Quick Details Classification: Chemical Auxiliary Agent CAS No.: 7473-98-5 Other Names: UV 1173 MF: C10H12O4
Cas:7473-98-5
Min.Order:500 Kilogram
Negotiable
Type:Other
inquiryKeycure POL-100F is suitable for water based UV curable systems when prediluted in a water compatible solvent ( i.e. isopropanol ). Main suggested applications are in the manufacturing of: - clear lacquers for wood, plastic, paper, metal, opt
We provide tailor-made photoinitiator solutions for different performances by custom synthesisi.blends or other technical supports low-odor uv formulations low odor, low yellowing, through-curing non-yellowing uv formulations ben
Cas:7473-98-5
Min.Order:20 Kilogram
Negotiable
Type:Trading Company
inquiryHRcure-1173 manufacturer CAS 7473-98-5 High efficiency, yellowing resistance UV absorption Peak: 244nm, 330nm Tianjin Huiren chemtech Co. , Ltd. , established in January 2016, is a national high-tech enterprise that integrates R&D,
Cas:7473-98-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquirywe provide tailor-made photoinitiator solutions for different performances by custom synthesisi.blends or other technical supports low-odor UV formulations Non-yellowing UV formulations Benzene-Free UV formulations Polymeric UV formulations
Cas:7473-98-5
Min.Order:100 Metric Ton
Negotiable
Type:Trading Company
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:7473-98-5
Min.Order:1 Metric Ton
Negotiable
Type:Manufacturers
inquiryPhotoinitiators 1173 is a versatile highly efficient Free Radical Type I liquid photoinitiator which is used to initiate the UV polymerization of chemically unsaturated prepolymers (e.g. acrylates) in combination with mono- or multi-f
Cas:7473-98-5
Min.Order:1 Kilogram
Negotiable
Type:Other
inquiryProduct description: Product name 2-Hydroxy-2-methylpropiophenone CAS number 7473-98-5 Assay >99% Appearance Colorless to yellowish transparent liquid Capacity 200mt/year Applicati
Cas:7473-98-5
Min.Order:10 Gram
FOB Price: $12.0
Type:Lab/Research institutions
inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
Cas:7473-98-5
Min.Order:1 Metric Ton
FOB Price: $1.0 / 3.0
Type:Manufacturers
inquiryUnique advantages for 2-Hydroxy-2-methylpropiophenone UV Photoinitiator 1173 Cas 7473-98-5 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White or slight yellow liquid Stora
Cas:7473-98-5
Min.Order:25 Kilogram
Negotiable
Type:Trading Company
inquiry1. Quality Our products meet MSDS safe standard and we have ISO and other certificate so yan can get high quality products from our company. 2. Price We are the company which is the joint of trade and industry so we cao provide the competiti
Cas:7473-98-5
Min.Order:0 Metric Ton
Negotiable
Type:Trading Company
inquiryT he company has advanced technology, as well as a large number of excellent R & D team, to provide customers from the grams to one hundred kilograms and tons of high-quality products, competitive prices and quality service Appearance:yellow li
Cas:7473-98-5
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:7473-98-5
Min.Order:1
Negotiable
Type:Other
inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:7473-98-5
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiry
Cas:7473-98-5
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Manufacturers
inquiryName:2-Hydroxy-2-Methyl-Phenyl-Propane-1-one CAS:7473-98-5 Grade:For chemical industry, scientific research and export Product Quality 12 years of chemical raw materials Mature operation of the industry System stability Data storage Security
Cas:7473-98-5
Min.Order:25 Kilogram
FOB Price: $1.0 / 2.0
Type:Other
inquiryProduct Name: 2-Hydroxy-2-methylpropiophenone Synonyms: 1-Phenyl-2-hydroxy-2-methylpropan-1-one;2-hydroxy-2-methyl-1-phenyl-1-propanon;a-Hyd[cl]roxyMethy1[e]propiophenone;photoinitiator1173;2-HYDROXY-2-METH
Cas:7473-98-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu
Cas:7473-98-5
Min.Order:1 Kilogram
FOB Price: $1.0 / 10.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:7473-98-5
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by email in time prod
Cas:7473-98-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryProduct Name 2-Hydroxy-2-Methyl-Phenyl-Propane-1-one CAS No. 7473-98-5 Molecular Formula C10O2H12
Cas:7473-98-5
Min.Order:5 Metric Ton
FOB Price: $1.0 / 2.0
Type:Other
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:7473-98-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryBeluga chemical professional supply 2-Hydroxy-2-methyl propiophenone CAS 7473-98-5 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and research capabilities. 2. Made in C
Cas:7473-98-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryProduct Detail Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,
Cas:7473-98-5
Min.Order:20 Metric Ton
Negotiable
Type:Trading Company
inquiryWe have overseas warehouses in California, New Laredo Mexico, Vancouver Canada, Amsterdam Netherlands, and Melbourne Australia. Overseas warehouses can provide some of the best-selling products. We look forward to the cooperation of local powerful
Cas:7473-98-5
Min.Order:0 Metric Ton
Negotiable
Type:Trading Company
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:7473-98-5
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryHangzhou Fanda Chemical Co.,Ltd (FandaChem) , a China-based chemical company, specialize in exporting Irgacure 1173( Photoinitiator 1173;Omnirad 1173; IGM 1173;Doublecure 173;UV 1173) CAS: 7473-98-5, Please contact us by email freely. We are
Cas:7473-98-5
Min.Order:0 Metric Ton
Negotiable
Type:Other
inquiryOur advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We have s
Cas:7473-98-5
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:7473-98-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:7473-98-5
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiry2-methyl-1-phenyl-1-trimethylsiloxy-1-propene
2-hydroxy-2-methylpropiophenone
Conditions | Yield |
---|---|
With oxygen; {[Cu(4,4'bipyridine)(BF4)2(H2O)2](4,4'bipyridine)}n/NH2-MNB In ethanol at 20℃; under 760.051 Torr; for 72h; | 99% |
Stage #1: 2-methyl-1-phenyl-1-trimethylsiloxy-1-propene With oxygen; [Cu(bpy)(BF4)2(H2O)2(bpy)]n In ethanol; water at 0℃; under 760 Torr; for 24h; Stage #2: With triethyl phosphite In ethanol; water | 79% |
With tris(dimethylamino)sulfonium trimethylsilyldifluoride; oxygen; triphenylphosphine In tetrahydrofuran at 0 - 5℃; for 2h; | 69% |
With 3-(4-nitrophenyl)-2-(phenylsulfonyl)-1,2-oxaziridine; tetrabutyl ammonium fluoride 1.) CHCl3, 60 deg C, 1 h, 2.) THF; Yield given. Multistep reaction; |
2-Methyl-1-phenyl-2-trimethylsilanyloxy-propan-1-one
2-hydroxy-2-methylpropiophenone
Conditions | Yield |
---|---|
With trifluoroacetic acid In methanol for 2h; | 99% |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate for 72h; Ambient temperature; | 98% |
With sodium hydroxide In water | 94.8% |
With diethyl methylmalonate anion In dimethyl sulfoxide Irradiation; | 62% |
Conditions | Yield |
---|---|
With di-tert-butyl peroxide In dichloromethane at 35℃; Temperature; Sonication; | 92.36% |
With oxygen; sodium hydroxide; sodium sulfite In ethanol at 15℃; for 6h; | 91.13% |
With oxygen; caesium carbonate; triethyl phosphite In dimethyl sulfoxide at 25℃; under 760.051 Torr; for 24h; Reagent/catalyst; Solvent; Schlenk technique; | 90% |
2-methyl-1-phenylpropane-1,2-diol
2-hydroxy-2-methylpropiophenone
Conditions | Yield |
---|---|
With sodium hypochlorite; potassium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical In water; toluene at 0 - 5℃; for 1.16667h; | 87% |
With tert.-butylhydroperoxide; tetrabutylammomium bromide In decane; benzene at 40℃; for 24h; Sealed tube; chemoselective reaction; | 83% |
With bromine In dichloromethane at 20℃; Reagent/catalyst; Large scale; | 1562 g |
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In acetonitrile at 80℃; for 1h; |
Conditions | Yield |
---|---|
With hydrogen bromide; dihydrogen peroxide In 1,2-dichloro-ethane at 60℃; for 12h; Irradiation; | 85% |
Multi-step reaction with 2 steps 1.1: dihydrogen peroxide; hydrogen bromide / 1,2-dichloro-ethane / 8 h / 0 °C / Irradiation 2.1: water / 1 h / 100 °C 2.2: 6 h / Cooling with ice; Irradiation View Scheme |
dimethyl sulfoxide
phenyl isopropyl ketone
2-hydroxy-2-methylpropiophenone
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate; iodine at 120℃; for 8h; | 85% |
With dipotassium peroxodisulfate; iodine at 120℃; for 8h; | 85% |
phenylglyoxylic acid ethyl ester
methylmagnesium bromide
2-hydroxy-2-methylpropiophenone
Conditions | Yield |
---|---|
Stage #1: phenylglyoxylic acid ethyl ester With n-butyllithium; trimethylaluminum; N,O-dimethylhydroxylamine*hydrochloride In tetrahydrofuran; hexane at 0 - 20℃; for 2h; Stage #2: methylmagnesium bromide In tetrahydrofuran; diethyl ether; hexane at 0 - 20℃; for 0.583333h; | 84% |
1-bromo-2-methyl-1-phenylpropan-2-ol
2-hydroxy-2-methylpropiophenone
Conditions | Yield |
---|---|
Stage #1: 1-bromo-2-methyl-1-phenylpropan-2-ol With water at 100℃; for 1h; Stage #2: With dihydrogen peroxide for 6h; Cooling with ice; Irradiation; | 82% |
2-hydroxy-2-methylpropanenitrile
chlorobenzene
2-hydroxy-2-methylpropiophenone
Conditions | Yield |
---|---|
Stage #1: 2-hydroxy-2-methylpropanenitrile With 3,4-dihydro-2H-pyran In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; Stage #2: chlorobenzene With magnesium In tetrahydrofuran; diethyl ether at 20 - 70℃; for 2h; Cooling with ice; | 82% |
Conditions | Yield |
---|---|
With magnesium In N,N-dimethyl-formamide at -20 - -10℃; for 2h; Inert atmosphere; | 82% |
Conditions | Yield |
---|---|
With N-sulfonyloxaziridine (4a) In tetrahydrofuran; methanol for 0.25h; Ambient temperature; | 79% |
A
2-methyl-1-phenylprop-2-en-1-one
B
2-hydroxy-2-methylpropiophenone
C
3-hydroxy-3-phenyl-butan-2-one
D
phenyl isocyanate
Conditions | Yield |
---|---|
In benzene at 450℃; Further byproducts given; | A 12% B 9% C 24% D 76% |
Conditions | Yield |
---|---|
Stage #1: rac-2-methyl-1-phenylpropan-1-ol With iodine; acetone In 1,4-dioxane at 20℃; for 0.0833333h; Stage #2: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In 1,4-dioxane at 80℃; for 24h; | 55% |
4-hydroxy-3,5,5-trimethyl-4-phenyl-oxazolidin-2-one
A
2-methyl-1-phenylprop-2-en-1-one
B
2-hydroxy-2-methylpropiophenone
C
3-hydroxy-3-phenyl-butan-2-one
D
methyl isocyanate
Conditions | Yield |
---|---|
In benzene at 550℃; | A 16% B 5% C 6% D 53% |
bromobenzene
2-hydroxy-2-methylpropanenitrile
2-hydroxy-2-methylpropiophenone
Conditions | Yield |
---|---|
Stage #1: 2-hydroxy-2-methylpropanenitrile With 3,4-dihydro-2H-pyran In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; Stage #2: bromobenzene With magnesium In tetrahydrofuran; diethyl ether at 20 - 70℃; for 2h; Cooling with ice; | 48% |
3-ethyl-4-hydroxy-5,5-dimethyl-4-phenyl-oxazolidin-2-one
A
2-methyl-1-phenylprop-2-en-1-one
B
2-hydroxy-2-methylpropiophenone
C
3-hydroxy-3-phenyl-butan-2-one
D
ethyl isocyanate
Conditions | Yield |
---|---|
In benzene at 550℃; | A 41% B 14% C 45% D 44% |
2-methyl-1-phenyl-1-acetoxy-1-propene
A
2-methyl-1-phenylprop-2-en-1-one
B
2-hydroxy-2-methylpropiophenone
C
2-fluoro-2-methyl-1-phenyl-1-propanone
Conditions | Yield |
---|---|
With triethylamine tris(hydrogen fluoride) In acetonitrile anodic oxidation; | A 8% B 9% C 44% |
4-cyanophenyl methyl ketone
Diethyl methylmalonate
2-hydroxy-2-methylpropiophenone
Conditions | Yield |
---|---|
With potassium tert-butylate In dimethyl sulfoxide Irradiation; RT., 4 h, 50 deg C, 19 h; | 37% |
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran | 35% |
2-methylmalononitrile
α-chloroisobutyrophenone
A
2-hydroxy-2-methylpropiophenone
Conditions | Yield |
---|---|
With potassium tert-butylate In dimethyl sulfoxide for 68h; Ambient temperature; | A 6% B 32% |
acetone
A
2-methyl-1-phenylprop-2-en-1-one
B
2-hydroxy-2-methylpropiophenone
Conditions | Yield |
---|---|
Stage #1: C11H13PolS2 With n-butyllithium In tetrahydrofuran at -35℃; for 2h; solid phase reaction; Stage #2: acetone In tetrahydrofuran; Petroleum ether at -10℃; solid phase reaction; Stage #3: With mercury(II) perchlorate; water; calcium carbonate In tetrahydrofuran | A 24% B 25% |
3-cyclohexyl-4-hydroxy-5,5-dimethyl-4-phenyl-oxazolidin-2-one
A
2-hydroxy-2-methylpropiophenone
B
3-hydroxy-3-phenyl-butan-2-one
C
Cyclohexyl isocyanate
D
1,3-Dicyclohexylurea
Conditions | Yield |
---|---|
In benzene at 550℃; Further byproducts given; | A 6% B 11% C 20% D 20% |
4-hydroxy-3-isopropyl-5,5-dimethyl-4-phenyl-oxazolidin-2-one
A
1,3-diisopropylurea
B
2-hydroxy-2-methylpropiophenone
C
3-hydroxy-3-phenyl-butan-2-one
D
Isopropyl isocyanate
Conditions | Yield |
---|---|
In benzene at 550℃; Further byproducts given; | A 9% B 6% C 17% D 17% |
3-bromo-2-methyl-1-phenylpropan-1-one
2-hydroxy-2-methylpropiophenone
Conditions | Yield |
---|---|
With water; barium carbonate |
2-bromo-2-methyl-1-phenyl-propan-1-one
2-hydroxy-2-methylpropiophenone
Conditions | Yield |
---|---|
With potassium hydroxide; diethyl ether | |
With sodium hydroxide | |
Multi-step reaction with 2 steps 1: 37 percent / diethyl ether; ethanol / 1 h / Ambient temperature 2: TsOH / H2O / Heating View Scheme |
α-chloroisobutyrophenone
A
2-methyl-2-phenylpropionic acid
B
2-hydroxy-2-methylpropiophenone
Conditions | Yield |
---|---|
With 1,4-dioxane; silver-salt | |
With 1,4-dioxane; mercury-salt |
Conditions | Yield |
---|---|
With diethyl ether Behandeln des Reaktionsgemisches mit wss.H2SO4; |
2-methoxy-3,3-dimethyl-2-phenyl-oxirane
2-hydroxy-2-methylpropiophenone
Conditions | Yield |
---|---|
With hydrogenchloride | |
With copper(l) iodide; tert-butyl alcohol In toluene at 130℃; for 16h; Inert atmosphere; | 85 %Spectr. |
Conditions | Yield |
---|---|
With lithium dimethylcuprate |
2-hydroxy-2-methylpropiophenone
(E)-2-hydroxy-2-methyl-1-phenylpropan-1-one oxime
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; sodium acetate In ethanol; water at 20℃; for 12h; | 97% |
Conditions | Yield |
---|---|
With dmap; triethylamine In tetrahydrofuran at 20℃; for 2h; | 95% |
With dmap; triethylamine In tetrahydrofuran at 20℃; for 2h; | 94% |
With triethylamine In dichloromethane at 20℃; for 2h; Inert atmosphere; |
2-hydroxy-2-methylpropiophenone
acetic anhydride
2-methyl-1-oxo-1-phenylpropan-2-yl acetate
Conditions | Yield |
---|---|
With pyridine at 20℃; Inert atmosphere; | 94% |
With 1,1,7,7-tetramethyl-9-azajulolidine; triethylamine In dichloromethane at 20℃; for 0.5h; Reagent/catalyst; Inert atmosphere; | 85 %Spectr. |
1,2-dichlorovinyl phenyl ether
2-hydroxy-2-methylpropiophenone
2-methyl-5-phenoxy-3-phenylpent-4-yne-2,3-diol
Conditions | Yield |
---|---|
Stage #1: 1,2-dichlorovinyl phenyl ether With n-butyllithium In diethyl ether; hexane at -78 - -20℃; for 2h; Stage #2: 2-hydroxy-2-methylpropiophenone In diethyl ether; hexane at -78 - 20℃; | 93% |
Conditions | Yield |
---|---|
With copper(l) iodide; water; sodium hydroxide In methanol at 80℃; for 24h; Schlenk technique; Inert atmosphere; | 93% |
2-hydroxy-2-methylpropiophenone
triphenylbismuth(V) diacetate
2-methyl-2-phenoxy-1-phenyl-propan-1-one
Conditions | Yield |
---|---|
With copper diacetate; dicyclohexylmethylamine In dichloromethane at 20℃; for 3h; | 92% |
2-hydroxy-2-methylpropiophenone
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 0.0833333h; | 90% |
With triethylamine In dichloromethane at 20℃; for 0.0833333h; | 90% |
Conditions | Yield |
---|---|
With copper(l) iodide; water; sodium hydroxide In methanol at 80℃; for 24h; Schlenk technique; Inert atmosphere; | 90% |
2-hydroxy-2-methylpropiophenone
2-fluoro-2-methyl-1-phenyl-1-propanone
Conditions | Yield |
---|---|
With Nonafluorobutanesulfonyl fluoride; triethylamine tris(hydrogen fluoride); triethylamine In acetonitrile at 95℃; for 9h; | 89% |
2-hydroxy-2-methylpropiophenone
phenylacetonitrile
5,5-Dimethyl-3,4-diphenyl-2(5H)-furanone
Conditions | Yield |
---|---|
With copper(l) iodide; water; sodium hydroxide In methanol at 80℃; for 24h; Reagent/catalyst; Schlenk technique; Inert atmosphere; | 88% |
3-methoxyphenylacetonitrile
2-hydroxy-2-methylpropiophenone
3-(3-methoxyphenyl)-5,5-dimethyl-4-phenylfuran-2(5H)-one
Conditions | Yield |
---|---|
With copper(l) iodide; water; sodium hydroxide In methanol at 80℃; for 24h; Schlenk technique; Inert atmosphere; | 88% |
2-hydroxy-2-methylpropiophenone
phenylacetonitrile
B
5,5-Dimethyl-3,4-diphenyl-2(5H)-furanone
Conditions | Yield |
---|---|
With copper(l) iodide; 18O-labeled water; sodium hydroxide In methanol at 80℃; for 24h; Schlenk technique; Inert atmosphere; | A 87% B 13% |
2-cyanomethylthiophene
2-hydroxy-2-methylpropiophenone
5,5-dimethyl-4-phenyl-3-(thiophen-2-yl)furan-2(5H)-one
Conditions | Yield |
---|---|
With copper(l) iodide; water; sodium hydroxide In methanol at 80℃; for 24h; Schlenk technique; Inert atmosphere; | 87% |
Conditions | Yield |
---|---|
With tris(pentafluorophenyl)borate In dichloromethane for 20h; Ambient temperature; | 86% |
With 2,3-Dihydro-1,3-diisopropyl-4,5-dimethylimidazol-2-ylidene In neat (no solvent) at 50℃; for 12h; Glovebox; Inert atmosphere; Schlenk technique; chemoselective reaction; | 42 %Spectr. |
Conditions | Yield |
---|---|
With aluminum (III) chloride In 1,2-dichloro-ethane at 30 - 35℃; Large scale; | 85.6% |
Conditions | Yield |
---|---|
With copper(l) iodide; water; sodium hydroxide In methanol at 80℃; for 24h; Schlenk technique; Inert atmosphere; | 85% |
2-hydroxy-2-methylpropiophenone
(1r,4r)-4-(5-phenyl-1,3,4-oxadiazol-2-yl)cyclohexanamine
2-methyl-1-phenyl-1-(((1r,4r)-4-(5-phenyl-1,3,4-oxadiazol-2-yl)cyclohexyl)amino)propan-2-ol
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride In acetic acid; 1,2-dichloro-ethane at 20℃; | 84% |
2-hydroxy-2-methylpropiophenone
acryloyl chloride
2-methyl-1-oxo-1-phenylpropan-2-yl acrylate
Conditions | Yield |
---|---|
Stage #1: 2-hydroxy-2-methylpropiophenone With triethylamine In dichloromethane for 0.5h; Inert atmosphere; Stage #2: acryloyl chloride In dichloromethane for 19h; Inert atmosphere; | 83% |
With triethylamine In 1,4-dioxane; ice-water | |
With triethylamine In dichloromethane for 12.5h; Inert atmosphere; | |
Stage #1: 2-hydroxy-2-methylpropiophenone With triethylamine In dichloromethane at 20℃; for 0.166667h; Stage #2: acryloyl chloride In dichloromethane at 20℃; for 8h; Cooling with ice; |
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere; | 83% |
2-hydroxy-2-methylpropiophenone
pivaloyl chloride
2-methyl-1-oxo-1-phenylpropan-2-yl pivalate
Conditions | Yield |
---|---|
With pyridine at 25℃; Inert atmosphere; | 82% |
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