α-α-α-2,4-PENTACHLOROTOLUENE supplier

Name
2,4-DICHLOROBENZOTRICHLORIDE
EINECS 235-868-1
CAS No. 13014-18-1
Article Data8
CAS DataBase
Density 1.605 g/cm1.605 g/cm3
Solubility Decomposes AUTOIGNITION
Melting Point 47 - 49 C
Formula C7H3 Cl5
Boiling Point 288 C
Molecular Weight 264.366
Flash Point > 112 C
Transport Information 300kgs
Appearance clear liquid
Safety Mutation data reported. When heated to decomposition it emits toxic vapors of Cl⁻.
Risk Codes 34
Molecular Structure
Hazard Symbols 8 (Packing group : II) UN NO.
Synonyms Toluene, a,a,a,2,4-pentachloro- (6CI,7CI,8CI); 1,3-Dichloro-4-(trichloromethyl)benzene;2,4,a,a,a-Pentachlorotoluene; 2,4-Dichloro-1-(trichloromethyl)benzene;2,4-Dichlorobenzotrichloride; 2,4-Dichlorophenyltrichloromethane; NSC 403840; a,a,a,2,4-Pentachlorotoluene
PSA 0.00000
LogP 4.82010

Synthetic route

: 95-73-8
2,4-dichlorotoluene

: 13014-18-1
2,4-dichlorobenzotrichloride

Conditions

Conditions	Yield
at 125℃; UV-Licht; Einleiten von Chlor;
With 2,2'-azobis(isobutyronitrile); chlorine at 95℃; for 7h; Temperature; Sealed tube;	489.8 g
With chlorine at 115 - 117℃; for 20h; Temperature;
With chlorine at 115 - 117℃; for 20h; Temperature;
With CuCl/Cu; chlorine at 115 - 117℃; for 24h; Temperature; Green chemistry;

: 42413-03-6
3-chloro-4-methylbenzenesulfonyl chloride

: 13014-18-1
2,4-dichlorobenzotrichloride

Conditions

Conditions	Yield
With chlorine at 150 - 200℃;

: 13014-18-1
2,4-dichlorobenzotrichloride

: 121-44-8
triethylamine

: 24309-78-2
2,4-dichloro-N,N-diethylbenzamide

Conditions

Conditions	Yield
With B12 complex immobilized on rhodium(III) modified anatase TiO2; air In acetonitrile at 20℃; for 3h; Irradiation;	97%
With heptamethyl Coβ-perchlorato-cob(II)yrinate; tetrabutylammonium perchlorate In acetonitrile at 20℃; for 3h; Electrolysis;	94%

: 67-56-1
methanol

: 13014-18-1
2,4-dichlorobenzotrichloride

: 35112-28-8
methyl 2,4-dichlorobenzoate

Conditions

Conditions	Yield
at 20℃; for 3h; UV-irradiation;	96%

: 13014-18-1
2,4-dichlorobenzotrichloride

: 89-75-8
2,4-dichlorobenzoyl chloride

Conditions

Conditions	Yield
With iron(III) chloride In water at 110℃; for 2h; Temperature;	93.05%

: 13014-18-1
2,4-dichlorobenzotrichloride

: 506-77-4
cyanogen chloride

: 14943-69-2
2,4-dichloro-6-(2,4-dichloro-phenyl)-[1,3,5]triazine

Conditions

Conditions	Yield
In aluminium trichloride	64%

: 106-44-5
p-cresol

: 13014-18-1
2,4-dichlorobenzotrichloride

: 37884-02-9
6-chloro-2-methyl-9H-xanthen-9-one

Conditions

Conditions	Yield
With carbon disulfide; aluminium trichloride

: 13014-18-1
2,4-dichlorobenzotrichloride

: 50-84-0
2,4 dichlorobenzoic acid

Conditions

Conditions	Yield
beim Verseifen;

: 13014-18-1
2,4-dichlorobenzotrichloride

: 545-06-2
trichloroacetonitrile

: 65934-92-1
N-Pentachlorethyl-2,4-dichlorbenzimidoylchlorid

Conditions

Conditions	Yield
With aluminium trichloride

: 13014-18-1
2,4-dichlorobenzotrichloride

: 717-43-1
2,4-Dichlor-5-nitrophenylchloroform

Conditions

Conditions	Yield
With sulfuric acid; nitric acid

: 13014-18-1
2,4-dichlorobenzotrichloride

A: C14H6Cl6

B: C14H6Cl6

Conditions

Conditions	Yield
With tetrakis(triphenylphosphine) palladium(0); 1,1,1,2,2,2-hexamethyldisilane In 1,3,5-trimethyl-benzene at 130℃; for 2h; Yield given. Yields of byproduct given;

: 13014-18-1
2,4-dichlorobenzotrichloride

: 506-77-4
cyanogen chloride

: 65866-99-1
2,4-Dichlor-N-dichlormethylen-N'-trichlormethylbenzamidin

: 7664-39-3
hydrogen fluoride

: 13014-18-1
2,4-dichlorobenzotrichloride

: 320-60-5
2,4-dichloro-benzotrifluoride

Conditions

Conditions	Yield
at 140 - 150℃;
at 140 - 150℃;

: 7664-93-9
sulfuric acid

: 13014-18-1
2,4-dichlorobenzotrichloride

: 19861-62-2
2,4-dichloro-5-nitrobenzoic acid

Conditions

Conditions	Yield
folgend Behandeln mit Nitriersaeure bei 10grad;

: 106-44-5
p-cresol

: 13014-18-1
2,4-dichlorobenzotrichloride

A: 92153-14-5
2,4-dichloro-2'-hydroxy-5'-methyl-benzophenone

B 6,12-bis-<2,4-dichloro-phenyl>-2,8-dimethyl-6H,12H-6,12-epoxido-dibenzo<b,f>dioxocin: 6,12-bis-<2,4-dichloro-phenyl>-2,8-dimethyl-6H,12H-6,12-epoxido-dibenzo<b,f>dioxocin

Conditions

Conditions	Yield
With carbon disulfide; aluminium trichloride Behandeln des erhaltenen Reaktionsprodukts mit H2O;

...Expand

: 13014-18-1
2,4-dichlorobenzotrichloride

: 37884-02-9
6-chloro-2-methyl-9H-xanthen-9-one

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: AlCl3; CS2 / Behandeln des erhaltenen Reaktionsprodukts mit H2O 2: potassium hydroxide; ethylene glycol View Scheme

: 13014-18-1
2,4-dichlorobenzotrichloride

: 713-28-0
2,4-dichloro-5-nitro benzoyl chloride

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: HNO3, H2SO4 2: aq. FeCl3 View Scheme

: 3201-29-4
1,3-dimethylpyrazol-5-one

: 75-34-3
1,1-dichloroethane

: 13014-18-1
2,4-dichlorobenzotrichloride

: 58010-98-3
4-(2,4-dichlorobenzoyl)-1,3-dimethyl-5-hydroxypyrazole

Conditions

Conditions	Yield
With potassium hydroxide; aluminium trichloride In water

...Expand

: 3201-29-4
1,3-dimethylpyrazol-5-one

6 N-HCl: 6 N-HCl

: 75-34-3
1,1-dichloroethane

: 13014-18-1
2,4-dichlorobenzotrichloride

: 58010-98-3
4-(2,4-dichlorobenzoyl)-1,3-dimethyl-5-hydroxypyrazole

Conditions

Conditions	Yield
With sodium hydrogencarbonate; aluminium trichloride

...Expand

: 4344-87-0
1,2-dihydro-5-methyl-3H-pyrazol-3-one

: 13014-18-1
2,4-dichlorobenzotrichloride

: 3-methyl-4-(2,4-dichlorobenzoyl)-5-hydroxypyrazole

Conditions

Conditions	Yield
With hydrogenchloride; aluminium trichloride In 1,1-dichloroethane

: 3201-29-4
1,3-dimethylpyrazol-5-one

: 13014-18-1
2,4-dichlorobenzotrichloride

: 58010-98-3
4-(2,4-dichlorobenzoyl)-1,3-dimethyl-5-hydroxypyrazole

Conditions

Conditions	Yield
With pyridine; potassium hydroxide In ethanol; dichloromethane; water
With hydrogenchloride; aluminium trichloride In 1,1-dichloroethane

: 13014-18-1
2,4-dichlorobenzotrichloride

: 400-70-4
2,4-dichloro-5-nitrobenzotrifluoride

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 140 - 150 °C 2: Nitrierung View Scheme

: 13014-18-1
2,4-dichlorobenzotrichloride

: 109-89-7
diethylamine

: 24309-78-2
2,4-dichloro-N,N-diethylbenzamide

Conditions

Conditions	Yield
With heptamethyl Coβ-perchlorato-cob(II)yrinate; (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 3h; Irradiation;	98 %Chromat.

: 13014-18-1
2,4-dichlorobenzotrichloride

: 320-60-5
2,4-dichloro-benzotrifluoride

Conditions

Conditions	Yield
With hydrogen fluoride at 110℃; under 11251.1 - 12751.3 Torr; Pressure; Temperature;
With hydrogen fluoride at 110℃; under 11251.1 - 12751.3 Torr; Temperature; Pressure;
With hydrogen fluoride at 110℃; under 11251.1 - 12751.3 Torr; Temperature; Pressure; Green chemistry;

α-α-α-2,4-PENTACHLOROTOLUENE Chemical Properties

Product Name: α-α-α-2,4-Pentachlorotoluene (CAS NO.13014-18-1)

Molecular Formula: C₇H₃Cl₅
Molecular Weight: 264.36g/mol
Mol File: 13014-18-1.mol
Einecs: 235-868-1
Appearance: Clear liquid
Melting Point: 49°C
Boiling point: 296.3 °C at 760 mmHg
Flash Point: 136.1 °C
Density: 1.605 g/cm³
Surface Tension: 43.5 dyne/cm
Enthalpy of Vaporization: 51.46 kJ/mol
Vapour Pressure: 0.00256 mmHg at 25°C
XLogP3-AA: 5.5
H-Bond Donor: 0
H-Bond Acceptor: 0

α-α-α-2,4-PENTACHLOROTOLUENE Toxicity Data With Reference

Organism	Test Type	Route	Reported Dose (Normalized Dose)	Effect	Source
rabbit	LD	skin	> 10gm/kg (10000mg/kg)	BEHAVIORAL: SOMNOLENCE (GENERAL DEPRESSED ACTIVITY) LUNGS, THORAX, OR RESPIRATION: DYSPNEA SKIN AND APPENDAGES (SKIN): "DERMATITIS, OTHER: AFTER SYSTEMIC EXPOSURE"	National Technical Information Service. Vol. OTS0537054,
rat	LD50	oral	3160mg/kg (3160mg/kg)	BEHAVIORAL: SOMNOLENCE (GENERAL DEPRESSED ACTIVITY) BEHAVIORAL: ATAXIA LUNGS, THORAX, OR RESPIRATION: DYSPNEA	National Technical Information Service. Vol. OTS0537054,

α-α-α-2,4-PENTACHLOROTOLUENE Consensus Reports

Reported in EPA TSCA Inventory.

α-α-α-2,4-PENTACHLOROTOLUENE Safety Profile

Mutation data reported. When heated to decomposition it emits toxic vapors of Cl⁻.
Safety Information of α-α-α-2,4-Pentachlorotoluene (CAS NO.13014-18-1):
Risk Statements: 34
34: Causes burns
Safety Statements: 26-36/37/39
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36: Wear suitable protective clothing
37: Wear suitable gloves
39: Wear eye/face protection

α-α-α-2,4-PENTACHLOROTOLUENE Specification

α-α-α-2,4-Pentachlorotoluene ,its CAS NO. is 13014-18-1,the synonyms is 1,3-Dichloro-4-(trichloromethyl)benzene ; 2,4-Dichloro-1-(trichloromethyl)-benzen ; 2,4-Dichloro-1-(trichloromethyl)benzene ; 2,4-Dichlorophenyltrichloromethane ; alpha,alpha,alpha,2,4-Pentachloro-toluen ; Benzene,2,4-dichloro-1-(trichloromethyl)- ; Dichlorobenzotrichloride ; Toluene, alpha,alpha,alpha,2,4-pentachloro- .

Product Name

2,4-DICHLOROBENZOTRICHLORIDE

Synthetic route

α-α-α-2,4-PENTACHLOROTOLUENE Chemical Properties

α-α-α-2,4-PENTACHLOROTOLUENE Toxicity Data With Reference

α-α-α-2,4-PENTACHLOROTOLUENE Consensus Reports

α-α-α-2,4-PENTACHLOROTOLUENE Safety Profile

α-α-α-2,4-PENTACHLOROTOLUENE Specification

Related Products

Hot Products