Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and
hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developmen
Cas:6285-05-8
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryHunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiry4'-Chloropropiophenone Basic information Product Name: 4'-Chloropropiophenone Synonyms: 1-(4-chlorophenyl)-1-propanon;4’-chloro-propiophenon;chloropro
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryProduct Name: 4'-Chloropropiophenone Synonyms: 1-(4-chlorophenyl)-1-propanon;4’-chloro-propiophenon;chloropropiophenone;Ethyl p-chlorophenyl ketone;p-chloro-propiophenon;Propiophenone, 4'-chloro-;Propiophenone, p-chloro-;
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inquiryProduct Description Product website: http://www.finerchem.com Product Name 4'-Chloropropiophenone CAS No. 6285-05-8
Cas:6285-05-8
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inquiryOur advantages: 1. High quality and competitive price: 1) Standard: BP/USP/EP/ enterprise standard 2) All purity ≥99% 3) We are manufacturers and can provide high quality products at factory prices. 2. Fast and safe delivery 1) The package c
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryOur Advantage 1. Rich experience We specialize in this filed for many years, our APIs exported to all over the world and and we established long friendly relations of cooperation with our clients. 2. Great quality,purity and favorable Good qual
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inquiry4'-Chloropropiophenone CAS:6285-05-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Hebei Mojin Biotechnology Co., Ltd,Our business covers more than 30 countries, most of the big customers come from Europe, America and other countries in the world, we can guarantee the quality and price. In recent decades, with the efforts of all em
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:6285-05-8
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inquiry4'-Chloropropiophenone cas 6285-05-8 Purity: 99% Min Application: Intermediates Appearance: Powder Package: Bag Delivery: 3-5days Our Advantage & Service 1.Top quality: Using high quality material and establishing a strict qualit
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:6285-05-8
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inquirySupply 4'-Chloropropiophenone/CAS NO.:6285-05-8Appearance:White crystalline powder Storage:Keep it in dry and cold place Package:according to customers' requirements Application:Research Chemicals Transportation:By air(EMS or EUB or FedEx or TNT ect.
Cas:6285-05-8
Min.Order:1 Gram
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inquirySuperior quality, moderate price & quick delivery. Appearance:white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediate
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; palladium diacetate; toluene-4-sulfonic acid In water; acetonitrile at 20℃; for 6h; Wacker Oxidation; chemoselective reaction; | 98% |
Conditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at 10 - 25℃; for 2h; Solvent; Temperature; Reagent/catalyst; | 96.5% |
With aluminum (III) chloride at 0 - 60℃; Inert atmosphere; | 87% |
With aluminium trichloride for 3h; Friedel-Crafts acylation; cooling; | 74% |
1-(4-chlorophenyl)-N-hydroxypropan-1-imine
4'-chloropropiophenone
Conditions | Yield |
---|---|
With cetyltrimethylammonium peroxodisulphate In acetonitrile for 0.366667h; Reflux; | 94% |
p-chlorophenylvinylcarbinol
4'-chloropropiophenone
Conditions | Yield |
---|---|
With 2C25H28N2OP(1-)*2Cl(1-)*2Ru(2+) In tetrahydrofuran at 80℃; for 4h; Inert atmosphere; Schlenk technique; Sealed tube; | 93% |
With tetrapropylammonium perruthennate; undecan-2-ol In fluorobenzene Isomerization; Heating; | 87% |
With C13H21Cl2N3PRu(1+)*Cl(1-); potassium carbonate In tetrahydrofuran at 75℃; for 20h; Catalytic behavior; Inert atmosphere; Sealed tube; | 80% |
C10H12ClN3O
4'-chloropropiophenone
Conditions | Yield |
---|---|
With cetyltrimethylammonium peroxodisulphate In acetonitrile for 0.466667h; Reflux; | 90% |
Conditions | Yield |
---|---|
With chlorine[2-(4,5-dihydro-1H-imidazol-2-yl)-6-methoxypyridine](pentamethylcyclopentadienyl)iridium(III) chloride; potassium hydroxide In water at 80℃; Schlenk technique; Inert atmosphere; | 90% |
With chlorine[2-(4,5-dihydro-1H-imidazol-2-yl)-6-methoxypyridine](pentamethylcyclopentadienyl)iridium(III) chloride; potassium hydroxide In water at 80℃; for 14h; Schlenk technique; Inert atmosphere; chemoselective reaction; | 90% |
4'-chloropropiophenone
Conditions | Yield |
---|---|
With dihydrogen peroxide; bromine In dichloromethane; water at 20℃; for 24h; | 89% |
1-(4-chlorophenyl)-1-propanol
4'-chloropropiophenone
Conditions | Yield |
---|---|
With peracetic acid; 4-acetylamino-2,2,6,6-tetramethyl-1-piperidinoxy In acetonitrile at 20℃; for 10h; | 88% |
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium acetate; (S)-3-phenyl-2-(phenylamino)propionic acid; copper(ll) bromide In water for 24h; Reflux; Schlenk technique; | 87% |
With diisopropoxyaluminium trifluoroacetate; 4-nitrobenzaldehdye In benzene for 0.75h; Ambient temperature; | 85% |
Conditions | Yield |
---|---|
With iron(III)-acetylacetonate In tetrahydrofuran at -78℃; | 87% |
C9H10BrClO
A
4'-chloropropiophenone
B
1-(4-chlorophenyl)propan-2-one
Conditions | Yield |
---|---|
With diethylzinc In dichloromethane at 20℃; for 2h; | A 5% B 86% |
Conditions | Yield |
---|---|
With 1,10-Phenanthroline; nickel(II) bromide 2-methoxyethyl ether complex; sodium hydrogencarbonate In water at 100℃; for 5h; Autoclave; | 81% |
1-(4-chlorophenyl)-2-nitro-1-propanone
4'-chloropropiophenone
Conditions | Yield |
---|---|
With tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) In benzene at 80℃; for 1.5h; | 78% |
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In benzene at 80℃; for 2h; | 78% |
With 1-Benzyl-1,4-dihydronicotinamide In N,N,N,N,N,N-hexamethylphosphoric triamide for 48h; Ambient temperature; Irradiation; | 62% |
With 1-Benzyl-1,4-dihydronicotinamide In N,N,N,N,N,N-hexamethylphosphoric triamide for 48h; Ambient temperature; Irradiation; | 45% |
N-<1-(4-chlorophenyl)propylidene>-2,6-xylylamine
4'-chloropropiophenone
Conditions | Yield |
---|---|
With hydrogenchloride In tetrahydrofuran for 15h; Ambient temperature; | 78% |
1-(4-chlorophenyl)-2-tosylethanone
methylmagnesium bromide
4'-chloropropiophenone
Conditions | Yield |
---|---|
With bis(triphenylphosphine)nickel(II) diiodide; tricyclohexylphosphine In tetrahydrofuran at 80℃; Kumada Cross-Coupling; Inert atmosphere; | 77% |
ethylmagnesium bromide
4-chloro-N-methoxy-N-methylbenzamide
4'-chloropropiophenone
Conditions | Yield |
---|---|
In diethyl ether at 0℃; for 3h; | 77% |
Conditions | Yield |
---|---|
Stage #1: para-chlorobenzoic acid With methyllithium In tetrahydrofuran; diethyl ether at -78℃; for 1h; Schlenk technique; Inert atmosphere; Stage #2: Zn(2+)*Li(1+)*2C3H7(1-)*C5H11(1-) In 1,4-dioxane at 50℃; for 18h; Schlenk technique; Inert atmosphere; chemoselective reaction; | 76% |
para-chloroacetophenone
N,N-dimethyl-formamide
4'-chloropropiophenone
Conditions | Yield |
---|---|
With ammonium peroxydisulfate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer In water at 110℃; for 3h; Inert atmosphere; Sealed tube; | 73% |
sodium p-chlorobenzenesulphinate
propiononitrile
4'-chloropropiophenone
Conditions | Yield |
---|---|
With palladium(II) trifluoroacetate; trifluoroacetic acid; 6-methyl-2,2'-bipyridine In tetrahydrofuran; water at 100℃; for 1h; Microwave irradiation; | 73% |
Conditions | Yield |
---|---|
With polyphosphoric acid for 0.025h; Microwave irradiation; | 70% |
2-chloro-1-(4-chlorophenyl)propan-1-one
A
4'-chloropropiophenone
B
1-(4-chlorophenyl)-2-hydroxypropan-1-one
C
2-(4-Chloro-phenyl)-propionic acid
Conditions | Yield |
---|---|
With methyloxirane In water; acetone Irradiation; pH neutral; | A 25% B 20% C 45% |
Conditions | Yield |
---|---|
Stage #1: bromochlorobenzene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Stage #2: propionaldehyde In tetrahydrofuran; hexane at -78℃; for 1h; Stage #3: With iodine; potassium carbonate In tert-butyl alcohol for 4h; Reflux; | 45% |
2-chloro-1-(4-chlorophenyl)propan-1-one
A
4'-chloropropiophenone
B
methyl 2-(p-chlorophenyl)propionate
C
α-methoxy-p-chloropropiophenone
Conditions | Yield |
---|---|
With methyloxirane In methanol Irradiation; pH neutral; | A 24% B n/a C 30% |
methylidene di(4-chlorobenzoate)
ethylmagnesium bromide
A
4'-chloropropiophenone
B
propyl 4-chloro benzoate
C
3-(4'-chlorophenyl)pentan-3-ol
D
para-chlorobenzoic acid
Conditions | Yield |
---|---|
In tetrahydrofuran at 0 - 20℃; for 3h; Substitution; addition; | A 21% B 26% C 16% D 17% |
propionaldehyde oxime
4-chlorophenyldiazonium salt
4'-chloropropiophenone
Conditions | Yield |
---|---|
With sodium acetate; copper(II) sulfate; sodium sulfite in wss. Loesung und anschl. mit wss. HCl; |
4-chlorophenyldiazonium salt
4'-chloropropiophenone
Conditions | Yield |
---|---|
With sodium hydroxide; water Behandeln des Reaktionsgemisches mit Luft und anschl. Erhitzen mit ws. HCl; |
1-(p-chlorophenyl)-1-methoxyethene
A
4'-chloropropiophenone
B
1,4-bis-(4-chloro-phenyl)-2-methyl-butane-1,4-dione
Conditions | Yield |
---|---|
at 300℃; |
Conditions | Yield |
---|---|
With carbon disulfide; aluminium trichloride |
4-Cyanochlorobenzene
ethyltriphenylphosphonium iodide
4'-chloropropiophenone
Conditions | Yield |
---|---|
(i) nBuLi, (ii) /BRN= 1072122/, (iii) aq. HCl; Multistep reaction; |
1-(4-chlorophenyl)-2,2-dichloro-1-propanone
4'-chloropropiophenone
Conditions | Yield |
---|---|
With hydrogen; methylamine; palladium on barium sulfate In methanol |
1-(4-Chlorophenyl)-2-(4-methoxyphenyl)-3-methylcyclopropane
A
4'-chloropropiophenone
r-3-(4-Chlorophenyl)-c-4-methyl-t-5-(4-methoxyphenyl)-1,2-dioxolane
r-3-(4-Chlorophenyl)-t-4-methyl-c-5-(4-methoxyphenyl)-1,2-dioxolane
D
4-chlorobenzaldehyde
E
4-methoxy-benzaldehyde
F
E-1-(4'-methoxyphenyl)prop-1-ene
Conditions | Yield |
---|---|
With magnesium(II) perchlorate; oxygen; 9,10-Dicyanoanthracene In acetonitrile for 0.0333333h; Rate constant; Thermodynamic data; Mechanism; Ambient temperature; Irradiation; ΔG; |
Conditions | Yield |
---|---|
With bromine at 20℃; for 0.333333h; | 100% |
Stage #1: 4'-chloropropiophenone With bromine In methanol at 20℃; for 0.166667h; Stage #2: With hydrogen bromide In methanol; water for 110h; Inert atmosphere; | 98% |
With bromine; hydrogen bromide In methanol at 20℃; for 110h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With potassium hydroxide; hydrogen; Aliquat 336; tetrakis(triphenylphosphine) palladium(0); 1-Decanol In 2,2,4-trimethylpentane at 25℃; for 2h; atmospheric pressure; | 100% |
With palladium on activated charcoal; formic acid; N,N-dimethyl-formamide for 6h; Heating; | 85% |
4'-chloropropiophenone
oxalic acid diethyl ester
4-(4-chlorophenyl)-3-methyl-2,4-dioxobutyric acid ethyl ester
Conditions | Yield |
---|---|
With sodium In ethanol at 20℃; for 18h; Claisen Condensation; | 100% |
With lithium tert-butoxide In tetrahydrofuran at 0 - 20℃; for 4h; Claisen Condensation; Inert atmosphere; | 82% |
Stage #1: oxalic acid diethyl ester With sodium ethanolate In ethanol at 20℃; for 0.166667h; Inert atmosphere; Stage #2: 4'-chloropropiophenone In ethanol at 20℃; for 24h; | 76.9% |
4'-chloropropiophenone
1-(4-chlorophenyl)-1-propanol
Conditions | Yield |
---|---|
With sodium tetrahydroborate In ethanol at 0 - 20℃; for 4h; | 99% |
With sodium tetrahydroborate In tetrahydrofuran; water for 0.25h; Heating; | 98% |
With sodium tetrahydroborate; sodium hydrogen sulfate In acetonitrile at 20℃; for 0.333333h; | 97% |
4'-chloropropiophenone
2-Allyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
Conditions | Yield |
---|---|
With indium iodide In tetrahydrofuran at 40℃; for 24h; | 99% |
With methanol; indium (III) tris(hexamethyldisilyl) amide In toluene at 20℃; for 6h; Inert atmosphere; | 98% |
4'-chloropropiophenone
benzoic acid
1-(4-chlorophenyl)-1-oxopropan-2-yl benzoate
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide In decane; ethyl acetate at 75℃; for 24h; Product distribution / selectivity; | 99% |
With tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide In ethyl acetate at 20 - 75℃; for 23h; | 91% |
With potassium carbonate; ethylene dibromide; potassium iodide In N,N-dimethyl-formamide at 60℃; Sealed tube; | 33% |
4'-chloropropiophenone
2,2,6,6-tetramethyl-piperidine-N-oxyl
1-(4-chlorophenyl)-2-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)propan-1-one
Conditions | Yield |
---|---|
With 2,6-di-tert-butyl-pyridine; 2-chloro-1,3,2-benzodioxaborole In dichloromethane at 0 - 20℃; for 3h; | 99% |
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; copper diacetate In 1,2-dichloro-benzene at 120℃; for 24h; Inert atmosphere; Schlenk technique; | 99% |
Conditions | Yield |
---|---|
With potassium phosphate; Pd(OAc)2*3H2O In 1,4-dioxane for 12h; Suzuki-Miyaura cross-coupling; Heating; | 98% |
With 4,4'-(phenylphosphinediyl)bis(2,6-dimethylmorpholine); caesium carbonate; tris(dibenzylideneacetone)dipalladium (0) In 1,4-dioxane for 16h; Suzuki-Miyaura coupling; Heating; | 96% |
Conditions | Yield |
---|---|
toluene-4-sulfonic acid In toluene Heating / reflux; Dean-Stark apparatus; | 98% |
morpholine
4'-chloropropiophenone
2-morpholino-1-(4-(chloro)phenyl)propan-1-one
Conditions | Yield |
---|---|
With 2,6-bis[(4,4-dimethyl)-2-oxazolin-2-yl]pyridine copper bromide In dimethyl sulfoxide at 10℃; for 15h; | 98% |
Stage #1: 4'-chloropropiophenone With 2,6-bis[(4,4-dimethyl)-2-oxazolin-2-yl]pyridine copper bromide In dimethyl sulfoxide at 20℃; for 0.166667h; Green chemistry; Stage #2: morpholine In dimethyl sulfoxide at 10℃; for 10h; Green chemistry; | 97% |
With sodium percarbonate; ammonium iodide In acetonitrile at 50℃; for 18h; | 78% |
With ammonium iodide In acetonitrile at 20℃; Electrolysis; | 48% |
Conditions | Yield |
---|---|
With copper(l) iodide; trans-N,N'-dimethylcyclohexane-1,2-diamine In acetonitrile at 200℃; for 1h; Microwave irradiation; Inert atmosphere; | 97% |
Conditions | Yield |
---|---|
Stage #1: 4'-chloropropiophenone With 2,6-bis[(4,4-dimethyl)-2-oxazolin-2-yl]pyridine copper bromide In dimethyl sulfoxide at 20℃; for 0.166667h; Green chemistry; Stage #2: piperidine In dimethyl sulfoxide at 10℃; for 10h; Green chemistry; | 97% |
With ammonium iodide In acetonitrile at 20℃; Electrolysis; | 70% |
4'-chloropropiophenone
1-(4-chlorophenyl)-2-(hydroxyimino)propan-1-one
Conditions | Yield |
---|---|
With chloro-trimethyl-silane; isopentyl nitrite In dichloromethane at -20℃; | 96% |
With n-Butyl nitrite In Petroleum ether for 5h; | 96.9% |
With chloro-trimethyl-silane; tert.-butylnitrite In tetrahydrofuran; dichloromethane at -20 - 20℃; Inert atmosphere; | 81% |
4'-chloropropiophenone
ethyl bromoacetate
3-(4-Chloro-phenyl)-3-hydroxy-pentanoic acid ethyl ester
Conditions | Yield |
---|---|
With zinc In diethyl ether; benzene for 5h; Heating; | 96.9% |
With zinc In diethyl ether; benzene for 3h; Heating; | 88% |
With zinc In toluene; benzene Heating; |
4'-chloropropiophenone
trimethyl orthoformate
methyl 2-(p-chlorophenyl)propionate
Conditions | Yield |
---|---|
With sulfuric acid; 3-[4-(diacetoxyiodo)phenoxy]-1-propyl-N,N,N-trimethylammonium 4-methylbenzenesulfonate at 60℃; for 5h; Inert atmosphere; | 96% |
With iodine; lithium perchlorate Ambient temperature; anodic oxidation at constant current; | 88% |
4'-chloropropiophenone
di-p-tolylcarbodiimide
4-chloro-N-(4-tolyl)benzamide
Conditions | Yield |
---|---|
With [{HMn(CO)4}3] In 1,4-dioxane at 135℃; for 24h; Sealed tube; Inert atmosphere; | 96% |
methanol
4'-chloropropiophenone
1-(4-chlorophenyl)-2-methylidenepropan-1-one
Conditions | Yield |
---|---|
With potassium carbonate; triphenylphosphine at 20℃; for 4h; Irradiation; Green chemistry; | 96% |
methanol
4'-chloropropiophenone
1-(4-chlorophenyl)-2-methylpropan-1-one
Conditions | Yield |
---|---|
With C34H27IrN2P(1+)*C32H12BF24(1-); caesium carbonate at 65℃; for 24h; Inert atmosphere; | 95% |
With trimethylamine-N-oxide; tricarbonyl(η4-1,3-bis(trimethylsilyl)-4,5,6,7-tetrahydro-2H-inden-2-one)iron; potassium carbonate at 80℃; for 24h; | 91% |
With C21H17ClN5ORu(1+)*Cl(1-); potassium tert-butylate at 85℃; for 24h; Inert atmosphere; Schlenk technique; Glovebox; Sealed tube; | 90% |
Conditions | Yield |
---|---|
With Selectfluor at 120℃; Mannich Aminomethylation; Sealed tube; | 95% |
Conditions | Yield |
---|---|
Stage #1: N-methyl-3-formylindole; acetophenone With sodium hydroxide In ethanol at 25℃; Stage #2: 4'-chloropropiophenone With [2,2]bipyridinyl; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; copper(II) choride dihydrate; acetic acid In chlorobenzene at 120℃; for 16h; | 95% |
4'-chloropropiophenone
Conditions | Yield |
---|---|
Stage #1: 4'-chloropropiophenone With lithium hexamethyldisilazane In tetrahydrofuran at 0℃; under 3750.38 Torr; for 0.0166667h; Flow reactor; Inert atmosphere; Green chemistry; Stage #2: With 1-chloro-1-nitrosocyclopentane In tetrahydrofuran; tert-butyl methyl ether at 0℃; under 3750.38 Torr; for 0.0166667h; Flow reactor; Inert atmosphere; Green chemistry; Stage #3: With hydrogenchloride In tetrahydrofuran; tert-butyl methyl ether; water at 60℃; under 3750.38 Torr; for 0.0166667h; Flow reactor; Inert atmosphere; Green chemistry; | 95% |
4'-chloropropiophenone
Conditions | Yield |
---|---|
With [hydroxy(tosyloxy)iodo]benzene; iodine; 1-butyl-3-methylimidazolium Tetrafluoroborate at 60℃; Ionic liquid; | 94% |
With N-iodo-succinimide; toluene-4-sulfonic acid Microwave irradiation; | 83% |
4'-chloropropiophenone
2-chloro-1-(4-chlorophenyl)propan-1-one
Conditions | Yield |
---|---|
With N-chloro-succinimide; urea-hydrogen peroxide; 1-butyl-3-methylimidazolium Tetrafluoroborate at 60℃; | 94% |
With Aluminum(III) chloride hexahydrate; urea-hydrogen peroxide; 1-butyl-3-methylimidazolium Tetrafluoroborate at 60℃; for 9h; | 80% |
2-Butylfuran
4'-chloropropiophenone
2-n-butyl-5-(4-propionylphenyl)furan
Conditions | Yield |
---|---|
With 1,1'-bis(dicyclohexylphosphanyl)-3,3'-di(triphenylmethyl)ferrocene; tetrabutylammomium bromide; potassium acetate; palladium diacetate In N,N-dimethyl acetamide at 150℃; for 16h; Inert atmosphere; | 94% |
With 1,1',2-tris(diphenylphosphino)-3',4-di-tert-butyl ferrocene; tetrabutylammomium bromide; potassium acetate; palladium diacetate In N,N-dimethyl acetamide at 150℃; for 16h; Inert atmosphere; | 84% |
4'-chloropropiophenone
2-(2-fluorophenoxy)-5-methylpyridine
1-{3'-fluoro-2'-[(5-methylpyridin-2-yl)oxy]-[1,1'-biphenyl]-4-yl}propan-1-one
Conditions | Yield |
---|---|
With (p-cymene)ruthenium(II) chloride; mesitylenecarboxylic acid; potassium carbonate In toluene at 120℃; for 20h; Inert atmosphere; | 94% |
Conditions | Yield |
---|---|
With p-nitrobenzenesulfonic acid; 3-chloro-benzenecarboperoxoic acid; sodium iodide In acetonitrile at 80℃; for 24h; Inert atmosphere; Schlenk technique; | 94% |
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