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inquiry3-Morpholinecarboxylic acid CAS:77873-76-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality orga
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryWe product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Product Name:3-Morpholinecarboxylic acid CAS No:778
factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiry1, High quality with competitive price:2, Fast and safe delivery3.Excellent pre-sales and after-sales service4. Well-trained and professional technologist and sales with rich experience in the field for 5-10 yearsAppearance:see detailed specification
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
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inquiryHunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
Our own factory produces direct sales with absolute price advantage Application:Pharmaceutical industry Transportation:By sea Port:Shanghai/tianjin
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inquiry3-Morpholinecarboxylic acid CAS NO.77873-76-8 Application:3-Morpholinecarboxylic acid CAS NO.77873-76-8
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inquiryMorpholine-3-carboxylic acidAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:pharmaceutical intermediate Transportation:by air, by sea, by express
Hangzhou ZeErRui Chemical Co., Ltd. is focused on customization, research and development and production of APIs and advanced intermediates, which can effectively compensate for the deficiencies of traditional CRO and CMO. Priority of high-tech barri
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inquiry77873-76-8 Application:intermediate
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inquiryN-acetyl-3-cyanomorpholine
morpholine-3-carboxylic acid
Conditions | Yield |
---|---|
acid hydrolysis; | 55% |
Stage #1: N-acetyl-3-cyanomorpholine With sodium hydroxide at 20℃; for 3h; Stage #2: With hydrogenchloride at 16℃; for 100h; |
Acetylamino-(2-chlor-aethoxymethyl)-malonsaeure-diaethylester
morpholine-3-carboxylic acid
Conditions | Yield |
---|---|
With ammonium hydroxide Erhitzen des Reaktionsprodukts mit wss. HCl; |
2-bromo-3-(2-chloro-ethoxy)-propionic acid methyl ester
ammonia
A
morpholine-3-carboxylic acid
B
O-(2-amino-ethyl)-serine
C
O-(2-chloro-ethyl)-serine
2-bromo-3-(2-chloro-ethoxy)-propionic acid methyl ester
A
morpholine-3-carboxylic acid
B
O-(2-amino-ethyl)-serine
C
O-(2-chloro-ethyl)-serine
Conditions | Yield |
---|---|
With acetyl chloride at 0℃; Heating / reflux; | 99% |
Stage #1: morpholine-3-carboxylic acid; ethanol With acetyl chloride at 0℃; Heating / reflux; Stage #2: With sodium hydrogencarbonate In dichloromethane; water | 99% |
With acetyl chloride at 0℃; Heating / reflux; | 99% |
With acetyl chloride at 0℃; Heating / reflux; | 99% |
morpholine-3-carboxylic acid
acetyl chloride
ethyl morpholine-3-carboxylate
Conditions | Yield |
---|---|
In ethanol Heating / reflux; | 99% |
morpholine-3-carboxylic acid
4-nitrosomorpholine-3-carboxylic acid
Conditions | Yield |
---|---|
With hydrogenchloride; sodium nitrite In water at 0℃; for 1h; | 96% |
181 mg | |
With hydrogenchloride; sodium nitrite at 0℃; for 1h; |
morpholine-3-carboxylic acid
di-tert-butyl dicarbonate
4-(tert-butoxycarbonyl)morpholine-3-carboxylic acid
Conditions | Yield |
---|---|
Stage #1: morpholine-3-carboxylic acid; di-tert-butyl dicarbonate With potassium carbonate In water; acetone at 0 - 20℃; for 24h; Stage #2: With hydrogenchloride In water | 84% |
With potassium carbonate In water; acetone at 0 - 20℃; | 34% |
With sodium hydroxide In 1,4-dioxane; water |
morpholine-3-carboxylic acid
bis(trichloromethyl) carbonate
Conditions | Yield |
---|---|
Stage #1: bis(trichloromethyl) carbonate; 6-amino-7-fluoro-4-(prop-2-yn-1-yl)spiro[benzo[b][1,4]oxazine-2,1'-cyclopropan]-3(4H)-one With triethylamine In tetrahydrofuran at 20℃; for 2h; Stage #2: morpholine-3-carboxylic acid With triethylamine In dichloromethane at 20℃; for 18h; Stage #3: With hydrogenchloride In 1,4-dioxane at 70℃; for 3h; | 80% |
morpholine-3-carboxylic acid
5-amino-2,4-dichloropyrimidine
2-chloro-6a,7,9,10-tetrahydro[1,4]oxazino[3,4-h]pteridin -6(5H)-one
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dimethyl sulfoxide at 100℃; | 70.3% |
With N-ethyl-N,N-diisopropylamine In dimethyl sulfoxide at 100℃; | 70.3% |
morpholine-3-carboxylic acid
2-chloro-1-isocyanato-4-nitro-benzene
2-(2-chloro-4-nitrophenyl)tetrahydro-1H-imidazo[5,1-c][1,4]oxazine-1,3(2H)-dione
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In 1,2-dichloro-ethane at 160℃; for 0.166667h; | 54% |
morpholine-3-carboxylic acid
3-(3-(4-chloro-5-fluoropyrimidin-2-yl)-1-(2-fluorobenzyl)-1H-pyrazol-5-yl)isoxazole
Conditions | Yield |
---|---|
With triethylamine In 1,4-dioxane; water at 100℃; for 48h; | 48% |
morpholine-3-carboxylic acid
ethyl 6-(bromomethyl)-4-(2-chloro-4-fluorophenyl)-1-methyl-2-(thiazol-2-yl)-1,4-dihydropyrimidine-5-carboxylate
4-((6-(2-chloro-4-fluorophenyl)-5-(ethoxycarbonyl)-3-methyl-2-(thiazol-2-yl)-3,6-dihydropyrimidin-4-yl)methyl)morpholine-3-carboxylic acid
Conditions | Yield |
---|---|
With potassium carbonate In ethanol at 25℃; for 12h; | 20% |
morpholine-3-carboxylic acid
di-tert-butyl dicarbonate
(S)-4-[(tert-butoxy)carbonyl]morpholine-3-carboxylic acid
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 3h; | 14% |
morpholine-3-carboxylic acid
6-chloropurine
4-(9H-purin-6-yl)morpholine-3-carboxylic acid
Conditions | Yield |
---|---|
In 1-methyl-pyrrolidin-2-one at 140℃; for 0.416667h; Inert atmosphere; Microwave irradiation; | 7% |
morpholine-3-carboxylic acid
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In chloroform-d1; N,N-dimethyl-formamide at 25℃; for 24h; | 3.51% |
Conditions | Yield |
---|---|
Heating; Yield given; |
morpholine-3-carboxylic acid
3-oxo-6,7-dihydro-3H-[1,2,3]oxadiazolo[4,3-c][1,4]oxazine-8(4H)ylium-3a-ide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NaNO2; aq. HCl / 1 h / 0 °C 2: 3.80 g / trifluoroacetic anhydride / tetrahydrofuran / 21 h / 0 - 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: sodium nitrite; hydrogenchloride / water / 0 - 25 °C 2: trifluoroacetic anhydride / toluene / 12 h / 0 - 15 °C View Scheme | |
Multi-step reaction with 2 steps 1: hydrogenchloride; sodium nitrite / water / 1 h / 0 °C 2: trifluoroacetic anhydride / dichloromethane / 0.5 h / 5 °C View Scheme | |
Multi-step reaction with 2 steps 1: hydrogenchloride; sodium nitrite / water / 1 h 2: trifluoromethylsulfonic anhydride / dichloromethane / 0.5 h / 5 °C View Scheme |
morpholine-3-carboxylic acid
4-methoxy-phenyl-sulphonyl chloride
4-[(4-methoxyphenyl) sulfonyl]-3-morpholinecarboxylic acid
Conditions | Yield |
---|---|
With triethylamine In dichloromethane |
Conditions | Yield |
---|---|
With hydrogenchloride; sodium hydroxide; N-ethyl-N,N-diisopropylamine In DMF (N,N-dimethyl-formamide); dichloromethane |
morpholine-3-carboxylic acid
di-tert-butyl dicarbonate
tert-Butyl 3-(hydroxymethyl)-4-morpholinecarboxylate
Conditions | Yield |
---|---|
With borane In tetrahydrofuran; sodium hydroxide |
morpholine-3-carboxylic acid
trimethylaluminum
4-chloro-2-fluoro-5-isopropoxyaniline
N-[4-Chloro-2-fluoro-5-(1-methylethoxy)phenyl]morpholine-3-carboxamide
Conditions | Yield |
---|---|
With hydrogenchloride; sodium hydroxide In dichloromethane; water |
morpholine-3-carboxylic acid
ethyl 4-[(3-aminopyridin-2-yl)amino]-N-(3-oxospiro[3.5]non-1-en-1-yl)-L-phenylalaninate
C30H37N5O5
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane |
morpholine-3-carboxylic acid
N-[1-{[3-(aminomethyl)phenyl]methyl}-4-methyloxy-1H-indazol-3-yl]-5-chloro-2-thiophenesulfonamide hydrochloride
Conditions | Yield |
---|---|
Stage #1: morpholine-3-carboxylic acid With N-ethyl-N,N-diisopropylamine; HATU In acetonitrile at 20℃; for 0.25h; Stage #2: N-[1-{[3-(aminomethyl)phenyl]methyl}-4-methyloxy-1H-indazol-3-yl]-5-chloro-2-thiophenesulfonamide hydrochloride In acetonitrile at 20℃; |
morpholine-3-carboxylic acid
benzyl chloroformate
4-((benzyloxy)carbonyl)morpholine-3-carboxylic acid
Conditions | Yield |
---|---|
Stage #1: morpholine-3-carboxylic acid; benzyl chloroformate With sodium hydroxide In water at 5 - 15℃; for 2h; pH=6 - 9; Stage #2: With hydrogenchloride In water pH=0; |
morpholine-3-carboxylic acid
5-amino-2,4,6-trichloropyrimidine
2,4-dichloro-6a,7,9,10-tetrahydro-[1,4]oxazino[3,4-h]pteridin-6(5H)-one
Conditions | Yield |
---|---|
With triethylamine In ethanol at 75℃; for 72h; |
morpholine-3-carboxylic acid
1-(4-(5-(cyclopropylmethyl)-6a-methyl-6-oxo-5,6,6a,7,9,10-hexahydro-[1,4]oxazino[3,4-h]pteridin-2-yl)phenyl)-3-methylurea
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 100 °C 2: sodium t-butanolate / dimethyl sulfoxide / 16.2 h / 20 °C / Cooling with ice 3: sodium t-butanolate / dimethyl sulfoxide / 16 h / 0 - 20 °C 4: sodium hydrogencarbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 0.67 h / 100 °C / Microwave Irradiation View Scheme | |
Multi-step reaction with 8 steps 1.1: sodium hydroxide / water / 2 h / 5 - 15 °C / pH 6 - 9 1.2: pH 0 2.1: sulfuric acid / 18 h / 34 - 50 °C 3.1: sodium hexamethyldisilazane / tetrahydrofuran / 5.03 h / -70 - -40 °C 4.1: hydrogen / palladium 10% on activated carbon / ethanol / 16 h / 760.05 Torr / Inert atmosphere 5.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 h / -10 - 20 °C 6.1: methanol / bis(acetylacetonate)oxovanadium / tetrahydrofuran / 18 h / 20 - 35 °C / 760.05 Torr 7.1: potassium carbonate / dimethyl sulfoxide / 2.5 h / 20 - 35 °C 8.1: sodium hydrogencarbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 0.67 h / 100 °C / Microwave Irradiation View Scheme |
morpholine-3-carboxylic acid
2-chloro-5-(cyclopropylmethyl)-6a,7,9,10-tetrahydro-[1,4]oxazino[3,4-h]pteridin-6(5H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 100 °C 2: sodium t-butanolate / dimethyl sulfoxide / 16.2 h / 20 °C / Cooling with ice View Scheme |
morpholine-3-carboxylic acid
2-chloro-5-(cyclopropylmethyl)-6a-methyl-6a,7,9,10-tetrahydro-[1,4]oxazino[3,4-h]pteridin-6(5H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 100 °C 2: sodium t-butanolate / dimethyl sulfoxide / 16.2 h / 20 °C / Cooling with ice 3: sodium t-butanolate / dimethyl sulfoxide / 16 h / 0 - 20 °C View Scheme | |
Multi-step reaction with 7 steps 1.1: sodium hydroxide / water / 2 h / 5 - 15 °C / pH 6 - 9 1.2: pH 0 2.1: sulfuric acid / 18 h / 34 - 50 °C 3.1: sodium hexamethyldisilazane / tetrahydrofuran / 5.03 h / -70 - -40 °C 4.1: hydrogen / palladium 10% on activated carbon / ethanol / 16 h / 760.05 Torr / Inert atmosphere 5.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 h / -10 - 20 °C 6.1: methanol / bis(acetylacetonate)oxovanadium / tetrahydrofuran / 18 h / 20 - 35 °C / 760.05 Torr 7.1: potassium carbonate / dimethyl sulfoxide / 2.5 h / 20 - 35 °C View Scheme |
morpholine-3-carboxylic acid
1-methyl-3-(4-(6a-methyl-5-((1-methyl-1H-pyrazol-3-yl)methyl)-6-oxo-5,6,6a,7,9,10-hexahydro-[1,4]oxazino[3,4-h]pteridin-2-yl)phenyl)urea
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 100 °C 2: N,N-dimethyl-formamide / 0 - 20 °C 3: sodium t-butanolate / dimethyl sulfoxide / 20 °C / Sealed tube; Freezing 4: sodium hydrogencarbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 0.75 h / 100 °C / Microwave Irradiation View Scheme |
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