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inquiryK(1+)*TeF5O(1-)=KTeF5O
fluorine
A
TeF5OF
B
tellurium hexafluoride
Conditions | Yield |
---|---|
In neat (no solvent) KTeF5O was treated with F2 (molar ratio 1:3.11) for 6 wk at -45°C; | A 0% B 80% |
In neat (no solvent) KTeF5O was treated with F2 (molar ratio 1:3.11) for 8 d at -45°C; | A 0% B 26% |
Conditions | Yield |
---|---|
In neat (no solvent) a mixture of TeO2:Te=1:1 was treated with F2 (4 l/h) dild. with N2 (10 l/h) at a furnace temp. of 50-60°C;; | A 25% B 2% C 73% |
In neat (no solvent) a mixture of TeO2:Te=1:1 was treated with F2 (4 l/h) dild. with O2 (10 l/h) at a furnace temp. of 50-60°C; the yield of Te2F10 is almost 50%;; |
fluorosulfuryl hypofluorite
A
teflic acid
B
TeF5OF
C
tellurium hexafluoride
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: CsSO3F; CsTeF5O was evacuated and cooled to -196°C, FOSO2F (molar ratio 1.22:1) was added from vac. line, closed, warmed slowly to -78°C in liq. N2-CO2 slush bath, kept at -45°C for 9 d, cooled to -196°C; pumped off, sepd. by fractional condensation in traps (-78, -126 and -196°C); | A n/a B 68% C n/a |
titanium(IV) tetrakis(pentafluoroorthotellurate)
A
titanium oxyfluoride
B
F5TeOTeF5
C
F5Te(OTeF4)OTeF5
D
tellurium hexafluoride
Conditions | Yield |
---|---|
heated at 250°C for 15 h in autoclave; | A 19% B 26% C 51% D 3.9% |
Conditions | Yield |
---|---|
In neat (no solvent) CsTeF5O was treated with F2 (molar ratio 1:3.11) for 2 wk at -10°C; | A 0% B 48% |
In neat (no solvent) CsTeF5O was treated with F2 (molar ratio 1:3.11) for 8 d at -45°C; | A 0% B 26% |
tellurium(IV) oxide
boron trifluoride
C
tellurium hexafluoride
D
tellurium(IV) fluoride
Conditions | Yield |
---|---|
In neat (no solvent) TeO2 was treated with a continous stream of BF3 with He as carrier gas at 100-450°C;; | |
In neat (no solvent) TeO2 was treated with a continous stream of BF3 with He as carrier gas at 100-450°C;; |
Conditions | Yield |
---|---|
In neat (no solvent) TeO2 was treated with F2 (0.5-10 l/h) dild. with N2 (0-5 l/h) at a furnace temp. of 100-200°C;; |
Conditions | Yield |
---|---|
In neat (no solvent) distd. Te; with inflammation;; |
Conditions | Yield |
---|---|
In neat (no solvent) product mixture of TeF6 and lower tellurium fluorides;; | |
In neat (no solvent) from F2 and Te in very dry glass apparatus; 10-15 hours; on cooling since begin of reaction no inflammation;; | |
In neat (no solvent) passing pure F2 (purified from HF by waterfree NaF in copper tube) over Te in copper tube (1.5l F2 / hour; no explosion);; condensation on cooling with carbon dioxide-alc.-freezing mixture in Pyrex glass vessel; fractionated sublimation in vac.;; |
fluorine
A
tellurium hexafluoride
B
tungsten(VI) fluoride
C
tellurium(IV) fluoride
Conditions | Yield |
---|---|
In neat (no solvent) WTe2 placed in a tungsten saucer, addn. of a small amt. of sulfur as fuse, react. with fluorine in a prefluorinated perforated nickel crucible; |
Conditions | Yield |
---|---|
In neat (no solvent) 50 mol% excess of F2; 250°C; 4 h; condensation onto dry NaF at -196°C; |
oxygen
B
tellurium hexafluoride
Conditions | Yield |
---|---|
In neat (no solvent) thermal treatment of RbTeF5 in air, 450°C, 3h; |
pentafluorotellurium chloride
cesium fluoride
B
tellurium hexafluoride
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: SiF4, ClF; TeClF5 (12.81 mmol) was allowed to react with CsF (3.40 mmol) at 90°C for 25 d;; | |
In neat (no solvent) byproducts: Cl2; TeClF5 (6.19 mmol) was allowed to react with CsF (3.82 mmol) at 55°C for 20 d in F.E.P react. vessel;; | |
In neat (no solvent) byproducts: SiF4, ClF, Cl2; TeClF5 (8.53 mmol) was condensed onto CsF (4.11 mmol) in a glass vessel and the mixt. stirred at room temp.; the react. was complete for 30 d;; TeF6, Cl2, TeFCl5 and SiF4 were removed leaving a solid; detected by IR-, Raman-, NMR-expt. and X-ray powder photography;; | |
In further solvent(s) byproducts: Cl2; TeClF5 (15.54 mmol) was allowed to react with CsF (3.33 mmol) at 80-90°C for 15 d in C6F6 soln.;; |
pentafluorotellurium chloride
B
tellurium hexafluoride
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: Cl2; TeFCl5 (5.22 mmol) was allowed to react with solid KOH (5.54 mmol) for 7 d;; detected by IR- and Raman expt.; |
boron tris{pentafluoro-oxotellurate(VI)}
B
boron trifluoride
C
tellurium oxide
D
tellurium hexafluoride
Conditions | Yield |
---|---|
decompn. above 140°C; | |
decompn. above 140°C; |
boron tris{pentafluoro-oxotellurate(VI)}
A
boron trifluoride
B
tellurium oxide
C
tellurium hexafluoride
Conditions | Yield |
---|---|
decompn. above 350°C; | |
decompn. above 350°C; |
boron tris{pentafluoro-oxotellurate(VI)}
FI(OTeF5)4
A
OI(OTeF5)3
B
tellurium hexafluoride
Conditions | Yield |
---|---|
+80°C; | |
+80°C; |
A
Cs(1+)*ClF2(1-) = CsClF2
B
pentafluorotellurium chloride
C
tellurium hexafluoride
Conditions | Yield |
---|---|
With chlorine monofluoride In solid byproducts: Cl2; High Pressure; ClF (7.52 mmol) was condensed onto CsTeF5 (5.85 mmol) in a Monel vessel and left at room temp. for 3 d;; detected by IR-, Raman, NMR-expt.;; | A n/a B <1 C n/a |
pentafluorotellurium chloride
A
tellurium hexafluoride
B
tellurium(IV) fluoride
Conditions | Yield |
---|---|
In neat (no solvent) High Pressure; heating at 250°C in a Monel vessel overnight;; detected by IR-expt.; |
pentafluorotellurium chloride
tellurium hexafluoride
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: SiF4, Cl2; High Pressure; heating at 70°C for 20 d in a Monel Parr bomb, then reheating at 110°C for 2 mo; then the mixt. of products was heated at 180°C for 20 d;; detected by IR-expt.; | <1 |
Conditions | Yield |
---|---|
In neat (no solvent) High Pressure; TeFCl5 (5.81 mmol) was allowed to react with F2 (23.2 mmol) for 3 d at 165°C in a Parr bomb;; detected by IR-, Raman and NMR-expt.; |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: Cl2; TeClF5 (3.72 mmol) was allowed to react with HNMe2 (2.99 mmol);; detected by IR-expt.; | A n/a B <1 |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: NF3, HF; TeF5OH was added to NF4NF2*99HF on vac. line at -196°C, warmed slowly to -23°C, kept for 8 h under dynamic vac.; volatiles sepd. by fractional condensation in traps (-95, -126, -142 and -210°C); | A 10-20 B <1 |
fluorine
tungsten
A
molybdenum(VI) fluoride
B
tellurium hexafluoride
C
tungsten(VI) fluoride
D
sulfur(VI) hexafluoride
Conditions | Yield |
---|---|
In neat (no solvent) Ensemble of MoTe2 on W-saucer with small quantities of S, resting on a perfluorinated Ni-crucible, is combusted with F2 in a calorimeter bomb.; Gases are condensed into a trap (liq. N2).; |
Xe(OTeF5)4
antimony pentafluoride
A
F5TeOTeF5
B
F2XeOTeF5(1+)
C
FXe(OTeF5)2(1+)
D
Xe(OTeF5)3(1+)
E
tellurium hexafluoride
Conditions | Yield |
---|---|
In neat (no solvent) heat sealing of the NMR tube with Xe-compound; cooling to -196°C; addn. of SbF5 via syringe; removing tube from drybox while cold- and heat sealing under a dynamic vac. at -196°C; not isolated; detection of compounds at 5°C by NMR; |
OXe(OTeF5)4
antimony pentafluoride
A
xenon fluoride cation
B
F5TeOTeF5
C
F5OTeXe(1+)
D
OXeF(OTeF5)2(1+)
E
tellurium hexafluoride
Conditions | Yield |
---|---|
In neat (no solvent) further products; heat sealing of the NMR tube with Xe-compound; cooling to -196°C; addn. of SbF5 via syringe; removing tube from drybox while cold- and heat sealing under a dynamic vac. at -196°C; not isolated; detection of compounds at 5°C by NMR; |
Conditions | Yield |
---|---|
at 363℃; Inert atmosphere; | |
at 500℃; Inert atmosphere; |
Conditions | Yield |
---|---|
at 500℃; Inert atmosphere; |
calcium hydride
tellurium hexafluoride
18O-labeled water
A
pentafluorotellurate(VI)
B
pyridinium hydrogen sulfate
Conditions | Yield |
---|---|
With H2SO4 In pyridine byproducts: H2, CaF2; Sonication; O2 and H2O excluded: H2(18)O added to CaH2 in pyridine, H2 evolution, reactn. mixt. stirred and sonicated (3d, room temp.), degassed, frozen (-196 ° C), TeF6 added (vac. transfer), heated and stirred (45 ° C, 12h), caution: TeF6-pressure!; pyridine and TeF6 removed (vac.), {pyH(1+)}{(18)OTeF5} extracted into warm CH2Cl2, CH2Cl2 removed (vac., white residue), (19)F NMR, concd. H2SO4 added, vac. distn., (19)F NMR; | A 88% B n/a |
Conditions | Yield |
---|---|
molar ratio NaF:TeF6=1:>2; 250°C in autoclave; cooling to room temp.; |
Conditions | Yield |
---|---|
In not given | |
In neat (no solvent) on heating to 200°C;; | |
In neat (no solvent) decomposition with Te;; |
Conditions | Yield |
---|---|
With liquid HF reaction of AgF and TeF6 in liquid HF;; evaporation of HF;; |
Conditions | Yield |
---|---|
In water on storage TeF6 over water, evaporation of the soln. and heating residue;; |
Conditions | Yield |
---|---|
In further solvent(s) in C6F6; inert atmosphere, 293 K; freezing, distn. (vac.); radioactivity measurement; | A 0% B 0% |
Conditions | Yield |
---|---|
In water hydrolysis; |
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