CAS No.66309-83-9,1H-Inden-1-one, 2,3-dihydro-2,6-dimethyl- Suppliers

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Chemwill Asia Co., Ltd.

Chemwill Asia co.,Ltd is one of the leading manufacturer in CHINA. Product quality, process, price and service 2,6-Dimethyl-1-indanone IN Stock CAS 66309-83-9 66309-83-9 CAS 66309-83-9 Highly quality and immedaite delivery 2,3-Dihydro-

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Hangzhou Fandachem Co.,Ltd

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Antimex Chemical Limied

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LEAP CHEM Co., Ltd.

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Changzhou Extraordinary Pharmatech co.,LTD

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Shanghai united Scientific Co.,Ltd.

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InventyS Research Company Pvt. Ltd.

The 2, 6-dimethyl-1-indanone is an important raw material of triazinyl indene amine, and the main synthetic route at present is to prepare the triazinyl indene amine by using p-methyl benzyl chloride as a raw material through four steps of condensati

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Skyrun Industrial Co.,Ltd

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Synthetic route

: 860256-66-2
2-methyl-3-p-tolyl-propionyl chloride

: 66309-83-9
2,6-dimethylindan-1-one

Conditions

Conditions	Yield
With aluminum (III) chloride In dichloromethane at 0 - 10℃; for 3h;	94.6%
With aluminum (III) chloride In dichloromethane at 0℃; for 4h; Heating / reflux;	89%

: 1012-15-3
α-methyl-β-(4-methylphenyl)propionic acid

: 66309-83-9
2,6-dimethylindan-1-one

Conditions

Conditions	Yield
With polyphosphoric acid at 80℃; for 12h; Friedel-Crafts Acylation;	87%
With PPA at 100℃; for 3h;	1.12 g
Multi-step reaction with 2 steps 1: thionyl chloride / dichloromethane / 1 h / 35 - 40 °C 2: aluminum (III) chloride / dichloromethane / 3 h / 0 - 10 °C View Scheme

: C11H13ClO

: 66309-83-9
2,6-dimethylindan-1-one

Conditions

Conditions	Yield
With aluminum (III) chloride In 1,2-dichloro-ethane at 80℃; for 4h;	82%

: 88632-72-8
2,5-dimethyl-α-chloropropiophenone

A: 35031-52-8
1-(2,5-dimethylphenyl)propan-1-one

B: 66309-83-9
2,6-dimethylindan-1-one

Conditions

Conditions	Yield
In tert-butyl alcohol for 16h; Quantum yield; Irradiation; other solvent;	A 6% B 81%

: 2,6-dimethyl-1H-inden-1-yl acetate

: 66309-83-9
2,6-dimethylindan-1-one

Conditions

Conditions	Yield
With methanol; sodium hydroxide at 20℃; for 24h;	81%

: methyl 2-allyl-5-methylbenzoate

: 66309-83-9
2,6-dimethylindan-1-one

Conditions

Conditions	Yield
With bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; 1-Phenylethanol; potassium tert-butylate; 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride In toluene at 100℃; for 16h; Inert atmosphere; Sealed tube;	71%

: 4606-07-9
ethyl cyclopropylcarboxylate

: 108-88-3
toluene

: 66309-83-9
2,6-dimethylindan-1-one

Conditions

Conditions	Yield
aluminium trichloride In toluene Heating;	67%

: 67-56-1
methanol

: 88632-72-8
2,5-dimethyl-α-chloropropiophenone

A: 35031-52-8
1-(2,5-dimethylphenyl)propan-1-one

B: 66309-83-9
2,6-dimethylindan-1-one

C: 99356-70-4
2-(2,5-Dimethyl-phenyl)-propionic acid methyl ester

D: 99356-69-1
1-(2-Methoxymethyl-5-methyl-phenyl)-propan-1-one

Conditions

Conditions	Yield
for 16h; Irradiation;	A 4% B 42% C 24% D 28%
for 16h; Quantum yield; Rate constant; Irradiation;	A 4% B 42% C 24% D 28%

...Expand

: 88632-72-8
2,5-dimethyl-α-chloropropiophenone

A: 35031-52-8
1-(2,5-dimethylphenyl)propan-1-one

B: 66309-83-9
2,6-dimethylindan-1-one

C: 99356-70-4
2-(2,5-Dimethyl-phenyl)-propionic acid methyl ester

D: 99356-69-1
1-(2-Methoxymethyl-5-methyl-phenyl)-propan-1-one

Conditions

Conditions	Yield
In methanol for 16h; Irradiation;	A 4% B 42% C 24% D 28%

...Expand

(+-)-2-methyl-3-p-tolyl-propionic acid-chloride: (+-)-2-methyl-3-p-tolyl-propionic acid-chloride

: 66309-83-9
2,6-dimethylindan-1-one

Conditions

Conditions	Yield
With aluminium trichloride; Petroleum ether anschliessendes Erwaermen;

: 106-42-3
para-xylene

: 66309-83-9
2,6-dimethylindan-1-one

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 72 percent / AlCl3 / 0 - 20 °C 2: 42 percent / methanol / 16 h / Irradiation View Scheme

: 73120-65-7
diethyl 2-methyl-2-(4-methylbenzyl)malonate

: 66309-83-9
2,6-dimethylindan-1-one

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: concd. HCl / acetic acid / 24 h / Heating 2: 1.12 g / polyphosphoric acid / 3 h / 100 °C View Scheme

: 104-81-4
4-Methylbenzyl bromide

: 66309-83-9
2,6-dimethylindan-1-one

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: K2CO3 / dimethylformamide / 10 h / 150 °C 2: concd. HCl / acetic acid / 24 h / Heating 3: 1.12 g / polyphosphoric acid / 3 h / 100 °C View Scheme

: 25860-59-7
2-methyl-3-p-tolylacrylic acid

: 66309-83-9
2,6-dimethylindan-1-one

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: palladium 10% on activated carbon; hydrogen / methanol / 24 h / 7600.51 Torr 2: polyphosphoric acid / 12 h / 80 °C View Scheme

: 104-87-0
4-methyl-benzaldehyde

: 66309-83-9
2,6-dimethylindan-1-one

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1.1: potassium carbonate / 0.08 h / 0 °C 1.2: 12 h / 160 - 180 °C 2.1: palladium 10% on activated carbon; hydrogen / methanol / 24 h / 7600.51 Torr 3.1: polyphosphoric acid / 12 h / 80 °C View Scheme

: 104-82-5
4-Methylbenzyl chloride

: 66309-83-9
2,6-dimethylindan-1-one

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1.1: sodium methylate / tetrahydrofuran / 2 h / 50 - 60 °C 1.2: 3 h / 55 - 60 °C 2.1: sodium hydroxide / 3 h / 60 - 65 °C 3.1: thionyl chloride / dichloromethane / 1 h / 35 - 40 °C 4.1: aluminum (III) chloride / dichloromethane / 3 h / 0 - 10 °C View Scheme

: 29417-79-6
methyl 2-methyl-3-(4-methylphenyl)propanoate

: 66309-83-9
2,6-dimethylindan-1-one

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: sodium hydroxide / 3 h / 60 - 65 °C 2: thionyl chloride / dichloromethane / 1 h / 35 - 40 °C 3: aluminum (III) chloride / dichloromethane / 3 h / 0 - 10 °C View Scheme

: 24623-20-9
2,3-dihydro-6-methyl-1H-inden-1-one

: 74-88-4
methyl iodide

: 66309-83-9
2,6-dimethylindan-1-one

Conditions

Conditions	Yield
Stage #1: 2,3-dihydro-6-methyl-1H-inden-1-one With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 2h; Inert atmosphere; Stage #2: methyl iodide In tetrahydrofuran at -78 - 20℃; Inert atmosphere;

: 103440-52-4
methyl 2-iodo-5-methylbenzoate

: 66309-83-9
2,6-dimethylindan-1-one

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: tetrakis(triphenylphosphine) palladium(0); lithium chloride / tetrahydrofuran / 12 h / 100 °C / Inert atmosphere; Sealed tube 2: bis(1,5-cyclooctadiene)nickel (0); potassium tert-butylate; potassium phosphate; 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride; 1-Phenylethanol / toluene / 16 h / 100 °C / Inert atmosphere; Sealed tube View Scheme

: 50-00-0
formaldehyd

: 66309-83-9
2,6-dimethylindan-1-one

: 285977-95-9
2-(hydroxymethyl)-2,6-dimethyl-2,3-dihydro-1H-inden-1-one

Conditions

Conditions	Yield
With potassium carbonate In methanol; toluene at 50℃;	97%

: 66309-83-9
2,6-dimethylindan-1-one

A: 945613-46-7
(1S,2S)-2,6-dimethylindan-1-ol

: trans-2,6-dimethylindan-1-ol

Conditions

Conditions	Yield
With formic acid; triethylamine; chloro {[(1S,2S)-(-)-2-amino-1,2-diphenylethyl](4-toluenesulfonyl)amido}(mesitylene)ruthenium(II) at 20℃; for 168h;	A 71% B n/a

: 66309-83-9
2,6-dimethylindan-1-one

: 107-11-9
1-amino-2-propene

: allyl-[(1S,2S)-2,6-dimethy-indan-1-yl]-amine

Conditions

Conditions	Yield
With formic acid; triethylamine; (S,S)-NH2-CH(Ph)-CH(Ph)-N(Ts)-RuCl-(p-cymene) In dichloromethane at 20℃; for 144h;	60%

: 66309-83-9
2,6-dimethylindan-1-one

A: 213381-54-5
7-Bromo-2,6-dimethyl-1-indanone

B: 940884-61-7
4,7-dibromo-2,6-dimethyl-1-indanone

C: 892574-45-7
4-bromo-2,6-dimethylindan-1-one

Conditions

Conditions	Yield
With aluminum (III) chloride; bromine In chloroform at 0℃; for 3h;	A n/a B 10% C n/a

...Expand

: 66309-83-9
2,6-dimethylindan-1-one

: 100-46-9
benzylamine

: Benzyl-[2,6-dimethyl-indan-(1Z)-ylidene]-amine

Conditions

Conditions	Yield
With toluene-4-sulfonic acid In toluene Heating;

: 66309-83-9
2,6-dimethylindan-1-one

: C11H13N3

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1.1: 71 percent / HCOOH; triethylamine / (S,S)-[RuCl(TsDPEN)(p-cymene)] / 168 h / 20 °C 2.1: diphenylphosphoryl azide / toluene / 0.17 h / 0 °C 2.2: DBU / toluene / 22 h / 0 - 20 °C View Scheme

: 66309-83-9
2,6-dimethylindan-1-one

: 752984-24-0
(1R,2S)-2,6-dimethyl-2,3-dihydro-1H-inden-1-yl-amine

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1.1: 71 percent / HCOOH; triethylamine / (S,S)-[RuCl(TsDPEN)(p-cymene)] / 168 h / 20 °C 2.1: diphenylphosphoryl azide / toluene / 0.17 h / 0 °C 2.2: DBU / toluene / 22 h / 0 - 20 °C 3.1: 232 mg / Ph3P; H2O / tetrahydrofuran / Heating View Scheme

: 66309-83-9
2,6-dimethylindan-1-one

: C18H19NO

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1.1: 71 percent / HCOOH; triethylamine / (S,S)-[RuCl(TsDPEN)(p-cymene)] / 168 h / 20 °C 2.1: diphenylphosphoryl azide / toluene / 0.17 h / 0 °C 2.2: DBU / toluene / 22 h / 0 - 20 °C 3.1: 232 mg / Ph3P; H2O / tetrahydrofuran / Heating 4.1: 86 percent / triethylamine / CH2Cl2 View Scheme

: 66309-83-9
2,6-dimethylindan-1-one

: 285977-87-9
(+)-(2S)-2,3-dihydro-2,5-dimethyl-1H-indene-2-methanol

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 97 percent / K2CO3 / toluene; methanol / 50 °C 2: MeSO3H; H2 / Pd/C / propan-2-ol / 7.5 h / 80 °C / 2250.18 Torr 3: 6.39 g / ethanol; various solvent(s) View Scheme

: 66309-83-9
2,6-dimethylindan-1-one

: (-)-(2R)-2,3-dihydro-2,5-dimethyl-1H-indene-2-methanol

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 97 percent / K2CO3 / toluene; methanol / 50 °C 2: MeSO3H; H2 / Pd/C / propan-2-ol / 7.5 h / 80 °C / 2250.18 Torr 3: 6.15 g / ethanol; various solvent(s) View Scheme

: 66309-83-9
2,6-dimethylindan-1-one

: 285977-85-7
(+/-)-2,3-dihydro-2,5-dimethyl-1H-indene-2-methanol

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 97 percent / K2CO3 / toluene; methanol / 50 °C 2: MeSO3H; H2 / Pd/C / propan-2-ol / 7.5 h / 80 °C / 2250.18 Torr View Scheme

: 66309-83-9
2,6-dimethylindan-1-one

: benzyl-[(1S,2S)-2,6-dimethyl-indan-1-yl]-amine

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: p-TsOH / toluene / Heating 2: HCOOH; Et3N / (S,S)-NH2-CH(Ph)-CH(Ph)-N(Ts)-RuCl-(p-cymene) complex / CH2Cl2 / 144 h / 20 °C View Scheme

: 66309-83-9
2,6-dimethylindan-1-one

: [(2S)-2,3-dihydro-2,5-dimethyl-1H-inden-2-yl]methyl-(1S,4R)-4,7,7-trimethyl-3-oxo-2-oxabicyclo[2.2.1]heptane-1-carboxylate

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: 97 percent / K2CO3 / toluene; methanol / 50 °C 2: MeSO3H; H2 / Pd/C / propan-2-ol / 7.5 h / 80 °C / 2250.18 Torr 3: 6.39 g / ethanol; various solvent(s) 4: 61 percent / pyridine / 20 °C View Scheme

: 66309-83-9
2,6-dimethylindan-1-one

: 285977-95-9
2-(hydroxymethyl)-2,6-dimethyl-2,3-dihydro-1H-inden-1-one

Conditions

Conditions	Yield
With potassium carbonate In water; toluene

: 50-00-0
formaldehyd

: 66309-83-9
2,6-dimethylindan-1-one

A: 1073511-12-2
(S)-2,3-dihydro-2-(hydroxymehtyl)-2,6-dimethylindane-1-one

B: 1073511-11-1
(R)-2,3-dihydro-2-(hydroxymethyl)-2,6-dimethylindane-1-one

Conditions

Conditions	Yield
With pyridine; C23H40N4O4; scandium tris(trifluoromethanesulfonate) In water at 20℃; for 24h; enantioselective reaction;

...Expand

: 66309-83-9
2,6-dimethylindan-1-one

: 1430230-20-8
ethyl 2-(2,5-dimethyl-1H-inden-3-yl)acetate

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C 1.2: 4 h / -78 °C 2.1: acetic acid; sulfuric acid / 4 h / 20 °C View Scheme

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