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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

1-Nitrobutane

Cas:627-05-4

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

1-Nitrobutane

Cas:627-05-4

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High Purity 1-nitrobutane

Cas:627-05-4

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard

factory directly supply CAS 627-05-4 with competitive price

Cas:627-05-4

Min.Order:1 Kilogram

FOB Price: $112.0

Type:Trading Company

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Butane, 1-nitro-

Cas:627-05-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

Butane, 1-nitro- Application:Organic Chemicals

627-05-4

Cas:627-05-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Changzhou Extraordinary Pharmatech co.,LTD

Changzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa

Butane, 1-nitro

Cas:627-05-4

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai united Scientific Co.,Ltd.

United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat

Butane, 1-nitro-

Cas:627-05-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Nanjing Raymon Biotech Co., Ltd.

1-nitrobutane Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shanghai/Shenzhen

1-nitrobutane

Cas:627-05-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hebei Ruishun Trade Co.,Ltd

Supply top quality products with a reasonable price Application:api

627-05-4

Cas:627-05-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Debye Scientific

Debyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four yearsOur key scientific leadership team has gained experience in top research and developmen

1-Nitrobutane

Cas:627-05-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Changzhou Foreign Trade Corp

CFTC?PharmaChem?is?a?service?based?company?in?China,?a?pharmachem?division?of?Changzhou?Foreign?Trade?Corp.,supplying?raw?materials,?intermediates,?APIs?and?fine?chemicals?for?the?pharmaceutical?and?specialty?chemical?industries?worldwide. Applicatio

1-nitrobutane

Cas:627-05-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Chemical Co.Ltd

Manufacturer,strong R&D,professional team Storage:Store in a cool, dry place. Store in a tightly closed container. Package:according to your requirement Application:ZhiShang Chemical is owned by ZhiShang Group, is a professional new-type chemicals en

Butane, 1-nitro-

Cas:627-05-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

NovaChemistry

high purity Application:Drug intermediates Materials intermediates and active molecules

1-nitrobutane

Cas:627-05-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Sigma-Aldrich Chemie GmbH

Low-energy velocity map photoelectron imaging of 1-nitrobutane anions by photoelectron spectroscopy has been reported. Hydrothermal reaction of 1-nitrobutane in high-temperature water has been reported. Package:5 g in glass bottle

1-Nitrobutane

Cas:627-05-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

1-bromo-butane
109-65-9

1-bromo-butane

1-nitrobutane
627-05-4

1-nitrobutane

Conditions
ConditionsYield
With poly(vinylbenzyltriphenylphosphonium nitrite) In toluene at 100℃; for 8h;98%
With poly(N-butyl-4-vinylpyridinium)nitrite In hexane at 20℃; for 72h;90%
With poly(vinylbenzyltriphenylphosphonium)*NO2(-) In benzene for 24h; Ambient temperature;21%
With silver(I) nitrite In dimethyl sulfoxide
butyraldehyde oxime
110-69-0

butyraldehyde oxime

1-nitrobutane
627-05-4

1-nitrobutane

Conditions
ConditionsYield
With triethanolamine; dihydrogen peroxide In water; acetonitrile at 85℃; under 4650.47 Torr;95.8%
With ammonium hydroxide; dihydrogen peroxide In methanol at 70℃; under 760.051 Torr; Green chemistry; chemoselective reaction;96 %Chromat.
trans-4-Octene
14850-23-8

trans-4-Octene

A

1-nitrobutane
627-05-4

1-nitrobutane

B

butyric acid
107-92-6

butyric acid

Conditions
ConditionsYield
A 90%
B n/a
N-butylamine
109-73-9

N-butylamine

1-nitrobutane
627-05-4

1-nitrobutane

Conditions
ConditionsYield
With tert.-butylhydroperoxide; chromium silicalite-2 In methanol at 65℃; for 5h;80%
With tert.-butylhydroperoxide; molecular sieve In methanol for 5h; Heating;80%
With 3,3-dimethyldioxirane In acetone for 0.5h; Ambient temperature;84 % Chromat.
butyl magnesium bromide
693-04-9

butyl magnesium bromide

1-nitrobutane
627-05-4

1-nitrobutane

Conditions
ConditionsYield
With dinitrogen tetraoxide In tetrahydrofuran -190 deg C -> room temperature;71%
1-nitrobut-1-ene
27675-37-2, 3156-71-6

1-nitrobut-1-ene

1-nitrobutane
627-05-4

1-nitrobutane

Conditions
ConditionsYield
With sodium tetrahydroborate; silica gel In i-Amyl alcohol; chloroform at 20℃; for 2h; Inert atmosphere;59%
n-butyllithium
109-72-8, 29786-93-4

n-butyllithium

1-nitrobutane
627-05-4

1-nitrobutane

Conditions
ConditionsYield
With dinitrogen tetraoxide In tetrahydrofuran -190 deg C -> room temperature;19%
1-bromo-butane
109-65-9

1-bromo-butane

A

n-Butyl nitrite
544-16-1

n-Butyl nitrite

B

1-nitrobutane
627-05-4

1-nitrobutane

Conditions
ConditionsYield
With tetraphenylphosphonium nitrite (ionic form) Yield given. Yields of byproduct given;
With silver(I) nitrite; diethyl ether
With silver(I) nitrite; Petroleum ether
With tetraphenylphosphonium nitrite (ionic form) Yield given. Yields of byproduct given;
1-nitroethylene
3638-64-0

1-nitroethylene

ethylmagnesium bromide
925-90-6

ethylmagnesium bromide

1-nitrobutane
627-05-4

1-nitrobutane

Conditions
ConditionsYield
With diethyl ether
1-iodo-butane
542-69-8

1-iodo-butane

A

n-Butyl nitrite
544-16-1

n-Butyl nitrite

B

1-nitrobutane
627-05-4

1-nitrobutane

Conditions
ConditionsYield
With tetraphenylphosphonium nitrite (ionic form) Yield given. Yields of byproduct given;
With silver(I) nitrite; Petroleum ether
With silver(I) nitrite; diethyl ether
With tetraphenylphosphonium nitrite (ionic form) Yield given. Yields of byproduct given;
potassium ethyl sulfate
563-17-7

potassium ethyl sulfate

1-nitrobutane
627-05-4

1-nitrobutane

Conditions
ConditionsYield
With potassium nitrite
With sodium nitrite
n-butane
106-97-8

n-butane

A

2-nitrobutane
600-24-8, 116783-22-3

2-nitrobutane

B

1-nitrobutane
627-05-4

1-nitrobutane

Conditions
ConditionsYield
With nitric acid at 420℃;
With nitric acid In water at 200℃; under 77574.3 Torr; for 0.0333333h; Product distribution / selectivity;
n-butane
106-97-8

n-butane

1-nitrobutane
627-05-4

1-nitrobutane

Conditions
ConditionsYield
With nitric acid at 400 - 440℃;
butyraldehyde oxime
110-69-0

butyraldehyde oxime

A

propyl cyanide
109-74-0

propyl cyanide

B

1-nitrobutane
627-05-4

1-nitrobutane

Conditions
ConditionsYield
With potassium phosphate; D-glucose 6-phosphate; phenobarbital-induced rat liver microsomes; potassium chloride; nicotinamide adenine dinucleotide phosphate; magnesium chloride; glucose 6-phosphate dehydrogenase Mechanism; multistep reaction; dehydration of n-butyraldoxime catalyzed by cytochrome P-450;
n-Butyl chloride
109-69-3

n-Butyl chloride

1-nitrobutane
627-05-4

1-nitrobutane

Conditions
ConditionsYield
With perhydrodibenzo-18-crown-6; potassium nitrite at 70℃; for 5h; Yield given;
Cyclopentane
287-92-3

Cyclopentane

A

formic acid
64-18-6

formic acid

B

ethene
74-85-1

ethene

C

1-nitrobutane
627-05-4

1-nitrobutane

D

1-Nitropropane
108-03-2

1-Nitropropane

E

nitrocyclopentane
2562-38-1

nitrocyclopentane

Conditions
ConditionsYield
With Nitrogen dioxide; sulfur(VI) hexafluoride for 0.0166667h; Product distribution; Irradiation; CO2 laser irradiation; products investigated on different reaction conditions; products identified with IR and MS spectra; further cycloalkanes measured;
n-butane
106-97-8

n-butane

A

n-Butyl nitrite
544-16-1

n-Butyl nitrite

B

butyl nitrate
928-45-0

butyl nitrate

C

sec-butyl nitrite
924-43-6

sec-butyl nitrite

D

2-nitrobutane
600-24-8, 116783-22-3

2-nitrobutane

E

2-butyl nitrate
924-52-7

2-butyl nitrate

F

1-nitrobutane
627-05-4

1-nitrobutane

Conditions
ConditionsYield
With dihydrogen peroxide; Nitrogen dioxide at 24.9℃; under 300.02 Torr; Rate constant; Product distribution; Mechanism; boric-acid-coated surface; various pressure and carrier-gas composition;A 6 % Chromat.
B 0.3 % Chromat.
C 31 % Chromat.
D 51 % Chromat.
E 3 % Chromat.
F 7 % Chromat.
N-butylamine
109-73-9

N-butylamine

A

(E)-1,2-dibutyldiazene 1,2-dioxide
3378-31-2, 26049-02-5

(E)-1,2-dibutyldiazene 1,2-dioxide

B

n-Butylnitrit
44426-95-1

n-Butylnitrit

C

1-nitrobutane
627-05-4

1-nitrobutane

Conditions
ConditionsYield
With oxaziridinium tetrafluoroborate derived from N-methyl-1,2,3,4-tetrahydroisoquinoline In dichloromethane at 20℃; for 48h; Yields of byproduct given;A n/a
B n/a
C 15 % Spectr.
sodium butylsulfate
1000-67-5

sodium butylsulfate

1-nitrobutane
627-05-4

1-nitrobutane

Conditions
ConditionsYield
With potassium nitrate; sodium nitrite at 190℃; Yield given;
With potassium nitrate; sodium nitrite Thermodynamic data; Heating; E;
1-bromo-butane
109-65-9

1-bromo-butane

silver nitrite

silver nitrite

A

n-Butyl nitrite
544-16-1

n-Butyl nitrite

B

1-nitrobutane
627-05-4

1-nitrobutane

1-iodo-butane
542-69-8

1-iodo-butane

silver nitrite

silver nitrite

A

n-Butyl nitrite
544-16-1

n-Butyl nitrite

B

1-nitrobutane
627-05-4

1-nitrobutane

nitric acid
7697-37-2

nitric acid

n-butane
106-97-8

n-butane

A

Nitroethane
79-24-3

Nitroethane

B

nitromethane
75-52-5

nitromethane

C

2-nitrobutane
600-24-8, 116783-22-3

2-nitrobutane

D

1-nitrobutane
627-05-4

1-nitrobutane

Conditions
ConditionsYield
at 420℃; Produkt ist noch:1-Nitro-propan;
at 420℃; Produkte sind noch: 1-Nitro-propan, Aethylen, Propylen, Buten-(1) und Buten-(2);
at 420℃; Produkt ist noch:1-Nitro-propan;
nitric acid
7697-37-2

nitric acid

n-butane
106-97-8

n-butane

A

Nitroethane
79-24-3

Nitroethane

B

nitromethane
75-52-5

nitromethane

C

1-nitrobutane
627-05-4

1-nitrobutane

D

1-Nitropropane
108-03-2

1-Nitropropane

Conditions
ConditionsYield
at 370 - 450℃; in der Gasphase;
nitric acid
7697-37-2

nitric acid

pentane
109-66-0

pentane

A

Nitroethane
79-24-3

Nitroethane

B

nitromethane
75-52-5

nitromethane

C

1-nitrobutane
627-05-4

1-nitrobutane

D

1-Nitropropane
108-03-2

1-Nitropropane

Conditions
ConditionsYield
at 400℃; bei der Nitrierung enstehen noch: 1-Nitro-pentan,2-Nitro-pentan,3-Nitro-pentan und Aethylen,Propylen und Buten-(1);
at 400℃; bei der Nitrierung enstehen noch: 1-Nitro-pentan,2-Nitro-pentan,3-Nitro-pentan;
1-nitroethylene
3638-64-0

1-nitroethylene

diethyl ether
60-29-7

diethyl ether

ethylmagnesium bromide
925-90-6

ethylmagnesium bromide

A

1-nitrobutane
627-05-4

1-nitrobutane

B

hexanone-(3)-oxime

hexanone-(3)-oxime

Conditions
ConditionsYield
at 10 - 15℃; und bei folgendem Kochen;
standardbutyl iodide

standardbutyl iodide

1-nitrobutane
627-05-4

1-nitrobutane

Conditions
ConditionsYield
With silver(I) nitrite
ethyl sulfate
540-82-9

ethyl sulfate

potassium nitrite

potassium nitrite

A

Nitroethane
79-24-3

Nitroethane

B

ethyl nitrite
109-95-5

ethyl nitrite

C

1-nitrobutane
627-05-4

1-nitrobutane

ethyl sulfate
540-82-9

ethyl sulfate

sodium nitrite

sodium nitrite

A

Nitroethane
79-24-3

Nitroethane

B

ethyl nitrite
109-95-5

ethyl nitrite

C

1-nitrobutane
627-05-4

1-nitrobutane

dibutyl ether
142-96-1

dibutyl ether

nitric acid
7697-37-2

nitric acid

A

Nitroethane
79-24-3

Nitroethane

B

nitromethane
75-52-5

nitromethane

C

1-nitrobutane
627-05-4

1-nitrobutane

D

1-Nitropropane
108-03-2

1-Nitropropane

Conditions
ConditionsYield
at 400℃; durch ein Glasrohr;Produkt 5:Butyl-nitrobutyl-aether;
1-nitrobutane
627-05-4

1-nitrobutane

Glyoxilic acid
298-12-4

Glyoxilic acid

2-hydroxy-3-nitrohexanoic acid
367258-42-2

2-hydroxy-3-nitrohexanoic acid

Conditions
ConditionsYield
With triethylamine In methanol; water at 0 - 20℃;99%
With triethylamine In methanol at 0 - 20℃;99%
With triethylamine In methanol at 0 - 20℃;99%
1-nitrobutane
627-05-4

1-nitrobutane

12percent nickel/Al-SBA-15 fiber

12percent nickel/Al-SBA-15 fiber

N-butylamine
109-73-9

N-butylamine

Conditions
ConditionsYield
With hydrogen In ethanol at 109.84℃; under 18751.9 Torr; for 7.5h; Autoclave; Green chemistry; chemoselective reaction;99%
1-nitrobutane
627-05-4

1-nitrobutane

3-methoxy 2-nitrobenzaldehyde
53055-05-3

3-methoxy 2-nitrobenzaldehyde

1-(3-methoxy-2-nitrophenyl)-2-nitropentanol
350821-45-3

1-(3-methoxy-2-nitrophenyl)-2-nitropentanol

Conditions
ConditionsYield
With potassium fluoride; 18-crown-6 ether In isopropyl alcohol at 20℃; for 20h;97%
1-nitrobutane
627-05-4

1-nitrobutane

N-butylamine
109-73-9

N-butylamine

Conditions
ConditionsYield
Stage #1: 1-nitrobutane In water; acetonitrile at 20℃; for 0.0833333h;
Stage #2: With sodium tetrahydroborate In water; acetonitrile at 20℃; for 0.333333h;
95%
Stage #1: 1-nitrobutane In water at 20℃; for 0.0166667h;
Stage #2: With sodium tetrahydroborate In water at 50℃; for 0.166667h;
93%
With triethylamine In water at 80℃; for 6h; Inert atmosphere; Green chemistry; chemoselective reaction;91%
4-penten-3-one
1629-58-9

4-penten-3-one

1-nitrobutane
627-05-4

1-nitrobutane

6-nitro-3-nonanone

6-nitro-3-nonanone

Conditions
ConditionsYield
With tri-n-octylmethylphosphonium hydrogen carbonate at 4℃; for 2h; Michael condensation;95%
With triethylamine at 20℃; for 6h; Michael reaction;83%
With cetyltrimethylammonium hydroxide at 20℃; for 1h; Michael reaction;75%
1-nitrobutane
627-05-4

1-nitrobutane

ethyl 2-((tert-butoxycarbonyloxy)(phenyl)methyl)acrylate

ethyl 2-((tert-butoxycarbonyloxy)(phenyl)methyl)acrylate

(S,E)-ethyl 2-benzylidene-4-nitroheptanoate
1344660-46-3

(S,E)-ethyl 2-benzylidene-4-nitroheptanoate

Conditions
ConditionsYield
With N-[3,5-bis(trifluoromethyl)phenyl]-N'-[(9R)-6'-methoxycinchonan-9-yl]thiourea In tetrahydrofuran at 20℃; for 48h; Neat (no solvent); optical yield given as %ee; enantioselective reaction;95%
1-nitrobutane
627-05-4

1-nitrobutane

dimethyl cis-but-2-ene-1,4-dioate
624-48-6

dimethyl cis-but-2-ene-1,4-dioate

dimethyl (E)-2-butylidenesuccinate
254098-83-4

dimethyl (E)-2-butylidenesuccinate

Conditions
ConditionsYield
With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 25℃; for 7h; Addition; Elimination;94%
1-nitrobutane
627-05-4

1-nitrobutane

methyl vinyl ketone
78-94-4

methyl vinyl ketone

(+/-)-1-(2-hydroxy-2-methyl-5-nitro-5-propylcyclohexyl)-1-ethanone
7404-75-3

(+/-)-1-(2-hydroxy-2-methyl-5-nitro-5-propylcyclohexyl)-1-ethanone

Conditions
ConditionsYield
With potassium carbonate In water at 20℃; for 24h; Cycloaddition;93%
With N-benzyl-trimethylammonium hydroxide; hydroquinone In 1,4-dioxane; methanol
1-nitrobutane
627-05-4

1-nitrobutane

ethyl 5-oxocyclopent-1-en-1-carboxylate
57020-97-0

ethyl 5-oxocyclopent-1-en-1-carboxylate

C12H19NO5
1236412-40-0

C12H19NO5

Conditions
ConditionsYield
With quinine In toluene at -20℃; for 72h; Michael condensation; optical yield given as %ee; enantioselective reaction;93%
1-nitrobutane
627-05-4

1-nitrobutane

cinnamyl methyl carbonate
85217-69-2, 87802-71-9

cinnamyl methyl carbonate

(3R,4R)-(4-nitrohept-1-en-3-yl)benzene
1444826-33-8

(3R,4R)-(4-nitrohept-1-en-3-yl)benzene

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; C40H41FeN2O3P In tetrahydrofuran; dimethyl sulfoxide at 0℃; Inert atmosphere; enantioselective reaction;93%
1-nitrobutane
627-05-4

1-nitrobutane

4-chlorobenzaldehyde
104-88-1

4-chlorobenzaldehyde

1-Chloro-4-((E)-2-nitro-pent-1-enyl)-benzene

1-Chloro-4-((E)-2-nitro-pent-1-enyl)-benzene

Conditions
ConditionsYield
With CsNaX zeolite at 120℃; Condensation;92%
piperonal
120-57-0

piperonal

1-nitrobutane
627-05-4

1-nitrobutane

4-methoxy-aniline
104-94-9

4-methoxy-aniline

2-(benzo[d][1,3]dioxol-5-yl)-4-ethyl-6-methoxyquinoline

2-(benzo[d][1,3]dioxol-5-yl)-4-ethyl-6-methoxyquinoline

Conditions
ConditionsYield
With iron(III) chloride at 90℃; for 6h; Sealed tube; regioselective reaction;92%
C13H23N3O3

C13H23N3O3

1-nitrobutane
627-05-4

1-nitrobutane

C17H32N4O5

C17H32N4O5

Conditions
ConditionsYield
Stage #1: 1-nitrobutane With sodium methylate at 20℃; for 0.25h;
Stage #2: C13H23N3O3 at 20℃; for 1.5h; Michael addition; Further stages.;
91%
1-nitrobutane
627-05-4

1-nitrobutane

(R)-2-((benzyloxy)methyl)-2,4-dimethylcyclopent-4-ene-1,3-dione

(R)-2-((benzyloxy)methyl)-2,4-dimethylcyclopent-4-ene-1,3-dione

(S)-2-((benzyloxy)methyl)-4-butyl-2,5-dimethylcyclopent-4-ene-1,3-dione
303142-74-7

(S)-2-((benzyloxy)methyl)-4-butyl-2,5-dimethylcyclopent-4-ene-1,3-dione

Conditions
ConditionsYield
With tetrabutylammomium bromide; potassium hydroxide In tetrahydrofuran at 20℃; for 1h; Inert atmosphere;91%
1-nitrobutane
627-05-4

1-nitrobutane

4-methoxy-aniline
104-94-9

4-methoxy-aniline

4-bromo-benzaldehyde
1122-91-4

4-bromo-benzaldehyde

2-(4-bromophenyl)-4-ethyl-6-methoxyquinoline

2-(4-bromophenyl)-4-ethyl-6-methoxyquinoline

Conditions
ConditionsYield
With iron(III) chloride at 90℃; for 6h; Sealed tube; regioselective reaction;91%
1-nitrobutane
627-05-4

1-nitrobutane

N-butyl-N-propylhydroxylamine

N-butyl-N-propylhydroxylamine

Conditions
ConditionsYield
With cerium(III) chloride In tetrahydrofuran at -40℃; for 0.5h; other nitroalkanes, other Grignard reagents, var. temp.;90%
1-nitrobutane
627-05-4

1-nitrobutane

CH3CH2CH2MgX

CH3CH2CH2MgX

N-butyl-N-propylhydroxylamine

N-butyl-N-propylhydroxylamine

Conditions
ConditionsYield
With cerium(III) chloride In tetrahydrofuran at -40℃; for 0.5h;90%
1-nitrobutane
627-05-4

1-nitrobutane

n-butylamine hydrochloride
3858-78-4

n-butylamine hydrochloride

Conditions
ConditionsYield
Stage #1: 1-nitrobutane With C36H56Cl3CrN2O; magnesium; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In tetrahydrofuran at 60℃; for 24h; Inert atmosphere; Schlenk technique;
Stage #2: With hydrogenchloride In tetrahydrofuran; water; ethyl acetate at 20℃;
90%
Stage #1: 1-nitrobutane With hydrazine hydrate; zinc In methanol at 20℃; for 0.1h;
Stage #2: With hydrogenchloride
75%
Stage #1: 1-nitrobutane With formic acid; nickel In methanol at 20℃; for 0.133333h; Reduction;
Stage #2: With hydrogenchloride Addition;
60%
C7H12N4O2

C7H12N4O2

1-nitrobutane
627-05-4

1-nitrobutane

C11H21N5O4

C11H21N5O4

Conditions
ConditionsYield
Stage #1: 1-nitrobutane With sodium methylate at 20℃; for 0.25h;
Stage #2: C7H12N4O2 at 20℃; for 1.5h; Michael addition; Further stages.;
90%
1-nitrobutane
627-05-4

1-nitrobutane

(S)-2-((benzyloxy)methyl)-2,4-dimethylcyclopent-4-ene-1,3-dione

(S)-2-((benzyloxy)methyl)-2,4-dimethylcyclopent-4-ene-1,3-dione

(R)-2-((benzyloxy)methyl)-4-butyl-2,5-dimethylcyclopent-4-ene-1,3-dione
1383003-83-5

(R)-2-((benzyloxy)methyl)-4-butyl-2,5-dimethylcyclopent-4-ene-1,3-dione

Conditions
ConditionsYield
With tetrabutylammomium bromide; potassium hydroxide In tetrahydrofuran at 20℃; for 1h; Inert atmosphere;90%
1-nitrobutane
627-05-4

1-nitrobutane

4-chlorobenzaldehyde
104-88-1

4-chlorobenzaldehyde

4-methoxy-aniline
104-94-9

4-methoxy-aniline

2-(4-chlorophenyl)-4-ethyl-6-methoxyquinoline

2-(4-chlorophenyl)-4-ethyl-6-methoxyquinoline

Conditions
ConditionsYield
With iron(III) chloride at 90℃; for 6h; Sealed tube; regioselective reaction;90%
C11H19N3O3

C11H19N3O3

1-nitrobutane
627-05-4

1-nitrobutane

C15H28N4O5

C15H28N4O5

Conditions
ConditionsYield
Stage #1: 1-nitrobutane With sodium methylate at 20℃; for 0.25h;
Stage #2: C11H19N3O3 at 20℃; for 0.5h; Michael addition; Further stages.;
89%
1-nitrobutane
627-05-4

1-nitrobutane

benzaldehyde
100-52-7

benzaldehyde

aniline
62-53-3

aniline

N-((1S,2R)-2-nitro-1-phenylpentyl)aniline

N-((1S,2R)-2-nitro-1-phenylpentyl)aniline

Conditions
ConditionsYield
With N,N-dimethyl-cyclohexanamine; C23H25F6N3O3 In aq. acetate buffer at 0℃; for 5h; pH=5.5; Henry Nitro Aldol Condensation; stereoselective reaction;89%
1-nitrobutane
627-05-4

1-nitrobutane

ethyl acrylate
140-88-5

ethyl acrylate

ethyl 3-propyl-4,5-dihydroisoxazole-5-carboxylate
120802-96-2

ethyl 3-propyl-4,5-dihydroisoxazole-5-carboxylate

Conditions
ConditionsYield
With dmap; di-tert-butyl dicarbonate In acetonitrile at 25℃; for 5h;89%

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