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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

2-Methylthiophenothiazine Manufacturer/High quality/Best price/In stock

Cas:7643-08-5

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 2-Methylthio Phenothiazine supplier in China

Cas:7643-08-5

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 2-(methylthio)-10H-phenothiazine

Cas:7643-08-5

Min.Order:1

Negotiable

Type:Other

inquiry

Henan Tianfu Chemical Co., Ltd.

cas 7643-08-5 2-Methylthiophenothiazine 1.Large qty in stock 2.High quality 3.Lowest price 4.Best service Our Advantage 1. Risk-free guarantee,15days refund 2. Most of the products in stock,can ship within 7days after the order

cas 7643-08-5 2-Methylthiophenothiazine

Cas:7643-08-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

2-Methylthiophenothiazine

Cas:7643-08-5

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 7643-08-5 with best quality

Cas:7643-08-5

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

10H-Phenothiazine,2-(methylthio)- 7643-08-5

Cas:7643-08-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

2-Methylthiophenothiazine CAS:7643-08-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic

2-Methylthiophenothiazine CAS:7643-08-5

Cas:7643-08-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

10H-Phenothiazine,2-(methylthio)-

Cas:7643-08-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

10H-Phenothiazine,2-(methylthio)-

Cas:7643-08-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

2-Methylthio Phenothiazine

Cas:7643-08-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Triumph International Development Limilted

Appearance:white or light yellow cryastalline pow... Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:C

2-methylthiophenothiazine

Cas:7643-08-5

Min.Order:100 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

2-METHYLTHIOPHENOTHIAZINE

Cas:7643-08-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

2-Methylthiophenothiazine

Cas:7643-08-5

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

10H-Phenothiazine,2-(methylthio)-

Cas:7643-08-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 2-Methylthio Phenothiazine

Cas:7643-08-5

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Siwei Development Group Ltd.

Product name: 2-Methylmercapto Phenothiazine CAS No.:7643-08-5 Molecule Formula:C13H11NS2 Molecule Weight:245.36 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard T

High Quality 2-Methylmercapto Phenothiazine

Cas:7643-08-5

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

2-Methylthiophenothiazine

Cas:7643-08-5

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

Shanghai Minstar Chemical Co., Ltd

2-Methylthiophenothiazine Basic information Product Name: 2-Methylthiophenothiazine Synonyms: 2-methylthieno[2,3-e]thiazine;2-(methylthio)-10h-phenothiazin;2-METHYLMERCAPTO PHENOTHIAZINE;2-METHYLSULFANYL-10H-PHENOTHIAZINE;2-METHYLTHIOPHENOTHIA

2-Methylthiophenothiazine

Cas:7643-08-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

2-Methylthiophenothiazine

Cas:7643-08-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier

2-Methylmercaptophenothiazine

Cas:7643-08-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

2-Methylthiophenothiazine

Cas:7643-08-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

2-Methylthio Phenothiazine

Cas:7643-08-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hubei Taiho Chemical Co.,LTD

TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp

2-methylthiophenothiazine

Cas:7643-08-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

2-Methylthiophenothiazine

Cas:7643-08-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

10H-Phenothiazine,2-(methylthio)-

Cas:7643-08-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen AmoyChem Co.,Ltd

Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi

2-(Methylthio)phenothiazine

Cas:7643-08-5

Min.Order:0

Negotiable

Type:Other

inquiry

HANGZHOU TIANYE CHEMICALS CO., LTD.

We product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Application:Chemical intermediate

2-Methylthiophenothiazine

Cas:7643-08-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

DB BIOTECH CO., LTD

best seller Application:API

2-Methylthiophenothiazine

Cas:7643-08-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Fandachem Co.,Ltd

2-Methylthiophenothiazine cas 7643-08-5Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

2-Methylthiophenothiazine cas 7643-08-5

Cas:7643-08-5

Min.Order:0

Negotiable

Type:Other

inquiry

Synthetic route

N-(3-methylthiophenyl)phenylamine
13313-45-6

N-(3-methylthiophenyl)phenylamine

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
With iodine In acetone for 0.0133333h; Irradiation;82%
With iodine; sulfur at 135℃; for 1h;
2-(2-fluorophenylthio)-5-(methylthio)aniline
129846-83-9

2-(2-fluorophenylthio)-5-(methylthio)aniline

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
With sodium hydride In xylene for 10h; Heating;65%
Multi-step reaction with 2 steps
1: 89 percent / 4 h / Heating
2: 1.) K2CO3, 2.) 20percent ethanolic KOH / 1.) DMF, reflux, 15 h, 2.) ethanol, reflux, 6 h
View Scheme
2-(2-bromophenylthio)-5-(methylthio)aniline
7623-78-1

2-(2-bromophenylthio)-5-(methylthio)aniline

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
With copper; potassium carbonate In N,N-dimethyl-formamide for 15h; Heating;55%
10H-phenothiazine-10-carbaldehyde
38076-67-4

10H-phenothiazine-10-carbaldehyde

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
In AlCl351%
In AlCl351%
In 1,1,2,2-tetrachloroethane40%
In 1,1,2,2-tetrachloroethane40%
N-(3-methylthiophenyl)phenylamine
13313-45-6

N-(3-methylthiophenyl)phenylamine

A

4-methylsulfanyl-phenothiazine
20349-56-8

4-methylsulfanyl-phenothiazine

B

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
With iodine; sulfur at 160℃;
10H-phenothiazine-2-thiol
99970-41-9

10H-phenothiazine-2-thiol

dimethyl sulfate
77-78-1

dimethyl sulfate

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
With sodium hydroxide
2-methylsulfanyl-phenothiazine-10-carboxylic acid hydrazide
16868-91-0

2-methylsulfanyl-phenothiazine-10-carboxylic acid hydrazide

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
With butanone In ethanol Product distribution; Heating; other ketones : diethyl ketone, acetophenone;
3-Acetamino-1-methylmercapto-4-<2-brom-phenylmercapto>-benzol
5166-81-4

3-Acetamino-1-methylmercapto-4-<2-brom-phenylmercapto>-benzol

A

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

B

2-(methylyhio)-7-(2-(methylthio)phenothiazine-10-yl)-phenothiazine
129847-12-7

2-(methylyhio)-7-(2-(methylthio)phenothiazine-10-yl)-phenothiazine

Conditions
ConditionsYield
With potassium hydroxide; copper; potassium carbonate 1.) DMF, reflux, 15 h, 2.) ethanol, reflux, 5 h; Yield given. Multistep reaction. Yields of byproduct given;
2-(2-fluorophenylthio)-5-(methylthio)acetanilide
129846-84-0

2-(2-fluorophenylthio)-5-(methylthio)acetanilide

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
With potassium hydroxide; potassium carbonate 1.) DMF, reflux, 15 h, 2.) ethanol, reflux, 6 h; Yield given. Multistep reaction;
1-chloro-4-(methylthio)-2-nitrobenzene
1199-36-6

1-chloro-4-(methylthio)-2-nitrobenzene

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 79 percent / NaOH / ethanol / 6 h / Heating
2: 1.) FeCl3*6H2O, active carbon, 2.) 80percent N2H4*H2O / 1.) ethanol, RT, 2.) RT, 10 h
3: 55 percent / K2CO3, Cu / dimethylformamide / 15 h / Heating
View Scheme
Multi-step reaction with 4 steps
1: 89 percent / K2CO3 / dimethylformamide / 3.5 h / 60 °C
2: 99 percent / active carbon, N2H4, FeCl3*6H2O / ethanol / 10 h / Heating
3: 89 percent / 4 h / Heating
4: 1.) K2CO3, 2.) 20percent ethanolic KOH / 1.) DMF, reflux, 15 h, 2.) ethanol, reflux, 6 h
View Scheme
Multi-step reaction with 3 steps
1: 89 percent / K2CO3 / dimethylformamide / 3.5 h / 60 °C
2: 99 percent / active carbon, N2H4, FeCl3*6H2O / ethanol / 10 h / Heating
3: 65 percent / 80percent NaH / xylene / 10 h / Heating
View Scheme
2-(2-bromophenolthio)-5-(methylthio)nitrobenzene
7623-76-9

2-(2-bromophenolthio)-5-(methylthio)nitrobenzene

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1.) FeCl3*6H2O, active carbon, 2.) 80percent N2H4*H2O / 1.) ethanol, RT, 2.) RT, 10 h
2: 55 percent / K2CO3, Cu / dimethylformamide / 15 h / Heating
View Scheme
2-fluorothiophenol
2557-78-0

2-fluorothiophenol

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 89 percent / K2CO3 / dimethylformamide / 3.5 h / 60 °C
2: 99 percent / active carbon, N2H4, FeCl3*6H2O / ethanol / 10 h / Heating
3: 89 percent / 4 h / Heating
4: 1.) K2CO3, 2.) 20percent ethanolic KOH / 1.) DMF, reflux, 15 h, 2.) ethanol, reflux, 6 h
View Scheme
Multi-step reaction with 3 steps
1: 89 percent / K2CO3 / dimethylformamide / 3.5 h / 60 °C
2: 99 percent / active carbon, N2H4, FeCl3*6H2O / ethanol / 10 h / Heating
3: 65 percent / 80percent NaH / xylene / 10 h / Heating
View Scheme
2-bromothiophenol
6320-02-1

2-bromothiophenol

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 79 percent / NaOH / ethanol / 6 h / Heating
2: 1.) FeCl3*6H2O, active carbon, 2.) 80percent N2H4*H2O / 1.) ethanol, RT, 2.) RT, 10 h
3: 55 percent / K2CO3, Cu / dimethylformamide / 15 h / Heating
View Scheme
2-(2-fluorophenylthio)-5-(methylthio)nitrobenzene
129846-82-8

2-(2-fluorophenylthio)-5-(methylthio)nitrobenzene

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 99 percent / active carbon, N2H4, FeCl3*6H2O / ethanol / 10 h / Heating
2: 89 percent / 4 h / Heating
3: 1.) K2CO3, 2.) 20percent ethanolic KOH / 1.) DMF, reflux, 15 h, 2.) ethanol, reflux, 6 h
View Scheme
Multi-step reaction with 2 steps
1: 99 percent / active carbon, N2H4, FeCl3*6H2O / ethanol / 10 h / Heating
2: 65 percent / 80percent NaH / xylene / 10 h / Heating
View Scheme
3-methylmercaptoaniline
1783-81-9

3-methylmercaptoaniline

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: copper-powder
3: iodine; sulfur / 160 °C
View Scheme
2-benzylsulfanyl-10H-phenothiazine
101895-74-3

2-benzylsulfanyl-10H-phenothiazine

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium; butan-1-ol
2: aqueous NaOH
View Scheme
N-(3'-methylthiophenyl)anthranylic acid
18902-93-7

N-(3'-methylthiophenyl)anthranylic acid

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
2: iodine; sulfur / 160 °C
View Scheme
potassium 2-chlorobenzoate
16463-38-0

potassium 2-chlorobenzoate

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: copper-powder
3: iodine; sulfur / 160 °C
View Scheme
3-Bromothiophenol
6320-01-0

3-Bromothiophenol

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: aq. NaOH
2: Cu, K2CO3 / 220 - 230 °C
3: sulfur, I2 / 1 h / 135 °C
View Scheme
3-bromo-1-(methylthio)benzene
33733-73-2

3-bromo-1-(methylthio)benzene

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Cu, K2CO3 / 220 - 230 °C
2: sulfur, I2 / 1 h / 135 °C
View Scheme
N-formyl-phenothiazine-2-sulfonyl chloride
139086-07-0

N-formyl-phenothiazine-2-sulfonyl chloride

dimethyl sulfate
77-78-1

dimethyl sulfate

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
With sodium hydroxide; sulfuric acid In dichloromethane; water
10H-phenothiazine
92-84-2

10H-phenothiazine

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: Heating
2: sulfuric acid / Heating
3: zinc; acetic acid
4: potassium carbonate / acetone
5: sodium hydroxide; methanol
View Scheme
10-acetyl-10H-phenothiazine
1628-29-1

10-acetyl-10H-phenothiazine

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: sulfuric acid / Heating
2: zinc; acetic acid
3: potassium carbonate / acetone
4: sodium hydroxide; methanol
View Scheme
C14H11NO4S2

C14H11NO4S2

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: zinc; acetic acid
2: potassium carbonate / acetone
3: sodium hydroxide; methanol
View Scheme
C14H11NOS2

C14H11NOS2

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: potassium carbonate / acetone
2: sodium hydroxide; methanol
View Scheme
1-[2-(methylsulfanyl)-10H-phenothiazin-10-yl]ethanone
23503-69-7

1-[2-(methylsulfanyl)-10H-phenothiazin-10-yl]ethanone

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
With methanol; sodium hydroxide
2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

10-(3-chloropropyl)-2-(methylthio)-10H-phenothiazine
40256-12-0

10-(3-chloropropyl)-2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
With sodium hydride; potassium carbonate In tetrahydrofuran; mineral oil at 65℃; Inert atmosphere;100%
Stage #1: 2-(methylthio)-10H-phenothiazine With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 0.333333h; Inert atmosphere;
Stage #2: 1.3-chlorobromopropane In N,N-dimethyl-formamide at 20℃; for 12h; Inert atmosphere;
93%
2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

t-butyl 2-(2-bromoethyl)piperidine-1-carboxylate
210564-52-6

t-butyl 2-(2-bromoethyl)piperidine-1-carboxylate

C25H32N2O2S2

C25H32N2O2S2

Conditions
ConditionsYield
With sodium hydride; potassium carbonate In tetrahydrofuran; mineral oil at 60℃; Inert atmosphere;100%
1-bromo-butane
109-65-9

1-bromo-butane

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

10-butyl-2-(methylthio)-10H-phenothiazine
1353744-07-6

10-butyl-2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
With potassium iodide; potassium hydroxide In dimethyl sulfoxide at 20℃; Inert atmosphere;95%
With potassium iodide; potassium hydroxide In dimethyl sulfoxide at 20℃; for 0.0833333h;
2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

acetyl chloride
75-36-5

acetyl chloride

1-[2-(methylsulfanyl)-10H-phenothiazin-10-yl]ethanone
23503-69-7

1-[2-(methylsulfanyl)-10H-phenothiazin-10-yl]ethanone

Conditions
ConditionsYield
In toluene at 20 - 30℃; for 1h; Temperature;93%
2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

1-(10H-phenothiazin-8-yl)hydrazine
1072135-10-4

1-(10H-phenothiazin-8-yl)hydrazine

Conditions
ConditionsYield
With hydrazine hydrate for 8h; Reflux;82%
With hydrazine Reflux;
2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

methyl 4-hydroxylbenzoate
99-76-3

methyl 4-hydroxylbenzoate

methyl 4-hydroxy-3-(2-(methylthio)-10H-phenothiazin-10-yl)benzoate

methyl 4-hydroxy-3-(2-(methylthio)-10H-phenothiazin-10-yl)benzoate

Conditions
ConditionsYield
With dipotassium hydrogenphosphate; oxygen; 10H-phenotellurazine In 1,2-dichloro-benzene at 130℃; for 3h; Reagent/catalyst; Sealed tube;81%
2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

10-(4-methoxybenzoyl)-2-(methylthio)-10H-phenothiazine
1309924-82-0

10-(4-methoxybenzoyl)-2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
In toluene Reflux;79%
2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

6-(2-chloroethyl)-1-methyl-2-piperidinone
134356-29-9

6-(2-chloroethyl)-1-methyl-2-piperidinone

10-<2-(1-methylpiperidin-2-on-6-yl)ethyl>-2-methylthio-10H-phenothiazine
89929-30-6

10-<2-(1-methylpiperidin-2-on-6-yl)ethyl>-2-methylthio-10H-phenothiazine

Conditions
ConditionsYield
With sodium hydride In toluene for 22h; Heating;78%
2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

4-Hydroxyacetophenone
99-93-4

4-Hydroxyacetophenone

N-(2-hydroxy-5-acetylphenyl)-2-(thiomethyl)-10H-phenothiazine

N-(2-hydroxy-5-acetylphenyl)-2-(thiomethyl)-10H-phenothiazine

Conditions
ConditionsYield
With dipotassium hydrogenphosphate; oxygen; 10H-phenotellurazine In 1,2-dichloro-benzene at 130℃; for 3h; Reagent/catalyst; Sealed tube;77%
2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

4-hydroxythioanisole
1073-72-9

4-hydroxythioanisole

N-(2-hydroxy-5-(thiomethyl)phenyl)-2-(thiomethyl)-10H-phenothiazine

N-(2-hydroxy-5-(thiomethyl)phenyl)-2-(thiomethyl)-10H-phenothiazine

Conditions
ConditionsYield
With dipotassium hydrogenphosphate; oxygen; 10H-phenotellurazine In 1,2-dichloro-benzene at 130℃; for 3h; Reagent/catalyst; Sealed tube;73%
Methyl 4-(bromomethyl)benzoate
2417-72-3

Methyl 4-(bromomethyl)benzoate

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

methyl 4-[(2-methylthio-10H-phenothiazin-10-yl)methyl]benzoate

methyl 4-[(2-methylthio-10H-phenothiazin-10-yl)methyl]benzoate

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; Inert atmosphere;69%
4-cyanobenzoic acid methyl ester
1129-35-7

4-cyanobenzoic acid methyl ester

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

10H-phenothiazine-2-carbonitrile
38642-74-9

10H-phenothiazine-2-carbonitrile

Conditions
ConditionsYield
With bis(1,5-cyclooctadiene)nickel (0); 1,2-bis-(dicyclohexylphosphino)ethane In o-xylene at 140℃; for 24h; Glovebox; Inert atmosphere;54%
2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

1,3-chlorohalopropane

1,3-chlorohalopropane

10-(3-chloropropyl)-2-(methylthio)-10H-phenothiazine
40256-12-0

10-(3-chloropropyl)-2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 100℃; for 24h; Sealed tube; Schlenk technique; Inert atmosphere;53%
2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

N,N-diethylaniline
91-66-7

N,N-diethylaniline

N,N-diethyl-4-(2-(methylthio)-10H-phenothiazin-10-yl)aniline

N,N-diethyl-4-(2-(methylthio)-10H-phenothiazin-10-yl)aniline

Conditions
ConditionsYield
With tert-butylammonium hexafluorophosphate(V) In acetonitrile at 20℃; for 3h; Electrolysis;50%
2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

1,4-chlorohalobutane

1,4-chlorohalobutane

10-(4’-chlorobutyl)-2-methylthio-10H-phenothiazine

10-(4’-chlorobutyl)-2-methylthio-10H-phenothiazine

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 100℃; for 24h; Sealed tube; Schlenk technique; Inert atmosphere;25.6%
phosgene
75-44-5

phosgene

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

2-methylsulfanyl-phenothiazine-10-carbonyl chloride
92161-48-3

2-methylsulfanyl-phenothiazine-10-carbonyl chloride

Conditions
ConditionsYield
With benzene
2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

2-(dimethylamino)ethyl chloride
107-99-3

2-(dimethylamino)ethyl chloride

dimethyl-[2-(2-methylsulfanyl-phenothiazin-10-yl)-ethyl]-amine
107273-41-6

dimethyl-[2-(2-methylsulfanyl-phenothiazin-10-yl)-ethyl]-amine

Conditions
ConditionsYield
With sodium hydroxide; toluene
With sodium amide; xylene
2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

1-diethylamino-2-chloropropane
761-21-7

1-diethylamino-2-chloropropane

diethyl-[β-(2-methylsulfanyl-phenothiazin-10-yl)-isopropyl]-amine
110150-17-9

diethyl-[β-(2-methylsulfanyl-phenothiazin-10-yl)-isopropyl]-amine

Conditions
ConditionsYield
With sodium amide; xylene
With sodium hydroxide; toluene
oxirane
75-21-8

oxirane

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

1-(3-chloro-propyl)-4-formyl-piperazine; hydrochloride

1-(3-chloro-propyl)-4-formyl-piperazine; hydrochloride

acetyl chloride
75-36-5

acetyl chloride

1-acetoxy-2-{4-[3-(2-methylsulfanyl-phenothiazin-10-yl)-propyl]-piperazin-1-yl}-ethane
103756-91-8

1-acetoxy-2-{4-[3-(2-methylsulfanyl-phenothiazin-10-yl)-propyl]-piperazin-1-yl}-ethane

Conditions
ConditionsYield
(i) NaNH2, (ii) aq. NaOH, (iii) /BRN= 102378/, MeOH, (iv) /BRN= 605303/; Multistep reaction;
3-(N-methylpiperazinyl)propyl chloride
104-16-5

3-(N-methylpiperazinyl)propyl chloride

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

10-(3-(4-methylpiperazin-1-yl)propyl)-2-(methylthio)-10H-phenothiazine
14978-58-6

10-(3-(4-methylpiperazin-1-yl)propyl)-2-(methylthio)-10H-phenothiazine

Conditions
ConditionsYield
With sodium amide
1-(3-chloro-2-methyl-propyl)-4-methyl-piperazine
39607-92-6

1-(3-chloro-2-methyl-propyl)-4-methyl-piperazine

2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

10-[2-methyl-3-(4-methyl-piperazin-1-yl)-propyl]-2-methylsulfanyl-10H-phenothiazine
106439-16-1

10-[2-methyl-3-(4-methyl-piperazin-1-yl)-propyl]-2-methylsulfanyl-10H-phenothiazine

Conditions
ConditionsYield
With sodium amide
2-(methylthio)-10H-phenothiazine
7643-08-5

2-(methylthio)-10H-phenothiazine

trans-2-bromo-cyclopropanecarboxylic acid dimethylamide
17824-40-7, 31191-78-3, 31191-79-4

trans-2-bromo-cyclopropanecarboxylic acid dimethylamide

dimethyl-[trans-2-(2-methylsulfanyl-phenothiazin-10-yl)-cyclopropylmethyl]-amine
47276-01-7

dimethyl-[trans-2-(2-methylsulfanyl-phenothiazin-10-yl)-cyclopropylmethyl]-amine

Conditions
ConditionsYield
(i) NaH, DMSO, (ii) LiAlH4, Et2O; Multistep reaction;

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