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English Name:Xanthine Test Method:HPLC Purity:≥98% [Synonyms] 2,6-Dihydroxypurine; Purine-2(3H),6(1H)-dione [CAS No.]69-89-6 [Mol. Formula]C5H4N4O2 [Mol. Weight]152.11 [Botanical Source]Organisms [Loss on drying] ≤2.0% [Catalogue No.
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Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Conditions | Yield |
---|---|
With perchloric acid at 110 - 130℃; for 0.25h; | 69% |
enzymatische Bildung; | |
With nitric acid |
Conditions | Yield |
---|---|
With hydrogenchloride |
Conditions | Yield |
---|---|
With sodium hydroxide; sodium hypochlorite |
Conditions | Yield |
---|---|
With sodium metabisulfite; formic acid at 180℃; | |
With sodium metabisulfite; formic acid at 180℃; |
Conditions | Yield |
---|---|
With calcium hydroxide; water Erhitzen bis zur beginnenden Gasentwicklung; |
Conditions | Yield |
---|---|
at 200℃; |
uric Acid
formamide
A
1,7-dihydro-6H-purin-6-one
B
xanthin
Conditions | Yield |
---|---|
With water at 180 - 200℃; |
Conditions | Yield |
---|---|
at 225 - 230℃; |
Conditions | Yield |
---|---|
With oxalic acid; glycerol at 200℃; | |
With nitrogen oxides; water; Nitrogen dioxide at 70℃; | |
With formic acid; glycerol at 225 - 230℃; | |
With cyclothionine; xanthine oxidase In phosphate buffer at 25℃; pH=6.5; Equilibrium constant; Further Variations:; Reagents; |
Conditions | Yield |
---|---|
With oxalic acid; glycerol at 200℃; |
6-amino-5-formylamino-1H-pyrimidine-2,4-dione
formamide
xanthin
Conditions | Yield |
---|---|
With formic acid |
5-acetylamino-6-amino-1H-pyrimidine-2,4-dione
formamide
xanthin
Conditions | Yield |
---|---|
enzymatische Bildung; | |
With xanthine oxidase Enzymatic reaction; |
Conditions | Yield |
---|---|
bei enzymatischen Oxydation; |
Conditions | Yield |
---|---|
With nickel; formamide at 180℃; under 66195.7 Torr; Hydrogenation; |
Conditions | Yield |
---|---|
at 39℃; bei der Einw. von waessr.Extrakt aus menschlicher Leber; |
Conditions | Yield |
---|---|
Verfuetterung an Enten; |
Conditions | Yield |
---|---|
With sodium azide; phosphate buffer; guanase in serum; McIlvaine buffer; (E)-(3-methyl-1,3-benzothiazol-2-ylidene)hydrazine;hydrochloride; N,N-dimethyl-aniline; citric acid; xanthine oxidase; peroxidase 1.) pH=6.2; 2.) pH=3.5; 3.) standard assay of guanase activity in serum; |
Conditions | Yield |
---|---|
With p-methoxyphenolate In water at 20℃; Rate constant; Equilibrium constant; pH 13.0; further reagent; |
Conditions | Yield |
---|---|
With hydrogenchloride In water at 25℃; Rate constant; |
xanthin
Conditions | Yield |
---|---|
With hydrogenchloride at 100℃; |
Conditions | Yield |
---|---|
With solution aqueuse d'hydroxide de sodium; tetrabutylammomium bromide In dichloromethane 1)room temp. 12h 2)reflux 3h; | 100% |
xanthin
Conditions | Yield |
---|---|
In ethyl acetate soln. of hydrated metal perchlorate in a mixt. of ethyl acetate and triethyl orthoformate, addn. of xanthanine (molar ratio metal:xanthine 1:3), mixt. refluxed (6 h or until no further change), cooled (ambient temp.); addn. of anhydrous Et2O, concn. (at low heat), pptn., filtration, washed (Et2O), stored (over anhydrous CaSO4); elem. anal.; | 100% |
xanthin
Conditions | Yield |
---|---|
In ethanol Zr-compound refluxed in ethanol/triethyl orthoformate for 2 h; N-compound added and refluxed for 36 h; cooled to room temp.; filtered; washed with acetone; elem. anal.; | 91% |
xanthin
8-bromo-3,7-dihydro-1H-purine-2,6-dione
Conditions | Yield |
---|---|
With bromine In water at 100℃; for 4h; Sealed tube; Inert atmosphere; | 90% |
With bromine In water at 100℃; Sealed tube; | 71% |
With bromine at 100℃; | |
With bromine In water at 100℃; | 18.4 g |
With bromine In water at 100℃; Inert atmosphere; | 3.05 g |
Conditions | Yield |
---|---|
With sodium hydroxide In acetone for 24h; Ambient temperature; | 90% |
[(AuBr)2(μ-1,3-bis(diphenylphosphino)propane)]
xanthin
[Au2(μ-xanthinate(2-))(μ-1,3-bis(diphenylphosphino)propane)]
Conditions | Yield |
---|---|
With KOH In ethanol byproducts: KBr; inert atmosphere; addn. of mixt. of purine ligand and 1 equiv. KOH to 1 equiv. diphosphine, refluxing for 30 min; filtration, crystn. (room temp.); elem. anal.; | 90% |
xanthin
Conditions | Yield |
---|---|
In ethyl acetate soln. of hydrated metal perchlorate in a mixt. of ethyl acetate and triethyl orthoformate, addn. of xanthanine (molar ratio metal:xanthine 1:3), mixt. refluxed (6 h or until no further change), cooled (ambient temp.); addn. of anhydrous Et2O, concn. (at low heat), pptn., filtration, washed (Et2O), stored (over anhydrous CaSO4); elem. anal.; | 86.2% |
Conditions | Yield |
---|---|
In water ligand was dissolved in a boiling mixt. of MeHgOH and MeHgNO3 in H2O, soln. was stirred for 1 h, allowed to cool,; after 3 d ppt. was filtered, washed with EtOH, dried in vac.; elem. anal.; | 86% |
xanthin
N,N'-dicyclohexyl-O-methyl isourea
3,7-dihydro-1,3,7-trimethyl-1H-purine-2,6-dione
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 100℃; for 48h; | 85% |
xanthin
methyl iodide
A
7,9-dimethylxanthinium iodide
B
1,7,9-trimethylxanthinium iodide
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 110℃; for 5h; closed Kjeldahl flask; | A 85% B 10% |
Conditions | Yield |
---|---|
With NaOH In methanol; water xanthine was dissolved in an aq. soln. of min NaOH, a methanolic soln. of Ni-salt was added, treated with amine, (xanthine:Cu-salt:amine=1:2:2),the mixt. (pH 7-8) was allowed to stand at room temp. for 2 weeks; elem. anal.; | 85% |
Conditions | Yield |
---|---|
With NH4OH In not given ligand was suspended in mixt. of concd. NH4OH and MeHgOH, suspn. was refluxed for 4 d, allowed to cool to room temp.; after 2 d ppt. was filtered, dried in vac.; elem. anal.; | 83% |
Conditions | Yield |
---|---|
In water ligand was dissolved in a boiling mixt. of MeHgOH and MeHgClO4 in H2O,soln. was stirred for 1 h, allowed to cool,; after 3 d ppt. was filtered, washed with EtOH, dried in vac.; elem. anal.; | 83% |
Conditions | Yield |
---|---|
In water ligand was dissolved in a boiling mixt. of MeHgOH and MeHgNO3 in H2O, soln. was stirred for 1 h; after 3 d ppt. was filtered, washed with EtOH, dried in vac.; elem. anal.; | 83% |
μ-{1,2-bis(diphenylphosphino)butane}-dibromodigold(I)
xanthin
[Au2(μ-xanthinate(2-))(μ-1,4-bis(diphenylphosphino)butane)] * H2O
Conditions | Yield |
---|---|
With KOH In ethanol byproducts: KBr; inert atmosphere; addn. of mixt. of purine ligand and 1 equiv. KOH to 1 equiv. diphosphine, refluxing for 30 min; filtration, crystn. (room temp.); elem. anal.; | 82% |
[(AuBr)2(μ-1,2-bis(dimethylphosphino)ethane)]
xanthin
Conditions | Yield |
---|---|
With KOH In ethanol byproducts: KBr; inert atmosphere; addn. of mixt. of purine ligand and 1 equiv. KOH to 1 equiv. diphosphine, refluxing for 30 min; filtration, crystn. (room temp.); elem. anal.; | 80% |
2,2',2''-triaminotriethylamine
xanthin
[Cd(tris(2-aminoethyl)amine)(xanthine-H)]ClO4*H2O
Conditions | Yield |
---|---|
With KOH In methanol; water xanthine was dissolved in an aq. soln. of min KOH, a methanolic soln. ofCd-salt was added, treated with amine, the mixt. (pH 9-10) was allowed to stand at room temp. for 1 week; elem. anal.; | 78% |
xanthin
Conditions | Yield |
---|---|
In methanol; dichloromethane addn. of 1 equiv. ligand (in MeOH) to Zn-complex (in CH2Cl2), stirring for 2 h; vol. reduction (vac.), crystn. (4°C, 1 d), collection (filtration), drying (vac.); elem. anal.; | 77% |
xanthin
Conditions | Yield |
---|---|
In ethyl acetate soln. of hydrated metal perchlorate in a mixt. of ethyl acetate and triethyl orthoformate, addn. of xanthanine (molar ratio metal:xanthine 1:2), mixt. refluxed (6 h or until no further change), cooled (ambient temp.); addn. of anhydrous Et2O, concn. (at low heat), pptn., filtration, washed (Et2O), stored (over anhydrous CaSO4); elem. anal.; | 76.2% |
xanthin
Conditions | Yield |
---|---|
In ethyl acetate soln. of hydrated metal perchlorate in a mixt. of ethyl acetate and triethyl orthoformate, addn. of xanthanine (molar ratio metal:xanthine 1:2), mixt. refluxed (6 h or until no further change), cooled (ambient temp.); addn. of anhydrous Et2O, concn. (at low heat), pptn., filtration, washed (Et2O), stored (over anhydrous CaSO4); elem. anal.; | 75.7% |
carbonic acid dimethyl ester
xanthin
3,7-dihydro-1,3,7-trimethyl-1H-purine-2,6-dione
Conditions | Yield |
---|---|
With 18-crown-6 ether In N,N-dimethyl-formamide at 90℃; for 12h; | 74% |
Conditions | Yield |
---|---|
In ethyl acetate Co salt dissolved in a 7:3 (vol./vol.) mixture of triethyl orthoformate-ethyl acetate, refluxed (1 h), addn. of a warmed slurry of the ligand in the same solvent, refluxed (1 wk), allowed to cool to room temp.; collected by gravity filtration, washed thoroughly (anhydrous diethyl ether), stored (vac., anhydrous CaSO4); elem. anal.; | 73% |
xanthin
Conditions | Yield |
---|---|
In ethyl acetate soln. of hydrated metal perchlorate in a mixt. of ethyl acetate and triethyl orthoformate, addn. of xanthanine (molar ratio metal:xanthine 1:2), mixt. refluxed (6 h or until no further change), cooled (ambient temp.); addn. of anhydrous Et2O, concn. (at low heat), pptn., filtration, washed (Et2O), stored (over anhydrous CaSO4); elem. anal.; | 71.6% |
Conditions | Yield |
---|---|
In water ligand was dissolved in a boiling mixt. of MeHgOH and MeHgClO4 in H2O,soln. was stirred for 1 h; after 3 d ppt. was filtered, washed with EtOH, dried in vac.; elem. anal.; | 70% |
Conditions | Yield |
---|---|
at 150℃; for 5h; closed Kjeldahl flask; | 69% |
2,2',2''-triaminotriethylamine
xanthin
[Zn(tris(2-aminoethyl)amine)(xanthine-H)]ClO4*H2O
Conditions | Yield |
---|---|
With NaOH In methanol; water xanthine was dissolved in an aq. soln. of min NaOH, a methanolic soln. of Zn-salt and amine-compound was added, the mixt. (pH 8-9) was allowed to stand at room temp. for 1 month; elem. anal.; | 69% |
xanthin
Conditions | Yield |
---|---|
In ethyl acetate soln. of hydrated metal perchlorate in a mixt. of ethyl acetate and triethyl orthoformate, addn. of xanthanine (molar ratio metal:xanthine 1:2), mixt. refluxed (6 h or until no further change), cooled (ambient temp.); addn. of anhydrous Et2O, concn. (at low heat), pptn., filtration, washed (Et2O), stored (over anhydrous CaSO4); elem. anal.; | 65.4% |
xanthin
Conditions | Yield |
---|---|
In ethyl acetate soln. of hydrated metal perchlorate in a mixt. of ethyl acetate and triethyl orthoformate, addn. of xanthanine (molar ratio metal:xanthine 1:2), mixt. refluxed (6 h or until no further change), cooled (ambient temp.); addn. of anhydrous Et2O, concn. (at low heat), pptn., filtration, washed (Et2O), stored (over anhydrous CaSO4); elem. anal.; | 62.5% |
2,2',2''-triaminotriethylamine
xanthin
[Ni(tris(2-aminoethyl)amine)(xanthine-H)(H2O)]ClO4*H2O
Conditions | Yield |
---|---|
With KOH In methanol; water xanthine was dissolved in an aq. soln. of min KOH, a methanolic soln. ofNi-salt was added, treated with amine, the mixt. (pH 8-9) was allowed t o stand at room temp. for 2 days; elem. anal.; | 62% |
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