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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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Type:Lab/Research institutions
inquiryProduct Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:627-05-4
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Butane, 1-nitro- Application:Organic Chemicals
Changzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa
United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat
1-nitrobutane Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shanghai/Shenzhen
Supply top quality products with a reasonable price Application:api
Debyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four yearsOur key scientific leadership team has gained experience in top research and developmen
CFTC?PharmaChem?is?a?service?based?company?in?China,?a?pharmachem?division?of?Changzhou?Foreign?Trade?Corp.,supplying?raw?materials,?intermediates,?APIs?and?fine?chemicals?for?the?pharmaceutical?and?specialty?chemical?industries?worldwide. Applicatio
Manufacturer,strong R&D,professional team Storage:Store in a cool, dry place. Store in a tightly closed container. Package:according to your requirement Application:ZhiShang Chemical is owned by ZhiShang Group, is a professional new-type chemicals en
high purity Application:Drug intermediates Materials intermediates and active molecules
Low-energy velocity map photoelectron imaging of 1-nitrobutane anions by photoelectron spectroscopy has been reported. Hydrothermal reaction of 1-nitrobutane in high-temperature water has been reported. Package:5 g in glass bottle
Conditions | Yield |
---|---|
With poly(vinylbenzyltriphenylphosphonium nitrite) In toluene at 100℃; for 8h; | 98% |
With poly(N-butyl-4-vinylpyridinium)nitrite In hexane at 20℃; for 72h; | 90% |
With poly(vinylbenzyltriphenylphosphonium)*NO2(-) In benzene for 24h; Ambient temperature; | 21% |
With silver(I) nitrite In dimethyl sulfoxide |
Conditions | Yield |
---|---|
With triethanolamine; dihydrogen peroxide In water; acetonitrile at 85℃; under 4650.47 Torr; | 95.8% |
With ammonium hydroxide; dihydrogen peroxide In methanol at 70℃; under 760.051 Torr; Green chemistry; chemoselective reaction; | 96 %Chromat. |
Conditions | Yield |
---|---|
A 90% B n/a |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; chromium silicalite-2 In methanol at 65℃; for 5h; | 80% |
With tert.-butylhydroperoxide; molecular sieve In methanol for 5h; Heating; | 80% |
With 3,3-dimethyldioxirane In acetone for 0.5h; Ambient temperature; | 84 % Chromat. |
Conditions | Yield |
---|---|
With dinitrogen tetraoxide In tetrahydrofuran -190 deg C -> room temperature; | 71% |
1-nitrobut-1-ene
1-nitrobutane
Conditions | Yield |
---|---|
With sodium tetrahydroborate; silica gel In i-Amyl alcohol; chloroform at 20℃; for 2h; Inert atmosphere; | 59% |
n-butyllithium
1-nitrobutane
Conditions | Yield |
---|---|
With dinitrogen tetraoxide In tetrahydrofuran -190 deg C -> room temperature; | 19% |
Conditions | Yield |
---|---|
With tetraphenylphosphonium nitrite (ionic form) Yield given. Yields of byproduct given; | |
With silver(I) nitrite; diethyl ether | |
With silver(I) nitrite; Petroleum ether | |
With tetraphenylphosphonium nitrite (ionic form) Yield given. Yields of byproduct given; |
Conditions | Yield |
---|---|
With diethyl ether |
Conditions | Yield |
---|---|
With tetraphenylphosphonium nitrite (ionic form) Yield given. Yields of byproduct given; | |
With silver(I) nitrite; Petroleum ether | |
With silver(I) nitrite; diethyl ether | |
With tetraphenylphosphonium nitrite (ionic form) Yield given. Yields of byproduct given; |
Conditions | Yield |
---|---|
With potassium nitrite | |
With sodium nitrite |
Conditions | Yield |
---|---|
With nitric acid at 420℃; | |
With nitric acid In water at 200℃; under 77574.3 Torr; for 0.0333333h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
With nitric acid at 400 - 440℃; |
Conditions | Yield |
---|---|
With potassium phosphate; D-glucose 6-phosphate; phenobarbital-induced rat liver microsomes; potassium chloride; nicotinamide adenine dinucleotide phosphate; magnesium chloride; glucose 6-phosphate dehydrogenase Mechanism; multistep reaction; dehydration of n-butyraldoxime catalyzed by cytochrome P-450; |
Conditions | Yield |
---|---|
With perhydrodibenzo-18-crown-6; potassium nitrite at 70℃; for 5h; Yield given; |
Cyclopentane
A
formic acid
B
ethene
C
1-nitrobutane
D
1-Nitropropane
E
nitrocyclopentane
Conditions | Yield |
---|---|
With Nitrogen dioxide; sulfur(VI) hexafluoride for 0.0166667h; Product distribution; Irradiation; CO2 laser irradiation; products investigated on different reaction conditions; products identified with IR and MS spectra; further cycloalkanes measured; |
n-butane
A
n-Butyl nitrite
B
butyl nitrate
C
sec-butyl nitrite
D
2-nitrobutane
E
2-butyl nitrate
F
1-nitrobutane
Conditions | Yield |
---|---|
With dihydrogen peroxide; Nitrogen dioxide at 24.9℃; under 300.02 Torr; Rate constant; Product distribution; Mechanism; boric-acid-coated surface; various pressure and carrier-gas composition; | A 6 % Chromat. B 0.3 % Chromat. C 31 % Chromat. D 51 % Chromat. E 3 % Chromat. F 7 % Chromat. |
N-butylamine
A
(E)-1,2-dibutyldiazene 1,2-dioxide
B
n-Butylnitrit
C
1-nitrobutane
Conditions | Yield |
---|---|
With oxaziridinium tetrafluoroborate derived from N-methyl-1,2,3,4-tetrahydroisoquinoline In dichloromethane at 20℃; for 48h; Yields of byproduct given; | A n/a B n/a C 15 % Spectr. |
Conditions | Yield |
---|---|
With potassium nitrate; sodium nitrite at 190℃; Yield given; | |
With potassium nitrate; sodium nitrite Thermodynamic data; Heating; E; |
nitric acid
n-butane
A
Nitroethane
B
nitromethane
C
2-nitrobutane
D
1-nitrobutane
Conditions | Yield |
---|---|
at 420℃; Produkt ist noch:1-Nitro-propan; | |
at 420℃; Produkte sind noch: 1-Nitro-propan, Aethylen, Propylen, Buten-(1) und Buten-(2); | |
at 420℃; Produkt ist noch:1-Nitro-propan; |
nitric acid
n-butane
A
Nitroethane
B
nitromethane
C
1-nitrobutane
D
1-Nitropropane
Conditions | Yield |
---|---|
at 370 - 450℃; in der Gasphase; |
nitric acid
pentane
A
Nitroethane
B
nitromethane
C
1-nitrobutane
D
1-Nitropropane
Conditions | Yield |
---|---|
at 400℃; bei der Nitrierung enstehen noch: 1-Nitro-pentan,2-Nitro-pentan,3-Nitro-pentan und Aethylen,Propylen und Buten-(1); | |
at 400℃; bei der Nitrierung enstehen noch: 1-Nitro-pentan,2-Nitro-pentan,3-Nitro-pentan; |
1-nitroethylene
diethyl ether
ethylmagnesium bromide
A
1-nitrobutane
Conditions | Yield |
---|---|
at 10 - 15℃; und bei folgendem Kochen; |
1-nitrobutane
Conditions | Yield |
---|---|
With silver(I) nitrite |
dibutyl ether
nitric acid
A
Nitroethane
B
nitromethane
C
1-nitrobutane
D
1-Nitropropane
Conditions | Yield |
---|---|
at 400℃; durch ein Glasrohr;Produkt 5:Butyl-nitrobutyl-aether; |
Conditions | Yield |
---|---|
With triethylamine In methanol; water at 0 - 20℃; | 99% |
With triethylamine In methanol at 0 - 20℃; | 99% |
With triethylamine In methanol at 0 - 20℃; | 99% |
Conditions | Yield |
---|---|
With hydrogen In ethanol at 109.84℃; under 18751.9 Torr; for 7.5h; Autoclave; Green chemistry; chemoselective reaction; | 99% |
1-nitrobutane
3-methoxy 2-nitrobenzaldehyde
1-(3-methoxy-2-nitrophenyl)-2-nitropentanol
Conditions | Yield |
---|---|
With potassium fluoride; 18-crown-6 ether In isopropyl alcohol at 20℃; for 20h; | 97% |
Conditions | Yield |
---|---|
Stage #1: 1-nitrobutane In water; acetonitrile at 20℃; for 0.0833333h; Stage #2: With sodium tetrahydroborate In water; acetonitrile at 20℃; for 0.333333h; | 95% |
Stage #1: 1-nitrobutane In water at 20℃; for 0.0166667h; Stage #2: With sodium tetrahydroborate In water at 50℃; for 0.166667h; | 93% |
With triethylamine In water at 80℃; for 6h; Inert atmosphere; Green chemistry; chemoselective reaction; | 91% |
Conditions | Yield |
---|---|
With tri-n-octylmethylphosphonium hydrogen carbonate at 4℃; for 2h; Michael condensation; | 95% |
With triethylamine at 20℃; for 6h; Michael reaction; | 83% |
With cetyltrimethylammonium hydroxide at 20℃; for 1h; Michael reaction; | 75% |
1-nitrobutane
(S,E)-ethyl 2-benzylidene-4-nitroheptanoate
Conditions | Yield |
---|---|
With N-[3,5-bis(trifluoromethyl)phenyl]-N'-[(9R)-6'-methoxycinchonan-9-yl]thiourea In tetrahydrofuran at 20℃; for 48h; Neat (no solvent); optical yield given as %ee; enantioselective reaction; | 95% |
1-nitrobutane
dimethyl cis-but-2-ene-1,4-dioate
dimethyl (E)-2-butylidenesuccinate
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 25℃; for 7h; Addition; Elimination; | 94% |
1-nitrobutane
methyl vinyl ketone
(+/-)-1-(2-hydroxy-2-methyl-5-nitro-5-propylcyclohexyl)-1-ethanone
Conditions | Yield |
---|---|
With potassium carbonate In water at 20℃; for 24h; Cycloaddition; | 93% |
With N-benzyl-trimethylammonium hydroxide; hydroquinone In 1,4-dioxane; methanol |
Conditions | Yield |
---|---|
With quinine In toluene at -20℃; for 72h; Michael condensation; optical yield given as %ee; enantioselective reaction; | 93% |
1-nitrobutane
cinnamyl methyl carbonate
(3R,4R)-(4-nitrohept-1-en-3-yl)benzene
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; C40H41FeN2O3P In tetrahydrofuran; dimethyl sulfoxide at 0℃; Inert atmosphere; enantioselective reaction; | 93% |
Conditions | Yield |
---|---|
With CsNaX zeolite at 120℃; Condensation; | 92% |
Conditions | Yield |
---|---|
With iron(III) chloride at 90℃; for 6h; Sealed tube; regioselective reaction; | 92% |
Conditions | Yield |
---|---|
Stage #1: 1-nitrobutane With sodium methylate at 20℃; for 0.25h; Stage #2: C13H23N3O3 at 20℃; for 1.5h; Michael addition; Further stages.; | 91% |
1-nitrobutane
(S)-2-((benzyloxy)methyl)-4-butyl-2,5-dimethylcyclopent-4-ene-1,3-dione
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; potassium hydroxide In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; | 91% |
Conditions | Yield |
---|---|
With iron(III) chloride at 90℃; for 6h; Sealed tube; regioselective reaction; | 91% |
1-nitrobutane
Conditions | Yield |
---|---|
With cerium(III) chloride In tetrahydrofuran at -40℃; for 0.5h; other nitroalkanes, other Grignard reagents, var. temp.; | 90% |
Conditions | Yield |
---|---|
With cerium(III) chloride In tetrahydrofuran at -40℃; for 0.5h; | 90% |
Conditions | Yield |
---|---|
Stage #1: 1-nitrobutane With C36H56Cl3CrN2O; magnesium; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In tetrahydrofuran at 60℃; for 24h; Inert atmosphere; Schlenk technique; Stage #2: With hydrogenchloride In tetrahydrofuran; water; ethyl acetate at 20℃; | 90% |
Stage #1: 1-nitrobutane With hydrazine hydrate; zinc In methanol at 20℃; for 0.1h; Stage #2: With hydrogenchloride | 75% |
Stage #1: 1-nitrobutane With formic acid; nickel In methanol at 20℃; for 0.133333h; Reduction; Stage #2: With hydrogenchloride Addition; | 60% |
Conditions | Yield |
---|---|
Stage #1: 1-nitrobutane With sodium methylate at 20℃; for 0.25h; Stage #2: C7H12N4O2 at 20℃; for 1.5h; Michael addition; Further stages.; | 90% |
1-nitrobutane
(R)-2-((benzyloxy)methyl)-4-butyl-2,5-dimethylcyclopent-4-ene-1,3-dione
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; potassium hydroxide In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
With iron(III) chloride at 90℃; for 6h; Sealed tube; regioselective reaction; | 90% |
Conditions | Yield |
---|---|
Stage #1: 1-nitrobutane With sodium methylate at 20℃; for 0.25h; Stage #2: C11H19N3O3 at 20℃; for 0.5h; Michael addition; Further stages.; | 89% |
Conditions | Yield |
---|---|
With N,N-dimethyl-cyclohexanamine; C23H25F6N3O3 In aq. acetate buffer at 0℃; for 5h; pH=5.5; Henry Nitro Aldol Condensation; stereoselective reaction; | 89% |
1-nitrobutane
ethyl acrylate
ethyl 3-propyl-4,5-dihydroisoxazole-5-carboxylate
Conditions | Yield |
---|---|
With dmap; di-tert-butyl dicarbonate In acetonitrile at 25℃; for 5h; | 89% |
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