1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:864070-18-8
Min.Order:1 Gram
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap
Cas:864070-18-8
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inquiryHigh quality. Factory supply. In stock. Best price.1.Quick response within 24 hours;2.Best quality in your requirement;?3.We pay more attention on delivery time, and usually ship on time;4.Under the premise of safety and effectiveness, we can produce
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:864070-18-8
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Type:Manufacturers
inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/1065.html Product Name 4-[(5-Bromo-2-chlorophenyl)methyl]phenol CAS No.
Cas:864070-18-8
Min.Order:1 Gram
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:864070-18-8
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Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:864070-18-8
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inquiryProduct name: 4-(5-Bromo-2-chlorobenzyl)phenol CAS: 864070-18-8 Molecular formula: C13H10BrCIO Molecular weight: 297.5749 Appearance: white powder Storage:Store in cool and dry place, away from sun light. Package: 25kgs/drum Application: APIs
Cas:864070-18-8
Min.Order:1 Kilogram
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Type:Other
inquiry4-[(5-Bromo-2-chlorophenyl)methyl]phenol Cas No.:864070-18-8 HANGZHOU THINK CHEMICAL CO., LTD. (THINKCHEM) is an integrative corporation of trade, research and contract manufacture. With about ten years of business experiences on the marke
Cas:864070-18-8
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Type:Other
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:864070-18-8
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the
Cas:864070-18-8
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:864070-18-8
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryAppearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:As
Cas:864070-18-8
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:864070-18-8
Min.Order:0 Metric Ton
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Type:Lab/Research institutions
inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:864070-18-8
Min.Order:1 Gram
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inquiryProduct Name: 4-(5-broMo-2-chlorobenzyl)phenol Synonyms: 4-(5-broMo-2-chlorobenzyl)phenol;4-[(5-bromo-2-chlorophenyl)methyl]-Phenol;Phenol, 4-[(5-bromo-2-chlorophenyl)methyl]- CAS: 864070-18-8 MF: C13
Cas:864070-18-8
Min.Order:1 Metric Ton
FOB Price: $20.0
Type:Lab/Research institutions
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:864070-18-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
Cas:864070-18-8
Min.Order:0
Negotiable
Type:Trading Company
inquiryProduct name: 4-[(5-Bromo-2-Chlorophenyl)Methyl]Phenol CAS No.: 864070-18-8 Molecule Formula:C13H10BrClO Molecule Weight:297.57 Purity: 99.0% Package: 25kg/drum Description:White or light yellow crystalline powder Manufacture Standard
Cas:864070-18-8
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:864070-18-8
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiry4-(5-broMo-2-chlorobenzyl)phenol is one of the most competitive products in our company. We can supply it with good quality and best price. Storage:Inert atmosphere,Room Temperature Package:Kilograms/MT Application:Pharmaceutical field Transportati
Cas:864070-18-8
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquirySAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
Cas:864070-18-8
Min.Order:0
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Type:Lab/Research institutions
inquirylow price high quality high purity good sevice stock Storage:Preserve In Well-Closed, Light-Resistant and Tight Containers. Store In Cool & Dry Place Package:1g、5g、10g…1kg、5kg… Application:Pharmaceutical intermediates Transportation:by lan
Cas:864070-18-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryUsed in organic synthesis and pharmaceutical intermediates Appearance:White powder Storage:Stored in the ventilated, low temperature and dry room away from direct sunlight. Package:200kg/drum Application:Used in organic synthesis and pharmaceutical
Cas:864070-18-8
Min.Order:1 Metric Ton
Negotiable
Type:Manufacturers
inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
Cas:864070-18-8
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryGOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:864070-18-8
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Trading Company
inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:864070-18-8
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryWhy is SINOWAY: 1) Specialized in pharmaceutical and healthcare industrial for 37 years. 2) ISO 9001:2015 & SGS audited supplier . 3) Accept various payment terms : T.T 30-60 days. 4) We have warehouse in USA with quickly shipment . 5) We c
Cas:864070-18-8
Min.Order:0 Kilogram
Negotiable
Type:Trading Company
inquiry4-bromo-1-chloro-2-[(4-ethoxyphenyl)methyl]benzene
4-(5-bromo-2-chlorobenzyl)phenol
Conditions | Yield |
---|---|
With boron tribromide; sodium hydrogencarbonate In dichloromethane at 20 - 30℃; for 0.5h; Inert atmosphere; | 100% |
Stage #1: 4-bromo-1-chloro-2-[(4-ethoxyphenyl)methyl]benzene With boron trichloride In dichloromethane at 0℃; for 0.5h; Inert atmosphere; Stage #2: With boron tribromide In dichloromethane at 0℃; | 98% |
With boron tribromide In dichloromethane for 1h; | 95% |
4-(5-bromo-2-chlorobenzyl)phenol
Conditions | Yield |
---|---|
Stage #1: 4-bromo-1-chloro-2-(4-methoxybenzyl)benzene With boron tribromide In dichloromethane at 20℃; for 2h; Stage #2: With potassium carbonate In dichloromethane; water at 20℃; Stage #3: With hydrogenchloride In dichloromethane; water pH=1; | 98% |
Stage #1: 4-bromo-1-chloro-2-(4-methoxybenzyl)benzene With boron tribromide In dichloromethane at 0 - 20℃; for 2h; Stage #2: With potassium carbonate In dichloromethane at 0℃; Stage #3: With hydrogenchloride In dichloromethane; water at 20℃; pH=1; | 98% |
Stage #1: 4-bromo-1-chloro-2-(4-methoxybenzyl)benzene With boron tribromide In dichloromethane at 0 - 20℃; for 2h; Stage #2: With water; potassium carbonate In dichloromethane at 0℃; | 98% |
(5-bromo-2-chlorophenyl)(4-hydroxyphenyl)methanone
4-(5-bromo-2-chlorobenzyl)phenol
Conditions | Yield |
---|---|
With triethylsilane; boron trifluoride diethyl etherate In diethyl ether; dichloromethane; acetonitrile at 20℃; for 16h; Inert atmosphere; | 94.8% |
5-bromo-2-chlorobenzoic acid
4-(5-bromo-2-chlorobenzyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 20 °C 2: aluminum (III) chloride / dichloromethane / 1 h / -5 - 0 °C 3: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / -20 - 20 °C 4: boron tribromide / dichloromethane / 25 h / -78 - 20 °C View Scheme | |
Multi-step reaction with 4 steps 1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 10 h / 20 °C 2.1: aluminum (III) chloride / dichloromethane / 1 h / -5 - 20 °C / Inert atmosphere 2.2: 2 h / -5 - 0 °C / Inert atmosphere 3.1: aluminum (III) chloride; sodium tetrahydroborate / tetrahydrofuran / 18 h / 5 - 20 °C / Inert atmosphere 4.1: boron tribromide / dichloromethane / -10 - 0 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 0 - 20 °C 2.1: aluminum (III) chloride / dichloromethane / 0.33 h / -5 °C / Inert atmosphere 2.2: 3 h / -5 °C / Inert atmosphere 3.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / 2.33 h / 0 - 20 °C / Inert atmosphere 4.1: boron tribromide / dichloromethane / 2 h / -78 - 20 °C / Inert atmosphere; Darkness View Scheme |
phenol
4-(5-bromo-2-chlorobenzyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: potassium carbonate / acetone / 0.5 h / 20 °C 1.2: 3 h / Reflux 2.1: aluminum (III) chloride / dichloromethane / 1 h / 0 °C 3.1: aluminum (III) chloride / dichloromethane / 12 h / 20 °C / Inert atmosphere 4.1: triethylsilane; boron trifluoride diethyl etherate / diethyl ether; dichloromethane; acetonitrile / 16 h / 20 °C / Inert atmosphere View Scheme |
5-bromo-2-chloro-benzoyl chloride
4-(5-bromo-2-chlorobenzyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: aluminum (III) chloride / dichloromethane / 1 h / -5 - 0 °C 2: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / -20 - 20 °C 3: boron tribromide / dichloromethane / 25 h / -78 - 20 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: aluminum (III) chloride / dichloromethane / 1 h / -5 - 20 °C / Inert atmosphere 1.2: 2 h / -5 - 0 °C / Inert atmosphere 2.1: aluminum (III) chloride; sodium tetrahydroborate / tetrahydrofuran / 18 h / 5 - 20 °C / Inert atmosphere 3.1: boron tribromide / dichloromethane / -10 - 0 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1.1: aluminum (III) chloride / dichloromethane / 0.33 h / -5 °C / Inert atmosphere 1.2: 3 h / -5 °C / Inert atmosphere 2.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / 2.33 h / 0 - 20 °C / Inert atmosphere 3.1: boron tribromide / dichloromethane / 2 h / -78 - 20 °C / Inert atmosphere; Darkness View Scheme |
(5-bromo-2-chlorophenyl)(4-ethyloxyphenyl)methanone
4-(5-bromo-2-chlorobenzyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / -20 - 20 °C 2: boron tribromide / dichloromethane / 25 h / -78 - 20 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: triethylsilane / acetonitrile / 10 - 15 °C 1.2: 10 - 45 °C 2.1: boron tribromide / dichloromethane / 0 - 5 °C View Scheme | |
Multi-step reaction with 2 steps 1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / 5 - 10 °C 2: boron tribromide / dichloromethane / 1 h View Scheme | |
Multi-step reaction with 2 steps 1: aluminum (III) chloride / dichloromethane / 12 h / 20 °C / Inert atmosphere 2: triethylsilane; boron trifluoride diethyl etherate / diethyl ether; dichloromethane; acetonitrile / 16 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: triethylsilane; trifluorormethanesulfonic acid; trifluoroacetic acid / 20 °C / Reflux 2: boron tribromide / dichloromethane / -78 - 20 °C View Scheme |
Phenetole
4-(5-bromo-2-chlorobenzyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h 1.2: 1 h / 4 - 5 °C 2.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / 5 - 10 °C 3.1: boron tribromide / dichloromethane / 1 h View Scheme | |
Multi-step reaction with 3 steps 1: aluminum (III) chloride / dichloromethane / 1 h / 0 °C 2: aluminum (III) chloride / dichloromethane / 12 h / 20 °C / Inert atmosphere 3: triethylsilane; boron trifluoride diethyl etherate / diethyl ether; dichloromethane; acetonitrile / 16 h / 20 °C / Inert atmosphere View Scheme |
(5-bromo-2-chlorophenyl)(4-methoxyphenyl)methanone
4-(5-bromo-2-chlorobenzyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aluminum (III) chloride; sodium tetrahydroborate / tetrahydrofuran / 18 h / 5 - 20 °C / Inert atmosphere 2: boron tribromide / dichloromethane / -10 - 0 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / 2.33 h / 0 - 20 °C / Inert atmosphere 2: boron tribromide / dichloromethane / 2 h / -78 - 20 °C / Inert atmosphere; Darkness View Scheme | |
Multi-step reaction with 2 steps 1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / 2.33 h / 0 - 20 °C / Inert atmosphere 2: boron tribromide / dichloromethane / 2 h / -78 - 20 °C / Inert atmosphere; Darkness View Scheme |
4-(5-bromo-2-chlorobenzyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: sodium tetrahydroborate; ethanol / 0 - 5 °C 2: 0.5 h 3: hydrogen; palladium on activated charcoal / methanol View Scheme |
4-(5-bromo-2-chlorobenzyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 0.5 h 2: hydrogen; palladium on activated charcoal / methanol View Scheme |
4-(5-bromo-2-chlorobenzyl)phenol
Conditions | Yield |
---|---|
With palladium on activated charcoal; hydrogen In methanol | 2.5 g |
4-(5-bromo-2-chlorobenzyl)phenol
tert-butyldimethylsilyl chloride
[4-(5-bromo-2-chloro-benzyl)-phenoxy]-tert-butyl-dimethyl-silane
Conditions | Yield |
---|---|
With 1H-imidazole; dmap In N,N-dimethyl-formamide at 0℃; | 99% |
With 1H-imidazole In dichloromethane at 25 - 35℃; | 97.54% |
With triethylamine In dichloromethane at 20℃; for 15h; | 97.7% |
4-(5-bromo-2-chlorobenzyl)phenol
d(4)-methanol
4-bromo-1-chloro-2-(4-(methoxy-d3)benzyl)benzene
Conditions | Yield |
---|---|
Stage #1: 4-(5-bromo-2-chlorobenzyl)phenol With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 30℃; for 0.5h; Stage #2: d(4)-methanol In tetrahydrofuran at 30℃; | 99% |
4-(5-bromo-2-chlorobenzyl)phenol
ethyl iodide
4-bromo-1-chloro-2-[(4-ethoxyphenyl)methyl]benzene
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In acetone at 20℃; | 96% |
4-(5-bromo-2-chlorobenzyl)phenol
2-(2,2-difluoroethoxy)ethyl-4-methylbenzenesulfonate
4-bromo-1-chloro-2-(4-(2-(2,2-difluoroethoxy)ethoxy)benzyl)benzene
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 50℃; for 24h; | 91.9% |
4-(5-bromo-2-chlorobenzyl)phenol
methyl-d3 4-methylbenzenesulfonate
4-bromo-1-chloro-2-(4-(methoxy-d3)benzyl)benzene
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 80℃; for 16h; | 91% |
4-(5-bromo-2-chlorobenzyl)phenol
ethanol-d6
4-bromo-1-chloro-2-(4-(ethoxy-d5)benzyl)benzene
Conditions | Yield |
---|---|
Stage #1: 4-(5-bromo-2-chlorobenzyl)phenol With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 30℃; for 0.5h; Stage #2: ethanol-d6 In tetrahydrofuran at 30℃; | 90% |
4-(5-bromo-2-chlorobenzyl)phenol
chloromethyl methyl ether
Conditions | Yield |
---|---|
Stage #1: 4-(5-bromo-2-chlorobenzyl)phenol With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 0.5h; Stage #2: chloromethyl methyl ether In N,N-dimethyl-formamide; mineral oil at 20℃; for 3h; | 90% |
Stage #1: 4-(5-bromo-2-chlorobenzyl)phenol With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 0.5h; Stage #2: chloromethyl methyl ether In N,N-dimethyl-formamide; mineral oil at 20℃; for 3h; | 90% |
4-(5-bromo-2-chlorobenzyl)phenol
allyl bromide
2-(4-(allyloxy)benzyl)-4-bromo-1-chlorobenzene
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 0 - 20℃; for 2h; | 89.6% |
With caesium carbonate In N,N-dimethyl-formamide at 0 - 20℃; for 2h; | 89.6% |
With caesium carbonate In N,N-dimethyl-formamide at 0 - 20℃; for 2h; | 89.6% |
[1-(trifluoromethyl)cyclopropyl]methyl-4-methylbenzene-1-sulfonate
4-(5-bromo-2-chlorobenzyl)phenol
4-bromo-1-chloro-2-(4-((1-(trifluoromethyl)cyclopropyl)methoxy)benzyl)benzene
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 120℃; for 5h; Inert atmosphere; | 88% |
4-(5-bromo-2-chlorobenzyl)phenol
2,2,2-Trifluoroethyl p-toluenesulfonate
4-bromo-1-chloro-2-[[4-(2,2,2-trifluoroethoxy)phenyl]methyl]benzene
Conditions | Yield |
---|---|
Stage #1: 4-(5-bromo-2-chlorobenzyl)phenol With potassium carbonate In N,N-dimethyl-formamide at 90℃; for 0.5h; Inert atmosphere; Stage #2: 2,2,2-Trifluoroethyl p-toluenesulfonate In N,N-dimethyl-formamide at 140℃; for 12h; Inert atmosphere; | 87.2% |
Stage #1: 4-(5-bromo-2-chlorobenzyl)phenol With caesium carbonate In N,N-dimethyl-formamide at 80℃; for 8h; Stage #2: 2,2,2-Trifluoroethyl p-toluenesulfonate In N,N-dimethyl-formamide | 39.2% |
1-bromo-2-propanol
4-(5-bromo-2-chlorobenzyl)phenol
1-(4-(5-bromo-2-chlorobenzyl)phenoxy)propan-2-ol
Conditions | Yield |
---|---|
With caesium carbonate In ISOPROPYLAMIDE at 80℃; | 82% |
4-(5-bromo-2-chlorobenzyl)phenol
2-(cyclopropyloxy)ethyl-4-methylbenzenesulfonate
4-bromo-1-chloro-2-[[4-[2-(cyclopropyloxy)ethoxy]phenyl]methyl]benzene
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 20℃; for 16h; | 81% |
Stage #1: 4-(5-bromo-2-chlorobenzyl)phenol With caesium carbonate In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: 2-(cyclopropyloxy)ethyl-4-methylbenzenesulfonate In N,N-dimethyl-formamide at 20℃; | 64% |
Stage #1: 4-(5-bromo-2-chlorobenzyl)phenol With caesium carbonate In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: 2-(cyclopropyloxy)ethyl-4-methylbenzenesulfonate In N,N-dimethyl-formamide at 20℃; | 64% |
4-(5-bromo-2-chlorobenzyl)phenol
(1-(trifluoromethyl)cyclobutyl)methyl 4-methylbenzenesulfonate
4-bromo-1-chloro-2-(4-((1-(trifluoromethyl)cyclobutyl)methoxy)benzyl)benzene
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 110℃; for 5h; Inert atmosphere; | 79.4% |
4-(5-bromo-2-chlorobenzyl)phenol
ethyl bromoacetate
ethyl 2-(4-(2-chloro-5-bromobenzyl)phenoxy)acetate
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 80℃; | 78% |
4-(5-bromo-2-chlorobenzyl)phenol
(4,4-difluoro-1-methylcyclohexyl)methyl 4-methylbenzenesulfonate
4-bromo-1-chloro-2-(4-((4,4-difluoro-1-methylcyclohexyl)methoxy)benzyl)benzene
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 120℃; for 5h; Inert atmosphere; | 77.9% |
2-iodo-propane
4-(5-bromo-2-chlorobenzyl)phenol
4-bromo-1-chloro-2-(4-isopropoxybenzyl)benzene
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 5h; | 77% |
4-(5-bromo-2-chlorobenzyl)phenol
2-bromoethanol
2-(4-(5-bromo-2-chlorobenzyl)phenoxy)ethanol
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 80℃; | 76% |
Stage #1: 4-(5-bromo-2-chlorobenzyl)phenol With caesium carbonate In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: 2-bromoethanol In N,N-dimethyl-formamide at 80℃; | 76% |
4-(5-bromo-2-chlorobenzyl)phenol
(1-ethylcyclobutyl)methyl 4-methylbenzenesulfonate
4-bromo-l-chloro-2-(4-((1-ethylcyclobutyl)methoxy)benzyl)benzene
Conditions | Yield |
---|---|
caesium carbonate In dichloromethane; N,N-dimethyl-formamide at 120℃; | 75% |
4-(5-bromo-2-chlorobenzyl)phenol
N,N-Dimethylthiocarbamoyl chloride
O-4-(5-bromo-2-chlorobenzyl)phenyl dimethylcarbamothioate
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 20℃; for 18h; Inert atmosphere; | 73% |
4-(5-bromo-2-chlorobenzyl)phenol
benzyl bromide
Conditions | Yield |
---|---|
With potassium carbonate In tetrahydrofuran at 20 - 30℃; for 12h; Inert atmosphere; | 70.4% |
With potassium hydroxide In tetrahydrofuran at 20 - 30℃; for 12h; | 70.4% |
With potassium carbonate In tetrahydrofuran at 20℃; for 12h; |
4-(5-bromo-2-chlorobenzyl)phenol
ethanol-1,1-d2
4-bromo-1-chloro-2-(4-(ethoxy-1,1-d2)benzyl)benzene
Conditions | Yield |
---|---|
Stage #1: 4-(5-bromo-2-chlorobenzyl)phenol With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 30℃; for 0.5h; Stage #2: ethanol-1,1-d2 In tetrahydrofuran at 30℃; | 63% |
4-(5-bromo-2-chlorobenzyl)phenol
(R)-3-Hydroxytetrahydrofuran
(S)-4-bromo-1-chloro-2-(4-tetrahydrofuran-3-yloxy-benzyl)benzene
Conditions | Yield |
---|---|
Stage #1: (R)-3-Hydroxytetrahydrofuran With di-isopropyl azodicarboxylate; triphenylphosphine In dichloromethane at 0 - 20℃; for 0.5h; Stage #2: 4-(5-bromo-2-chlorobenzyl)phenol In dichloromethane at 20℃; for 20h; | 55% |
4-(5-bromo-2-chlorobenzyl)phenol
(1-methylcyclopentyl)methyl 4-methylbenzenesulfonate
4-bromo-1-chloro-2-(4-((1-methylcyclopentyl)methoxy)benzyl)benzene
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 120℃; for 5h; Inert atmosphere; | 53.8% |
4-(5-bromo-2-chlorobenzyl)phenol
(1R,3r,5S)-bicyclo[3.1.0]hexan-3-yl methanesulfonate
Conditions | Yield |
---|---|
With N-benzyl-N,N,N-triethylammonium chloride; caesium carbonate In 1-methyl-pyrrolidin-2-one at 50℃; | 50% |
With N-benzyl-N,N,N-triethylammonium chloride; caesium carbonate In 1-methyl-pyrrolidin-2-one at 20 - 50℃; | 50% |
With N-benzyl-N,N,N-triethylammonium chloride; caesium carbonate In 1-methyl-pyrrolidin-2-one at 20 - 50℃; | 50% |
4-(5-bromo-2-chlorobenzyl)phenol
(1R,3r,5S)-bicyclo[3.1.0]hexan-3-yl methanesulfonate
Conditions | Yield |
---|---|
With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide In water; toluene at 70℃; for 2h; | 27% |
With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide In water; toluene at 70℃; for 2h; | 27% |
With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide In water; toluene at 70℃; for 2h; | 27% |
4-(5-bromo-2-chlorobenzyl)phenol
cyclopentyl iodide
4-bromo-1-chloro-2-(4-cyclopentyloxy-benzyl)-benzene
Conditions | Yield |
---|---|
With caesium carbonate In ethanol at 60℃; |
oxetan-3-yl 4-methylbenzenesulfonate
4-(5-bromo-2-chlorobenzyl)phenol
3-(4-(5-bromo-2-chlorobenzyl)phenoxy)oxetane
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 0 - 120℃; |
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