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Lonwin Chemical Group Limited

Quick Details Classification: Chemical Auxiliary Agent CAS No.: 7473-98-5 Other Names: UV 1173 MF: C10H12O4

Low price with good quality UV-1173

Cas:7473-98-5

Min.Order:500 Kilogram

Negotiable

Type:Other

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King Brother Chem Co., Ltd

Keycure POL-100F is suitable for water based UV curable systems when prediluted in a water compatible solvent ( i.e. isopropanol ). Main suggested applications are in the manufacturing of: - clear lacquers for wood, plastic, paper, metal, opt

Keycure POL-100F

Cas:7473-98-5

Min.Order:0 Metric Ton

Negotiable

Type:Trading Company

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Guangdong Juda Chemical Industrial Co.,Limited

We provide tailor-made photoinitiator solutions for different performances by custom synthesisi.blends or other technical supports low-odor uv formulations low odor, low yellowing, through-curing non-yellowing uv formulations ben

Photoinitiator 1173 CAS NO.7473-98-5 factory low price high quality

Cas:7473-98-5

Min.Order:20 Kilogram

Negotiable

Type:Trading Company

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Tianjin Huiren Chemtech Co., Ltd

HRcure-1173 manufacturer CAS 7473-98-5 High efficiency, yellowing resistance UV absorption Peak: 244nm, 330nm Tianjin Huiren chemtech Co. , Ltd. , established in January 2016, is a national high-tech enterprise that integrates R&D,

HRcure-1173 manufacturer CAS 7473-98-5

Cas:7473-98-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hunan Russell Chemicals Technology Co.,Ltd

we provide tailor-made photoinitiator solutions for different performances by custom synthesisi.blends or other technical supports low-odor UV formulations Non-yellowing UV formulations Benzene-Free UV formulations Polymeric UV formulations

factory low price high quality Photoinitiator 1173

Cas:7473-98-5

Min.Order:100 Metric Ton

Negotiable

Type:Trading Company

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 2-Hydroxy-2-Methylpropiophenone(1173) supplier in China

Cas:7473-98-5

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Kono Chem Co.,Ltd

Photoinitiators 1173 is a versatile highly efficient Free Radical Type I liquid photoinitiator which is used to initiate the UV polymerization of chemically unsaturated prepolymers (e.g. acrylates) in combination with mono- or multi-f

CAS: 7473-98-5 2-Hydroxy-2-methylpropiophenone

Cas:7473-98-5

Min.Order:1 Kilogram

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Type:Other

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Jinan Finer Chemical Co., Ltd

Product description: Product name 2-Hydroxy-2-methylpropiophenone CAS number 7473-98-5 Assay >99% Appearance Colorless to yellowish transparent liquid Capacity 200mt/year Applicati

2-Hydroxy-2-methylpropiophenone

Cas:7473-98-5

Min.Order:10 Gram

FOB Price: $12.0

Type:Lab/Research institutions

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Hebei yanxi chemical co.,LTD.

hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm

2-hydroxy-2-methylpropiophenone CAS NO.7473-98-5

Cas:7473-98-5

Min.Order:1 Metric Ton

FOB Price: $1.0 / 3.0

Type:Manufacturers

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Wuhan Fortuna Chemical Co.,Ltd

Unique advantages for 2-Hydroxy-2-methylpropiophenone UV Photoinitiator 1173 Cas 7473-98-5 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White or slight yellow liquid Stora

High quality 2-Hydroxy-2-methylpropiophenone UV Photoinitiator 1173 Cas 7473-98-5 with best price

Cas:7473-98-5

Min.Order:25 Kilogram

Negotiable

Type:Trading Company

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Hefei TNJ chemical industry co.,ltd

1. Quality Our products meet MSDS safe standard and we have ISO and other certificate so yan can get high quality products from our company. 2. Price We are the company which is the joint of trade and industry so we cao provide the competiti

2-Hydroxy-2-methylpropiophenone/CAS 7473-98-5

Cas:7473-98-5

Min.Order:0 Metric Ton

Negotiable

Type:Trading Company

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Henan Allgreen Chemical Co.,Ltd

T he company has advanced technology, as well as a large number of excellent R & D team, to provide customers from the grams to one hundred kilograms and tons of high-quality products, competitive prices and quality service Appearance:yellow li

2-Hydroxy-2-methylpropiophenone

Cas:7473-98-5

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 2-hydroxy-2-methylpropiophenone

Cas:7473-98-5

Min.Order:1

Negotiable

Type:Other

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

High Quality Oled CAS 7473-98-5 2-Hydroxy-2-methylpropiophenone

Cas:7473-98-5

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Chemwill Asia Co., Ltd.

CHemwill -- 2-Hydroxy-2-methylpropiophenone

Cas:7473-98-5

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Manufacturers

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Hubei DiBo chemical co., LTD

Name:2-Hydroxy-2-Methyl-Phenyl-Propane-1-one CAS:7473-98-5 Grade:For chemical industry, scientific research and export Product Quality 12 years of chemical raw materials Mature operation of the industry System stability Data storage Security

Photoinitiator 1173 CAS NO.7473-98-5 factory low price high quality

Cas:7473-98-5

Min.Order:25 Kilogram

FOB Price: $1.0 / 2.0

Type:Other

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Henan Tianfu Chemical Co., Ltd.

Product Name: 2-Hydroxy-2-methylpropiophenone Synonyms: 1-Phenyl-2-hydroxy-2-methylpropan-1-one;2-hydroxy-2-methyl-1-phenyl-1-propanon;a-Hyd[cl]roxyMethy1[e]propiophenone;photoinitiator1173;2-HYDROXY-2-METH

TIANFU-CHEM 2-Hydroxy-2-methylpropiophenone _

Cas:7473-98-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu

1173 CAS 7473-98-5 for UV Coatings & Inks 2-Hydroxy-2-Methyl-Phenyl-Propane-1-One

Cas:7473-98-5

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 7473-98-5 with best quality

Cas:7473-98-5

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by email in time prod

2-(2-Chlorophenyl)-2-nitrocyclohexanone.manufacturer

Cas:7473-98-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Sinotech Import&Export Corporation

Product Name 2-Hydroxy-2-Methyl-Phenyl-Propane-1-one CAS No. 7473-98-5 Molecular Formula C10O2H12

2-Hydroxy-2-Methyl-Phenyl-Propane-1-one

Cas:7473-98-5

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

2-Hydroxy-2-methylpropiophenone 7473-98-5

Cas:7473-98-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Qingdao Beluga Import and Export Co., LTD

Beluga chemical professional supply 2-Hydroxy-2-methyl propiophenone CAS 7473-98-5 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and research capabilities. 2. Made in C

2-Hydroxy-2-methyl propiophenone CAS 7473-98-5

Cas:7473-98-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Changchun Artel lmport and Export trade company

Product Detail Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,

Photoinitiator 1173 CAS NO.: 7473-98-5

Cas:7473-98-5

Min.Order:20 Metric Ton

Negotiable

Type:Trading Company

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Shanghai Terui OP New Material Technology Co., Ltd.

We have overseas warehouses in California, New Laredo Mexico, Vancouver Canada, Amsterdam Netherlands, and Melbourne Australia. Overseas warehouses can provide some of the best-selling products. We look forward to the cooperation of local powerful

Safe Delivery Inventory CAS 7473-98-5 2-Hydroxy-2-methylpropiophenone

Cas:7473-98-5

Min.Order:0 Metric Ton

Negotiable

Type:Trading Company

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

2-Hydroxy-2-methylpropiophenone

Cas:7473-98-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hangzhou Fandachem Co.,Ltd

Hangzhou Fanda Chemical Co.,Ltd (FandaChem) , a China-based chemical company, specialize in exporting Irgacure 1173( Photoinitiator 1173;Omnirad 1173; IGM 1173;Doublecure 173;UV 1173) CAS: 7473-98-5, Please contact us by email freely. We are

Wuhan Han Sheng New Material Technology Co.,Ltd

Our advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We have s

2-Hydroxy-2-methyl-1-phenyl-1-propanone

Cas:7473-98-5

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Hubei Jiutian Bio-medical Technology Co., Ltd

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie

CAS7473-98-5 2-Hydroxy-2-methylpropiophenone

Cas:7473-98-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

2-Hydroxy-2-methyl-1-phenyl-1-propanone;YF-PI 1173;Photoinitiator-1173

Cas:7473-98-5

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Synthetic route

2-methyl-1-phenyl-1-trimethylsiloxy-1-propene
39158-85-5

2-methyl-1-phenyl-1-trimethylsiloxy-1-propene

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
With oxygen; {[Cu(4,4'bipyridine)(BF4)2(H2O)2](4,4'bipyridine)}n/NH2-MNB In ethanol at 20℃; under 760.051 Torr; for 72h;99%
Stage #1: 2-methyl-1-phenyl-1-trimethylsiloxy-1-propene With oxygen; [Cu(bpy)(BF4)2(H2O)2(bpy)]n In ethanol; water at 0℃; under 760 Torr; for 24h;
Stage #2: With triethyl phosphite In ethanol; water
79%
With tris(dimethylamino)sulfonium trimethylsilyldifluoride; oxygen; triphenylphosphine In tetrahydrofuran at 0 - 5℃; for 2h;69%
With 3-(4-nitrophenyl)-2-(phenylsulfonyl)-1,2-oxaziridine; tetrabutyl ammonium fluoride 1.) CHCl3, 60 deg C, 1 h, 2.) THF; Yield given. Multistep reaction;
2-Methyl-1-phenyl-2-trimethylsilanyloxy-propan-1-one
55418-35-4

2-Methyl-1-phenyl-2-trimethylsilanyloxy-propan-1-one

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
With trifluoroacetic acid In methanol for 2h;99%
α-chloroisobutyrophenone
7473-99-6

α-chloroisobutyrophenone

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
With sodium hydrogencarbonate for 72h; Ambient temperature;98%
With sodium hydroxide In water94.8%
With diethyl methylmalonate anion In dimethyl sulfoxide Irradiation;62%
phenyl isopropyl ketone
611-70-1

phenyl isopropyl ketone

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
With di-tert-butyl peroxide In dichloromethane at 35℃; Temperature; Sonication;92.36%
With oxygen; sodium hydroxide; sodium sulfite In ethanol at 15℃; for 6h;91.13%
With oxygen; caesium carbonate; triethyl phosphite In dimethyl sulfoxide at 25℃; under 760.051 Torr; for 24h; Reagent/catalyst; Solvent; Schlenk technique;90%
2-methyl-1-phenylpropane-1,2-diol
20907-13-5

2-methyl-1-phenylpropane-1,2-diol

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
With sodium hypochlorite; potassium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical In water; toluene at 0 - 5℃; for 1.16667h;87%
With tert.-butylhydroperoxide; tetrabutylammomium bromide In decane; benzene at 40℃; for 24h; Sealed tube; chemoselective reaction;83%
With bromine In dichloromethane at 20℃; Reagent/catalyst; Large scale;1562 g
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In acetonitrile at 80℃; for 1h;
2-Methyl-1-phenyl-2-propanol
100-86-7

2-Methyl-1-phenyl-2-propanol

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
With hydrogen bromide; dihydrogen peroxide In 1,2-dichloro-ethane at 60℃; for 12h; Irradiation;85%
Multi-step reaction with 2 steps
1.1: dihydrogen peroxide; hydrogen bromide / 1,2-dichloro-ethane / 8 h / 0 °C / Irradiation
2.1: water / 1 h / 100 °C
2.2: 6 h / Cooling with ice; Irradiation
View Scheme
dimethyl sulfoxide
67-68-5

dimethyl sulfoxide

phenyl isopropyl ketone
611-70-1

phenyl isopropyl ketone

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
With dipotassium peroxodisulfate; iodine at 120℃; for 8h;85%
With dipotassium peroxodisulfate; iodine at 120℃; for 8h;85%
phenylglyoxylic acid ethyl ester
1603-79-8

phenylglyoxylic acid ethyl ester

methylmagnesium bromide
75-16-1

methylmagnesium bromide

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
Stage #1: phenylglyoxylic acid ethyl ester With n-butyllithium; trimethylaluminum; N,O-dimethylhydroxylamine*hydrochloride In tetrahydrofuran; hexane at 0 - 20℃; for 2h;
Stage #2: methylmagnesium bromide In tetrahydrofuran; diethyl ether; hexane at 0 - 20℃; for 0.583333h;
84%
1-bromo-2-methyl-1-phenylpropan-2-ol
21020-19-9, 70412-41-8

1-bromo-2-methyl-1-phenylpropan-2-ol

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
Stage #1: 1-bromo-2-methyl-1-phenylpropan-2-ol With water at 100℃; for 1h;
Stage #2: With dihydrogen peroxide for 6h; Cooling with ice; Irradiation;
82%
2-hydroxy-2-methylpropanenitrile
75-86-5

2-hydroxy-2-methylpropanenitrile

chlorobenzene
108-90-7

chlorobenzene

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
Stage #1: 2-hydroxy-2-methylpropanenitrile With 3,4-dihydro-2H-pyran In tetrahydrofuran at 20℃; for 1h; Inert atmosphere;
Stage #2: chlorobenzene With magnesium In tetrahydrofuran; diethyl ether at 20 - 70℃; for 2h; Cooling with ice;
82%
Benzotrichlorid
98-07-7

Benzotrichlorid

acetone
67-64-1

acetone

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
With magnesium In N,N-dimethyl-formamide at -20 - -10℃; for 2h; Inert atmosphere;82%
α-Pyrrolidino-β,β-dimethyl styrene
7721-20-2

α-Pyrrolidino-β,β-dimethyl styrene

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
With N-sulfonyloxaziridine (4a) In tetrahydrofuran; methanol for 0.25h; Ambient temperature;79%
4-Hydroxy-5,5-dimethyl-3,4-diphenyl-oxazolidin-2-one

4-Hydroxy-5,5-dimethyl-3,4-diphenyl-oxazolidin-2-one

A

2-methyl-1-phenylprop-2-en-1-one
769-60-8

2-methyl-1-phenylprop-2-en-1-one

B

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

C

3-hydroxy-3-phenyl-butan-2-one
3155-01-9

3-hydroxy-3-phenyl-butan-2-one

D

phenyl isocyanate
103-71-9

phenyl isocyanate

Conditions
ConditionsYield
In benzene at 450℃; Further byproducts given;A 12%
B 9%
C 24%
D 76%
rac-2-methyl-1-phenylpropan-1-ol
611-69-8

rac-2-methyl-1-phenylpropan-1-ol

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
Stage #1: rac-2-methyl-1-phenylpropan-1-ol With iodine; acetone In 1,4-dioxane at 20℃; for 0.0833333h;
Stage #2: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In 1,4-dioxane at 80℃; for 24h;
55%
4-hydroxy-3,5,5-trimethyl-4-phenyl-oxazolidin-2-one
61031-52-5

4-hydroxy-3,5,5-trimethyl-4-phenyl-oxazolidin-2-one

A

2-methyl-1-phenylprop-2-en-1-one
769-60-8

2-methyl-1-phenylprop-2-en-1-one

B

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

C

3-hydroxy-3-phenyl-butan-2-one
3155-01-9

3-hydroxy-3-phenyl-butan-2-one

D

methyl isocyanate
624-83-9

methyl isocyanate

Conditions
ConditionsYield
In benzene at 550℃;A 16%
B 5%
C 6%
D 53%
bromobenzene
108-86-1

bromobenzene

2-hydroxy-2-methylpropanenitrile
75-86-5

2-hydroxy-2-methylpropanenitrile

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
Stage #1: 2-hydroxy-2-methylpropanenitrile With 3,4-dihydro-2H-pyran In tetrahydrofuran at 20℃; for 1h; Inert atmosphere;
Stage #2: bromobenzene With magnesium In tetrahydrofuran; diethyl ether at 20 - 70℃; for 2h; Cooling with ice;
48%
3-ethyl-4-hydroxy-5,5-dimethyl-4-phenyl-oxazolidin-2-one
61031-53-6

3-ethyl-4-hydroxy-5,5-dimethyl-4-phenyl-oxazolidin-2-one

A

2-methyl-1-phenylprop-2-en-1-one
769-60-8

2-methyl-1-phenylprop-2-en-1-one

B

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

C

3-hydroxy-3-phenyl-butan-2-one
3155-01-9

3-hydroxy-3-phenyl-butan-2-one

D

ethyl isocyanate
109-90-0

ethyl isocyanate

Conditions
ConditionsYield
In benzene at 550℃;A 41%
B 14%
C 45%
D 44%
2-methyl-1-phenyl-1-acetoxy-1-propene
5170-76-3

2-methyl-1-phenyl-1-acetoxy-1-propene

A

2-methyl-1-phenylprop-2-en-1-one
769-60-8

2-methyl-1-phenylprop-2-en-1-one

B

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

C

2-fluoro-2-methyl-1-phenyl-1-propanone
71057-10-8

2-fluoro-2-methyl-1-phenyl-1-propanone

Conditions
ConditionsYield
With triethylamine tris(hydrogen fluoride) In acetonitrile anodic oxidation;A 8%
B 9%
C 44%
4-cyanophenyl methyl ketone
1443-80-7

4-cyanophenyl methyl ketone

Diethyl methylmalonate
609-08-5

Diethyl methylmalonate

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
With potassium tert-butylate In dimethyl sulfoxide Irradiation; RT., 4 h, 50 deg C, 19 h;37%
benzoyltrimethylsilane
5908-41-8

benzoyltrimethylsilane

acetone
67-64-1

acetone

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
With tetrabutyl ammonium fluoride In tetrahydrofuran35%
2-methylmalononitrile
3696-36-4

2-methylmalononitrile

α-chloroisobutyrophenone
7473-99-6

α-chloroisobutyrophenone

A

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

B

(β-Benzoylisopropyl)(methyl)malononitrile

(β-Benzoylisopropyl)(methyl)malononitrile

Conditions
ConditionsYield
With potassium tert-butylate In dimethyl sulfoxide for 68h; Ambient temperature;A 6%
B 32%
C11H13PolS2

C11H13PolS2

acetone
67-64-1

acetone

A

2-methyl-1-phenylprop-2-en-1-one
769-60-8

2-methyl-1-phenylprop-2-en-1-one

B

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
Stage #1: C11H13PolS2 With n-butyllithium In tetrahydrofuran at -35℃; for 2h; solid phase reaction;
Stage #2: acetone In tetrahydrofuran; Petroleum ether at -10℃; solid phase reaction;
Stage #3: With mercury(II) perchlorate; water; calcium carbonate In tetrahydrofuran
A 24%
B 25%
3-cyclohexyl-4-hydroxy-5,5-dimethyl-4-phenyl-oxazolidin-2-one
61031-55-8

3-cyclohexyl-4-hydroxy-5,5-dimethyl-4-phenyl-oxazolidin-2-one

A

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

B

3-hydroxy-3-phenyl-butan-2-one
3155-01-9

3-hydroxy-3-phenyl-butan-2-one

C

Cyclohexyl isocyanate
3173-53-3

Cyclohexyl isocyanate

D

1,3-Dicyclohexylurea
2387-23-7

1,3-Dicyclohexylurea

Conditions
ConditionsYield
In benzene at 550℃; Further byproducts given;A 6%
B 11%
C 20%
D 20%
4-hydroxy-3-isopropyl-5,5-dimethyl-4-phenyl-oxazolidin-2-one
61031-49-0

4-hydroxy-3-isopropyl-5,5-dimethyl-4-phenyl-oxazolidin-2-one

A

1,3-diisopropylurea
4128-37-4

1,3-diisopropylurea

B

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

C

3-hydroxy-3-phenyl-butan-2-one
3155-01-9

3-hydroxy-3-phenyl-butan-2-one

D

Isopropyl isocyanate
1795-48-8

Isopropyl isocyanate

Conditions
ConditionsYield
In benzene at 550℃; Further byproducts given;A 9%
B 6%
C 17%
D 17%
3-bromo-2-methyl-1-phenylpropan-1-one
56011-31-5

3-bromo-2-methyl-1-phenylpropan-1-one

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
With water; barium carbonate
2-bromo-2-methyl-1-phenyl-propan-1-one
10409-54-8

2-bromo-2-methyl-1-phenyl-propan-1-one

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
With potassium hydroxide; diethyl ether
With sodium hydroxide
Multi-step reaction with 2 steps
1: 37 percent / diethyl ether; ethanol / 1 h / Ambient temperature
2: TsOH / H2O / Heating
View Scheme
α-chloroisobutyrophenone
7473-99-6

α-chloroisobutyrophenone

A

2-methyl-2-phenylpropionic acid
826-55-1

2-methyl-2-phenylpropionic acid

B

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
With 1,4-dioxane; silver-salt
With 1,4-dioxane; mercury-salt
phenylmagnesium bromide

phenylmagnesium bromide

2-hydroxy-2-methylpropanenitrile
75-86-5

2-hydroxy-2-methylpropanenitrile

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
With diethyl ether Behandeln des Reaktionsgemisches mit wss.H2SO4;
2-methoxy-3,3-dimethyl-2-phenyl-oxirane
13694-96-7

2-methoxy-3,3-dimethyl-2-phenyl-oxirane

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
With hydrogenchloride
With copper(l) iodide; tert-butyl alcohol In toluene at 130℃; for 16h; Inert atmosphere;85 %Spectr.
2-methyl-1-oxo-1-phenylpropan-2-yl acetate
7476-41-7

2-methyl-1-oxo-1-phenylpropan-2-yl acetate

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

Conditions
ConditionsYield
With lithium dimethylcuprate
2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

(E)-2-hydroxy-2-methyl-1-phenylpropan-1-one oxime
829-08-3

(E)-2-hydroxy-2-methyl-1-phenylpropan-1-one oxime

Conditions
ConditionsYield
With hydroxylamine hydrochloride; sodium acetate In ethanol; water at 20℃; for 12h;97%
2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

chloro-diphenylphosphine
1079-66-9

chloro-diphenylphosphine

2-[(diphenylphosphino)oxy]-2-methylpropiophenone

2-[(diphenylphosphino)oxy]-2-methylpropiophenone

Conditions
ConditionsYield
With dmap; triethylamine In tetrahydrofuran at 20℃; for 2h;95%
With dmap; triethylamine In tetrahydrofuran at 20℃; for 2h;94%
With triethylamine In dichloromethane at 20℃; for 2h; Inert atmosphere;
2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

acetic anhydride
108-24-7

acetic anhydride

2-methyl-1-oxo-1-phenylpropan-2-yl acetate
7476-41-7

2-methyl-1-oxo-1-phenylpropan-2-yl acetate

Conditions
ConditionsYield
With pyridine at 20℃; Inert atmosphere;94%
With 1,1,7,7-tetramethyl-9-azajulolidine; triethylamine In dichloromethane at 20℃; for 0.5h; Reagent/catalyst; Inert atmosphere;85 %Spectr.
1,2-dichlorovinyl phenyl ether
89894-42-8

1,2-dichlorovinyl phenyl ether

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

2-methyl-5-phenoxy-3-phenylpent-4-yne-2,3-diol
1448620-95-8

2-methyl-5-phenoxy-3-phenylpent-4-yne-2,3-diol

Conditions
ConditionsYield
Stage #1: 1,2-dichlorovinyl phenyl ether With n-butyllithium In diethyl ether; hexane at -78 - -20℃; for 2h;
Stage #2: 2-hydroxy-2-methylpropiophenone In diethyl ether; hexane at -78 - 20℃;
93%
pyridine-2-acetonitrile
2739-97-1

pyridine-2-acetonitrile

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

5,5-dimethyl-4-phenyl-3-(pyridin-2-yl)furan-2(5H)-one

5,5-dimethyl-4-phenyl-3-(pyridin-2-yl)furan-2(5H)-one

Conditions
ConditionsYield
With copper(l) iodide; water; sodium hydroxide In methanol at 80℃; for 24h; Schlenk technique; Inert atmosphere;93%
2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

triphenylbismuth(V) diacetate
28899-97-0

triphenylbismuth(V) diacetate

2-methyl-2-phenoxy-1-phenyl-propan-1-one
7476-46-2

2-methyl-2-phenoxy-1-phenyl-propan-1-one

Conditions
ConditionsYield
With copper diacetate; dicyclohexylmethylamine In dichloromethane at 20℃; for 3h;92%
2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

2-((trifluoromethyl)thio)benzo[d]isothiazol-3(2H)-one 1,1-dioxide

2-((trifluoromethyl)thio)benzo[d]isothiazol-3(2H)-one 1,1-dioxide

(2-methyl-1-phenyl-2-(((trifluoromethyl)Thio)oxy)propan-1-one)

(2-methyl-1-phenyl-2-(((trifluoromethyl)Thio)oxy)propan-1-one)

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 0.0833333h;90%
With triethylamine In dichloromethane at 20℃; for 0.0833333h;90%
(4-methylphenyl)acetonitrile
2947-61-7

(4-methylphenyl)acetonitrile

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

5,5-dimethyl-4-phenyl-3-(p-tolyl)furan-2(5H)-one

5,5-dimethyl-4-phenyl-3-(p-tolyl)furan-2(5H)-one

Conditions
ConditionsYield
With copper(l) iodide; water; sodium hydroxide In methanol at 80℃; for 24h; Schlenk technique; Inert atmosphere;90%
2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

2-fluoro-2-methyl-1-phenyl-1-propanone
71057-10-8

2-fluoro-2-methyl-1-phenyl-1-propanone

Conditions
ConditionsYield
With Nonafluorobutanesulfonyl fluoride; triethylamine tris(hydrogen fluoride); triethylamine In acetonitrile at 95℃; for 9h;89%
2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

phenylacetonitrile
140-29-4

phenylacetonitrile

5,5-Dimethyl-3,4-diphenyl-2(5H)-furanone
21994-87-6

5,5-Dimethyl-3,4-diphenyl-2(5H)-furanone

Conditions
ConditionsYield
With copper(l) iodide; water; sodium hydroxide In methanol at 80℃; for 24h; Reagent/catalyst; Schlenk technique; Inert atmosphere;88%
3-methoxyphenylacetonitrile
19924-43-7

3-methoxyphenylacetonitrile

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

3-(3-methoxyphenyl)-5,5-dimethyl-4-phenylfuran-2(5H)-one
83253-77-4

3-(3-methoxyphenyl)-5,5-dimethyl-4-phenylfuran-2(5H)-one

Conditions
ConditionsYield
With copper(l) iodide; water; sodium hydroxide In methanol at 80℃; for 24h; Schlenk technique; Inert atmosphere;88%
2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

phenylacetonitrile
140-29-4

phenylacetonitrile

A

C18H16O(18)O

C18H16O(18)O

B

5,5-Dimethyl-3,4-diphenyl-2(5H)-furanone
21994-87-6

5,5-Dimethyl-3,4-diphenyl-2(5H)-furanone

Conditions
ConditionsYield
With copper(l) iodide; 18O-labeled water; sodium hydroxide In methanol at 80℃; for 24h; Schlenk technique; Inert atmosphere;A 87%
B 13%
2-cyanomethylthiophene
20893-30-5

2-cyanomethylthiophene

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

5,5-dimethyl-4-phenyl-3-(thiophen-2-yl)furan-2(5H)-one
83253-79-6

5,5-dimethyl-4-phenyl-3-(thiophen-2-yl)furan-2(5H)-one

Conditions
ConditionsYield
With copper(l) iodide; water; sodium hydroxide In methanol at 80℃; for 24h; Schlenk technique; Inert atmosphere;87%
triethylsilane
617-86-7

triethylsilane

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

2-methyl-2-triethylsiloxypropiophenone

2-methyl-2-triethylsiloxypropiophenone

Conditions
ConditionsYield
With tris(pentafluorophenyl)borate In dichloromethane for 20h; Ambient temperature;86%
With 2,3-Dihydro-1,3-diisopropyl-4,5-dimethylimidazol-2-ylidene In neat (no solvent) at 50℃; for 12h; Glovebox; Inert atmosphere; Schlenk technique; chemoselective reaction;42 %Spectr.
formaldehyd
50-00-0

formaldehyd

2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

4'-chloromethyl-2-hydroxy-2-methyl-1-phenyl-1-propan-1-one

4'-chloromethyl-2-hydroxy-2-methyl-1-phenyl-1-propan-1-one

Conditions
ConditionsYield
With aluminum (III) chloride In 1,2-dichloro-ethane at 30 - 35℃; Large scale;85.6%
2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

2-methoxy-benzeneacetonitrile
7035-03-2

2-methoxy-benzeneacetonitrile

3-(2-methoxyphenyl)-5,5-dimethyl-4-phenylfuran-2(5H)-one

3-(2-methoxyphenyl)-5,5-dimethyl-4-phenylfuran-2(5H)-one

Conditions
ConditionsYield
With copper(l) iodide; water; sodium hydroxide In methanol at 80℃; for 24h; Schlenk technique; Inert atmosphere;85%
2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

(1r,4r)-4-(5-phenyl-1,3,4-oxadiazol-2-yl)cyclohexanamine
1456507-49-5

(1r,4r)-4-(5-phenyl-1,3,4-oxadiazol-2-yl)cyclohexanamine

2-methyl-1-phenyl-1-(((1r,4r)-4-(5-phenyl-1,3,4-oxadiazol-2-yl)cyclohexyl)amino)propan-2-ol
1456507-51-9

2-methyl-1-phenyl-1-(((1r,4r)-4-(5-phenyl-1,3,4-oxadiazol-2-yl)cyclohexyl)amino)propan-2-ol

Conditions
ConditionsYield
With sodium tris(acetoxy)borohydride In acetic acid; 1,2-dichloro-ethane at 20℃;84%
2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

acryloyl chloride
814-68-6

acryloyl chloride

2-methyl-1-oxo-1-phenylpropan-2-yl acrylate
103658-85-1

2-methyl-1-oxo-1-phenylpropan-2-yl acrylate

Conditions
ConditionsYield
Stage #1: 2-hydroxy-2-methylpropiophenone With triethylamine In dichloromethane for 0.5h; Inert atmosphere;
Stage #2: acryloyl chloride In dichloromethane for 19h; Inert atmosphere;
83%
With triethylamine In 1,4-dioxane; ice-water
With triethylamine In dichloromethane for 12.5h; Inert atmosphere;
Stage #1: 2-hydroxy-2-methylpropiophenone With triethylamine In dichloromethane at 20℃; for 0.166667h;
Stage #2: acryloyl chloride In dichloromethane at 20℃; for 8h; Cooling with ice;
2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

pyruvoyl chloride
5704-66-5

pyruvoyl chloride

methyl (2-methyl-1-oxo-1-phenylpropan-2-yl) oxalate

methyl (2-methyl-1-oxo-1-phenylpropan-2-yl) oxalate

Conditions
ConditionsYield
With dmap; triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere;83%
2-hydroxy-2-methylpropiophenone
7473-98-5

2-hydroxy-2-methylpropiophenone

pivaloyl chloride
3282-30-2

pivaloyl chloride

2-methyl-1-oxo-1-phenylpropan-2-yl pivalate
1196070-16-2

2-methyl-1-oxo-1-phenylpropan-2-yl pivalate

Conditions
ConditionsYield
With pyridine at 25℃; Inert atmosphere;82%
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