3,4-Dinitrochlorobenzene supplier

Name
3,4-Dinitrochlorobenzene
EINECS 210-223-7
CAS No. 610-40-2
Article Data11
CAS DataBase
Density 1.619 g/cm³
Solubility insoluble in water, soluble in hot ethanol, ethyl ether
Melting Point 40-41 ºC
Formula C₆H₃ClN₂O₄
Boiling Point 335.1 °C at 760 mmHg
Molecular Weight 202.554
Flash Point 156.5 °C
Transport Information UN 3441
Appearance yellow liquid or needle-like crystals
Safety 28-36/37-45-60-61
Risk Codes 23/24/25-33-50/53
Molecular Structure
Hazard Symbols T,N
Synonyms 1,2-Dinitro-4-chlorobenzene;1-Chloro-3,4-dinitrobenzene;3,4-Dinitrochlorobenzene;4-Chloro-1,2-dinitrobenzene;NSC 119343;
PSA 91.64000
LogP 3.20280

Synthetic route

: 121-73-3
3-Chloronitrobenzene

: 610-40-2
3,4-dinitro-chlorobenzene

Conditions

Conditions	Yield
With sulfuric acid; nitric acid at 30℃; for 1h;	97%
With sulfuric acid; uronium nitrate at 0 - 20℃; Nitration;	77%
With sulfuric acid; potassium nitrate
With sulfuric acid; potassium nitrate

: 89-63-4
4-Chloro-2-nitroaniline

: 610-40-2
3,4-dinitro-chlorobenzene

Conditions

Conditions	Yield
With sulfuric acid; acetic acid; tetra-n-propylammonium bromate for 1.5h; Heating;	86%

: 610-41-3
3,4-dinitroaniline

: 610-40-2
3,4-dinitro-chlorobenzene

Conditions

Conditions	Yield
With phosphonic Acid; nitrosylsulfuric acid; sulfuric acid Diazotization.Behandlung der Diazoniumsalz-Loesung mit CuCl in konz. wss. HCl;

: 88-73-3
2-Chloronitrobenzene

: 610-40-2
3,4-dinitro-chlorobenzene

Conditions

Conditions	Yield
durch Nitrieren;

: 577-71-9
3,4-dinitophenol

: 610-40-2
3,4-dinitro-chlorobenzene

Conditions

Conditions	Yield
With trichlorophosphate In N,N-dimethyl-formamide for 2h; Ambient temperature;

α-form: α-form

: 610-40-2
3,4-dinitro-chlorobenzene

Conditions

Conditions	Yield
at 39 - 40℃; (Herstellung der β-Form);

β-form: β-form

: 610-40-2
3,4-dinitro-chlorobenzene

Conditions

Conditions	Yield
at 42℃; (Herstellung der fluessigen Form);

: 121-73-3
3-Chloronitrobenzene

: 7664-93-9
sulfuric acid

: 7697-37-2
nitric acid

: 610-40-2
3,4-dinitro-chlorobenzene

...Expand

: 610-40-2
3,4-dinitro-chlorobenzene

: 95-83-0
4-Chloro-1,2-phenylenediamine

Conditions

Conditions	Yield
With sodium tetrahydroborate; C16H18Cl2N4O2Pd In water at 27℃; for 0.25h;	99%
With hydrogenchloride; tin
With sodium tetrahydroborate In water at 20℃; for 40h;

: 610-40-2
3,4-dinitro-chlorobenzene

: 1226-42-2
1,2-bis(4-methoxyphenyl)-1,2-ethanedione

: 6-chloro-2,3-bis(4-methoxyphenyl)quinoxaline

Conditions

Conditions	Yield
With tin(ll) chloride In ethanol; water for 4h; Reflux;	98%

: 64-18-6
formic acid

: 610-40-2
3,4-dinitro-chlorobenzene

: 4887-82-5
5-chloro-1H-benzimidazole

Conditions

Conditions	Yield
With gold nano particles supported on rutile TiO2 In toluene at 70℃; under 750.075 Torr; for 6h; Inert atmosphere; chemoselective reaction;	95%

: 35578-47-3
4,4'-dibromobenzil

: 610-40-2
3,4-dinitro-chlorobenzene

: 1094618-65-1
2,3-bis(4-bromophenyl)-6-chloroquinoxaline

Conditions

Conditions	Yield
With tin(ll) chloride In ethanol; water for 4h; Reflux;	94%

: 492-94-4
furil

: 610-40-2
3,4-dinitro-chlorobenzene

: 70976-04-4
6-chloro-2,3-di(furan-2-yl)-quinoxaline

Conditions

Conditions	Yield
With tin(ll) chloride In ethanol; water for 4h; Reflux;	94%

: 610-40-2
3,4-dinitro-chlorobenzene

: 134-81-6
benzil

: 36305-60-9
2,3-diphenyl-6-chloroquinoxaline

Conditions

Conditions	Yield
With tin(ll) chloride In ethanol; water for 4h; Reflux;	94%

: 610-40-2
3,4-dinitro-chlorobenzene

: 536-74-3
phenylacetylene

: 1,2-Dinitro-4-phenylethynyl-benzene

Conditions

Conditions	Yield
With potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); (1RS,2RS,3SR,4SR)-1,2,3,4-tetrakis((diphenylphosphanyl)methyl)cyclopentane In N,N-dimethyl-formamide at 140℃; for 20h; Sonogashira cross-coupling;	93%

: 610-40-2
3,4-dinitro-chlorobenzene

: 62-53-3
aniline

: 25781-92-4
5-chloro-2-nitro-N-phenylaniline

Conditions

Conditions	Yield
In ethanol at 20℃; for 10h; Solvent; Temperature; Time;	90%

: 610-40-2
3,4-dinitro-chlorobenzene

: 89-63-4
4-Chloro-2-nitroaniline

Conditions

Conditions	Yield
With sodium tetrahydroborate In ethanol; water at 20℃; for 4h; Green chemistry;	90%

: 64-17-5
ethanol

: 610-40-2
3,4-dinitro-chlorobenzene

: 2818-69-1
6-chloro-2-methyl-1H-benzo[d]imidazole

Conditions

Conditions	Yield
With titanium(IV) oxide for 4h; Irradiation;	89%

: 610-40-2
3,4-dinitro-chlorobenzene

: 95-54-5
1,2-diamino-benzene

Conditions

Conditions	Yield
With palladium 10% on activated carbon; hydrazine hydrate In methanol at 120℃; for 0.25h; Microwave irradiation;	89%

: 610-40-2
3,4-dinitro-chlorobenzene

: 120-82-1
1,2,4-Trichlorobenzene

Conditions

Conditions	Yield
With Dichlorophenylphosphine In various solvent(s) at 170℃; for 5h;	86%

: 108-91-8
cyclohexylamine

: 610-40-2
3,4-dinitro-chlorobenzene

: 28096-58-4
N-cyclohexyl-2-nitro-5-chloro-aniline

Conditions

Conditions	Yield
In ethanol for 8h; Ambient temperature;	85%

: 71-23-8
propan-1-ol

: 610-40-2
3,4-dinitro-chlorobenzene

: 6-chloro-2-ethylbenzimidazole

Conditions

Conditions	Yield
With titanium(IV) oxide for 4h; Irradiation;	84%

: 610-40-2
3,4-dinitro-chlorobenzene

: 122-52-1
triethyl phosphite

: C10H13N2O7P

Conditions

Conditions	Yield
In toluene Michaelis-Arbuzov Synthesis; Reflux;	84%

: 610-40-2
3,4-dinitro-chlorobenzene

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 127291-62-7
3,4-dinitro-1-(4-methylphenylsulfonyl)-benzene

Conditions

Conditions	Yield
With sodium acetate In ethanol for 1h; Heating;	80%

: 610-40-2
3,4-dinitro-chlorobenzene

: 1966-16-1
5-chloro-2-nitrophenylhydrazine

Conditions

Conditions	Yield
With hydrazine hydrate; urea In ethanol	76%
With hydrazine In ethanol at 20℃; for 1h;	62%
With hydrazine hydrate
With ethanol; hydrazine hydrate

: 3360-41-6
4-phenyl-butan-1-ol

: 610-40-2
3,4-dinitro-chlorobenzene

: 4-(4-phenylbutoxy)-1,2-dinitrobenzene

Conditions

Conditions	Yield
In tetrahydrofuran; mineral oil	72%

: 75336-86-6
(2R)-methylpiperazine

: 610-40-2
3,4-dinitro-chlorobenzene

A: (R)-1-(3,4-Dinitro-phenyl)-3-methyl-piperazine

B: 907991-13-3
(R)-1-(5-chloro-2-nitrophenyl)-3-methylpiperazine

Conditions

Conditions	Yield
With potassium carbonate In ethanol; water for 1h; Heating;	A n/a B 71%

...Expand

: 123-75-1
pyrrolidine

: 610-40-2
3,4-dinitro-chlorobenzene

A: 133387-30-1
4-chloro-2-(1-pyrrolidinyl)nitrobenzene

B: 1-(3,4-dinitro-phenyl)-pyrrolidine

Conditions

Conditions	Yield
In methanol at 20℃; for 5h;	A 70% B n/a

...Expand

: 610-40-2
3,4-dinitro-chlorobenzene

: 100-46-9
benzylamine

A: 10066-19-0
N-benzyl-N-(2-nitro-5-chlorophenyl)-amine

B: N-Benzyl-2,4-dinitroanilin

Conditions

Conditions	Yield
In methanol at 20℃; for 3h;	A 70% B n/a

...Expand

: 610-40-2
3,4-dinitro-chlorobenzene

: 618-36-0
rac-methylbenzylamine

A: 330830-31-4
N-(1-phenylethyl)-5-chloro-2-nitroaniline

B: (3,4-dinitro-phenyl)-(1-phenyl-ethyl)-amine

Conditions

Conditions	Yield
In methanol at 20℃; for 3h;	A 68% B n/a

...Expand

: 110-89-4
piperidine

: 610-40-2
3,4-dinitro-chlorobenzene

A: 53013-43-7
1-(5-chloro-2-nitrophenyl)piperidine

B: 1-(3,4-Dinitro-phenyl)-piperidine

Conditions

Conditions	Yield
In methanol at 20℃; for 5h;	A 65% B n/a

...Expand

: 141-43-5
ethanolamine

: 610-40-2
3,4-dinitro-chlorobenzene

A: 50610-29-2
2-<(5-chloro-2-nitro)phenylamino>ethanol

B: 2-(3,4-dinitro-phenylamino)-ethanol

Conditions

Conditions	Yield
In methanol at 20℃; for 3h;	A 65% B n/a

...Expand

: 5813-64-9
2,2-dimethylpropylamine

: 610-40-2
3,4-dinitro-chlorobenzene

A: 725705-48-6
N-(2,2-dimethylpropyl)-5-chloro-2-nitroaniline

B: (2,2-dimethyl-propyl)-(3,4-dinitro-phenyl)-amine

Conditions

Conditions	Yield
In methanol at 20℃; for 3h;	A 65% B n/a

...Expand

: 610-40-2
3,4-dinitro-chlorobenzene

: 31302-52-0
(4-aminophenyl)-α-D-glucopyranoside

: 4-(3,4-dinitrophenylamino)phenyl α-D-glucopyranoside

Conditions

Conditions	Yield
With sodium hydrogencarbonate In ethanol; water for 1h;	63%

: 84145-43-7
1-(para-methoxyphenyl)piperazine hydrochloride

: 610-40-2
3,4-dinitro-chlorobenzene

: 150916-81-7
1-(5-chloro-2-nitrophenyl)-4-(4-methoxyphenyl)piperazine

Conditions

Conditions	Yield
With potassium carbonate In ethanol; water for 5h; Heating;	62%

: 610-40-2
3,4-dinitro-chlorobenzene

: 122-52-1
triethyl phosphite

: O,O-diethyl-5-chloro-2-nitrophenylphosphonate

Conditions

Conditions	Yield
In toluene for 6h; Heating;	60.3%

3,4-Dinitrochlorobenzene Specification

The Benzene,4-chloro-1,2-dinitro-, with the CAS registry number 610-40-2, is also known as 3,4-Dinitrochlorobenzene. It belongs to the product categories of Benzene derivates; API intermediates. Its EINECS number is 210-223-7. This chemical's molecular formula is C₆H₃ClN₂O₄ and formula weight is 202.55. What's more, its IUPAC name is 4-chloro-1,2-dinitrobenzene.

Physical properties of Benzene,4-chloro-1,2-dinitro- are: (1)ACD/LogP: 2.58; (2)ACD/LogD (pH 5.5): 2.58; (3)ACD/LogD (pH 7.4): 2.58; (4)ACD/BCF (pH 5.5): 53.99; (5)ACD/BCF (pH 7.4): 53.99; (6)ACD/KOC (pH 5.5): 604.8; (7)ACD/KOC (pH 7.4): 604.8; (8)#H bond acceptors: 6; (9)#H bond donors: 0; (10)#Freely Rotating Bonds: 2; (11)Polar Surface Area: 91.64 Å²; (12)Index of Refraction: 1.625; (13)Molar Refractivity: 44.23 cm³; (14)Molar Volume: 125 cm³; (15)Surface Tension: 64.2 dyne/cm; (16)Density: 1.619 g/cm³; (17)Flash Point: 156.5 °C; (18)Enthalpy of Vaporization: 55.52 kJ/mol; (19)Boiling Point: 335.1 °C at 760 mmHg; (20)Vapour Pressure: 0.000237 mmHg at 25°C.

Uses of Benzene,4-chloro-1,2-dinitro-: it can be used to produce N-cyclohexyl-2-nitro-5-chloro-aniline at the ambient temperature. It will need solvent ethanol with the reaction time of 8 hours. The yield is about 85%.

When you are using this chemical, please be cautious about it as the following:
It is toxic by inhalation, in contact with skin and if swallowed. It is danger of cumulative effects. It is very toxic to aquatic organisms, and may cause long-term adverse effects in the aquatic environment. After contact with skin, you should wash immediately with plenty of ... (to be specified by the manufacturer). When using it, you must wear suitable protective clothing and gloves. In case of accident or if you feel unwell seek medical advice immediately (show the label where possible). This material and its container must be disposed of as hazardous waste. This chemical should avoid release to the environment. You need refer to special instructions/safety data sheet.

You can still convert the following datas into molecular structure:
(1)Canonical SMILES: C1=CC(=C(C=C1Cl)[N+](=O)[O-])[N+](=O)[O-]
(2)InChI: InChI=1S/C6H3ClN2O4/c7-4-1-2-5(8(10)11)6(3-4)9(12)13/h1-3H
(3)InChIKey: QVQSOXMXXFZAKU-UHFFFAOYSA-N

Product Name

3,4-Dinitrochlorobenzene

Synthetic route

3,4-Dinitrochlorobenzene Specification

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