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inquiry3-METHYL-3-BUTEN-1-OL Basic information Product Name: 3-METHYL-3-BUTEN-1-OL Synonyms: 2-Methyl-1-buten-4-ol;3-Isopentenyl alcohol;3-methyl-3-buten-1-o;3-methyl-3-butenol;3-Methylbut-3-en
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inquiryProduct Name 3-Methyl-3-buten-1-ol CAS No. 763-32-6 EINECS No. 212-110-8 Molecular Formula C5H10O Molecular Weight 86.13 g·
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inquirySuperior quality, moderate price & quick delivery. Appearance:clear colorless to light yellow liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:For medic
Product name: 3-Methyl-3-Butene-1-ol CAS No.:763-32-6 Molecule Formula:C5H10O Molecule Weight:86.13 Purity: 99.0% Package: 200kg/drum Description:Colorless and clear liquid Manufacture Standards:Enterprise Standard TESTING ITEMS
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3-METHYL-3-BUTEN-1-OL Basic information Product Name: 3-METHYL-3-BUTEN-1-OL Synonyms: 2-Methyl-1-buten-4-ol 2-Methyl-4-hydroxy-1-butene;NSC 12267;3-Methylenebutan-1-ol;4-Hydroxy-2-methyl-1-butene;NSC 122673;3-Methyl-3-buten-1-ol, 97% 500ML;3-M
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inquiryConditions | Yield |
---|---|
In water at 280℃; under 150015 Torr; for 0.166667h; | 95% |
at 200℃; under 235362 - 478080 Torr; | |
In methanol; water; isopropyl alcohol |
3,4-epoxy-3-methylbutanol
2-methyl-1-buten-4-ol
Conditions | Yield |
---|---|
With zirconium(IV) chloride; sodium iodide In acetonitrile for 0.0166667h; Heating; | 90% |
Conditions | Yield |
---|---|
With triphenylphosphine; paraformaldehyde; hexacarbonyl molybdenum In benzene | 70% |
With paraformaldehyde In benzene | 59% |
With paraformaldehyde In benzene | 50% |
Conditions | Yield |
---|---|
In diethyl ether Heating; | 65% |
With diethyl ether | |
In diethyl ether for 12h; Heating; Yield given; |
Conditions | Yield |
---|---|
With oxygen at 200℃; under 75007.5 Torr; Pressure; Temperature; | 61.2% |
Conditions | Yield |
---|---|
With paraformaldehyde In benzene | 60% |
Conditions | Yield |
---|---|
With paraformaldehyde In benzene | 58% |
Conditions | Yield |
---|---|
With paraformaldehyde In benzene | 57% |
2-isopropyloxirane
A
3-methyl-butan-2-one
B
2-methyl-1-buten-4-ol
C
2-isopropyl-5-methyl-hex-2-enal
D
3-methyl-2-buten-1-ol
Conditions | Yield |
---|---|
With magnesium bromide In N,N-dimethyl-formamide at 130℃; for 0.666667h; Further byproducts given; | A 52.2% B 23.2% C 8.7% D 13.7% |
Conditions | Yield |
---|---|
With paraformaldehyde In acetonitrile | 44% |
Conditions | Yield |
---|---|
With paraformaldehyde In benzene | 40% |
Conditions | Yield |
---|---|
With formaldehyd | A 36% B n/a |
Conditions | Yield |
---|---|
With [Ru(η(5)-C5,κ-N-Cp(N))(CH3CN)2]PF6 In tetrahydrofuran-d8 at 60℃; for 5.33333h; Inert atmosphere; | A 31% B 16% |
3-methyl-2-buten-1-ol
A
2-methyl-1-buten-4-ol
B
i-Amyl alcohol
C
3,3-dimethyl acrylaldehyde
Conditions | Yield |
---|---|
With hydrogen In water at 20℃; under 759.826 Torr; for 24h; | A 10% B 21% C 7% |
With hydrogen In water at 20℃; under 759.826 Torr; for 24h; | A 18% B 15% C 7% |
With hydrogen In water at 20℃; under 759.826 Torr; for 24h; | A 16% B 9% C 18% |
3-methyl-2-buten-1-ol
A
2-methyl-1-buten-4-ol
B
3,3-dimethyl acrylaldehyde
Conditions | Yield |
---|---|
With hydrogen In water at 20℃; under 759.826 Torr; for 24h; | A 18% B 14% |
Conditions | Yield |
---|---|
With zinc(II) chloride at 80℃; under 750.075 Torr; for 2h; Reagent/catalyst; Time; Temperature; Inert atmosphere; | 14.77% |
Conditions | Yield |
---|---|
With hydrogen In water at 20℃; under 759.826 Torr; for 24h; | A 10% B 6% |
3-methyl-2-buten-1-ol
A
2-methyl-1-buten-4-ol
B
3,3-dimethyl acrylaldehyde
C
isovaleraldehyde
D
isoprene
Conditions | Yield |
---|---|
(sulphos)Rh(CO)2 In 1,2-dichloro-ethane at 100℃; for 1h; Product distribution; Further Variations:; Solvents; autoclave; | A 4% B 4% C 4% D 9% |
formaldehyd
isobutene
A
4,4-dimethyl-1,3-dioxane
B
4-methyl-3,6-dihydro-2H-pyran
C
2-methyl-1-buten-4-ol
D
2-methyl-3-buten-2-ol
Conditions | Yield |
---|---|
With sulfuric acid In nitromethane at 30℃; for 0.333333h; Mechanism; | A 8.16% B n/a C 1.79% D 2.5% |
Conditions | Yield |
---|---|
With sulfuric acid |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; diethyl ether |
Conditions | Yield |
---|---|
With potassium hydroxide | |
Multi-step reaction with 2 steps 1: 81 percent / HBF4*Et2O / CH2Cl2 / -30 °C 2: 10N NaOH / CH2Cl2; methanol / 24 h / Ambient temperature View Scheme |
formaldehyd
isobutene
A
2-methyl-1-buten-4-ol
B
bis-(3-methyl-but-3-enyloxy)-methane
Conditions | Yield |
---|---|
With tin(IV) chloride unter Druck; |
formaldehyd
isobutene
A
2-methyl-1-buten-4-ol
B
3-methylenepentane-1,5-diol
Conditions | Yield |
---|---|
at 200℃; under 320 - 640 Torr; | |
at 200℃; |
2,2-dimethyl-oxetane
benzaldehyde
A
2-methyl-1-buten-4-ol
B
i-Amyl alcohol
C
2,2-dimethyl-1-phenylbutane-1,4-diol
D
benzyl alcohol
Conditions | Yield |
---|---|
With 4,4'-di-tert-butylbiphenylide; triethylaluminum 1) THF, -70 deg C; Yield given. Multistep reaction. Yields of byproduct given; |
4,4-dimethyl-1,3-dioxane
A
4-methyl-3,6-dihydro-2H-pyran
B
2-methyl-1-buten-4-ol
C
3-methyl-butane-1,3-diol
D
4-hydroxy-4-methyltetrahydropyran
E
2-methyl-3-buten-2-ol
F
3-methyl-2-buten-1-ol
Conditions | Yield |
---|---|
With sulfuric acid at 120℃; for 3h; Product distribution; various catalyst, various temperature, various time, extent of conversion, solvent cyclohexane; |
3-methyl-butane-1,3-diol
A
2-methyl-1-buten-4-ol
B
2-methyl-3-buten-2-ol
C
3-methyl-2-buten-1-ol
D
isoprene
Conditions | Yield |
---|---|
With potassium hydrogensulfate at 140℃; for 0.75h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; | A n/a B 8 % Chromat. C n/a D 30 % Chromat. |
With potassium hydrogensulfate at 140℃; for 0.75h; Product distribution; investigation of regioselectivity of dehydration with var. reagents in terpene derivatives; | A n/a B 8 % Chromat. C n/a D 30 % Chromat. |
Conditions | Yield |
---|---|
With pyridine at 0℃; for 2.5h; | 100% |
With triethylamine In dichloromethane at 20℃; for 18h; | 100% |
With triethylamine In dichloromethane 1.) 0 deg C, 1 h, 2.) r.t., 12 h; | 98% |
2-methyl-1-buten-4-ol
methanesulfonyl chloride
4-mesyloxy-2-methylbutene
Conditions | Yield |
---|---|
With triethylamine In diethyl ether at 0℃; for 1h; | 100% |
With triethylamine In dichloromethane at 0 - 20℃; | 100% |
With triethylamine In dichloromethane at 0 - 20℃; for 3h; | 100% |
2-methyl-1-buten-4-ol
benzenesulfonyl chloride
3-methyl-3-butenyl-1-benznesulfonate
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0℃; for 4h; | 100% |
With dmap; triethylamine In dichloromethane at 0 - 20℃; for 4.33333h; |
Conditions | Yield |
---|---|
With di-tert-butyl-diazodicarboxylate; triphenylphosphine In tetrahydrofuran at 70℃; Mitsunobu reaction; | 100% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran; toluene for 1.5h; Inert atmosphere; Reflux; | 91% |
With di-isopropyl azodicarboxylate; triphenylphosphine In dichloromethane for 3h; Ambient temperature; | 79% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 70℃; | 53% |
With dicyclohexyl-carbodiimide; copper(l) chloride 1.) 5h, 60 deg C, 2.) 12h, 100 deg C; Yield given. Multistep reaction; |
2-methyl-1-buten-4-ol
4-methoxy-phenol
1-methoxy-4-((3-methylbut-3-en-1-yl)oxy)benzene
Conditions | Yield |
---|---|
With diethyl diazodicarboxylate; triphenylphosphine In tetrahydrofuran; toluene at 20℃; for 1h; Heating / reflux; | 100% |
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran for 4h; Heating; | 99% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran Mitsunobu reaction; | 98% |
2-methyl-1-buten-4-ol
tert-butylchlorodiphenylsilane
tert-butyl((3-methylbut-3-en-1-yl)oxy)diphenylsilane
Conditions | Yield |
---|---|
With 1H-imidazole In dichloromethane | 100% |
With 1H-imidazole In tetrahydrofuran for 1h; Ambient temperature; | 99% |
With dmap; triethylamine In dichloromethane at 0℃; for 12h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; for 0.666667h; | 100% |
With triethylamine In dichloromethane at 0 - 20℃; for 16h; Inert atmosphere; | 99% |
With dmap In dichloromethane at 0 - 20℃; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With dmap; carbodiimide | 100% |
2-methyl-1-buten-4-ol
2-acetoxy-2-phenylacetic acid
Conditions | Yield |
---|---|
With dmap; carbodiimide | 100% |
2-methyl-1-buten-4-ol
L-Pyroglutamic acid
(5S)-2-pyrrolidone-5-carboxylic acid 3-methyl-3-butenyl ester
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; | 100% |
With dmap; dicyclohexyl-carbodiimide In dichloromethane |
2-methyl-1-buten-4-ol
Allylchlorodimethylsilane
allyl(dimethyl)[(3-methylbut-3-en-1-yl)oxy]silane
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 20℃; | 100% |
With triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere; | 99% |
2-methyl-1-buten-4-ol
N-phenyl-benzimidoyl chloride
3-methylbut-3-enyl N-phenylbenzimidate
Conditions | Yield |
---|---|
Stage #1: 2-methyl-1-buten-4-ol With sodium hydride In tetrahydrofuran; mineral oil at 0 - 30℃; for 1.25h; Stage #2: N-phenyl-benzimidoyl chloride In tetrahydrofuran; mineral oil at 0 - 20℃; for 20h; | 100% |
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0℃; for 1.5h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 100% |
2-methyl-1-buten-4-ol
2,4-Dinitrofluorobenzene
isopentenyl 2,4-dinitrophenyl ether
Conditions | Yield |
---|---|
With triethylamine 1.) 30 min, 70 deg C, 2.) 12 h, room temperature; | 99% |
2-methyl-1-buten-4-ol
ortho-nitrofluorobenzene
1-((3-methylbut-3-en-1-yl)oxy)-2-nitrobenzene
Conditions | Yield |
---|---|
Stage #1: 2-methyl-1-buten-4-ol With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 0.25h; Stage #2: ortho-nitrofluorobenzene In tetrahydrofuran; mineral oil at 0 - 20℃; for 2h; | 99% |
Stage #1: 2-methyl-1-buten-4-ol With sodium hydride; N,N-dimethyl-formamide Stage #2: ortho-nitrofluorobenzene at 50℃; | 84% |
Conditions | Yield |
---|---|
With triphenylphosphine; diethylazodicarboxylate In dichloromethane at 0 - 20℃; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran; toluene at 20℃; for 22h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran; toluene at 20℃; for 1h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 0℃; for 2h; Inert atmosphere; | 99% |
With dmap; triethylamine In dichloromethane at 20℃; | 90% |
With dmap; triethylamine In dichloromethane at 0 - 20℃; | 83% |
Conditions | Yield |
---|---|
Stage #1: 4-Bromobenzoic acid With 1,1'-carbonyldiimidazole In dichloromethane at 20℃; for 1h; Stage #2: 2-methyl-1-buten-4-ol In dichloromethane at 20℃; | 99% |
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 24h; | 90% |
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; |
2-methyl-1-buten-4-ol
phthalic anhydride
o-((3-methylbut-3-enoxy)carbonyl)benzoic acid
Conditions | Yield |
---|---|
In pyridine; benzene at 100℃; for 2h; | 98% |
2-methyl-1-buten-4-ol
tert-butyldimethylsilyl chloride
1-(tert-butyldimethylsiloxy)-3-methyl-3-butene
Conditions | Yield |
---|---|
With 1H-imidazole In dichloromethane at 20℃; for 18h; | 98% |
With 1H-imidazole In dichloromethane at 20℃; for 18h; | 94% |
With 1H-imidazole In N,N-dimethyl-formamide for 4h; Ambient temperature; | 90% |
2-methyl-1-buten-4-ol
4-Methyl-3,4,5,6-tetrahydro-2H-pyran-2-ol
Conditions | Yield |
---|---|
In hexane | 98% |
2-methyl-1-buten-4-ol
N-phthaloylglycine
3-methylbut-3-en-1-yl 2-(1,3-dioxoisoindolin-2-yl)acetate
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 12h; | 98% |
Conditions | Yield |
---|---|
With potassium carbonate; eosin y; triisopropylsilanethiol In 1,4-dioxane; water at 32 - 34℃; for 12h; Inert atmosphere; Irradiation; | 98% |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene at 100 - 105℃; for 4h; | 97.3% |
2-methyl-1-buten-4-ol
2,4-Dinitrofluorobenzene
1-(dinitro-2,4-phenoxy)-3-methyl-2-butene
Conditions | Yield |
---|---|
With triethylamine 1.) 30 min, 70 deg C, 2.) 12 h, room temperature; | 97% |
2-methyl-1-buten-4-ol
benzyl bromide
(((3-methylbut-3-en-1-yl)oxy)methyl)benzene
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 20℃; for 12h; | 97% |
With tetra-(n-butyl)ammonium iodide; sodium hydride In tetrahydrofuran 1.) r.t., 2.) 40 deg C, 4 h; | 91% |
With tetra-(n-butyl)ammonium iodide; sodium hydride In tetrahydrofuran at 20℃; | 89% |
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