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Allylchlorodimethylsilane cas 4028-23-3Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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allyl(2-chloropropyl)dimethylsilane
A
Allylchlorodimethylsilane
Conditions | Yield |
---|---|
Heating; | A 95% B 5% |
dimethylsilicon dichloride
allyl bromide
A
Allylchlorodimethylsilane
B
diallyl(dimethyl)silane
Conditions | Yield |
---|---|
Stage #1: allyl bromide With indium In 1,3-dimethylimidazolidine at 20℃; for 1h; Stage #2: dimethylsilicon dichloride In 1,3-dimethylimidazolidine at 70℃; for 3h; | A 90% B 8% |
allyl-trimethyl-silane
A
chloro-trimethyl-silane
B
Allylchlorodimethylsilane
C
dimethylsilicon dichloride
Conditions | Yield |
---|---|
With tungsten(VI) oxychloride In benzene at 50℃; for 60h; | A 87% B 7% C 4% |
allylmagnesium bromide
dimethylsilicon dichloride
Allylchlorodimethylsilane
Conditions | Yield |
---|---|
In tetrahydrofuran at 0 - 25℃; for 16h; | 80% |
diallyl(dimethyl)silane
A
Allylchlorodimethylsilane
B
dimethylsilicon dichloride
Conditions | Yield |
---|---|
With tungsten(VI) oxychloride In benzene at 50℃; for 60h; | A 25% B 74% |
With tungsten(VI) oxychloride In benzene at 50℃; for 60h; | A 25% B 74% |
dimethylsilicon dichloride
allylmagnesium bromide
Allylchlorodimethylsilane
Conditions | Yield |
---|---|
In diethyl ether for 2h; Heating; | 66% |
28% | |
In diethyl ether |
Conditions | Yield |
---|---|
Stage #1: 3-chloroprop-1-ene With iodine; magnesium In diethyl ether at 20℃; for 12h; Stage #2: dimethylsilicon dichloride In diethyl ether at 20℃; for 18h; Further stages.; | 44% |
diethyl ether
allyltrichlorosilane
methylmagnesium bromide
A
Allylchlorodimethylsilane
B
allyldichloromethylsilane
Conditions | Yield |
---|---|
With diethyl ether |
(3-chloropropyl)dimethylchlorosilane
Allylchlorodimethylsilane
Conditions | Yield |
---|---|
With piperidine |
Dimethylcyclopropylchlorosilane
Allylchlorodimethylsilane
Conditions | Yield |
---|---|
at 480℃; |
Conditions | Yield |
---|---|
With magnesium In diethyl ether | |
Stage #1: allyl bromide With 1,3-dimethyl-2-imidazolidinone; indium at 20℃; for 2h; Inert atmosphere; Stage #2: dimethylsilicon dichloride at 70℃; for 3h; Inert atmosphere; |
Conditions | Yield |
---|---|
In benzene Mechanism; |
Conditions | Yield |
---|---|
at 590℃; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: HCl / 20 °C 2: 95 percent / Heating View Scheme |
Conditions | Yield |
---|---|
With CH3MgBr In not given |
Conditions | Yield |
---|---|
at 520℃; Product distribution / selectivity; Inert atmosphere; | 58 %Chromat. |
dimethylmonochlorosilane
3-chloroprop-1-ene
A
Allylchlorodimethylsilane
B
Chloro-dimethyl-((E)-propenyl)-silane
Conditions | Yield |
---|---|
at 500℃; Product distribution / selectivity; Inert atmosphere; | A 79 %Chromat. B 20 %Chromat. |
Conditions | Yield |
---|---|
In diethyl ether at -20 - 20℃; for 16h; |
Allylchlorodimethylsilane
(RS)-methyl mandelate
allyl<<α-(methoxycarbonyl)benzyl>oxy>dimethylsilane
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran for 2h; Ambient temperature; | 100% |
Allylchlorodimethylsilane
1-<5'-O-(monomethoxytrityl)-2'-deoxy-2'-phenylseleno-β-D-xylofuranosyl>thymine
1-<5'-O-(monomethoxytrityl)-(3'-O-allyldimethylsilyl)-2'-deoxy-2'-phenylseleno-β-D-xylofuranosyl>thymine
Conditions | Yield |
---|---|
With pyridine for 2h; Ambient temperature; | 100% |
Allylchlorodimethylsilane
1-<5'-O-(monomethoxytrityl)-2'-deoxy-2'-phenylseleno-β-D-ribofuranosyl>thymine
1-<5'-O-(monomethoxytrityl)-(3'-O-allyldimethylsilyl)-2'-deoxy-2'-phenylseleno-β-D-ribofuranosyl>thymine
Conditions | Yield |
---|---|
With pyridine for 2h; Ambient temperature; | 100% |
Allylchlorodimethylsilane
1-<5'-O-(monomethoxytrityl)-3'-deoxy-3'-phenylseleno-β-D-xylofuranosyl>thymine
1-<5'-O-(monomethoxytrityl)-(2'-O-allyldimethylsilyl)-3'-deoxy-3'-phenylseleno-β-D-ribofuranosyl>thymine
Conditions | Yield |
---|---|
With pyridine for 2h; Ambient temperature; | 100% |
Allylchlorodimethylsilane
1-<5'-O-(monomethoxytrityl)-3'-deoxy-3'-phenylseleno-β-D-arabinofuranosyl>thymine
1-<5'-O-(monomethoxytrityl)-(2'-O-allyldimethylsilyl)-3'-deoxy-3'-phenylseleno-β-D-arabinofuranosyl>thymine
Conditions | Yield |
---|---|
With pyridine for 2h; Ambient temperature; | 100% |
Allylchlorodimethylsilane
1-phenyl-4-penten-1-ol
Allyl-dimethyl-(1-phenyl-pent-4-enyloxy)-silane
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane | 100% |
Allylchlorodimethylsilane
(1SR,2SR)-2-methyl-1-phenylbut-3-en-1-ol
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane | 100% |
Allylchlorodimethylsilane
phenyl 3,4,6-tri-O-benzyl-1-seleno-β-D-glucopyranoside
phenyl 2-O-(allyl(dimethyl)silyl)-3,4,6-tri-O-benzyl-1-seleno-β-D-glucopyranoside
Conditions | Yield |
---|---|
With dmap; triethylamine In toluene at 20℃; Condensation; | 100% |
With dmap; triethylamine In toluene at 20℃; for 3h; | 98% |
Conditions | Yield |
---|---|
With 1H-imidazole; N-ethyl-N,N-diisopropylamine In dichloromethane at -78 - 20℃; | 100% |
Allylchlorodimethylsilane
1-(benzyloxy)-4-penten-2-ol
benzyl 2-(allyldimethylsilyloxy)-4-penten-1-yl ether
Conditions | Yield |
---|---|
With 1H-imidazole; N-ethyl-N,N-diisopropylamine In dichloromethane at -78 - 20℃; for 4h; | 100% |
2-methyl-1-buten-4-ol
Allylchlorodimethylsilane
allyl(dimethyl)[(3-methylbut-3-en-1-yl)oxy]silane
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 20℃; | 100% |
With triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere; | 99% |
Allylchlorodimethylsilane
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 0℃; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
Stage #1: ((2-bromo-4-methoxyphenyl)ethynyl)trimethylsilane With n-butyllithium In tetrahydrofuran at -78℃; for 1h; Stage #2: Allylchlorodimethylsilane In tetrahydrofuran at -78 - 20℃; for 1h; Stage #3: With potassium hydroxide In tetrahydrofuran; methanol at 20℃; for 0.166667h; | 100% |
Allylchlorodimethylsilane
1-Phenyl-2-propen-1-ol
allyldimethyl(1-phenylallyloxy)silane
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane | 99% |
With 1H-imidazole; triethylamine In dichloromethane at 0 - 20℃; for 1h; | 93% |
Allylchlorodimethylsilane
1-Phenyl-3-buten-1-ol
Allyl-dimethyl-(1-phenyl-but-3-enyloxy)-silane
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane | 99% |
With 1H-imidazole; triethylamine In dichloromethane at -10 - 20℃; for 1h; | 73% |
With triethylamine In dichloromethane Yield given; |
Allylchlorodimethylsilane
(R)-1-benzyloxypent-4-en-2-ol
Allyl-((R)-1-benzyloxymethyl-but-3-enyloxy)-dimethyl-silane
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; | 99% |
Allylchlorodimethylsilane
isopropyl alcohol
allyl(isopropoxy)dimethylsilane
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 3h; | 99% |
Conditions | Yield |
---|---|
Stage #1: 2-bromonaphthalene With n-butyllithium In tetrahydrofuran at -78℃; Stage #2: Allylchlorodimethylsilane In tetrahydrofuran at -78℃; for 5h; Further stages.; | 99% |
Allylchlorodimethylsilane
Conditions | Yield |
---|---|
With 1H-imidazole In tetrahydrofuran for 12h; Ambient temperature; | 98% |
Allylchlorodimethylsilane
(2R,3S,5aR,6aS,9R,10S,11aR,13aS)-2,10-Divinyl-tetradecahydro-1,6,11-trioxa-cyclohepta[b]heptalene-3,9-diol
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 0 - 25℃; for 12h; Etherification; | 98% |
Allylchlorodimethylsilane
1,3,5,7,9,11,14-heptacyclopentyltricyclo[7.3.3.15,11]heptasiloxane-endo-3,7,14-triol
(cyclopentyl)7Si7O11(OH)2(OSiMe2-allyl)
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 18h; | 98% |
Allylchlorodimethylsilane
1,3,5,7,9,11,14-heptacyclopentyltricyclo[7.3.3.15,11]heptasiloxane-endo-3,7,14-triol
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 18h; | 98% |
Allylchlorodimethylsilane
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 18h; | 98% |
Conditions | Yield |
---|---|
With 1H-imidazole; N-ethyl-N,N-diisopropylamine In dichloromethane at -78 - 20℃; for 4h; | 98% |
(1,3-dimesityl-4,5-dihydroimidazol-2-ylidene)(PCy3)Cl2Ru=CHPh
Allylchlorodimethylsilane
Conditions | Yield |
---|---|
In dichloromethane 22°C, 1 h; | 98% |
Allylchlorodimethylsilane
1-bromo-2-((methoxymethoxy)methyl)benzene
allyl[2-{(methoxymethoxy)methyl}phenyl]dimethylsilane
Conditions | Yield |
---|---|
Stage #1: 1-bromo-2-((methoxymethoxy)methyl)benzene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Stage #2: Allylchlorodimethylsilane at -78 - 20℃; | 98% |
Allylchlorodimethylsilane
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; for 1h; | 97% |
Allylchlorodimethylsilane
2-hydroxybromobenzene
Allyl-(2-bromo-phenoxy)-dimethyl-silane
Conditions | Yield |
---|---|
With triethylamine at 30℃; for 0.333333h; | 97% |
Allylchlorodimethylsilane
(1R,4S)-4-hydroxy-2-cyclopentene-1-yl acetate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 25℃; for 3h; Substitution; | 97% |
Allylchlorodimethylsilane
phenyl 3,4-bis-O-tert-butyldimethylsilyl-6-O-trityl-1-seleno-β-D-glucose
phenyl 2-O-(allyl(dimethyl)silyl)-3,4-bis-O-(tert-butyl(dimethyl)silyl)-6-O-(triphenylmethyl)-1-seleno-β-D-glucopyranoside
Conditions | Yield |
---|---|
With pyridine; 3 A molecular sieve at 20℃; for 1h; | 97% |
With dmap; triethylamine In toluene Condensation; | 67% |
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