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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

4-Methoxybenzenesulfonyl chloride

Cas:98-68-0

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 4-Methoxy Benzenesulphonyl Chloride supplier in China

Cas:98-68-0

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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COLORCOM LTD.

Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on

4-Methoxybenzenesulfonyl Chloride

Cas:98-68-0

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

4-Methoxybenzenesulfonyl chloride

Cas:98-68-0

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Hebei Nengqian Chemical Import and Export Co., LTD

Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con

4-Methoxybenzenesulfonyl chloride 98-68-0

Cas:98-68-0

Min.Order:1 Kilogram

FOB Price: $15.0 / 50.0

Type:Trading Company

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Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

98-68-0 4-Methoxybenzenesulfonyl chloride

Cas:98-68-0

Min.Order:1 Kilogram

FOB Price: $1000.0

Type:Lab/Research institutions

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 98-68-0 with best quality

Cas:98-68-0

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Product Name: 4-Methoxybenzenesulfonyl chloride Synonyms: 4-Methoxybenzenesulfonylchlorid;Benzenesulfonyl chloride, p-methoxy-;p-Anisylsulfonyl chloride;p-Methoxyphenylsulfonyl chloride;P-ANISOLESULFONYL CH

4-Methoxybenzenesulfonyl chloride CAS: 98-68-0

Cas:98-68-0

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

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Shijiazhuang Sdyano Fine Chemical Co., Ltd

1. Best prices with satisfied quality; 2. It's clients' right to choose the package's Courier (EMS, DHL, FedEx, UPS); 3.It's clients' right to choose the packing way for his produccts from many recent effective packing ways;

4-Methoxybenzenesulfonyl Chloride

Cas:98-68-0

Min.Order:0 Metric Ton

Negotiable

Type:Trading Company

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Hangzhou Sartort Biopharma Co., Ltd

Appearance:White to beige?Crystalline Solid Storage:2-8°C Package:25kg/drum Application:4-Methoxybenzenesulfonyl chloride is used as an anti-HIV as Pharmaceutical Intermediates. It also acts as protecting group agent for various nitrogen functions.

4-Methoxybenzenesulfonyl chloride factory price

Cas:98-68-0

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

Benzenesulfonylchloride, 4-methoxy-

Cas:98-68-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:98-68-0

Cas:98-68-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We have s

4-Methoxybenzenesulfonyl Chloride 98-68-0

Cas:98-68-0

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

4-Methoxybenzenesulfonyl chloride

Cas:98-68-0

Min.Order:1 Kilogram

FOB Price: $80.0 / 100.0

Type:Lab/Research institutions

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

4-Methoxybenzenesulfonyl Chloride

Cas:98-68-0

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

4-Methoxybenzenesulfonyl chloride

Cas:98-68-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and als

4-Methoxybenzenesulfonyl chloride

Cas:98-68-0

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

4-Methoxybenzenesulfonyl Chloride

Cas:98-68-0

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

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HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:White crystal Storage:Store in a cool, ventilated, dry warehouse, Package:25kg/drum, or as per your request. Application:For medicine , pesticide intermediates Transportation:as

4-Methoxybenzenesulfonyl chloride

Cas:98-68-0

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Siwei Development Group Ltd.

Product name: 4-Methyoxybenzenesulfonyl Chloride CAS No.: 98-68-0 Molecule Formula:C7H7ClO3S Molecule Weight:206.65 Purity: 99.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard

Lower Price 4-Methyoxybenzenesulfonyl Chloride

Cas:98-68-0

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

4-Methoxybenzenesulfonyl chloride

Cas:98-68-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Minstar Chemical Co., Ltd

Product Name: 4-Methoxybenzenesulfonyl chloride CAS: 98-68-0 MF: C7H7ClO3S MW: 206.65 EINECS: 202-692-1 Mol File: 98-68-0.mol 4-Methoxybenzenesulfonyl chloride Structure 4-Methoxybenzenesulfonyl chloride Chemical Properties Meltin

4-Methoxybenzenesulfonyl chloride

Cas:98-68-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

4-Methoxybenzenesulfonyl Chloride

Cas:98-68-0

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

4-Methoxybenzenesulfonyl chloride

Cas:98-68-0

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

4-Methoxybenzenesulfonyl Chloride

Cas:98-68-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

4-Methoxybenzenesulfonyl Chloride

Cas:98-68-0

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

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Hangzhou ZeErRui Chemical Co., Ltd.

Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home

4-Methoxy benzenesulphonyl chloride china manufacture

Cas:98-68-0

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

4-methoxybenzenesulfonyl Chloride

Cas:98-68-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

4-Methoxybenzenesulfonyl Chloride

Cas:98-68-0

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

4-Methoxybenzenesulfonyl Chloride cas no. 98-68-0 98%

Cas:98-68-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

4-Methoxybenzenethiol
696-63-9

4-Methoxybenzenethiol

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
With N,N,N',N'-tetrachlorobenzene-1,3-disulphonamide; tetrabutyl-ammonium chloride; water In acetonitrile at 0 - 20℃; for 0.333333h;99%
With trichloroisocyanuric acid; water In acetonitrile at 0 - 20℃; for 0.333333h;99%
With thionyl chloride; dihydrogen peroxide In water; acetonitrile at 25℃; for 0.0166667h;98%
methylthiocarbamic acid S-(4-methoxyphenyl)ester

methylthiocarbamic acid S-(4-methoxyphenyl)ester

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
With hydrogenchloride; N-chloro-succinimide In acetonitrile at 10℃;98.1%
S-(4-methoxyphenyl) ethanethioate
60787-31-7

S-(4-methoxyphenyl) ethanethioate

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
With hydrogenchloride; N-chloro-succinimide In acetonitrile at 10℃;97.7%
4,4'-dimethoxyphenyl disulfide
5335-87-5

4,4'-dimethoxyphenyl disulfide

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
With dihydrogen peroxide; zirconium(IV) chloride In water; acetonitrile at 25℃; for 0.0166667h;96%
With dihydrogen peroxide; trichlorophosphate In water at 25℃; for 0.5h; Micellar solution;95%
With 1,3-dichloro-5,5-dimethylhydantoin; acetic acid In dichloromethane; water at 0 - 20℃; Inert atmosphere;92%
4-methoxybenzenesulfonic acid
5857-42-1

4-methoxybenzenesulfonic acid

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
With 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; potassium chloride at 25℃; for 0.0333333h; Neat (no solvent);94%
methoxybenzene
100-66-3

methoxybenzene

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
With sulfuryl dichloride; sulfuric acid In N,N-dimethyl-formamide88%
With chlorosulfonic acid at 0 - 5℃;71.32%
With chlorosulfonic acid at 0 - 5℃;71.42%
1-benzylsulfanyl-4-methoxy-benzene
26905-24-8

1-benzylsulfanyl-4-methoxy-benzene

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
With 1,3-dichloro-5,5-dimethylhydantoin; acetic acid In dichloromethane; water at 0 - 5℃; Inert atmosphere;86%
S-4-methoxyphenyl benzothioate
24197-73-7

S-4-methoxyphenyl benzothioate

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
With trichloroisocyanuric acid; benzyltrimethylammonium chloride; sodium carbonate In water; acetonitrile at 0℃; for 0.333333h;81%
4-methoxybenzenediazonium tetrafluoroborate
459-64-3

4-methoxybenzenediazonium tetrafluoroborate

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
With thionyl chloride; tris(bipyridine)ruthenium(II) dichloride hexahydrate In water; acetonitrile at 20℃; for 20h; Concentration; Sealed tube; Irradiation;71%
4-Methoxybenzenethiol
696-63-9

4-Methoxybenzenethiol

chloroamine-T
127-65-1

chloroamine-T

A

N-chloro-N-(4-methylbenzenesulfonyl)-4-methoxybenzenesulfinamide

N-chloro-N-(4-methylbenzenesulfonyl)-4-methoxybenzenesulfinamide

B

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
With N-chloro-succinimide In water; acetonitrile at 35℃; for 0.25h;A 70%
B 27%
4-methoxy-aniline
104-94-9

4-methoxy-aniline

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
Stage #1: 4-methoxy-aniline With tris(bipyridine)ruthenium(II) dichloride hexahydrate; isopentyl nitrite In acetonitrile at 20℃; for 0.0833333h; Sealed tube;
Stage #2: With thionyl chloride In water; acetonitrile at 20℃; for 20h; Irradiation;
63%
Stage #1: 4-methoxy-aniline With hydrogenchloride; acetic acid
Stage #2: With sodium nitrite In water at -10 - -5℃; for 0.75h;
Stage #3: With hydrogenchloride; sulfur dioxide; acetic acid; copper(l) chloride In water at 10℃; for 0.5h;
27%
With tert.-butylnitrite; sulfur dioxide; N-benzyl-N,N,N-triethylammonium chloride; ethylene glycol; copper dichloride In dichloromethane; acetonitrile at 0 - 20℃; Automated synthesizer;
Stage #1: 4-methoxy-aniline With tetrafluoroboric acid; tert.-butylnitrite In ethanol; water at 0 - 20℃; for 1h;
Stage #2: With 6,6'-dimethyl-2,2'-bipyridine; 1,4-diazabicyclo [2.2.2] octane-1,4-diium-1,4-disulfinate; potassium chloride; copper dichloride In acetonitrile at 20℃; for 12h; Sealed tube; Inert atmosphere;
50 mg
chlorosulfonic acid
7790-94-5

chlorosulfonic acid

methoxybenzene
100-66-3

methoxybenzene

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
In dichloromethane for 2h;60%
(2-nitroethenyl)benzene
102-96-5

(2-nitroethenyl)benzene

para-methoxyphenyldiazonium chloride
4346-59-2

para-methoxyphenyldiazonium chloride

A

4-(4-methoxyphenylsulfonyl)-1-phenyl-2-nitroethane
56129-62-5

4-(4-methoxyphenylsulfonyl)-1-phenyl-2-nitroethane

B

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
With sulfur dioxide In acetic acid; acetoneA 30%
B n/a
nitrostyrene
5153-67-3

nitrostyrene

para-methoxyphenyldiazonium chloride
4346-59-2

para-methoxyphenyldiazonium chloride

A

4-(4-methoxyphenylsulfonyl)-1-phenyl-2-nitroethane
56129-62-5

4-(4-methoxyphenylsulfonyl)-1-phenyl-2-nitroethane

B

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
With sulfur dioxide In acetic acid; acetone at 15 - 20℃;A 30%
B n/a
phenylchlorosulfate
16475-29-9

phenylchlorosulfate

4-methoxyphenylboronic acid
5720-07-0

4-methoxyphenylboronic acid

A

4-methoxybenzolsulfonsaeure-phenylester
62141-81-5

4-methoxybenzolsulfonsaeure-phenylester

B

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
With t-BuBrettPhos; palladium diacetate; potassium carbonate In toluene at 75℃; for 12h; Reagent/catalyst; Suzuki-Miyaura Coupling;A 15%
B 22%
para-methoxyphenyldiazonium chloride
4346-59-2

para-methoxyphenyldiazonium chloride

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
With sulfur dioxide; copper(l) chloride
1-bromo-4-methoxy-benzene
104-92-7

1-bromo-4-methoxy-benzene

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
Yield given. Multistep reaction;
Stage #1: 1-bromo-4-methoxy-benzene With iodine; magnesium In tetrahydrofuran for 1h; Heating;
Stage #2: With sulfur dioxide In tetrahydrofuran at -40℃; for 0.5h;
Stage #3: With sulfuryl dichloride In tetrahydrofuran at -40 - 20℃;
(p-methoxyphenyl)tri-n-butylstannane
70744-47-7

(p-methoxyphenyl)tri-n-butylstannane

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
With sulfuryl dichloride at 20℃; for 4h;
Trifluoro-acetic acid 4-methoxy-phenylsulfanylmethyl ester

Trifluoro-acetic acid 4-methoxy-phenylsulfanylmethyl ester

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
With chlorine; acetic acid In dichloromethane Yield given;
potassium salt of/the/ p-anisolesulfonic acid

potassium salt of/the/ p-anisolesulfonic acid

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
With phosphorus pentachloride at 100℃;
sodium-<4-methoxy-benzene sulfonate-(1)>

sodium-<4-methoxy-benzene sulfonate-(1)>

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
With phosphorus pentachloride
para-iodoanisole
696-62-8

para-iodoanisole

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: copper(l) iodide; 1,10-Phenanthroline; N-ethyl-N,N-diisopropylamine / toluene / 16 h / Reflux
2: trichloroisocyanuric acid; benzyltrimethylammonium chloride; sodium carbonate / water; acetonitrile / 0.33 h / 0 °C
View Scheme
4-methylphenyl chlorosulfate
772-80-5

4-methylphenyl chlorosulfate

2,6-diisopropylphenyl chlorosulfate
1447963-66-7

2,6-diisopropylphenyl chlorosulfate

4-methoxyphenylboronic acid
5720-07-0

4-methoxyphenylboronic acid

A

p-cresol
106-44-5

p-cresol

B

2,6-diisopropylphenol
2078-54-8

2,6-diisopropylphenol

C

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
Stage #1: 4-methoxyphenylboronic acid With C43H43NO3PPdS; sodium carbonate In [(2)H6]acetone at 20℃; Inert atmosphere; Sealed tube;
Stage #2: 4-methylphenyl chlorosulfate; 2,6-diisopropylphenyl chlorosulfate In [(2)H6]acetone at 50℃; for 10h;
A 43 %Spectr.
B 72 %Spectr.
C 97 %Spectr.
4-methylphenyl chlorosulfate
772-80-5

4-methylphenyl chlorosulfate

4-methoxyphenylboronic acid
5720-07-0

4-methoxyphenylboronic acid

A

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

B

p-tolylboric acid
274251-50-2

p-tolylboric acid

Conditions
ConditionsYield
With C43H43NO3PPdS; sodium carbonate In [(2)H6]acetone at 60℃; for 6h;
4-methoxyphenylboronic acid
5720-07-0

4-methoxyphenylboronic acid

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
With phenylchlorosulfate; C43H43NO3PPdS; sodium carbonate In acetone at 50℃; for 12h; Inert atmosphere;
phenol
108-95-2

phenol

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: potassium hydroxide / methanol / 5 h / 0 - 60 °C / Inert atmosphere
2: dichloromethane / 2 h
View Scheme
Multi-step reaction with 2 steps
1: potassium hydroxide / methanol / 5 h / 0 - 20 °C / Inert atmosphere
2: chlorosulfonic acid / dichloromethane / -5 °C
View Scheme
sodium 4-methoxy-benzenesulfonate
6140-09-6

sodium 4-methoxy-benzenesulfonate

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
With thionyl chloride; N,N-dimethyl-formamide for 4h; Reflux;
sodium p-hydroxybenzenesulfonate
825-90-1

sodium p-hydroxybenzenesulfonate

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium carbonate / methanol / Reflux
2: thionyl chloride; N,N-dimethyl-formamide / 4 h / Reflux
View Scheme
4-methoxybenzene sulfonamide
1129-26-6

4-methoxybenzene sulfonamide

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Conditions
ConditionsYield
With pyrylium tetrafluoroborate; magnesium chloride In tert-butyl alcohol at 60℃; for 3h;
4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

4-methoxybenzenesulfonyl azide
4547-64-2

4-methoxybenzenesulfonyl azide

Conditions
ConditionsYield
With sodium azide In water; acetone at 0 - 20℃; for 11h; Sealed tube;100%
With sodium azide In water; acetone97%
With sodium azide; tributyl methyl phsophonium chloride immobibized on polystyrene matrix In 1,2-dichloro-ethane at 45℃; for 4h;96%
4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

4-methoxybenzenesulfonyl hydrazide
1950-68-1

4-methoxybenzenesulfonyl hydrazide

Conditions
ConditionsYield
With hydrazine hydrate In tetrahydrofuran at 0℃;100%
With hydrazine hydrate In tetrahydrofuran at 5℃; for 0.5h;95%
With hydrazine hydrate In tetrahydrofuran at 5℃; for 0.5h; Cooling with ice;95%
Tr-Trp-OBzl
83595-58-8

Tr-Trp-OBzl

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

Tr-Trp(Mbs)-OBzl
83595-60-2

Tr-Trp(Mbs)-OBzl

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide Ambient temperature; 1.) 2 h, 2.) 15 h;100%
2-Aminobenzyl alcohol
5344-90-1

2-Aminobenzyl alcohol

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

N-(2-hydroxymethylphenyl)-4-methoxybenzenesulfonamide
601481-95-2

N-(2-hydroxymethylphenyl)-4-methoxybenzenesulfonamide

Conditions
ConditionsYield
With pyridine In dichloromethane at 20℃; for 3h;100%
With pyridine In dichloromethane at 20℃;
With pyridine In dichloromethane Reflux;
With pyridine In dichloromethane at 0 - 20℃; for 2h;
With pyridine In dichloromethane at 20℃; for 4h;
3,4,5-triacetoxy-6-[4-(3-amino-pyridin-2-ylamino)-phenoxy]-tetrahydro-pyran-2-carboxylic acid methyl ester
930121-05-4

3,4,5-triacetoxy-6-[4-(3-amino-pyridin-2-ylamino)-phenoxy]-tetrahydro-pyran-2-carboxylic acid methyl ester

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

3,4,5-triacetoxy-6-{4-[3-(4-methoxy-benzenesulfonylamino)-pyridin-2-ylamino]-phenoxy}-tetrahydro-pyran-2-carboxylic acid methyl ester
930121-03-2

3,4,5-triacetoxy-6-{4-[3-(4-methoxy-benzenesulfonylamino)-pyridin-2-ylamino]-phenoxy}-tetrahydro-pyran-2-carboxylic acid methyl ester

Conditions
ConditionsYield
With pyridine100%
4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

1-amino-2-propene
107-11-9

1-amino-2-propene

N-allyl-4-methoxybenzenesulfonamide
34954-40-0

N-allyl-4-methoxybenzenesulfonamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 19h; Inert atmosphere;100%
With triethylamine In dichloromethane at 0 - 20℃;96%
With sodium hydroxide In diethyl ether; water at 20℃; for 5h; Schotten-Baumann reaction;73%
4-(4-aminomethylbenzyl)-nitrobenzene

4-(4-aminomethylbenzyl)-nitrobenzene

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

4-[4-(4-methoxyphenyl)sulfonylaminomethylbenzyl]-nitrobenzene

4-[4-(4-methoxyphenyl)sulfonylaminomethylbenzyl]-nitrobenzene

Conditions
ConditionsYield
With triethylamine In dichloromethane100%
tert-butyl (2S,3R)-3-hydroxy-4-[((S)-5-oxopyrrolidin-2-yl)-methylamino]-1-phenylbutan-2-ylcarbamate
1161026-84-1

tert-butyl (2S,3R)-3-hydroxy-4-[((S)-5-oxopyrrolidin-2-yl)-methylamino]-1-phenylbutan-2-ylcarbamate

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

tert-butyl (2S,3R)-3-hydroxy-4-(4-methoxy-N-(((S)-5-oxopyrrolidin-2-yl)methyl)phenylsulfonamido)-1-phenylbutan-2-ylcarbamate
1053613-59-4

tert-butyl (2S,3R)-3-hydroxy-4-(4-methoxy-N-(((S)-5-oxopyrrolidin-2-yl)methyl)phenylsulfonamido)-1-phenylbutan-2-ylcarbamate

Conditions
ConditionsYield
With sodium hydrogencarbonate In dichloromethane; water for 12h;100%
piperidin-4-one
41661-47-6

piperidin-4-one

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

1-(4-methoxybenzenesulfonyl)-4-piperidone
196085-08-2

1-(4-methoxybenzenesulfonyl)-4-piperidone

Conditions
ConditionsYield
With pyridine at 20℃; for 18h;100%
C21H35NO12

C21H35NO12

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

methyl 2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl-(1->4)-6-deoxy-6-(4-methoxyphenylsulfonylamino)-2,3-di-O-methyl-α-D-galactopyranoside
1356387-27-3

methyl 2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl-(1->4)-6-deoxy-6-(4-methoxyphenylsulfonylamino)-2,3-di-O-methyl-α-D-galactopyranoside

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere;100%
2-(1,1-dimethylethyl)-benzenamine
6310-21-0

2-(1,1-dimethylethyl)-benzenamine

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

N-(2-(tert-butyl)phenyl)-4-methoxybenzenesulfonamide

N-(2-(tert-butyl)phenyl)-4-methoxybenzenesulfonamide

Conditions
ConditionsYield
With pyridine In dichloromethane at 0 - 20℃; for 18h; Inert atmosphere;100%
4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

sodium 4-methoxybenzenesulfinate
6462-50-6

sodium 4-methoxybenzenesulfinate

Conditions
ConditionsYield
With sodium hydrogencarbonate; sodium sulfite In tetrahydrofuran; water at 0 - 20℃;99.9%
With sodium hydrogencarbonate; sodium sulfite In water at 80℃; for 4h;92%
With sodium hydrogencarbonate; sodium sulfite In water at 80℃; for 4h;92%
m-Anisidine
536-90-3

m-Anisidine

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

4-methoxy-N-(3-methoxyphenyl)benzenesulfonamide
169945-40-8

4-methoxy-N-(3-methoxyphenyl)benzenesulfonamide

Conditions
ConditionsYield
Stage #1: m-Anisidine With pyridine In dichloromethane for 0.166667h;
Stage #2: 4-methoxy-phenyl-sulphonyl chloride In dichloromethane for 0.25h;
99.6%
2.50 g (99.7%)
In dichloromethane at 20℃; for 3h; Inert atmosphere;
piperazine
110-85-0

piperazine

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

1‐(4‐methoxyphenylsulfonyl)piperazine
121751-67-5

1‐(4‐methoxyphenylsulfonyl)piperazine

Conditions
ConditionsYield
In dichloromethane at 0℃;99%
In dichloromethane at 0 - 20℃;96%
Stage #1: piperazine; 4-methoxy-phenyl-sulphonyl chloride With pyridine In dichloromethane at 20℃; for 15h;
Stage #2: With hydrogenchloride In water
88%
2-phenylethynylaniline
13141-38-3

2-phenylethynylaniline

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

4-methoxy-N-(2-(phenylethynyl)phenyl)benzenesulfonamide
946161-94-0

4-methoxy-N-(2-(phenylethynyl)phenyl)benzenesulfonamide

Conditions
ConditionsYield
With pyridine In dichloromethane at 20℃; for 19.5h;99%
With pyridine In dichloromethane at 0 - 20℃;
With pyridine In chloroform at 20℃;
With pyridine In dichloromethane at 0 - 25℃; for 72h; Inert atmosphere; Schlenk technique;0.96 g
3-methyl-1-[3-(4-methylbenzyl)-[1,2,4]thiadiazol-5-yl]piperazine
854539-15-4

3-methyl-1-[3-(4-methylbenzyl)-[1,2,4]thiadiazol-5-yl]piperazine

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

1-[4-methoxyphenylsulfonyl]-4-[3-(4-methylbenzyl)-1,2,4-thiadiazol-5-yl]-2-methylpiperazine

1-[4-methoxyphenylsulfonyl]-4-[3-(4-methylbenzyl)-1,2,4-thiadiazol-5-yl]-2-methylpiperazine

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 4h;99%
With triethylamine In dichloromethane at 20℃; for 4h;99%
3-acetylindole
703-80-0

3-acetylindole

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

3-acetyl-1-((4-methoxyphenyl)sulfonyl)indole

3-acetyl-1-((4-methoxyphenyl)sulfonyl)indole

Conditions
ConditionsYield
Stage #1: 3-acetylindole With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.5h; Inert atmosphere;
Stage #2: 4-methoxy-phenyl-sulphonyl chloride In N,N-dimethyl-formamide at 20℃; Inert atmosphere; Cooling with ice;
99%
With potassium carbonate In acetone at 20℃; for 12h; Inert atmosphere;
1-(1H-indol-3-yl)hexan-1-one
42925-75-7

1-(1H-indol-3-yl)hexan-1-one

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

C21H23NO4S
1352537-20-2

C21H23NO4S

Conditions
ConditionsYield
Stage #1: 1-(1H-indol-3-yl)hexan-1-one With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.5h; Inert atmosphere;
Stage #2: 4-methoxy-phenyl-sulphonyl chloride In N,N-dimethyl-formamide at 20℃; Inert atmosphere; Cooling with ice;
99%
1-(1H-indol-3-yl)pentan-1-one
42925-74-6

1-(1H-indol-3-yl)pentan-1-one

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

C20H21NO4S
1352537-18-8

C20H21NO4S

Conditions
ConditionsYield
Stage #1: 1-(1H-indol-3-yl)pentan-1-one With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.5h; Inert atmosphere;
Stage #2: 4-methoxy-phenyl-sulphonyl chloride In N,N-dimethyl-formamide at 20℃; Inert atmosphere; Cooling with ice;
99%
7-benzyloxy-5-bromoindoline

7-benzyloxy-5-bromoindoline

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

7-benzyloxy-5-bromo-1-(4-methoxyphenylsulfonyl)indoline

7-benzyloxy-5-bromo-1-(4-methoxyphenylsulfonyl)indoline

Conditions
ConditionsYield
With pyridine at 95℃; Inert atmosphere;99%
C12H19N3O4

C12H19N3O4

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

C19H25N3O7S

C19H25N3O7S

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 16h;99%
4-tert-Butylaniline
769-92-6

4-tert-Butylaniline

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

N-(4-(tert-butyl)phenyl)-4-methoxybenzenesulfonamide

N-(4-(tert-butyl)phenyl)-4-methoxybenzenesulfonamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 16h; Inert atmosphere;99%
2-bromobenzylamine
3959-05-5

2-bromobenzylamine

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

N-(2-bromobenzyl)-4-methoxybenzenesulfonamide

N-(2-bromobenzyl)-4-methoxybenzenesulfonamide

Conditions
ConditionsYield
With pyridine at 90℃; Inert atmosphere;99%
D-Ser(O-t-Bu) methyl ester hydrochloride
78537-14-1

D-Ser(O-t-Bu) methyl ester hydrochloride

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

C15H23NO6S

C15H23NO6S

Conditions
ConditionsYield
Stage #1: D-Ser(O-t-Bu) methyl ester hydrochloride With triethylamine In dichloromethane at 0 - 20℃; for 0.5h;
Stage #2: 4-methoxy-phenyl-sulphonyl chloride In dichloromethane at 0 - 20℃; for 4h;
99%
Stage #1: D-Ser(O-t-Bu) methyl ester hydrochloride With triethylamine In dichloromethane at 0 - 20℃; for 0.5h;
Stage #2: 4-methoxy-phenyl-sulphonyl chloride With dmap In dichloromethane at 0 - 20℃; for 4h;
99%
glycine tert-butyl ester hydrochloride
27532-96-3

glycine tert-butyl ester hydrochloride

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

tert-butyl ((4-methoxyphenyl)sulfonyl)glycinate

tert-butyl ((4-methoxyphenyl)sulfonyl)glycinate

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 16h; Inert atmosphere;99%
With pyridine at 20℃; for 4h;54%
6-((4S,5S)-4,5-diphenyl-4,5-dihydro-1H-imidazol-2-yl)-2,2′-bipyridine

6-((4S,5S)-4,5-diphenyl-4,5-dihydro-1H-imidazol-2-yl)-2,2′-bipyridine

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

6-((4S,5S)-1-((4-methoxyphenyl)sulfonyl)-4,5-diphenyl-4,5-dihydro-1H-imidazol-2-yl)-2,2′-bipyridine

6-((4S,5S)-1-((4-methoxyphenyl)sulfonyl)-4,5-diphenyl-4,5-dihydro-1H-imidazol-2-yl)-2,2′-bipyridine

Conditions
ConditionsYield
With dmap In dichloromethane at 0℃; for 4h; Schlenk technique;99%
4-((4-methoxyphenyl)ethynyl)naphthalen-1-amine

4-((4-methoxyphenyl)ethynyl)naphthalen-1-amine

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

4-methoxy-N-(4-((4-methoxyphenyl)ethynyl)naphthalen-1-yl)benzenesulfonamide

4-methoxy-N-(4-((4-methoxyphenyl)ethynyl)naphthalen-1-yl)benzenesulfonamide

Conditions
ConditionsYield
With pyridine Sealed tube;99%
With pyridine at 20℃; for 18h;99%
(R)-N-(5,6-dimethoxybenzo[d]thiazol-2-yl)pyrrolidine-2-carboxamide hydrochloride

(R)-N-(5,6-dimethoxybenzo[d]thiazol-2-yl)pyrrolidine-2-carboxamide hydrochloride

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

(R)-N-(5,6-dimethoxybenzo[d] thiazol-2-yl)-1-((4-methoxyphenyl)sulfonyl)pyrrolidine-2-carboxamide

(R)-N-(5,6-dimethoxybenzo[d] thiazol-2-yl)-1-((4-methoxyphenyl)sulfonyl)pyrrolidine-2-carboxamide

Conditions
ConditionsYield
With pyridine In acetonitrile for 14h;99%
methyl (R,E)-4-(3-amino-1-benzyl-5-bromo-2-oxoindolin-3-yl)but-2-enoate

methyl (R,E)-4-(3-amino-1-benzyl-5-bromo-2-oxoindolin-3-yl)but-2-enoate

4-methoxy-phenyl-sulphonyl chloride
98-68-0

4-methoxy-phenyl-sulphonyl chloride

methyl (R,E)-4-[1-benzyl-5-bromo-3-(4-methoxybenzenesulfonamide)-2-oxoindolin-3-yl]but-2-enoate

methyl (R,E)-4-[1-benzyl-5-bromo-3-(4-methoxybenzenesulfonamide)-2-oxoindolin-3-yl]but-2-enoate

Conditions
ConditionsYield
With pyridine In chloroform at 0 - 20℃; for 26h; Inert atmosphere;99%

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