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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

3-methyl-3-buten-1-ol

Cas:763-32-6

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Wuhan Fortuna Chemical Co.,Ltd

Factory supply 3-Methyl-3-buten-1-ol CAS 763-32-6 with fast delivery Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed

Factory supply 3-Methyl-3-buten-1-ol CAS 763-32-6 with fast delivery

Cas:763-32-6

Min.Order:10 Kilogram

FOB Price: $10.0

Type:Trading Company

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Henan Allgreen Chemical Co.,Ltd

3-METHYL-3-BUTEN-1-OL Basic information Product Name: 3-METHYL-3-BUTEN-1-OL Synonyms: 2-Methyl-1-buten-4-ol;3-Isopentenyl alcohol;3-methyl-3-buten-1-o;3-methyl-3-bu

763-32-6

Cas:763-32-6

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 3-methylbut-3-en-1-ol

Cas:763-32-6

Min.Order:1

Negotiable

Type:Other

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

3-Methyl-3-buten-1-ol

Cas:763-32-6

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

3-METHYL-3-BUTEN-1-OL Basic information Product Name: 3-METHYL-3-BUTEN-1-OL Synonyms: 2-Methyl-1-buten-4-ol;3-Isopentenyl alcohol;3-methyl-3-buten-1-o;3-methyl-3-butenol;3-Methylbut-3-en

3-Methyl-3-buten-1-ol, 97%

Cas:763-32-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

3-METHYL-3-BUTEN-1-OL

Cas:763-32-6

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 763-32-6 with best quality

Cas:763-32-6

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Product Name 3-Methyl-3-buten-1-ol CAS No. 763-32-6 EINECS No. 212-110-8 Molecular Formula C5H10O Molecular Weight 86.13 g·

3-Methyl-2-buten-1-ol CAS: 763-32-6

Cas:763-32-6

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

2-Methyl-1-buten-4-ol 763-32-6

Cas:763-32-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Qingdao Beluga Import and Export Co., LTD

3-METHYL-3-BUTEN-1-OL CAS:763-32-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inter

3-METHYL-3-BUTEN-1-OL CAS:763-32-6

Cas:763-32-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

2-Methyl-1-buten-4-ol

Cas:763-32-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:763-32-6

Cas:763-32-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

3-METHYL-3-BUTEN-1-OL

Cas:763-32-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

3-Methyl-3-buten-1-ol

Cas:763-32-6

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

2-Methyl-1-buten-4-ol

Cas:763-32-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

3-METHYL-3-BUTEN-1-OL

Cas:763-32-6

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

2-Methyl-1-buten-4-ol

Cas:763-32-6

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:clear colorless to light yellow liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:For medic

2-Methyl-1-buten-4-ol

Cas:763-32-6

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Siwei Development Group Ltd.

Product name: 3-Methyl-3-Butene-1-ol CAS No.:763-32-6 Molecule Formula:C5H10O Molecule Weight:86.13 Purity: 99.0% Package: 200kg/drum Description:Colorless and clear liquid Manufacture Standards:Enterprise Standard TESTING ITEMS

Best Quality 3-Methyl-3-Butene-1-ol with good supplier

Cas:763-32-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

High purity 3-methyl-3-buten-1-ol

Cas:763-32-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

Top Purity 3-METHYL-3-BUTEN-1-OL

Cas:763-32-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shanghai Minstar Chemical Co., Ltd

3-METHYL-3-BUTEN-1-OL Basic information Product Name: 3-METHYL-3-BUTEN-1-OL Synonyms: 2-Methyl-1-buten-4-ol 2-Methyl-4-hydroxy-1-butene;NSC 12267;3-Methylenebutan-1-ol;4-Hydroxy-2-methyl-1-butene;NSC 122673;3-Methyl-3-buten-1-ol, 97% 500ML;3-M

3-METHYL-3-BUTEN-1-OL

Cas:763-32-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

TIANFUCHEM--High purity 3-METHYL-3-BUTEN-1-OL factory price

Cas:763-32-6

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

3-METHYL-3-BUTEN-1-OL

Cas:763-32-6

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

TIANFUCHEM--High purity 3-METHYL-3-BUTEN-1-OL factory price

Cas:763-32-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

TIANFUCHEM--High purity 3-METHYL-3-BUTEN-1-OL factory price

Cas:763-32-6

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Golden Pharma Co., Limited

GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation

3-METHYL-3-BUTEN-1-OL

Cas:763-32-6

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

3-METHYL-3-BUTEN-1-OL Cas no.763-32-6 98%

Cas:763-32-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

TIANFUCHEM--High purity 3-METHYL-3-BUTEN-1-OL factory price

Cas:763-32-6

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Synthetic route

formaldehyd
50-00-0

formaldehyd

isobutene
115-11-7

isobutene

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

Conditions
ConditionsYield
In water at 280℃; under 150015 Torr; for 0.166667h;95%
at 200℃; under 235362 - 478080 Torr;
In methanol; water; isopropyl alcohol
3,4-epoxy-3-methylbutanol
59954-67-5

3,4-epoxy-3-methylbutanol

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

Conditions
ConditionsYield
With zirconium(IV) chloride; sodium iodide In acetonitrile for 0.0166667h; Heating;90%
isobutene
115-11-7

isobutene

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

Conditions
ConditionsYield
With triphenylphosphine; paraformaldehyde; hexacarbonyl molybdenum In benzene70%
With paraformaldehyde In benzene59%
With paraformaldehyde In benzene50%
formaldehyd
50-00-0

formaldehyd

2-methylallylmagnesium chloride
5674-01-1

2-methylallylmagnesium chloride

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

Conditions
ConditionsYield
In diethyl ether Heating;65%
With diethyl ether
In diethyl ether for 12h; Heating; Yield given;
methanol
67-56-1

methanol

isobutene
115-11-7

isobutene

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

Conditions
ConditionsYield
With oxygen at 200℃; under 75007.5 Torr; Pressure; Temperature;61.2%
hexacarbonyl chromium

hexacarbonyl chromium

isobutene
115-11-7

isobutene

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

Conditions
ConditionsYield
With paraformaldehyde In benzene60%
ferrocene (dicyclopentadienyl iron)

ferrocene (dicyclopentadienyl iron)

isobutene
115-11-7

isobutene

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

Conditions
ConditionsYield
With paraformaldehyde In benzene58%
molybdenum dioxide (MoO2)

molybdenum dioxide (MoO2)

isobutene
115-11-7

isobutene

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

Conditions
ConditionsYield
With paraformaldehyde In benzene57%
2-isopropyloxirane
1438-14-8

2-isopropyloxirane

A

3-methyl-butan-2-one
563-80-4

3-methyl-butan-2-one

B

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

C

2-isopropyl-5-methyl-hex-2-enal
35158-25-9

2-isopropyl-5-methyl-hex-2-enal

D

3-methyl-2-buten-1-ol
556-82-1

3-methyl-2-buten-1-ol

Conditions
ConditionsYield
With magnesium bromide In N,N-dimethyl-formamide at 130℃; for 0.666667h; Further byproducts given;A 52.2%
B 23.2%
C 8.7%
D 13.7%
palladium(II) cyanide

palladium(II) cyanide

isobutene
115-11-7

isobutene

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

Conditions
ConditionsYield
With paraformaldehyde In acetonitrile44%
rhodium(III) chloride

rhodium(III) chloride

isobutene
115-11-7

isobutene

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

Conditions
ConditionsYield
With paraformaldehyde In benzene40%
isoprene
78-79-5

isoprene

A

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

B

isobutene
115-11-7

isobutene

Conditions
ConditionsYield
With formaldehydA 36%
B n/a
3-methyl-2-buten-1-ol
556-82-1

3-methyl-2-buten-1-ol

A

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

B

isovaleraldehyde
590-86-3

isovaleraldehyde

Conditions
ConditionsYield
With [Ru(η(5)-C5,κ-N-Cp(N))(CH3CN)2]PF6 In tetrahydrofuran-d8 at 60℃; for 5.33333h; Inert atmosphere;A 31%
B 16%
3-methyl-2-buten-1-ol
556-82-1

3-methyl-2-buten-1-ol

A

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

B

i-Amyl alcohol
123-51-3

i-Amyl alcohol

C

3,3-dimethyl acrylaldehyde
107-86-8

3,3-dimethyl acrylaldehyde

Conditions
ConditionsYield
With hydrogen In water at 20℃; under 759.826 Torr; for 24h;A 10%
B 21%
C 7%
With hydrogen In water at 20℃; under 759.826 Torr; for 24h;A 18%
B 15%
C 7%
With hydrogen In water at 20℃; under 759.826 Torr; for 24h;A 16%
B 9%
C 18%
3-methyl-2-buten-1-ol
556-82-1

3-methyl-2-buten-1-ol

A

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

B

3,3-dimethyl acrylaldehyde
107-86-8

3,3-dimethyl acrylaldehyde

Conditions
ConditionsYield
With hydrogen In water at 20℃; under 759.826 Torr; for 24h;A 18%
B 14%
formaldehyd
50-00-0

formaldehyd

tert-butyl alcohol
75-65-0

tert-butyl alcohol

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

Conditions
ConditionsYield
With zinc(II) chloride at 80℃; under 750.075 Torr; for 2h; Reagent/catalyst; Time; Temperature; Inert atmosphere;14.77%
3-methyl-2-buten-1-ol
556-82-1

3-methyl-2-buten-1-ol

A

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

B

i-Amyl alcohol
123-51-3

i-Amyl alcohol

Conditions
ConditionsYield
With hydrogen In water at 20℃; under 759.826 Torr; for 24h;A 10%
B 6%
3-methyl-2-buten-1-ol
556-82-1

3-methyl-2-buten-1-ol

A

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

B

3,3-dimethyl acrylaldehyde
107-86-8

3,3-dimethyl acrylaldehyde

C

isovaleraldehyde
590-86-3

isovaleraldehyde

D

isoprene
78-79-5

isoprene

Conditions
ConditionsYield
(sulphos)Rh(CO)2 In 1,2-dichloro-ethane at 100℃; for 1h; Product distribution; Further Variations:; Solvents; autoclave;A 4%
B 4%
C 4%
D 9%
formaldehyd
50-00-0

formaldehyd

isobutene
115-11-7

isobutene

A

4,4-dimethyl-1,3-dioxane
766-15-4

4,4-dimethyl-1,3-dioxane

B

4-methyl-3,6-dihydro-2H-pyran
16302-35-5

4-methyl-3,6-dihydro-2H-pyran

C

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

D

2-methyl-3-buten-2-ol
115-18-4

2-methyl-3-buten-2-ol

Conditions
ConditionsYield
With sulfuric acid In nitromethane at 30℃; for 0.333333h; Mechanism;A 8.16%
B n/a
C 1.79%
D 2.5%
3-methyl-butane-1,3-diol
2568-33-4

3-methyl-butane-1,3-diol

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

Conditions
ConditionsYield
With sulfuric acid
3-methylbut-3-enoic acid
1617-31-8

3-methylbut-3-enoic acid

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

Conditions
ConditionsYield
With lithium aluminium tetrahydride; diethyl ether
3-methyl-3-buten-1-yl acetate
5205-07-2

3-methyl-3-buten-1-yl acetate

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

Conditions
ConditionsYield
With potassium hydroxide
Multi-step reaction with 2 steps
1: 81 percent / HBF4*Et2O / CH2Cl2 / -30 °C
2: 10N NaOH / CH2Cl2; methanol / 24 h / Ambient temperature
View Scheme
formaldehyd
50-00-0

formaldehyd

isobutene
115-11-7

isobutene

A

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

B

bis-(3-methyl-but-3-enyloxy)-methane
1708-94-7

bis-(3-methyl-but-3-enyloxy)-methane

Conditions
ConditionsYield
With tin(IV) chloride unter Druck;
formaldehyd
50-00-0

formaldehyd

isobutene
115-11-7

isobutene

A

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

B

3-methylenepentane-1,5-diol
40760-35-8

3-methylenepentane-1,5-diol

Conditions
ConditionsYield
at 200℃; under 320 - 640 Torr;
at 200℃;
2,2-dimethyl-oxetane
6245-99-4

2,2-dimethyl-oxetane

benzaldehyde
100-52-7

benzaldehyde

A

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

B

i-Amyl alcohol
123-51-3

i-Amyl alcohol

C

2,2-dimethyl-1-phenylbutane-1,4-diol
136175-39-8

2,2-dimethyl-1-phenylbutane-1,4-diol

D

benzyl alcohol
100-51-6

benzyl alcohol

Conditions
ConditionsYield
With 4,4'-di-tert-butylbiphenylide; triethylaluminum 1) THF, -70 deg C; Yield given. Multistep reaction. Yields of byproduct given;
4,4-dimethyl-1,3-dioxane
766-15-4

4,4-dimethyl-1,3-dioxane

A

4-methyl-3,6-dihydro-2H-pyran
16302-35-5

4-methyl-3,6-dihydro-2H-pyran

B

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

C

3-methyl-butane-1,3-diol
2568-33-4

3-methyl-butane-1,3-diol

D

4-hydroxy-4-methyltetrahydropyran
7525-64-6

4-hydroxy-4-methyltetrahydropyran

E

2-methyl-3-buten-2-ol
115-18-4

2-methyl-3-buten-2-ol

F

3-methyl-2-buten-1-ol
556-82-1

3-methyl-2-buten-1-ol

Conditions
ConditionsYield
With sulfuric acid at 120℃; for 3h; Product distribution; various catalyst, various temperature, various time, extent of conversion, solvent cyclohexane;
formaldehyd
50-00-0

formaldehyd

(2-methylallyl)magnesium bromide
33324-92-4

(2-methylallyl)magnesium bromide

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

3-methyl-butane-1,3-diol
2568-33-4

3-methyl-butane-1,3-diol

A

2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

B

2-methyl-3-buten-2-ol
115-18-4

2-methyl-3-buten-2-ol

C

3-methyl-2-buten-1-ol
556-82-1

3-methyl-2-buten-1-ol

D

isoprene
78-79-5

isoprene

Conditions
ConditionsYield
With potassium hydrogensulfate at 140℃; for 0.75h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;A n/a
B 8 % Chromat.
C n/a
D 30 % Chromat.
With potassium hydrogensulfate at 140℃; for 0.75h; Product distribution; investigation of regioselectivity of dehydration with var. reagents in terpene derivatives;A n/a
B 8 % Chromat.
C n/a
D 30 % Chromat.
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

isopentenyl tosylate
781-03-3

isopentenyl tosylate

Conditions
ConditionsYield
With pyridine at 0℃; for 2.5h;100%
With triethylamine In dichloromethane at 20℃; for 18h;100%
With triethylamine In dichloromethane 1.) 0 deg C, 1 h, 2.) r.t., 12 h;98%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

methanesulfonyl chloride
124-63-0

methanesulfonyl chloride

4-mesyloxy-2-methylbutene
80352-66-5

4-mesyloxy-2-methylbutene

Conditions
ConditionsYield
With triethylamine In diethyl ether at 0℃; for 1h;100%
With triethylamine In dichloromethane at 0 - 20℃;100%
With triethylamine In dichloromethane at 0 - 20℃; for 3h;100%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

benzenesulfonyl chloride
98-09-9

benzenesulfonyl chloride

3-methyl-3-butenyl-1-benznesulfonate
90545-36-1

3-methyl-3-butenyl-1-benznesulfonate

Conditions
ConditionsYield
With pyridine In dichloromethane at 0℃; for 4h;100%
With dmap; triethylamine In dichloromethane at 0 - 20℃; for 4.33333h;
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

phenol
108-95-2

phenol

((3-methylbut-3-en-1-yl)oxy)benzene
58584-26-2

((3-methylbut-3-en-1-yl)oxy)benzene

Conditions
ConditionsYield
With di-tert-butyl-diazodicarboxylate; triphenylphosphine In tetrahydrofuran at 70℃; Mitsunobu reaction;100%
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran; toluene for 1.5h; Inert atmosphere; Reflux;91%
With di-isopropyl azodicarboxylate; triphenylphosphine In dichloromethane for 3h; Ambient temperature;79%
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 70℃;53%
With dicyclohexyl-carbodiimide; copper(l) chloride 1.) 5h, 60 deg C, 2.) 12h, 100 deg C; Yield given. Multistep reaction;
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

4-methoxy-phenol
150-76-5

4-methoxy-phenol

1-methoxy-4-((3-methylbut-3-en-1-yl)oxy)benzene
169310-73-0

1-methoxy-4-((3-methylbut-3-en-1-yl)oxy)benzene

Conditions
ConditionsYield
With diethyl diazodicarboxylate; triphenylphosphine In tetrahydrofuran; toluene at 20℃; for 1h; Heating / reflux;100%
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran for 4h; Heating;99%
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran Mitsunobu reaction;98%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

tert-butylchlorodiphenylsilane
58479-61-1

tert-butylchlorodiphenylsilane

tert-butyl((3-methylbut-3-en-1-yl)oxy)diphenylsilane
177606-52-9

tert-butyl((3-methylbut-3-en-1-yl)oxy)diphenylsilane

Conditions
ConditionsYield
With 1H-imidazole In dichloromethane100%
With 1H-imidazole In tetrahydrofuran for 1h; Ambient temperature;99%
With dmap; triethylamine In dichloromethane at 0℃; for 12h; Inert atmosphere;99%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

benzoyl chloride
98-88-4

benzoyl chloride

3-methylbut-3-enyl benzoate
5205-12-9

3-methylbut-3-enyl benzoate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0℃; for 0.666667h;100%
With triethylamine In dichloromethane at 0 - 20℃; for 16h; Inert atmosphere;99%
With dmap In dichloromethane at 0 - 20℃; Inert atmosphere;99%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

rac-methoxyphenylacetic acid
7021-09-2

rac-methoxyphenylacetic acid

methoxy-phenyl-acetic acid 3-methyl-but-3-enyl ester

methoxy-phenyl-acetic acid 3-methyl-but-3-enyl ester

Conditions
ConditionsYield
With dmap; carbodiimide100%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

2-acetoxy-2-phenylacetic acid
29071-09-8

2-acetoxy-2-phenylacetic acid

acetoxy-phenyl-acetic acid 3-methyl-but-3-enyl ester

acetoxy-phenyl-acetic acid 3-methyl-but-3-enyl ester

Conditions
ConditionsYield
With dmap; carbodiimide100%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

L-Pyroglutamic acid
98-79-3

L-Pyroglutamic acid

(5S)-2-pyrrolidone-5-carboxylic acid 3-methyl-3-butenyl ester
865183-91-1

(5S)-2-pyrrolidone-5-carboxylic acid 3-methyl-3-butenyl ester

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃;100%
With dmap; dicyclohexyl-carbodiimide In dichloromethane
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

Allylchlorodimethylsilane
4028-23-3

Allylchlorodimethylsilane

allyl(dimethyl)[(3-methylbut-3-en-1-yl)oxy]silane
1012314-18-9

allyl(dimethyl)[(3-methylbut-3-en-1-yl)oxy]silane

Conditions
ConditionsYield
With dmap; triethylamine In dichloromethane at 20℃;100%
With triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere;99%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

N-phenyl-benzimidoyl chloride
4903-36-0

N-phenyl-benzimidoyl chloride

3-methylbut-3-enyl N-phenylbenzimidate
1252581-35-3

3-methylbut-3-enyl N-phenylbenzimidate

Conditions
ConditionsYield
Stage #1: 2-methyl-1-buten-4-ol With sodium hydride In tetrahydrofuran; mineral oil at 0 - 30℃; for 1.25h;
Stage #2: N-phenyl-benzimidoyl chloride In tetrahydrofuran; mineral oil at 0 - 20℃; for 20h;
100%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

chloro-trimethyl-silane
75-77-4

chloro-trimethyl-silane

4-mesyloxy-2-methylbutene
80352-66-5

4-mesyloxy-2-methylbutene

Conditions
ConditionsYield
With pyridine In dichloromethane at 0℃; for 1.5h; Inert atmosphere;100%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

pivaloyl chloride
3282-30-2

pivaloyl chloride

3-methylbut-3-en-1-yl pivalate

3-methylbut-3-en-1-yl pivalate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃;100%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

2,4-Dinitrofluorobenzene
70-34-8

2,4-Dinitrofluorobenzene

isopentenyl 2,4-dinitrophenyl ether
107909-39-7

isopentenyl 2,4-dinitrophenyl ether

Conditions
ConditionsYield
With triethylamine 1.) 30 min, 70 deg C, 2.) 12 h, room temperature;99%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

ortho-nitrofluorobenzene
1493-27-2

ortho-nitrofluorobenzene

1-((3-methylbut-3-en-1-yl)oxy)-2-nitrobenzene
847256-40-0

1-((3-methylbut-3-en-1-yl)oxy)-2-nitrobenzene

Conditions
ConditionsYield
Stage #1: 2-methyl-1-buten-4-ol With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 0.25h;
Stage #2: ortho-nitrofluorobenzene In tetrahydrofuran; mineral oil at 0 - 20℃; for 2h;
99%
Stage #1: 2-methyl-1-buten-4-ol With sodium hydride; N,N-dimethyl-formamide
Stage #2: ortho-nitrofluorobenzene at 50℃;
84%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

N-tosyl-2-iodoaniline
61613-20-5

N-tosyl-2-iodoaniline

C18H20INO2S
1454769-83-5

C18H20INO2S

Conditions
ConditionsYield
With triphenylphosphine; diethylazodicarboxylate In dichloromethane at 0 - 20℃; Inert atmosphere;99%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

4-Fluorophenol
371-41-5

4-Fluorophenol

C11H13FO

C11H13FO

Conditions
ConditionsYield
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran; toluene at 20℃; for 22h; Inert atmosphere;99%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

methyl 4-hydroxylbenzoate
99-76-3

methyl 4-hydroxylbenzoate

C13H16O3

C13H16O3

Conditions
ConditionsYield
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran; toluene at 20℃; for 1h; Inert atmosphere;99%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

2-Thiophenecarbonyl chloride
5271-67-0

2-Thiophenecarbonyl chloride

3-methylbut-3-en-1-yl thiophene-2-carboxylate

3-methylbut-3-en-1-yl thiophene-2-carboxylate

Conditions
ConditionsYield
With dmap; triethylamine In dichloromethane at 0℃; for 2h; Inert atmosphere;99%
With dmap; triethylamine In dichloromethane at 20℃;90%
With dmap; triethylamine In dichloromethane at 0 - 20℃;83%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

4-Bromobenzoic acid
586-76-5

4-Bromobenzoic acid

3-methylbut-3-en-1-yl 4-bromobenzoate

3-methylbut-3-en-1-yl 4-bromobenzoate

Conditions
ConditionsYield
Stage #1: 4-Bromobenzoic acid With 1,1'-carbonyldiimidazole In dichloromethane at 20℃; for 1h;
Stage #2: 2-methyl-1-buten-4-ol In dichloromethane at 20℃;
99%
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 24h;90%
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃;
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

phthalic anhydride
85-44-9

phthalic anhydride

o-((3-methylbut-3-enoxy)carbonyl)benzoic acid
113793-37-6

o-((3-methylbut-3-enoxy)carbonyl)benzoic acid

Conditions
ConditionsYield
In pyridine; benzene at 100℃; for 2h;98%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

tert-butyldimethylsilyl chloride
18162-48-6

tert-butyldimethylsilyl chloride

1-(tert-butyldimethylsiloxy)-3-methyl-3-butene
74915-94-9

1-(tert-butyldimethylsiloxy)-3-methyl-3-butene

Conditions
ConditionsYield
With 1H-imidazole In dichloromethane at 20℃; for 18h;98%
With 1H-imidazole In dichloromethane at 20℃; for 18h;94%
With 1H-imidazole In N,N-dimethyl-formamide for 4h; Ambient temperature;90%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

4-Methyl-3,4,5,6-tetrahydro-2H-pyran-2-ol
18653-57-1

4-Methyl-3,4,5,6-tetrahydro-2H-pyran-2-ol

tetrahydro-2-(3-methyl-3-butenoxy)-4-methyl-2H-pyran

tetrahydro-2-(3-methyl-3-butenoxy)-4-methyl-2H-pyran

Conditions
ConditionsYield
In hexane98%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

N-phthaloylglycine
4702-13-0

N-phthaloylglycine

3-methylbut-3-en-1-yl 2-(1,3-dioxoisoindolin-2-yl)acetate
1454661-80-3

3-methylbut-3-en-1-yl 2-(1,3-dioxoisoindolin-2-yl)acetate

Conditions
ConditionsYield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 12h;98%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

HSiPh3
789-25-3

HSiPh3

3-methyl-4-(triphenylsilyl)butan-1-ol

3-methyl-4-(triphenylsilyl)butan-1-ol

Conditions
ConditionsYield
With potassium carbonate; eosin y; triisopropylsilanethiol In 1,4-dioxane; water at 32 - 34℃; for 12h; Inert atmosphere; Irradiation;98%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

lauric acid
143-07-7

lauric acid

3-methylbut-3-en-1-yl dodecanoate

3-methylbut-3-en-1-yl dodecanoate

Conditions
ConditionsYield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; Inert atmosphere;98%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

acetic acid
64-19-7

acetic acid

3-methyl-3-buten-1-yl acetate
5205-07-2

3-methyl-3-buten-1-yl acetate

Conditions
ConditionsYield
With toluene-4-sulfonic acid In toluene at 100 - 105℃; for 4h;97.3%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

2,4-Dinitrofluorobenzene
70-34-8

2,4-Dinitrofluorobenzene

1-(dinitro-2,4-phenoxy)-3-methyl-2-butene
61078-10-2

1-(dinitro-2,4-phenoxy)-3-methyl-2-butene

Conditions
ConditionsYield
With triethylamine 1.) 30 min, 70 deg C, 2.) 12 h, room temperature;97%
2-methyl-1-buten-4-ol
763-32-6

2-methyl-1-buten-4-ol

benzyl bromide
100-39-0

benzyl bromide

(((3-methylbut-3-en-1-yl)oxy)methyl)benzene
58558-53-5

(((3-methylbut-3-en-1-yl)oxy)methyl)benzene

Conditions
ConditionsYield
With sodium hydride In tetrahydrofuran at 20℃; for 12h;97%
With tetra-(n-butyl)ammonium iodide; sodium hydride In tetrahydrofuran 1.) r.t., 2.) 40 deg C, 4 h;91%
With tetra-(n-butyl)ammonium iodide; sodium hydride In tetrahydrofuran at 20℃;89%
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