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inquiryMETHYL BETA-D-RIBOFURANOSIDE; METHYL BD-RIBOFURANOSIDE; 1-OME-BETA-D-RIB; 1-O-METHYL-BETA-D-RIBOFURANOSIDE;.beta.-D-Ribofuranoside, methyl;METHYL-SS-D- RIBOFURANOSIDE; (2R, 3S, 4R, 5R)-2-(hydroxymethyl)-5-methoxytetrahydrofuran-3,4-diol; 1-O-Methyl
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiryMethyl beta-D-ribofuranoside cas 7473-45-2Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiry2,3,5-tri-O-acetyl-1-O-methyl-β-D-ribofuranose
1-O-methyl-D-ribofuranose
Conditions | Yield |
---|---|
With tris(2,4,6-trimethoxyphenyl)phosphine In methanol at 20℃; for 28h; | 93% |
With potassium carbonate In methanol |
Conditions | Yield |
---|---|
With sodium for 12h; Ambient temperature; | 90% |
methanol
(2R,3R,4S,5R)-2-azido-5-(hydroxymethyl)tetrahydrofuran-3,4-diol
1-O-methyl-D-ribofuranose
Conditions | Yield |
---|---|
With sodium 1.) reflux, 3 h, 2.) RT, overnight; | 89% |
methyl 2,3,3'-tri-O-benzoyl-β-D-apiofuranoside
1-O-methyl-D-ribofuranose
Conditions | Yield |
---|---|
With potassium hydroxide In methanol for 0.5h; Ambient temperature; | 82% |
methanol
D-ribose
A
1-O-methyl-D-ribofuranose
B
methyl α-D-ribofuranoside
Conditions | Yield |
---|---|
With hydrogenchloride | A 70.9% B 20% |
With hydrogenchloride | |
With iodine for 7h; Product distribution; Heating; HPLC analysis (used dihydrogen sulphate form column) of product distribution in iodine-catalyzed methyl glycosidation; |
methanol
D-Ribose
1-O-methyl-D-ribofuranose
Conditions | Yield |
---|---|
With Dowex-50 (HCl form) at 0 - 25℃; for 72h; Inert atmosphere; | 68% |
With hydrogenchloride; water at 20℃; for 3.5h; | 63% |
With hydrogenchloride at 20℃; for 3.5h; | 63% |
With sulfuric acid | |
With sulfuric acid for 20h; Ambient temperature; |
methanol
D-Ribose
A
1-O-methyl-D-ribofuranose
B
methyl α-D-ribofuranoside
Conditions | Yield |
---|---|
With sulfuric acid at 4℃; for 24h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; | |
With sulfuric acid at 0 - 4℃; Yield given. Yields of byproduct given. Title compound not separated from byproducts; | |
With hydrogenchloride at 25℃; for 1.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; | |
sulfuric acid at 20℃; Cooling with ice; | |
With Dowex 50Wx8 H+ form at 4℃; for 20h; | A n/a B n/a |
Conditions | Yield |
---|---|
In tetrachloromethane for 24h; Ambient temperature; Yield given; |
β-D-ribofuranose
(1R,2R,4aS,5S,8aR)-2-(2-Hydroxy-ethyl)-5-methoxymethoxy-1-methyl-1,2,4a,5,6,7,8,8a-octahydro-naphthalene-1-carboxylic acid methyl ester
1-O-methyl-D-ribofuranose
Conditions | Yield |
---|---|
With hydrogenchloride Ambient temperature; |
methyl 5-benzoyl-2,3-benzoxonium-α-D-xylofuranoside
A
1-O-methyl-D-ribofuranose
B
methyl α-D-ribofuranoside
Conditions | Yield |
---|---|
With sodium methylate; sodium hydrogencarbonate 2.) CH3OH; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; |
hydrogenchloride
methanol
methyl β-D-ribopyranoside
A
methyl α-D-ribopyranoside
B
1-O-methyl-D-ribofuranose
C
methyl α-D-ribofuranoside
Conditions | Yield |
---|---|
at 35℃; Kinetics; |
methyl 5-azido-2,3-di-O-benzoyl-5-deoxy-α-D-xylofuranoside
1-O-methyl-D-ribofuranose
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: nitrosonium hexafluorophosphate / acetonitrile / 0.25 h / 0 °C 2: 1.) NaHCO3 (aq.), 2.) NaOCH3 / 2.) CH3OH View Scheme |
methyl 2,3-di-O-benzoyl-5-O-p-toluenesulfonyl-α-D-xylofuranoside
1-O-methyl-D-ribofuranose
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 0.8 g / NaN3 / dimethylformamide / 6 h / 90 °C 2: nitrosonium hexafluorophosphate / acetonitrile / 0.25 h / 0 °C 3: 1.) NaHCO3 (aq.), 2.) NaOCH3 / 2.) CH3OH View Scheme |
methyl 2-O-benzoyl-α-D-xylofuranoside
1-O-methyl-D-ribofuranose
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 2.) pyridine 2: 0.8 g / NaN3 / dimethylformamide / 6 h / 90 °C 3: nitrosonium hexafluorophosphate / acetonitrile / 0.25 h / 0 °C 4: 1.) NaHCO3 (aq.), 2.) NaOCH3 / 2.) CH3OH View Scheme |
1-azido-2,3,4-tri-O-acetylribose
1-O-methyl-D-ribofuranose
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 86 percent / methanol, sodium / 12 h / Ambient temperature 2: 89 percent / sodium / 1.) reflux, 3 h, 2.) RT, overnight View Scheme |
1,2,3,5-tetraacetylribose
1-O-methyl-D-ribofuranose
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 98 percent / trimethylsilylazide, stannic chloride / CH2Cl2 / 48 h / Ambient temperature 2: 90 percent / sodium / 12 h / Ambient temperature View Scheme | |
Multi-step reaction with 3 steps 1: 98 percent / trimethylsilylazide, stannic chloride / CH2Cl2 / 48 h / Ambient temperature 2: 86 percent / methanol, sodium / 12 h / Ambient temperature 3: 89 percent / sodium / 1.) reflux, 3 h, 2.) RT, overnight View Scheme |
di-O-benzoyl-1,2-O-(α-methoxybenzylidene)-α-D-ribofuranose
1-O-methyl-D-ribofuranose
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 92 percent / HgBr2, pyridinium toluene-p-sulphonate / CH2Cl2; methanol / Heating 2: 82 percent / KOH / methanol / 0.5 h / Ambient temperature View Scheme |
Conditions | Yield |
---|---|
In methanol |
(6aR,8R,9R,9aS)-2,2,4,4-tetraisopropyl-8-methoxytetrahydro-6H-furo[3,2- f][1,3,5,2,4]trioxadisilocin-9-ol
1-O-methyl-D-ribofuranose
Conditions | Yield |
---|---|
With tetramethylammonium fluoride; acetic acid In N,N-dimethyl-formamide at 20℃; for 2h; |
methanol
1,2,3,5-tetra-O-acetyl-D-ribofuranose
A
1-O-methyl-D-ribofuranose
B
methyl α-D-ribofuranoside
Conditions | Yield |
---|---|
Stage #1: methanol; 1,2,3,5-tetra-O-acetyl-D-ribofuranose With sodium methylate at 20℃; Stage #2: In methanol at 20℃; for 15h; pH=3; optical yield given as %de; |
Conditions | Yield |
---|---|
With Dowex-50W | |
Stage #1: methanol With acetyl chloride at 0 - 5℃; for 0.333333h; Stage #2: β-D-ribofuranose at 20℃; for 24h; Time; | 55 mg |
With sulfuric acid | |
With toluene-4-sulfonic acid at 30 - 50℃; Temperature; Reagent/catalyst; |
D-Ribose
1-O-methyl-D-ribofuranose
Conditions | Yield |
---|---|
Stage #1: D-Ribose With sulfuric acid In methanol for 16h; Cooling with ice; Stage #2: In methanol |
methanol
D-ribose
A
methyl β-D-ribopyranoside
B
methyl α-D-ribopyranoside
C
1-O-methyl-D-ribofuranose
D
methyl α-D-ribofuranoside
Conditions | Yield |
---|---|
With QuadraPure sulfonic acid 450-800 micron beads at 120℃; for 0.0666667h; Flow reactor; | A 56 %Spectr. B 13 %Spectr. C 20 %Spectr. D 11 %Spectr. |
Conditions | Yield |
---|---|
Acidic conditions; |
1-O-methyl-D-ribofuranose
Conditions | Yield |
---|---|
With 5% active carbon-supported ruthenium; hydrogen; water-d2; sodium hydroxide at 80℃; for 24h; | 100% |
1-Methoxy-4-(1-methoxy-vinyl)-benzene
1-O-methyl-D-ribofuranose
methyl 2,3-O-<(methoxyphenyl)ethylidene>-β-D-ribofuranoside
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate In dichloromethane for 0.5h; Ambient temperature; | 97% |
benzoyl chloride
1-O-methyl-D-ribofuranose
methyl 2,3,3'-tri-O-benzoyl-β-D-apiofuranoside
Conditions | Yield |
---|---|
With pyridine 1.) from 0 deg C to 4 deg C, 20 h, 2.) RT, 4 h; | 96.5% |
In pyridine; chloroform at 0℃; for 0.75h; | 95% |
With pyridine Ambient temperature; | |
Stage #1: 1-O-methyl-D-ribofuranose With dmap; triethylamine In 1,2-dichloro-ethane Stage #2: benzoyl chloride In 1,2-dichloro-ethane at 30℃; Solvent; Temperature; |
chlorophosphoric acid diphenyl ester
1-O-methyl-D-ribofuranose
β-methyl-5-(diphenoxyphosphoryl)ribofuranoside
Conditions | Yield |
---|---|
With pyridine; dmap at 20℃; for 3h; | 96% |
Trimethyl orthoacetate
1-O-methyl-D-ribofuranose
methyl 5-O-acetyl-β-D-ribofuranoside
Conditions | Yield |
---|---|
With lanthanum chloride on silica gel In methanol | 94% |
p-Anisaldehyde dimethyl acetal
1-O-methyl-D-ribofuranose
methyl 2,3-O-p-methoxybenzylidene-β-D-ribofuranoside
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In N,N-dimethyl-formamide at 70℃; for 4h; | 93% |
With toluene-4-sulfonic acid In N,N-dimethyl-formamide at 70℃; for 4h; | 93% |
1-O-methyl-D-ribofuranose
methyl β-D-2,3-dideoxyribofuranoside
Conditions | Yield |
---|---|
With hydrogen In 1,4-dioxane at 139.84℃; under 60006 Torr; for 24h; Autoclave; | 93% |
With hydrogen In 1,4-dioxane at 139.84℃; under 57755.8 Torr; for 8h; |
1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane
1-O-methyl-D-ribofuranose
(6aR,8R,9R,9aS)-2,2,4,4-tetraisopropyl-8-methoxytetrahydro-6H-furo[3,2- f][1,3,5,2,4]trioxadisilocin-9-ol
Conditions | Yield |
---|---|
With pyridine for 2h; Ambient temperature; | 90% |
With pyridine at 0 - 20℃; for 24h; | 90% |
With pyridine at 20℃; for 1h; | 83% |
tert-butylchlorodiphenylsilane
1-O-methyl-D-ribofuranose
(2R,3S,4R,5R)-2-(((tert-butyldiphenylsilyl)oxy)methyl)-5-methoxytetrahydrofuran-3,4-diol
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 0 - 20℃; for 24h; | 90% |
With triethylamine In dichloromethane for 18h; Ambient temperature; | 54.8% |
Conditions | Yield |
---|---|
Stage #1: 1-O-methyl-D-ribofuranose With BDMDAP; dimethyltin dichloride In 1-methyl-pyrrolidin-2-one at 80℃; for 12h; Stage #2: triethylamine carbonate In 1-methyl-pyrrolidin-2-one; water regioselective reaction; | 90% |
trityl chloride
1-O-methyl-D-ribofuranose
(-)-Methyl-5-O-trityl-β-D-ribofuranosid
Conditions | Yield |
---|---|
With pyridine at 120℃; for 3h; | 87% |
With pyridine at 120℃; for 3h; tritylation; | 87% |
With pyridine; dmap for 24h; Ambient temperature; | |
With pyridine for 24h; Ambient temperature; | |
With pyridine at 120℃; for 3h; |
2,2-dimethoxy-propane
1-O-methyl-D-ribofuranose
((3aR,4R,6R,6aR)-6-methoxy-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methanol
Conditions | Yield |
---|---|
With camphor-10-sulfonic acid In acetone for 22h; Ambient temperature; | 87% |
With camphor-10-sulfonic acid In acetone at 25℃; for 18h; Inert atmosphere; | 73% |
With toluene-4-sulfonic acid In N,N-dimethyl-formamide for 24h; Etherification; |
4,4'-dimethoxytrityl chloride
1-O-methyl-D-ribofuranose
2-[bis(4-methoxyphenyl)phenylmethoxymethyl]-5-methoxy-tetrahydrofuran-3,4-diol
Conditions | Yield |
---|---|
With pyridine at 120℃; for 3h; | 87% |
triisopropylsilyl chloride
1-O-methyl-D-ribofuranose
(6aR,8R,9R,9aS)-2,2,4,4-tetraisopropyl-8-methoxytetrahydro-6H-furo[3,2- f][1,3,5,2,4]trioxadisilocin-9-ol
Conditions | Yield |
---|---|
In pyridine at 20℃; for 1h; | 83% |
1-O-methyl-D-ribofuranose
methyl 5-deoxy-5-iodo-β-D-ribofuranoside
Conditions | Yield |
---|---|
With 1H-imidazole; iodine; triphenylphosphine In tetrahydrofuran Heating; | 80% |
Conditions | Yield |
---|---|
With pyridine In chloroform at 20℃; for 5h; Tosylation; | 76% |
acetone
1-O-methyl-D-ribofuranose
((3aR,4R,6R,6aR)-6-methoxy-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methanol
Conditions | Yield |
---|---|
zeolite HY at 50℃; for 48h; | 75% |
With hydrogenchloride In methanol; water |
thioacetic acid
1-O-methyl-D-ribofuranose
Methyl 5-S-acetyl-5-thio-β-D-ribofuranoside
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; | 71% |
tert-butyldimethylsilyl chloride
1-O-methyl-D-ribofuranose
methyl 5-O-[(tert-butyl)dimethylsilyl]-β-D-ribofuranoside
Conditions | Yield |
---|---|
With dmap; triethylamine In N,N-dimethyl-formamide at 25℃; for 20h; Inert atmosphere; | 68% |
phenyl isocyanate
1-O-methyl-D-ribofuranose
A
methyl 2-O-(phenylcarbamoyl)-β-D-ribofuranoside
Conditions | Yield |
---|---|
With Zn naphthenate In N,N-dimethyl-formamide at -15℃; Product distribution; | A 9% B 63% |
With Zn naphthenate In N,N-dimethyl-formamide at -15℃; | A 9% B 63% |
Dibenzyl N,N-diisopropylphosphoramidite
1-O-methyl-D-ribofuranose
Conditions | Yield |
---|---|
Stage #1: Dibenzyl N,N-diisopropylphosphoramidite; 1-O-methyl-D-ribofuranose With 4,5-dicyano-1H-imidazole In N,N-dimethyl-formamide at -10℃; for 5h; Inert atmosphere; Stage #2: With 3-chloro-benzenecarboperoxoic acid In N,N-dimethyl-d6-formamide at -10 - 25℃; for 0.5h; Inert atmosphere; | 60% |
1-chloromethyl-3-methyl-benzene
1-O-methyl-D-ribofuranose
methyl 2,3,5-tri-O-(3-methylbenzyl)-β-D-ribofuranoside
Conditions | Yield |
---|---|
With sodium hydride In dimethyl sulfoxide at 25℃; for 2h; | 57% |
tert-butylchlorodiphenylsilane
1-O-methyl-D-ribofuranose
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane | 54.8% |
With dmap; triethylamine In dichloromethane |
m-methoxybenzyl chloride
1-O-methyl-D-ribofuranose
methyl 2,3,5-tri-O-(3-methoxybenzyl)-β-D-ribofuranoside
Conditions | Yield |
---|---|
With sodium hydroxide In dimethyl sulfoxide for 2h; Ambient temperature; | 28.5% |
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