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inquiryProduct description: Product name Sodium acetate trihydrate CAS number 6131-90-4 Assay ≥99% Appearance White or off-white crystal Capacity 200mt/year Application Organic int
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inquiry1) Product Information Chemical Name: Sodium acetate trihydrate Other name: ACETIC ACID SODIUM SALT TRIHYDRATE;SODIUM ACETATE 3H2O;SODIUM ACETATE-3-HYDRATE;SODIUM ACETATE TRIHYDRATE;SODA CAUSTIC; Natriumacetat-trihydrat;sodiumethanoatetrihy
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inquirySodium acetate trihydrate Basic information Product Name: Sodium acetate trihydrate Synonyms: SODIUM ACETATE 3H2O;SODIUM ACETATE-3-HYDRATE;SODIUM ACETATE TRIHYDRATE;SODA CAUSTIC;ACETIC A
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inquiryChemical name: Acetic acid,sodium salt trihydrate English name: Acetic acid sodium salt trihydrate;Sodium acetate trihydrate CAS No: 6131-90-4 Molecular formula: C2H3NaO2.3H2O Structura
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inquiry1.Prompt Goods; 2.Flexible payment terms; 3.Documents & Certificate support. Name: Sodium acetate trihydrate Structure: Formula: C2H9NaO5 Molecular Weight : 136.08 Synonyms: Aceticacid,sodiumsalttrihydrate,foranalysis;Aceticacid,sodiumsal
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inquiryConditions | Yield |
---|---|
With sodium carbonate |
Conditions | Yield |
---|---|
With water In neat (no solvent) formation of supersaturated soln. via H2O uptake, solidification after contact with solid materials and slow formation of NaCH3CO2*3H2O;; | |
With water in moist air at ambient temp.;; | |
With H2O in moist air at ambient temp.;; | |
With H2O In neat (no solvent) formation of supersaturated soln. via H2O uptake, solidification after contact with solid materials and slow formation of NaCH3CO2*3H2O;; |
Conditions | Yield |
---|---|
In neat (no solvent) equlibrium reaction, uptake of 3 mol H2O from moist air;; | |
In neat (no solvent) equlibrium reaction, uptake of 3 mol H2O from moist air;; |
Conditions | Yield |
---|---|
With copper(I) oxide In neat (no solvent) byproducts: HCl; reaction without influence of air via stirring NaCl with acetic acid in presence of Cu2O;; | |
With Cu2O In neat (no solvent) byproducts: HCl; reaction without influence of air via stirring NaCl with acetic acid in presence of Cu2O;; |
sodium carbonate
acetic acid
sodium hydroxide
sodium acetate trihydrate
Conditions | Yield |
---|---|
In neat (no solvent) addition of solid NaOH to soln. of acetic acid and Na2CO3 yileds yellow crystalls;; via recrystallization;; | |
In neat (no solvent) addition of solid NaOH to soln. of acetic acid and Na2CO3 yileds yellow crystalls;; via recrystallization;; |
Conditions | Yield |
---|---|
react. of glacial acetic acid (distd. over CrO3, storage over Br2, distd. over KMnO4) and Na2CO3 ( several times recrystn. from soln. containing hypobromite);; fractionated crystn.; very pure product;; | |
react. of glacial acetic acid (distd. over CrO3, storage over Br2, distd. over KMnO4) and Na2CO3 ( several times recrystn. from soln. containing hypobromite);; fractionated crystn.; very pure product;; |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: NH3; | |
In neat (no solvent) byproducts: NH3; |
Conditions | Yield |
---|---|
In neat (no solvent) | |
In neat (no solvent) |
Conditions | Yield |
---|---|
In water byproducts: alcohol; saponification of CH3CO2C2H5 with solid NaOH in presence of H2O or in presence of NaCH3CO2*3H2O or its concd. soln.;; | |
In water byproducts: alcohol; saponification of CH3CO2C2H5 with solid NaOH in presence of H2O or in presence of NaCH3CO2*3H2O or its concd. soln.;; |
methanol
carbon monoxide
sodium hydroxide
sodium acetate trihydrate
Conditions | Yield |
---|---|
In neat (no solvent) reaction of CH3OH with CO or CO containing gases at 200 to 300°C and small excess NaOH;; | |
In neat (no solvent) reaction of CH3OH with CO or CO containing gases at 200 to 300°C and small excess NaOH;; | |
In neat (no solvent) reaction of CH3OH with CO or CO containing gases at 200 to 300°C and small excess NaOH;; |
methanol
carbon monoxide
sodium carbonate
sodium acetate trihydrate
Conditions | Yield |
---|---|
In neat (no solvent) reaction of CH3OH with CO or CO containing gases at 200 to 300°C and small excess Na2CO3;; | |
In neat (no solvent) reaction of CH3OH with CO or CO containing gases at 200 to 300°C and small excess Na2CO3;; | |
In neat (no solvent) reaction of CH3OH with CO or CO containing gases at 200 to 300°C and small excess Na2CO3;; |
Conditions | Yield |
---|---|
With water In neat (no solvent) heating NaHCO2 in autoclave to 200 to 300°C unnder pressure in presence of little H2O while treating with CH3OH vapor;; | |
With H2O In neat (no solvent) heating NaHCO2 in autoclave to 200 to 300°C unnder pressure in presence of little H2O while treating with CH3OH vapor;; | |
With water In neat (no solvent) heating NaHCO2 in autoclave to 200 to 300°C unnder pressure in presence of little H2O while treating with CH3OH vapor;; |
Conditions | Yield |
---|---|
With water | |
With H2O |
sodium acetate acetic acid
sodium acetate trihydrate
Conditions | Yield |
---|---|
With H2O In neat (no solvent) in moist air;; |
Conditions | Yield |
---|---|
With H2O |
sodium acetate trihydrate
Me2N-Arg(Teoc)2-Thz-MeOxz-Thz-MeOxz-OMe
Conditions | Yield |
---|---|
Stage #1: C37H55N9O9S2Si2; sodium acetate trihydrate With formaldehyd In tetrahydrofuran; water at 0℃; for 0.0833333h; Inert atmosphere; Stage #2: With sodium cyanoborohydride In tetrahydrofuran; water at 0℃; for 1h; Inert atmosphere; | 99% |
CH(O)C6H2(CH3)(CO)ORh(P(C6H5)3)2Cl
sodium acetate trihydrate
CH(O)C6H2(CH3)(CO)ORh(P(C6H5)3)2OOCCH3
Conditions | Yield |
---|---|
In dichloromethane; water; acetone stirring (0.5 h), evapn.; filtering, washing (H2O), drying (vac.); | 98% |
sodium acetate trihydrate
Conditions | Yield |
---|---|
With NaClO4 In water addn. of CH3COONa to aq. Ru complex soln., adjusting ph to 4 with few drops of CH3COOH, heating soln to 70°C, 0.5 h, cooling, addn. of NaClO4; pptn., storage in a refrigerator overnight, filtration, washing (MeOH, ether), air-drying; elem. anal.; | 95% |
sodium acetate trihydrate
CH(O)C6H2(CH3)(CO)ORh(P(C6H5)3)2OOCCH3
Conditions | Yield |
---|---|
In dichloromethane; water; acetone NaOAc soln. (H2O) addn., stirring (0.5 h), evapn. (reduced pressure); filtering, washing (H2O), drying (vac.); | 93% |
Conditions | Yield |
---|---|
With hydroxylamine chloride In tetrahydrofuran for 3h; | 93% |
tris(triphenylphosphine)ruthenium(II) chloride
sodium acetate trihydrate
RuCl(OAc)(PPh3)3
Conditions | Yield |
---|---|
In tert-butyl alcohol Ru-complex and AcONa*3H2O were intimately ground together in a mortar and pestle in air, mixt. was exposed to vac. for 30 min, flask filled with Ar, t-BuOH added, solm. was refluxed with rapid stirring for 1 h; ppt. was isolated by filtration in air, washed successively with Et2O, water, MeOH, Et2O, dried under reduced pressure; elem. anal.; | 92% |
sodium acetate trihydrate
di-μ-acetatotetrakis(dihaptoethene)dirhodium(I)
Conditions | Yield |
---|---|
In diethyl ether (argon); stirring (-30°C to room temp., 1 h); filtration, evapn. (vac.), recrystn. (pentane); elem. anal.; | 92% |
sodium acetate trihydrate
Conditions | Yield |
---|---|
With hydrogen In ethanol H2-atmosphere; molar ratio Ru-complex:ligand:NaOAc=1:1:2, refluxing (16h); cooling (pptn.), filtration, washing (acetone); elem. anal.; | 90% |
2-Hydroxy-1,4-naphthoquinone
copper(II) acetate monohydrate
sodium acetate trihydrate
Conditions | Yield |
---|---|
With orthoformic acid triethyl ester In methanol dissol. of Cu salt in MeOH, addn. of triethylorthoformate, purging with N2, addn. of soln. of lawsone in MeOH/triethylorthoformate, purging withN2, stirring (in N2 atmosphere, 15 min), addn. of NaOAc in MeOH to pH = 6, pptn.; filtration, washing (MeOH, Et2O), drying (vac.); elem. anal.; | 90% |
Conditions | Yield |
---|---|
In tetrahydrofuran; methanol (O2-free solvents); VOSO4*5H2O and NaCH3COO*3H2O dissolved in MeOH, treated with a THF soln. of HOC6H4CHO, a MeOH soln. of (BrCH2CH(NH3)COOCH3)Br added dropwise, stirred at room temp. overnight in the dark; filtered under inert atmosphere, evapd. (vac.); elem. anal.; | A n/a B 90% |
sodium acetate trihydrate
acetic acid
2-Bromo-4'-methoxyacetophenone
p-methoxyphenacyl acetate
Conditions | Yield |
---|---|
In ethanol; water for 2.5h; Reflux; | 90% |
Conditions | Yield |
---|---|
In acetonitrile byproducts: (PPN)ClO4; stoich. amts., stirring (room temp., 4 h); crystn. on vapor diffusion of ether, collection, washing (ether); elem.anal.; | 89.2% |
Conditions | Yield |
---|---|
In water at 20℃; for 2h; | 89% |
Conditions | Yield |
---|---|
In water at 20℃; for 2h; | 87.2% |
sodium acetate trihydrate
RuCl(O2CCH3)(bis(3-(diphenylphosphino)propyl)phenylphosphine)
Conditions | Yield |
---|---|
In tetrahydrofuran soln. of complex and excess NaOCOCH3*3H2O refluxed for 3 h; concd. (vac.), ether added, solid collected, washed with H2O, EtOH, ether, dried (vac.); elem. anal.; | 87% |
[IrH2Cl(PiPr3)2]
sodium acetate trihydrate
[IrH2(OCOCH3)(P(C3H7)3)2]
Conditions | Yield |
---|---|
In diethyl ether (argon); stirring (room temp., 15 h); filtration, solvent removal; elem. anal.; | 87% |
[(η(5)-semiquinone)Mn(CO)3]
sodium acetate trihydrate
Conditions | Yield |
---|---|
In dimethyl sulfoxide to soln. of Mn complex in DMSO added NaOAc*3H2O under N2 at room temp.; after 20 min pptd. by acetone; washed (acetone); elem. anal.; | 85% |
sodium acetate trihydrate
[Ir(C2H4)2(OCOCH3)]2
Conditions | Yield |
---|---|
In diethyl ether (argon); stirring (-78 to 0°C, 30 min), recooling to -78°C, kept under 0.5 bar ethene, slow warming to 0°C, repeating the procedure 3x, finally warming to room temp.; solvent removal, extn. (pentane), pptn. upon concn. (vac.), yield is for2 steps; elem. anal.; | 85% |
Conditions | Yield |
---|---|
In methanol for 4h; Reflux; | 85% |
xanthurenic acid
sodium acetate trihydrate
{VO(8-oxy-4-hydroxychinoline-2-carboxylate)(H2O)}
Conditions | Yield |
---|---|
In water N2; stirring for 3 h at 80 ° C and overnight at room temperature;; filtration; washing with water; elem. anal.;; | 84% |
sodium acetate trihydrate
Conditions | Yield |
---|---|
In methanol pptn. on mixing stoich. amts., stirring (room temp., 30 min); cooling to -20°C overnight, collection (filtration), washing (cold MeOH), drying in air, recrystn. (vapor diffusion of ether into MeCN soln.), collection, drying in air; elem. anal.; | 84% |
tetrahydrofuran
methyl 5-((1,2:3,4-di-O-isopropylidene-α-D-galactosyl)oxycarbonyl)-2-pyridinecarboxylate
sodium acetate trihydrate
Conditions | Yield |
---|---|
In tetrahydrofuran; water stoich., a soln. of N compd. and Na compd. (THF/water) mixed with a soln. of V compd. (water), refluxed for ca. 6 h; solvent evapd., residue dissolved (THF), filtered, evapd. to dryness; elem. anal.; | 84% |
pyridine-4-carbonitrile
dihydrogen peroxide
sodium acetate trihydrate
CoIII4(μ3-O)4(μ-O2CCH3 )4(4-CNpy)4
Conditions | Yield |
---|---|
In methanol for 4h; Reflux; | 84% |
sodium acetate trihydrate
N,N,N'-tris-(2-pyridylmethyl)-1,3-diaminopropan-2-ol
Conditions | Yield |
---|---|
In methanol MeOH soln. of ligand and NaOAc*3H2O was added to MeOH soln. of Cu-complex, allowed to stand at 10°C for 1 wk; filtered off; elem. anal.; | 83% |
2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine
sodium acetate trihydrate
Conditions | Yield |
---|---|
In 1,4-dioxane; water byproducts: H2O, NaCl, CH3CO2H; addn. of aq. soln. of NaO2CCH3 to dioxane soln. of (PNCl2)3 with stirring, stirring (60°C, 24 h); filtration, washing (EtOH, acetone), fractional recrystn. (water/EtOH); | 83% |
sodium acetate trihydrate
[Rh(C8H14)2(OCOCH3)]2
Conditions | Yield |
---|---|
In diethyl ether (argon); -30°C to room temp., stirring (6 h); filtration, evapn. (vac.), recrystn. (pentane); elem. anal.; | 83% |
sodium acetate trihydrate
[RuCl2(κ2-O2CCH3)(=C=CHPh)(PiPr3)2]
Conditions | Yield |
---|---|
In tetrahydrofuran under Ar atm. soln. dichloro(vinylidene)ruthenium complex in THF was treated with CH3COONa*3H2O and stirred for 22 h at room temp.; solvent was removed, residue was extd. with Et2O, extract was evapd. in vacuo, residue was washed with pentane at -78°C and dried; elem.anal.; | 82% |
sodium acetate trihydrate
Conditions | Yield |
---|---|
In methanol at 40℃; for 0.166667h; Glovebox; Inert atmosphere; | 82% |
sodium acetate trihydrate
Conditions | Yield |
---|---|
In ethanol byproducts: sodium nitrate; phenanthroline is added to the rare earth acetate soln. prepared at the first step; 24 h standing; washing with alcohol, drying in vac.; | 80% |
In ethanol byproducts: sodium nitrate; phenanthroline is added to the rare earth acetate soln. prepared at the first step; 24 h standing; washing with alcohol, drying in vac.; | 80% |
N-salicylidene-butylamine
sodium acetate trihydrate
bis(N-butylsalicylideneaminato)palladium(II)
Conditions | Yield |
---|---|
With potassium chloride In water; acetone dissoln. of PdCl2 in hot aq. KCl, addn. of NaAc*3H2O, addn. to soln. of org. compd. in acetone, refluxing (30 min), cooling (room temp.); removal of acetone (vac.), filtration, washing (MeOH), recrystn. (EtOH-benzene); elem. anal.; | 80% |
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