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Cas:80-17-1
Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With hydrazine hydrate In chloroform at 0℃; for 2h; | 98% |
With hydrazine hydrate In tetrahydrofuran at -8℃; for 0.5h; | 90% |
With hydrazine hydrate In dichloromethane for 0.25h; | 90% |
N-benzene sulfonyl-N'-carbo-tert-butoxy hydrazine
benzenesufonyl hydrazide
Conditions | Yield |
---|---|
With trifluoroacetic acid for 0.5h; | 84% |
With trifluoroacetic acid for 1h; Ambient temperature; Yield given; |
C13H19N2O2S(1-)*K(1+)
A
2,4-dimethyl-2-pentene
B
benzenesufonyl hydrazide
Conditions | Yield |
---|---|
With Δ In dimethyl sulfoxide at 110℃; Rate constant; Kinetics; Thermodynamic data; other temp.; Ea, ΔH(excit.), ΔS(excit.) ΔG(excit.); | A 42% B 18% |
Conditions | Yield |
---|---|
With hydrazine hydrate |
D-glucose-benzenesulfonylhydrazone
water
glucose
B
benzenesufonyl hydrazide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylamine / acetonitrile / 0.01 h / 20 °C / Sonication 2: hydrazine hydrate / 0.02 h / Sonication View Scheme |
benzenesulfonic acid imidazolide
benzenesufonyl hydrazide
Conditions | Yield |
---|---|
With hydrazine hydrate for 0.0166667h; Sonication; |
7,7-dideuteriobicyclo<3.2.0>hept-2-en-6-one
benzenesufonyl hydrazide
Conditions | Yield |
---|---|
In methanol for 0.166667h; Heating; | 100% |
Tricyclo[4.4.4.01,6]tetradeca-4,7,13-triene-3,9,12-trione
benzenesufonyl hydrazide
C32H30N6O6S3
Conditions | Yield |
---|---|
With hydrogenchloride In methanol for 144h; Ambient temperature; | 100% |
Tricyclo[4.4.4.01,6]tetradeca-4,9,13-triene-3,8,12-trione
benzenesufonyl hydrazide
C32H30N6O6S3
Conditions | Yield |
---|---|
With hydrogenchloride In methanol for 144h; Ambient temperature; | 100% |
Yield given; |
(+)-Daunomycinone
benzenesufonyl hydrazide
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 18h; | 100% |
para-bromobenzenethiol
benzenesufonyl hydrazide
benzenethiosulfonic acid S-(4-bromophenyl) ester
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 25℃; for 8h; | 100% |
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 20℃; for 12h; | 99% |
With ammonium iodide In acetonitrile at 20℃; for 3h; Electrochemical reaction; | 65% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 25℃; for 10h; | 100% |
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 20℃; for 12h; | 99% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 25℃; | 100% |
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 20℃; for 12h; | 99% |
With ammonium iodide In acetonitrile at 20℃; for 3h; Electrochemical reaction; | 78% |
benzenesufonyl hydrazide
2-thiocresol
benzenethiosulfonic acid S-o-tolyl ester
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 25℃; for 6h; | 100% |
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 20℃; for 12h; | 99% |
With ammonium iodide In acetonitrile at 20℃; for 3h; Electrochemical reaction; | 75% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 25℃; for 6h; | 100% |
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 20℃; for 12h; | 99% |
With ammonium iodide In acetonitrile at 20℃; for 3h; Electrochemical reaction; | 78% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 25℃; for 12h; | 100% |
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 20℃; for 12h; | 99% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 25℃; for 6h; Reagent/catalyst; Solvent; | 100% |
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 20℃; for 12h; Reagent/catalyst; Solvent; | 99% |
With ammonium iodide In acetonitrile at 20℃; for 3h; Solvent; Reagent/catalyst; Electrochemical reaction; | 82% |
Conditions | Yield |
---|---|
With acetic acid In ethanol Reflux; | 100% |
trifluoronitrosomethane
benzenesufonyl hydrazide
N-trifluoromethyl-N-hydroxybenzenesulfonamide
Conditions | Yield |
---|---|
In tetrahydrofuran for 1.5h; Product distribution; Ambient temperature; oth. arenesulfonohydrazides, oth. solvent,; | 99% |
(4bR,8aS,9S)-4b-methoxy-7-oxo-4b,7,8,8a,9,10-hexahydrophenanthrene-9-carbaldehyde
benzenesufonyl hydrazide
(E)-N'-(((4bS,8aR,9R)-4b-methoxy-7-oxo-4b,7,8,8a,9,10-hexahydrophenanthrene-9-yl)methylene)benzenesulfonylhydrazide
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 0.25h; | 99% |
ortho-anisaldehyde
benzenesufonyl hydrazide
(E)-N'-(2-methoxybenzylidene)benzenesulfonohydrazide
Conditions | Yield |
---|---|
In ethanol at 20℃; for 1h; | 99% |
In ethanol at 20℃; for 3h; | 51% |
3-(1-naphthyl)propiolic acid
benzenesufonyl hydrazide
1-phenylethynyl-naphthalene
Conditions | Yield |
---|---|
With palladium(II) trifluoroacetate; 1,3-bis-(diphenylphosphino)propane; copper diacetate In N,N-dimethyl-formamide at 100℃; for 0.5h; | 99% |
p-Chlorothiophenol
benzenesufonyl hydrazide
S-(4-chlorophenyl)benzene thiosulfonate
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 20℃; for 12h; | 99% |
With ammonium iodide In acetonitrile at 20℃; for 3h; Electrochemical reaction; | 72% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 20℃; for 12h; | 99% |
With ammonium iodide In acetonitrile at 20℃; for 3h; Electrochemical reaction; | 70% |
4-Methoxybenzenethiol
benzenesufonyl hydrazide
benzenethiosulfonic acid S-(4-methoxyphenyl) ester
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 20℃; for 12h; | 99% |
With ammonium iodide In acetonitrile at 20℃; for 3h; Electrochemical reaction; | 85% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 20℃; for 12h; | 99% |
With ammonium iodide In acetonitrile at 20℃; for 3h; Electrochemical reaction; | 78% |
3-methoxybenzenethiol
benzenesufonyl hydrazide
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 20℃; for 12h; | 99% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 20℃; for 12h; | 99% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 20℃; for 12h; | 99% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 20℃; for 12h; | 99% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 20℃; for 12h; | 99% |
2-fluorothiophenol
benzenesufonyl hydrazide
S-(2-fluorophenyl) benzenesulfonothioate
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 20℃; for 12h; | 99% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; sodium iodide In acetonitrile at 20℃; for 12h; | 99% |
Conditions | Yield |
---|---|
In ethanol at 20℃; for 1h; | 99% |
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; propylene glycol dimethyl ether dimer at 100℃; for 12h; Schlenk technique; | 99% |
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