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Cas:6923-52-0
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Chemwill Asia co.,Ltd is one of the leading manufacturer in CHINA. Product quality, process, price and service Antimony triacetate CAS 6923-52-0 IN STOCK Antimony(III) acetate CAS 6923-52-0 6923-52-0 CAS 6923-52-0 highly quality and immeda
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inquiryAppearance:White powder Storage:room temperature Package:25kg/drum Application:Antimony(III) acetate is a catalyst used in the production of synthetic fibers. Antimony(III) acetate was used in the one-pot three-component synthesis of multigram quan
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Name: antimony triacetate CAS: 6923-52-0 Molecular Formula: C6H9O6Sb Molecular Weight: 298.892 Application:Fine chemical
Cas:6923-52-0
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Product name Antimony Triacetate CAS NO. 6923-52-0;3643-76-3 EINECS 230-043-2 Molecular formula Sb(CH3COO)3 Molecular weight 298.75 Appearance: White or off-white powder Storage:Store
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Conditions | Yield |
---|---|
In acetic anhydride byproducts: CH3CO2H; heating Sb2O3*nH2O and acetic anhydride under reflux, 2h; filtration; evapn.; cooling; solidification; elem. anal.; | 95% |
dichlorophenylstibine
sodium acetate trihydrate
A
antimony(III) acetate
B
diphenylantimony(III) acetate
Conditions | Yield |
---|---|
In ethanol byproducts: NaCl; refluxing, filtering, evapn., extrn. with benzene, evapn.; | A n/a B 74% |
In ethanol byproducts: NaCl; refluxing, filtering, evapn., extrn. with benzene, evapn.; | A n/a B 74% |
Conditions | Yield |
---|---|
In carbon disulfide at ambient temp.; | |
In carbon disulfide |
Conditions | Yield |
---|---|
In neat (no solvent) pptn. at 100°C;; extractn. of Sb-acetate with CS2;; | |
In neat (no solvent) pptn. at 100°C;; extractn. of Sb-acetate with CS2;; |
Conditions | Yield |
---|---|
In neat (no solvent) react. of starting materials;; recrystn. (twice) from toluene contg. ca 5 vol% acetic anhydride in order to prevent hydrolysis;; |
Conditions | Yield |
---|---|
In formic acid byproducts: CH3CO2H; heating antimony acetate and formic acid (100-fold excess) under reflux, 2h; evapn.; | 100% |
Conditions | Yield |
---|---|
In water High Pressure; H2O:Sb-acetate:1,2-ethanedisulfonic acid molar ratio 100:1:5, heated in autoclave for 3 days at 150°C, pH 3.5 -> 2.5; vac. filtered, rinsed with ethanol; elem. anal.; | 97.4% |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: CH3CO2H; heating antimony acetate and (CH3)2CHCO2H (50-70% excess) in a Claisen flask with condenser; distn. off acetic acid, 0.5h; cooling to room temp.; fractionating under vac.; elem. anal.; | 97% |
5,5-dimethyl-2-thiolo-2-thiono-1,3,2-dioxaphosphorinane
antimony(III) acetate
(2,2-dimethyl-trimethylene)dithiophosphato-antimony(III)diacetate
Conditions | Yield |
---|---|
In benzene to a soln. of dithiophosphoric acid in benzene was added dropwise a soln. of Sb-acetate (molar ratio 1:1) in benzene with stirring at room temp. for 2 h; the ppt. was filtered, washed with n-hexane repeatedly and finally dried under reduced pressure, elem. anal.; | 94% |
4,4,5,5-tetramethyl-2-thioxo-2λ5-[1,3,2]dioxaphospholane-2-thiol
antimony(III) acetate
(1,1,2,2-tetramethyl-dimethylene)dithiophosphato-antimony(III)diacetate
Conditions | Yield |
---|---|
In benzene to a soln. of dithiophosphoric acid in benzene was added dropwise a soln. of Sb-acetate (molar ratio 1:1) in benzene with stirring at room temp. for 2 h; the ppt. was filtered, washed with n-hexane repeatedly and finally dried under reduced pressure, elem. anal.; | 94% |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: CH3CO2H; heating antimony acetate and (CH3)3CCO2H (50-70% excess) in a Claisen flask with condenser; distn. off acetic acid, 0.5h; cooling to room temp.; fractionating under vac.; elem. anal.; | 88% |
Conditions | Yield |
---|---|
In methanol; water at 160℃; for 144h; Autoclave; High pressure; | 88% |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: CH3CO2H; heating antimony acetate and (CH3)2CHCH2CO2H (50-70% excess) in a Claisen flask with condenser; distn. off acetic acid, 0.5h; cooling to room temp.; fractionating under vac.; elem. anal.; | 86% |
antimony(III) acetate
Conditions | Yield |
---|---|
In acetonitrile mixt. of solns. stirred for 2 h, filtered; evapd. slowly at room temp., ppt. filtered off, recrystd. (acetonitrile); elem. anal.; | 84% |
Conditions | Yield |
---|---|
In propionic acid byproducts: CH3CO2H; heating antimony acetate and propionic acid (50-70% excess) in a Claisen flask with condenser; distn. off acetic acid, 0.5h; cooling to room temp.; fractionating under vac.; elem. anal.; | 82% |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: CH3CO2H; heating antimony acetate and CH3(CH2)3CO2H (50-70% excess) in a Claisen flask with condenser; distn. off acetic acid, 0.5h; cooling to room temp.; fractionating under vac.; elem. anal.; | 79% |
antimony(III) acetate
N-bis(trimethylsilyl)-N'-<(N''-trimethylsilyl)imino-(P-diphenyl)-phosphoranyl>imino-(P-diphenyl)phosphoranylamin
N[P(C6H5)2NSi(CH3)3]2Sb(OOCCH3)2
Conditions | Yield |
---|---|
77% |
Conditions | Yield |
---|---|
In methanol at 160℃; for 144h; Autoclave; High pressure; | 71% |
2-Mercaptopyridine
antimony(III) acetate
tris(pyridine-2-thiolato)antimony(III)
Conditions | Yield |
---|---|
With triethylamine In methanol under Ar, room temp., stirring; filtration, concentration, addn. of Et2O, the soln. was allowed stand at -20°C for 4 d, elem.anal.; | 70% |
Conditions | Yield |
---|---|
In dichloromethane soln. PhCSOH in CH2Cl2 treated with Sb(CH3COO)3 dissolved in CH2Cl2 andmixt. stirred for 1 h; ppt. filtered, dried and recrystd. from CH2Cl2; elem. anal.; | 64% |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: CH3CO2H; heating antimony acetate and CH3(CH2)4CO2H (50-70% excess) in a Claisen flask with condenser; distn. off acetic acid, 0.5h; cooling to room temp.; fractionating under vac.; elem. anal.; | 63% |
antimony(III) acetate
ethylene glycol
Sb(3+)*OCH2CH2O(2-)*CH3COO(1-)=(Sb(OCH2CH2O)(CH3COO))
Conditions | Yield |
---|---|
In benzene soln. Sb(OAc)3 in benzene was treated with soln. ethylene glycol in benzene and stirred at room temp. overnight; ppt. was filtered and washed with benzene; | 55% |
antimony(III) acetate
tris{(3-trimethylsilyl)pyridine-2-thiolato}antimony(III)
Conditions | Yield |
---|---|
In methanol under Ar, stirred at room temp. for 8h; filtration, concentration, the soln. was allowed to stand for 3 d at -20°C, elem.anal.; | 50% |
pyridine
water
antimony(III) acetate
benzene-1,2-diol
[(py)Sb(1,2-O2C6H4)]2O
Conditions | Yield |
---|---|
In pyridine mixt. catechol and Sb(OAc)3 was treated with pyridine, water was added and stirred for 4 days; ppt. was fitered, washed with benzene and dried in vacuo; elem. anal.; | 45% |
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