As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryProduct Name: 4-Methoxybenzenesulfonyl chloride Synonyms: 4-Methoxybenzenesulfonylchlorid;Benzenesulfonyl chloride, p-methoxy-;p-Anisylsulfonyl chloride;p-Methoxyphenylsulfonyl chloride;P-ANISOLESULFONYL CH
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inquiry1. Best prices with satisfied quality; 2. It's clients' right to choose the package's Courier (EMS, DHL, FedEx, UPS); 3.It's clients' right to choose the packing way for his produccts from many recent effective packing ways;
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inquiryAppearance:White to beige?Crystalline Solid Storage:2-8°C Package:25kg/drum Application:4-Methoxybenzenesulfonyl chloride is used as an anti-HIV as Pharmaceutical Intermediates. It also acts as protecting group agent for various nitrogen functions.
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inquiry1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We have s
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inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and als
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:98-68-0
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inquirySuperior quality, moderate price & quick delivery. Appearance:White crystal Storage:Store in a cool, ventilated, dry warehouse, Package:25kg/drum, or as per your request. Application:For medicine , pesticide intermediates Transportation:as
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inquiryProduct name: 4-Methyoxybenzenesulfonyl Chloride CAS No.: 98-68-0 Molecule Formula:C7H7ClO3S Molecule Weight:206.65 Purity: 99.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryProduct Name: 4-Methoxybenzenesulfonyl chloride CAS: 98-68-0 MF: C7H7ClO3S MW: 206.65 EINECS: 202-692-1 Mol File: 98-68-0.mol 4-Methoxybenzenesulfonyl chloride Structure 4-Methoxybenzenesulfonyl chloride Chemical Properties Meltin
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
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inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiryConditions | Yield |
---|---|
With N,N,N',N'-tetrachlorobenzene-1,3-disulphonamide; tetrabutyl-ammonium chloride; water In acetonitrile at 0 - 20℃; for 0.333333h; | 99% |
With trichloroisocyanuric acid; water In acetonitrile at 0 - 20℃; for 0.333333h; | 99% |
With thionyl chloride; dihydrogen peroxide In water; acetonitrile at 25℃; for 0.0166667h; | 98% |
4-methoxy-phenyl-sulphonyl chloride
Conditions | Yield |
---|---|
With hydrogenchloride; N-chloro-succinimide In acetonitrile at 10℃; | 98.1% |
S-(4-methoxyphenyl) ethanethioate
4-methoxy-phenyl-sulphonyl chloride
Conditions | Yield |
---|---|
With hydrogenchloride; N-chloro-succinimide In acetonitrile at 10℃; | 97.7% |
Conditions | Yield |
---|---|
With dihydrogen peroxide; zirconium(IV) chloride In water; acetonitrile at 25℃; for 0.0166667h; | 96% |
With dihydrogen peroxide; trichlorophosphate In water at 25℃; for 0.5h; Micellar solution; | 95% |
With 1,3-dichloro-5,5-dimethylhydantoin; acetic acid In dichloromethane; water at 0 - 20℃; Inert atmosphere; | 92% |
Conditions | Yield |
---|---|
With 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; potassium chloride at 25℃; for 0.0333333h; Neat (no solvent); | 94% |
Conditions | Yield |
---|---|
With sulfuryl dichloride; sulfuric acid In N,N-dimethyl-formamide | 88% |
With chlorosulfonic acid at 0 - 5℃; | 71.32% |
With chlorosulfonic acid at 0 - 5℃; | 71.42% |
1-benzylsulfanyl-4-methoxy-benzene
4-methoxy-phenyl-sulphonyl chloride
Conditions | Yield |
---|---|
With 1,3-dichloro-5,5-dimethylhydantoin; acetic acid In dichloromethane; water at 0 - 5℃; Inert atmosphere; | 86% |
S-4-methoxyphenyl benzothioate
4-methoxy-phenyl-sulphonyl chloride
Conditions | Yield |
---|---|
With trichloroisocyanuric acid; benzyltrimethylammonium chloride; sodium carbonate In water; acetonitrile at 0℃; for 0.333333h; | 81% |
Conditions | Yield |
---|---|
With thionyl chloride; tris(bipyridine)ruthenium(II) dichloride hexahydrate In water; acetonitrile at 20℃; for 20h; Concentration; Sealed tube; Irradiation; | 71% |
Conditions | Yield |
---|---|
With N-chloro-succinimide In water; acetonitrile at 35℃; for 0.25h; | A 70% B 27% |
Conditions | Yield |
---|---|
Stage #1: 4-methoxy-aniline With tris(bipyridine)ruthenium(II) dichloride hexahydrate; isopentyl nitrite In acetonitrile at 20℃; for 0.0833333h; Sealed tube; Stage #2: With thionyl chloride In water; acetonitrile at 20℃; for 20h; Irradiation; | 63% |
Stage #1: 4-methoxy-aniline With hydrogenchloride; acetic acid Stage #2: With sodium nitrite In water at -10 - -5℃; for 0.75h; Stage #3: With hydrogenchloride; sulfur dioxide; acetic acid; copper(l) chloride In water at 10℃; for 0.5h; | 27% |
With tert.-butylnitrite; sulfur dioxide; N-benzyl-N,N,N-triethylammonium chloride; ethylene glycol; copper dichloride In dichloromethane; acetonitrile at 0 - 20℃; Automated synthesizer; | |
Stage #1: 4-methoxy-aniline With tetrafluoroboric acid; tert.-butylnitrite In ethanol; water at 0 - 20℃; for 1h; Stage #2: With 6,6'-dimethyl-2,2'-bipyridine; 1,4-diazabicyclo [2.2.2] octane-1,4-diium-1,4-disulfinate; potassium chloride; copper dichloride In acetonitrile at 20℃; for 12h; Sealed tube; Inert atmosphere; | 50 mg |
Conditions | Yield |
---|---|
In dichloromethane for 2h; | 60% |
(2-nitroethenyl)benzene
para-methoxyphenyldiazonium chloride
A
4-(4-methoxyphenylsulfonyl)-1-phenyl-2-nitroethane
B
4-methoxy-phenyl-sulphonyl chloride
Conditions | Yield |
---|---|
With sulfur dioxide In acetic acid; acetone | A 30% B n/a |
nitrostyrene
para-methoxyphenyldiazonium chloride
A
4-(4-methoxyphenylsulfonyl)-1-phenyl-2-nitroethane
B
4-methoxy-phenyl-sulphonyl chloride
Conditions | Yield |
---|---|
With sulfur dioxide In acetic acid; acetone at 15 - 20℃; | A 30% B n/a |
phenylchlorosulfate
4-methoxyphenylboronic acid
A
4-methoxybenzolsulfonsaeure-phenylester
B
4-methoxy-phenyl-sulphonyl chloride
Conditions | Yield |
---|---|
With t-BuBrettPhos; palladium diacetate; potassium carbonate In toluene at 75℃; for 12h; Reagent/catalyst; Suzuki-Miyaura Coupling; | A 15% B 22% |
Conditions | Yield |
---|---|
With sulfur dioxide; copper(l) chloride |
Conditions | Yield |
---|---|
Yield given. Multistep reaction; | |
Stage #1: 1-bromo-4-methoxy-benzene With iodine; magnesium In tetrahydrofuran for 1h; Heating; Stage #2: With sulfur dioxide In tetrahydrofuran at -40℃; for 0.5h; Stage #3: With sulfuryl dichloride In tetrahydrofuran at -40 - 20℃; |
(p-methoxyphenyl)tri-n-butylstannane
4-methoxy-phenyl-sulphonyl chloride
Conditions | Yield |
---|---|
With sulfuryl dichloride at 20℃; for 4h; |
4-methoxy-phenyl-sulphonyl chloride
Conditions | Yield |
---|---|
With chlorine; acetic acid In dichloromethane Yield given; |
4-methoxy-phenyl-sulphonyl chloride
Conditions | Yield |
---|---|
With phosphorus pentachloride at 100℃; |
4-methoxy-phenyl-sulphonyl chloride
Conditions | Yield |
---|---|
With phosphorus pentachloride |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: copper(l) iodide; 1,10-Phenanthroline; N-ethyl-N,N-diisopropylamine / toluene / 16 h / Reflux 2: trichloroisocyanuric acid; benzyltrimethylammonium chloride; sodium carbonate / water; acetonitrile / 0.33 h / 0 °C View Scheme |
4-methylphenyl chlorosulfate
2,6-diisopropylphenyl chlorosulfate
4-methoxyphenylboronic acid
A
p-cresol
B
2,6-diisopropylphenol
C
4-methoxy-phenyl-sulphonyl chloride
Conditions | Yield |
---|---|
Stage #1: 4-methoxyphenylboronic acid With C43H43NO3PPdS; sodium carbonate In [(2)H6]acetone at 20℃; Inert atmosphere; Sealed tube; Stage #2: 4-methylphenyl chlorosulfate; 2,6-diisopropylphenyl chlorosulfate In [(2)H6]acetone at 50℃; for 10h; | A 43 %Spectr. B 72 %Spectr. C 97 %Spectr. |
4-methylphenyl chlorosulfate
4-methoxyphenylboronic acid
A
4-methoxy-phenyl-sulphonyl chloride
B
p-tolylboric acid
Conditions | Yield |
---|---|
With C43H43NO3PPdS; sodium carbonate In [(2)H6]acetone at 60℃; for 6h; |
Conditions | Yield |
---|---|
With phenylchlorosulfate; C43H43NO3PPdS; sodium carbonate In acetone at 50℃; for 12h; Inert atmosphere; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium hydroxide / methanol / 5 h / 0 - 60 °C / Inert atmosphere 2: dichloromethane / 2 h View Scheme | |
Multi-step reaction with 2 steps 1: potassium hydroxide / methanol / 5 h / 0 - 20 °C / Inert atmosphere 2: chlorosulfonic acid / dichloromethane / -5 °C View Scheme |
Conditions | Yield |
---|---|
With thionyl chloride; N,N-dimethyl-formamide for 4h; Reflux; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium carbonate / methanol / Reflux 2: thionyl chloride; N,N-dimethyl-formamide / 4 h / Reflux View Scheme |
Conditions | Yield |
---|---|
With pyrylium tetrafluoroborate; magnesium chloride In tert-butyl alcohol at 60℃; for 3h; |
Conditions | Yield |
---|---|
With sodium azide In water; acetone at 0 - 20℃; for 11h; Sealed tube; | 100% |
With sodium azide In water; acetone | 97% |
With sodium azide; tributyl methyl phsophonium chloride immobibized on polystyrene matrix In 1,2-dichloro-ethane at 45℃; for 4h; | 96% |
Conditions | Yield |
---|---|
With hydrazine hydrate In tetrahydrofuran at 0℃; | 100% |
With hydrazine hydrate In tetrahydrofuran at 5℃; for 0.5h; | 95% |
With hydrazine hydrate In tetrahydrofuran at 5℃; for 0.5h; Cooling with ice; | 95% |
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide Ambient temperature; 1.) 2 h, 2.) 15 h; | 100% |
2-Aminobenzyl alcohol
4-methoxy-phenyl-sulphonyl chloride
N-(2-hydroxymethylphenyl)-4-methoxybenzenesulfonamide
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 20℃; for 3h; | 100% |
With pyridine In dichloromethane at 20℃; | |
With pyridine In dichloromethane Reflux; | |
With pyridine In dichloromethane at 0 - 20℃; for 2h; | |
With pyridine In dichloromethane at 20℃; for 4h; |
3,4,5-triacetoxy-6-[4-(3-amino-pyridin-2-ylamino)-phenoxy]-tetrahydro-pyran-2-carboxylic acid methyl ester
4-methoxy-phenyl-sulphonyl chloride
3,4,5-triacetoxy-6-{4-[3-(4-methoxy-benzenesulfonylamino)-pyridin-2-ylamino]-phenoxy}-tetrahydro-pyran-2-carboxylic acid methyl ester
Conditions | Yield |
---|---|
With pyridine | 100% |
4-methoxy-phenyl-sulphonyl chloride
1-amino-2-propene
N-allyl-4-methoxybenzenesulfonamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 19h; Inert atmosphere; | 100% |
With triethylamine In dichloromethane at 0 - 20℃; | 96% |
With sodium hydroxide In diethyl ether; water at 20℃; for 5h; Schotten-Baumann reaction; | 73% |
4-methoxy-phenyl-sulphonyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane | 100% |
tert-butyl (2S,3R)-3-hydroxy-4-[((S)-5-oxopyrrolidin-2-yl)-methylamino]-1-phenylbutan-2-ylcarbamate
4-methoxy-phenyl-sulphonyl chloride
tert-butyl (2S,3R)-3-hydroxy-4-(4-methoxy-N-(((S)-5-oxopyrrolidin-2-yl)methyl)phenylsulfonamido)-1-phenylbutan-2-ylcarbamate
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In dichloromethane; water for 12h; | 100% |
piperidin-4-one
4-methoxy-phenyl-sulphonyl chloride
1-(4-methoxybenzenesulfonyl)-4-piperidone
Conditions | Yield |
---|---|
With pyridine at 20℃; for 18h; | 100% |
4-methoxy-phenyl-sulphonyl chloride
methyl 2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl-(1->4)-6-deoxy-6-(4-methoxyphenylsulfonylamino)-2,3-di-O-methyl-α-D-galactopyranoside
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0 - 20℃; for 18h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate; sodium sulfite In tetrahydrofuran; water at 0 - 20℃; | 99.9% |
With sodium hydrogencarbonate; sodium sulfite In water at 80℃; for 4h; | 92% |
With sodium hydrogencarbonate; sodium sulfite In water at 80℃; for 4h; | 92% |
m-Anisidine
4-methoxy-phenyl-sulphonyl chloride
4-methoxy-N-(3-methoxyphenyl)benzenesulfonamide
Conditions | Yield |
---|---|
Stage #1: m-Anisidine With pyridine In dichloromethane for 0.166667h; Stage #2: 4-methoxy-phenyl-sulphonyl chloride In dichloromethane for 0.25h; | 99.6% |
2.50 g (99.7%) | |
In dichloromethane at 20℃; for 3h; Inert atmosphere; |
piperazine
4-methoxy-phenyl-sulphonyl chloride
1‐(4‐methoxyphenylsulfonyl)piperazine
Conditions | Yield |
---|---|
In dichloromethane at 0℃; | 99% |
In dichloromethane at 0 - 20℃; | 96% |
Stage #1: piperazine; 4-methoxy-phenyl-sulphonyl chloride With pyridine In dichloromethane at 20℃; for 15h; Stage #2: With hydrogenchloride In water | 88% |
2-phenylethynylaniline
4-methoxy-phenyl-sulphonyl chloride
4-methoxy-N-(2-(phenylethynyl)phenyl)benzenesulfonamide
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 20℃; for 19.5h; | 99% |
With pyridine In dichloromethane at 0 - 20℃; | |
With pyridine In chloroform at 20℃; | |
With pyridine In dichloromethane at 0 - 25℃; for 72h; Inert atmosphere; Schlenk technique; | 0.96 g |
3-methyl-1-[3-(4-methylbenzyl)-[1,2,4]thiadiazol-5-yl]piperazine
4-methoxy-phenyl-sulphonyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 4h; | 99% |
With triethylamine In dichloromethane at 20℃; for 4h; | 99% |
Conditions | Yield |
---|---|
Stage #1: 3-acetylindole With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.5h; Inert atmosphere; Stage #2: 4-methoxy-phenyl-sulphonyl chloride In N,N-dimethyl-formamide at 20℃; Inert atmosphere; Cooling with ice; | 99% |
With potassium carbonate In acetone at 20℃; for 12h; Inert atmosphere; |
1-(1H-indol-3-yl)hexan-1-one
4-methoxy-phenyl-sulphonyl chloride
C21H23NO4S
Conditions | Yield |
---|---|
Stage #1: 1-(1H-indol-3-yl)hexan-1-one With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.5h; Inert atmosphere; Stage #2: 4-methoxy-phenyl-sulphonyl chloride In N,N-dimethyl-formamide at 20℃; Inert atmosphere; Cooling with ice; | 99% |
1-(1H-indol-3-yl)pentan-1-one
4-methoxy-phenyl-sulphonyl chloride
C20H21NO4S
Conditions | Yield |
---|---|
Stage #1: 1-(1H-indol-3-yl)pentan-1-one With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.5h; Inert atmosphere; Stage #2: 4-methoxy-phenyl-sulphonyl chloride In N,N-dimethyl-formamide at 20℃; Inert atmosphere; Cooling with ice; | 99% |
4-methoxy-phenyl-sulphonyl chloride
Conditions | Yield |
---|---|
With pyridine at 95℃; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 16h; | 99% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 16h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With pyridine at 90℃; Inert atmosphere; | 99% |
D-Ser(O-t-Bu) methyl ester hydrochloride
4-methoxy-phenyl-sulphonyl chloride
Conditions | Yield |
---|---|
Stage #1: D-Ser(O-t-Bu) methyl ester hydrochloride With triethylamine In dichloromethane at 0 - 20℃; for 0.5h; Stage #2: 4-methoxy-phenyl-sulphonyl chloride In dichloromethane at 0 - 20℃; for 4h; | 99% |
Stage #1: D-Ser(O-t-Bu) methyl ester hydrochloride With triethylamine In dichloromethane at 0 - 20℃; for 0.5h; Stage #2: 4-methoxy-phenyl-sulphonyl chloride With dmap In dichloromethane at 0 - 20℃; for 4h; | 99% |
glycine tert-butyl ester hydrochloride
4-methoxy-phenyl-sulphonyl chloride
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 16h; Inert atmosphere; | 99% |
With pyridine at 20℃; for 4h; | 54% |
4-methoxy-phenyl-sulphonyl chloride
Conditions | Yield |
---|---|
With dmap In dichloromethane at 0℃; for 4h; Schlenk technique; | 99% |
4-methoxy-phenyl-sulphonyl chloride
Conditions | Yield |
---|---|
With pyridine Sealed tube; | 99% |
With pyridine at 20℃; for 18h; | 99% |
4-methoxy-phenyl-sulphonyl chloride
Conditions | Yield |
---|---|
With pyridine In acetonitrile for 14h; | 99% |
4-methoxy-phenyl-sulphonyl chloride
Conditions | Yield |
---|---|
With pyridine In chloroform at 0 - 20℃; for 26h; Inert atmosphere; | 99% |
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