamine In dichloromethane at 20℃; for 0.5h; Cooling with ice; | 90.7% |
Conditions | Yield |
---|---|
With oxygen; potassium iodide; palladium(II) iodide In 1,2-dimethoxyethane at 100℃; under 15201 Torr; for 15h; | 96% |
With oxygen; sodium iodide; salen-Co(II) complex In 1,4-dioxane at 120℃; under 45004.5 Torr; for 2h; | 96% |
With oxygen; potassium iodide; palladium(II) iodide at 100℃; under 15001.5 Torr; for 24h; Autoclave; | 94% |
2-Amino-1-propanol
3-chloro-4-fluorobenzonitrile
3-chloro-4-(2-hydroxy-1-methyl-ethylamino)-benzonitrile
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 60℃; for 2h; | 96% |
In dimethyl sulfoxide at 60℃; for 2h; | 96% |
Conditions | Yield |
---|---|
With 3 A molecular sieve for 8h; Ambient temperature; | 95% |
Conditions | Yield |
---|---|
With dentritic zwitterionic imidazolium ionic liquid immobilized on mesoporous silica nanoparticles at 70℃; for 8h; Autoclave; | 95% |
With nanoparticulated CeO2 In ethanol at 160℃; under 5250.53 Torr; for 8h; Sealed reactor; |
Conditions | Yield |
---|---|
With sodium carbonate In water for 2h; Ambient temperature; | 94% |
With diethyl ether |
2-Amino-1-propanol
(fluorenylmethoxy)carbonyl chloride
(2-hydroxy-1-methylethyl)carbamic acid 9H-fluoren-9-yl methyl ester
Conditions | Yield |
---|---|
In diethyl ether at 20℃; for 2h; | 94% |
Conditions | Yield |
---|---|
With nitromethane for 0.0833333h; Microwave irradiation; | 94% |
2-Amino-1-propanol
ethyl 3-(2,6-dichloro-5-fluoro-3-pyridyl)-2--3-oxopropionate
(+/-)-ethyl 3-(2,6-dichloro-5-fluoro-3-pyridyl)-2-(4-methyloxazolidin-2-ylidene)-3-oxopropionate
Conditions | Yield |
---|---|
In toluene for 2.5h; Heating; | 93% |
Conditions | Yield |
---|---|
In benzene at 80℃; for 4h; | 93% |
2-Amino-1-propanol
n-hexadecanoyl chloride
(S)-2-methyl-2-(N-palmitoylamino)ethanol
Conditions | Yield |
---|---|
With triethylamine In chloroform; water | 93% |
2-Amino-1-propanol
p-toluenesulfonyl chloride
(+/-)-N-<2-hydroxy-1-methylethyl>-p-toluolsulfonamid
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 93% |
With triethylamine In dichloromethane at 0 - 20℃; for 18h; | 84% |
With triethylamine In dichloromethane at 20℃; |
2-Amino-1-propanol
2-{6,6-dimethyl-1-[2-(trimethylsilyl)ethoxymethyl]-4,5,6,7-tetrahydro-1H-indazol-3-yl}-1-[2-(trimethylsilyl)ethoxymethyl]-1H-indole-6-carboxylic acid
2-{6,6-dimethyl-1-[2-(trimethylsilyl)ethoxymethyl]-4,5,6,7-tetrahydro-1H-indazol-3-yl}-1-[2-(trimethylsilyl)ethoxymethyl]-1H-indole-6-carboxylic acid (2-hydroxy-1-methylethyl)amide
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 7h; | 93% |
Conditions | Yield |
---|---|
With triethylamine In methanol Reflux; | 93% |
2-Amino-1-propanol
5-bromo-1,3-difluoro-2-nitro-benzene
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 1h; | 93% |
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