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Iron(III) fluoride Basic information Product Name: Iron(III) fluoride Synonyms: IRON FLUORIDE;FE F2;FERROUS FLUORIDE;Iron (III) fluoride, anhydrous;Iron(III)fluoride,anhydrous,97%min;Iron(III) trifluoride;FERRIC FLUORIDE, ANHYDROUS;Iron(III)fluoride
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iron(III) fluoride
Conditions | Yield |
---|---|
With F reaction of Fe2O3 with F on slight heating with flaming up; formation of FeF3;; |
iron(III) fluoride
Conditions | Yield |
---|---|
With F reaction of Fe2O3 with F on slight heating with flaming up; formation of FeF3;; |
B
iron(III) fluoride
C
hydrogen fluoride
D
nitrogen
E
ammonia
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: H2O; heating up to 600°C; detd. by X-ray diffraction; |
B
iron(III) fluoride
C
hydrogen fluoride
D
nitrogen
E
ammonia
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: H2O; heating up to 600°C; detd. by X-ray diffraction; |
Conditions | Yield |
---|---|
In neat (no solvent) heating (3 h, 400°C); |
Conditions | Yield |
---|---|
In neat (no solvent) decompn. with gaseous HF, formation of FeF3;; | |
In neat (no solvent) reaction in coldness to amorphous FeF3; at 1000 °C formation of crystalline FeF3;; | |
In neat (no solvent) decompn. with gaseous HF, formation of FeF3;; |
Conditions | Yield |
---|---|
With alkali fluoride In water byproducts: iron(III) fluoro anion; |
Conditions | Yield |
---|---|
In neat (no solvent) reaction of FeCl3 with F2 to FeF3 at elevated temp.;; | |
In not given reaction of FeCl3 with F2;; | |
In not given reaction of FeCl3 with F2;; | |
In neat (no solvent) reaction of FeCl3 with F2 to FeF3 at elevated temp.;; |
Conditions | Yield |
---|---|
In water | |
In neat (no solvent) in Monel or glassy carbon or corundum vessel; at 100-370°C for 3h in F2 flow; elem. anal.; | |
In neat (no solvent) fluorination of mixt. of FeF2 and FeF3 with F2 (350 - 400°C); |
Conditions | Yield |
---|---|
In neat (no solvent) heating (3 h, 400°C); |
Conditions | Yield |
---|---|
In solid byproducts: H2O, HF, NH3; react. product: (NH4)3FeF6 at 180°C, NH4FeF4 at 320°C, FeF3 at 430°C; XRD, IR, chem. anal.; |
Conditions | Yield |
---|---|
In neat (no solvent) heated in a stream of HF;; contaminated by red oxyfluoride that can be removed by washing with warm dild. aq. HCl;; | |
In neat (no solvent) heated in a stream of HF;; contaminated by red oxyfluoride that can be removed by washing with warm dild. aq. HCl;; |
Conditions | Yield |
---|---|
In neat (no solvent) decompn. with gaseous HF, formation of FeF3;; | |
In neat (no solvent) reaction in coldness to amorphous FeF3; at 1000 °C formation of crystalline FeF3;; | |
In neat (no solvent) decompn. with gaseous HF, formation of FeF3;; |
Conditions | Yield |
---|---|
In neat (no solvent) 710°C; elem. anal.; | |
710°C; elem. anal.; |
Conditions | Yield |
---|---|
With alkali fluoride In water byproducts: iron(III) fluoro anion; |
Conditions | Yield |
---|---|
In water hydrothermal synthesis; | A 0% B n/a |
Conditions | Yield |
---|---|
With fluorine on slight warming of FeO and fluorine vigorous glowing and formation of iron fluoride;; |
Conditions | Yield |
---|---|
In neat (no solvent) reaction of FeCl3 with F2 to FeF3 at elevated temp.;; | |
In not given reaction of FeCl3 with F2;; | |
In not given reaction of FeCl3 with F2;; | |
In neat (no solvent) reaction of FeCl3 with F2 to FeF3 at elevated temp.;; |
Conditions | Yield |
---|---|
In neat (no solvent) a mixt. of iron filings and XeF2 was heated at 500°C in a nickelvessel; |
iron(III) fluoride
Conditions | Yield |
---|---|
With fluorine In neat (no solvent) react. at dark red heat; formation of iron fluoride;; | |
With F2 In neat (no solvent) react. at dark red heat; formation of iron fluoride;; |
Conditions | Yield |
---|---|
In water | |
In neat (no solvent) in Monel or glassy carbon or corundum vessel; at 100-370°C for 3h in F2 flow; elem. anal.; | |
In neat (no solvent) fluorination of mixt. of FeF2 and FeF3 with F2 (350 - 400°C); |
Conditions | Yield |
---|---|
In solid byproducts: H2O, HF, NH3; react. product: (NH4)3FeF6 at 180°C, NH4FeF4 at 320°C, FeF3 at 430°C; XRD, IR, chem. anal.; |
Conditions | Yield |
---|---|
In neat (no solvent) heated in a stream of HF;; contaminated by red oxyfluoride that can be removed by washing with warm dild. aq. HCl;; | |
In neat (no solvent) heated in a stream of HF;; contaminated by red oxyfluoride that can be removed by washing with warm dild. aq. HCl;; |
Conditions | Yield |
---|---|
With H2O2 In hydrogen fluoride aq. HF; dissolving of pure iron powder in 48% HF, oxidatn. of the product by H2O2 in a strong acid medium; | |
fluorination of metallic Fe-powder; |
Conditions | Yield |
---|---|
With F2 In neat (no solvent) HF then F2-stream; |
Conditions | Yield |
---|---|
In neat (no solvent) 710°C; elem. anal.; | |
710°C; elem. anal.; |
Conditions | Yield |
---|---|
With tungsten In neat (no solvent) byproducts: FeF2; in calorimetric bomb; iron combusted in fluorine; XRD; TG; elem.anal.; cromy.; calorimetry; | |
In not given reaction of Fe with F2;; | |
Fe-powder, F2/N2 for 3 d at 300°C, cooled, powdered, pure F2 for 2 d at 400°C; | |
In not given reaction of Fe with F2;; |
Conditions | Yield |
---|---|
In neat (no solvent) heated in a stream of HF;; by washing with warm dild. aq. HCl contaminating red oxyfluoride can be removed;; | |
In neat (no solvent) heated in a stream of HF;; by washing with warm dild. aq. HCl contaminating red oxyfluoride can be removed;; |
Conditions | Yield |
---|---|
In hydrogen fluoride Fe(OH)3 dissolved in aq. HF and heated;; not isolated;; | |
In hydrogen fluoride aq. HF; Fe(OH)3 dissolved in aq. HF and heated;; not isolated;; |
Conditions | Yield |
---|---|
In water hydrothermal synthesis; | A 0% B n/a |
Conditions | Yield |
---|---|
In neat (no solvent) at 500°C for 2 days; powder XRD; | |
In water excess of aq. HF, evapn. (60°C), slow dehydration (anhydrous HF stream, 750°C, 6 h); |
Conditions | Yield |
---|---|
With fluorine on slight warming of FeO and fluorine vigorous glowing and formation of iron fluoride;; |
Conditions | Yield |
---|---|
In neat (no solvent) heating (6 h, 750°C, HF stream); |
Conditions | Yield |
---|---|
With nitric acid In water oxidized by HNO3 with excess of HF;; not isolated;; | |
With HNO3 In water oxidized by HNO3 with excess of HF;; not isolated;; |
iron(III) fluoride
Conditions | Yield |
---|---|
With ammonium fluoride; hydrogen fluoride In further solvent(s) FeF3*(x)H2O given into molten NH4F; heating in an inert gas stream gave an amorphous FeF3; heating in a stream of HF at 1000 °C formed crystals under partial sublimation;; contaminating red oxyfluoride can be removed by washing with warm dild. aq. HCl;; | |
With NH4F; HF In further solvent(s) FeF3*(x)H2O given into molten NH4F; heating in an inert gas stream gave an amorphous FeF3; heating in a stream of HF at 1000 °C formed crystals under partial sublimation;; contaminating red oxyfluoride can be removed by washing with warm dild. aq. HCl;; |
Conditions | Yield |
---|---|
In neat (no solvent) a mixt. of iron filings and XeF2 was heated at 500°C in a nickelvessel; |
iron(III) fluoride
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: H2O; under HF stream, 750°C; | |
In neat (no solvent) at 120℃; for 48h; |
Conditions | Yield |
---|---|
In neat (no solvent) 650°C; elem. anal.; | |
650°C; elem. anal.; |
iron(III) fluoride
Conditions | Yield |
---|---|
With fluorine In neat (no solvent) react. at dark red heat; formation of iron fluoride;; | |
With F2 In neat (no solvent) react. at dark red heat; formation of iron fluoride;; |
oxygen
B
iron(III) fluoride
Conditions | Yield |
---|---|
In solid dried oxygen passed for 30 min over FeF2 sample mounted in platinum device at 620-800°C; powder X-ray diffraction anal.; | A n/a B n/a C 0% |
Conditions | Yield |
---|---|
With steel corrosion of steel by UF6 at 120-400°C; | |
With steel corrosion of steel by UF6 at 120-400°C; |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: N2; heating in NO stream to 600°C; X-ray diffraction; |
Conditions | Yield |
---|---|
With H2O2 In hydrogen fluoride aq. HF; dissolving of pure iron powder in 48% HF, oxidatn. of the product by H2O2 in a strong acid medium; | |
fluorination of metallic Fe-powder; |
Conditions | Yield |
---|---|
With F2 In neat (no solvent) HF then F2-stream; |
Conditions | Yield |
---|---|
With H2S In methanol; triethylamine; N,N-dimethyl-formamide stirring mixt. of FeF3 and org. compd. in MeOH and DMF (2 min), addn. of Et3N, introduction of H2S (6 l/h); filtn., addn. of diethyl ether, standing (2-3 d, room temp., Ar atmosphere), filtn. washing (isopropanol, CS2 and Et2O), drying (air); elem. anal.; | 52% |
Conditions | Yield |
---|---|
With tungsten In neat (no solvent) byproducts: FeF2; in calorimetric bomb; iron combusted in fluorine; XRD; TG; elem.anal.; cromy.; calorimetry; | |
In not given reaction of Fe with F2;; | |
Fe-powder, F2/N2 for 3 d at 300°C, cooled, powdered, pure F2 for 2 d at 400°C; | |
In not given reaction of Fe with F2;; |
Conditions | Yield |
---|---|
In neat (no solvent) heated in a stream of HF;; by washing with warm dild. aq. HCl contaminating red oxyfluoride can be removed;; | |
In neat (no solvent) heated in a stream of HF;; by washing with warm dild. aq. HCl contaminating red oxyfluoride can be removed;; |
Conditions | Yield |
---|---|
In hydrogen fluoride Fe(OH)3 dissolved in aq. HF and heated;; not isolated;; | |
In hydrogen fluoride aq. HF; Fe(OH)3 dissolved in aq. HF and heated;; not isolated;; |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: HF; heated in a stream of HCl at red heat;; |
Conditions | Yield |
---|---|
In neat (no solvent) at 500°C for 2 days; powder XRD; | |
In water excess of aq. HF, evapn. (60°C), slow dehydration (anhydrous HF stream, 750°C, 6 h); |
Conditions | Yield |
---|---|
In neat (no solvent) heating (6 h, 750°C, HF stream); |
Conditions | Yield |
---|---|
With nitric acid In water oxidized by HNO3 with excess of HF;; not isolated;; | |
With HNO3 In water oxidized by HNO3 with excess of HF;; not isolated;; |
iron(III) fluoride
Conditions | Yield |
---|---|
With ammonium fluoride; hydrogen fluoride In further solvent(s) FeF3*(x)H2O given into molten NH4F; heating in an inert gas stream gave an amorphous FeF3; heating in a stream of HF at 1000 °C formed crystals under partial sublimation;; contaminating red oxyfluoride can be removed by washing with warm dild. aq. HCl;; | |
With NH4F; HF In further solvent(s) FeF3*(x)H2O given into molten NH4F; heating in an inert gas stream gave an amorphous FeF3; heating in a stream of HF at 1000 °C formed crystals under partial sublimation;; contaminating red oxyfluoride can be removed by washing with warm dild. aq. HCl;; |
Conditions | Yield |
---|---|
With hydrogen fluoride In water | |
With HF In water |
iron(III) fluoride
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: H2O; under HF stream, 750°C; | |
In neat (no solvent) at 120℃; for 48h; |
Conditions | Yield |
---|---|
In neat (no solvent) 650°C; elem. anal.; | |
650°C; elem. anal.; |
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