CAS No.7783-55-3,PHOSPHORUS TRIFLUORIDE Suppliers,MSDS download

Dayang Chem (Hangzhou) Co.,Ltd.

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Hangzhou J&H Chemical Co., Ltd.

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Zibo Hangyu Biotechnology Development Co., Ltd

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Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates

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Henan Tianfu Chemical Co., Ltd.

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Antimex Chemical Limied

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Hubei Langyou International Trading Co., Ltd

Trifluorophosphane Application:Trifluorophosphane

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SAGECHEM LIMITED

laboratory Application:Synthetic building block

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Hunan Longxianng Runhui Trading Co.,Ltd

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Qingdao Sigma Chemical Co., Ltd.

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Hangzhou Share Chemical Co., Ltd

At Share Chemical Company, we scrupulously abide by our policy of “Excellent Quality at a Reasonable Price”. We strive to satisfy all of our customers by providing the finest quality products supported by the finest in customer servi

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HuBei Ipure Biotech CO.,ltd

Strict quality control system and PHD We has passed through the ISO9001:2016 Quality System Certificate, we have strict quality control system. we have about 300 employees, including 90 full-time PHD 15 PHD and masters above, 153 undergraduates, w

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Hebei mingxing biotech co.,ltd

Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers. Prompt reaction, good quality and best service make us reliable and outstanding in this industry.Appearance:yellow to white solid or po

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Nanjing Raymon Biotech Co., Ltd.

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Hebei Minshang Biotechnology Co., Ltd

Trifluorophosphane Application:intermediates

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Skyrun Industrial Co.,Ltd

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Phosphorus(III) fluoride, 99%

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Hangzhou Fenjun Chemical Co Ltd.

Trifluorophosphane Application:Trifluorophosphane

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Hebei Ruishun Trade Co.,Ltd

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Chemical Co.Ltd

Phosphorus(III) fluoride, 99%Appearance:Off white to slight yellow solid Storage:Stored in shaded, cool and dry places Package:1L 5L 10L 25L bottle Application:pharma intermediate Transportation:Handle with cares to avoid damaging the packages. Prote

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Synthetic route

: 1279123-63-5
potassium hydrogenfluoride

: 7789-60-8
phosphorus tribromide

: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
In acetonitrile byproducts: KBr, HBr; PBr3 in MeCN was slowly added to a boiling suspn. of KHF2 in MeCN;; the gaseous prod. was condensed in trap cooled by liq. N2 and distd. at -100°C; elem. anal.; IR;	90%

: 1279123-63-5
potassium hydrogenfluoride

: 7719-12-2, 52843-90-0
phosphorus trichloride

: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
In acetonitrile byproducts: KCl, HCl; PCl3 in MeCN was slowly added to a boiling suspn. of KHF2 in MeCN;; the gaseous prod. was condensed in trap cooled by liq. N2 and distd. at -100°C; elem. anal.; IR;	87.7%

: 14791-57-2
silyl bromide

: 34326-59-5
bis(difluorophosphino)amine

: 75-50-3
trimethylamine

A: 11128-24-8
fluorosilane

B: 71579-72-1
bis(difluorophosphine)silylamine

C: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
In neat (no solvent) byproducts: (NHMe3)Br; absence of air and moisture (vac. line); condensing NMe3 onto mixt. of NH(PF2)2 and SiBrH3, warming to room temp. for 15 s; fractional distn.;	A n/a B 87% C n/a

...Expand

: bis(trifluoromethyl)cadmium*(pyridine)2

: 13455-01-1
phosphorous triiodide

: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
In pyridine	69%

: 14335-40-1
chlorodifluorophosphine

: 7664-41-7
ammonia

A: 25757-74-8
aminodifluorophosphine

: 60448-09-1
diaminodifluorophosphorane

C: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
In neat (no solvent) expanding excess of NH3 into PClF2, standing for 3 min; removal of volatiles, fractional low-temp. distn. (vac., trap at 227 K);mass spectroscopy;	A n/a B 42% C n/a

...Expand

: fluoride

: 7719-12-2, 52843-90-0
phosphorus trichloride

: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
In melt passing PCl3 vapour into a melt of alkali fluorides at 500°C;;	20%

: phosphorous

: 7664-39-3
hydrogen fluoride

: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
500°C, closed reactor;	5%
In not given heating red P with Hf under pressure;;

: phosphorous

: 13465-66-2, 271781-78-3
selenium(IV) fluoride

A: 7446-08-4
selenium(IV) oxide

B: 13478-20-1
trifluorophosphoric acid

C: 1087413-67-9
nitrosylsulfuric acid fluoride

D: 7783-55-3
trifluorophosphane

...Expand

: ammonium fluoride

: 7719-12-2, 52843-90-0
phosphorus trichloride

A: 15597-63-4
phosphorus fluoride dichloride

B: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
In neat (no solvent) refluxing with dry NH4F;;
In neat (no solvent) heating PCl3 with dry NH4F with a reflux condenser;;
In neat (no solvent) refluxing with dry NH4F;;
In neat (no solvent) heating PCl3 with dry NH4F with a reflux condenser;;

...Expand

: calcium fluoride

: phosphorus pentoxide

: 7647-14-5
sodium chloride

A: 13478-20-1
trifluorophosphoric acid

B: 13769-76-1
phosphoryl dichloride fluoride

C: 13769-75-0
phosphorus oxydifluorochloride

D: 7783-55-3
trifluorophosphane

E: 10025-87-3, 12599-09-6, 63736-95-8
trichlorophosphate

Conditions

Conditions	Yield
In neat (no solvent) heating with CaF2 in presence of NaCl;;
In neat (no solvent) heating with CaF2 in presence of NaCl;;

...Expand

: phosphorus

: 7647-19-0, 874483-74-6
phosphorus pentafluoride

: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
at red heat;	0%

: phosphorus

: 13454-99-4
dichloro-trifluoro-phosphorane

A: 7783-55-3
trifluorophosphane

B: 7719-12-2, 52843-90-0
phosphorus trichloride

Conditions

Conditions	Yield
In neat (no solvent) heating PF3Cl2 with P at 120 °C;;
In neat (no solvent) decompn. with P at 110 °C;;

...Expand

: phosphorus

: 13454-99-4
phosphorus dichloride trifluoride

A: 7783-55-3
trifluorophosphane

B: 7719-12-2, 52843-90-0
phosphorus trichloride

...Expand

: 7439-92-1
lead

: 13454-99-4
phosphorus dichloride trifluoride

A: 7783-55-3
trifluorophosphane

B: lead(II) chloride

Conditions

Conditions	Yield
In neat (no solvent) at 180°C;;

...Expand

: 1087413-67-9
nitrosylsulfuric acid fluoride

: 7719-12-2, 52843-90-0
phosphorus trichloride

A: 16921-91-8
nitrosyl hexafluorophosphate

B: 7446-09-5
sulfur dioxide

C: 10102-43-9
nitrogen(II) oxide

D: 2696-92-6
nitrosylchloride

E: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
In not given react. with FSO2NO; formation of NO(PF6), NO, NOCl, SO2 and PF3;;
In not given react. with FSO2NO; formation of NO(PF6), NO, NOCl, SO2 and PF3;;

...Expand

: 7446-08-4
selenium(IV) oxide

: phosphorous

: 7664-39-3
hydrogen fluoride

A: 13478-20-1
trifluorophosphoric acid

B: 7783-55-3
trifluorophosphane

...Expand

: phosphorous

: 7664-39-3
hydrogen fluoride

A: 1333-74-0
hydrogen

B: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
High Pressure; 200°C, conversion increases in presence of alkali or alkaline earth fluride;	A n/a B 23-27

...Expand

: 10026-13-8, 874483-75-7
phosphorus pentachloride

: 7783-56-4
antimony(III) fluoride

: 7647-19-0, 874483-74-6
phosphorus pentafluoride

B: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
In neat (no solvent) byproducts: phosphorus fluoride chloride; react. of PCl5 with SbF3;;
In neat (no solvent) vigorous react. of solid PCl5 with SbF3;;
In neat (no solvent) byproducts: phosphorus fluoride chloride; react. of PCl5 with SbF3;;

...Expand

: 14913-58-7
antimony tetrachloride fluoride

: 7719-12-2, 52843-90-0
phosphorus trichloride

A: 18460-56-5
{PCl4}(1+)*{SbCl6}(1-)={PCl4}{SbCl6}

B: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
In not given react. with SbCl4F;;
In not given react. with SbCl4F;;

...Expand

: 7783-70-2
antimony pentafluoride

: 7719-12-2, 52843-90-0
phosphorus trichloride

: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
byproducts: HCl; at room temp.;
at low temp.;	0%
In not given byproducts: HCl; vigorous react. of PCl3 with SbF5 at ambient temp.;;
byproducts: HCl; at room temp.;
at low temp.;	0%

: 7783-77-9
molybdenum(VI) fluoride

: 7719-12-2, 52843-90-0
phosphorus trichloride

A: 13819-84-6, 194303-41-8
molybdenum(V) fluoride

: 7647-19-0, 874483-74-6
phosphorus pentafluoride

C: 7782-50-5
chlorine

D: 7783-55-3
trifluorophosphane

E: 13320-71-3
molybdenum(IV) chloride

Conditions

Conditions	Yield
In not given react. with an excess of MoF6 forming PF3, MoCl5 and Cl2; react. of MoCl5 forming MoCl4 and Cl2; further react. of MoF6 with PF3 forming PF5 and MoF5;;
In not given react. with an excess of MoF6 forming PF3, MoCl5 and Cl2; react. of MoCl5 forming MoCl4 and Cl2; further react. of MoF6 with PF3 forming PF5 and MoF5;;

...Expand

: 7783-77-9
molybdenum(VI) fluoride

: 7719-12-2, 52843-90-0
phosphorus trichloride

A: 10026-13-8, 874483-75-7
phosphorus pentachloride

B: 10241-05-1
molybdenum(V) chloride

C: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
In not given react. of an excess of PCl3 with MoF6 forming PF3, MoCl5, Cl2; further react. of an excess of PCl3 with Cl2 forming PCl5;;
In not given react. of an excess of PCl3 with MoF6 forming PF3, MoCl5, Cl2; further react. of an excess of PCl3 with Cl2 forming PCl5;;

...Expand

: 112926-00-8, 7631-86-9
silica gel

: 7783-61-1
silicon tetrafluoride

: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
In neat (no solvent) byproducts: O2, P; decompn. of PF3 by SiO2;;
In neat (no solvent) byproducts: O2, P; decompn. of PF3 by SiO2;;

: fluorapatite

: phosphorus pentoxide

A: 13478-20-1
trifluorophosphoric acid

B: 124-38-9
carbon dioxide

C: 7783-61-1
silicon tetrafluoride

D: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
In neat (no solvent) heating at 700 °C;;
In neat (no solvent) heating at 700 °C;;

...Expand

: 14335-40-1
chlorodifluorophosphine

: L-Selectride

A: 14984-74-8
difluorophosphine

B: 7803-51-2
phosphan

C: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
In tetrahydrofuran under inert atmosphere, equimolar amt. of PF2Cl was reacted with L-Selectride in THF at temperature from -100 to -90°C; product contained other unidentified PF2-containing species;	A 0% B n/a C n/a

...Expand

: phosphorous

: 2314-97-8
iodotrifluoromethane

A: 76-16-4
Hexafluoroethane

B: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
by heating, mol. ratio 3:1;
by heating, mol. ratio 3:1;

...Expand

: 14335-40-1
chlorodifluorophosphine

: 67276-04-4
sodium tri-sec-butylborohydride

A: 14984-74-8
difluorophosphine

B: 7803-51-2
phosphan

C: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
In tetrahydrofuran under inert atmosphere, equimolar amt. of PF2Cl was reacted with N-Selectride in THF at temperature from -100 to -90°C; product contained other unidentified PF2-containing species;	A 0% B n/a C n/a

...Expand

: 14335-40-1
chlorodifluorophosphine

: potassium tri-sec-butyl-borohydride

A: 14984-74-8
difluorophosphine

B: 7803-51-2
phosphan

C: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
In tetrahydrofuran under inert atmosphere, equimolar amt. of PF2Cl was reacted with K-Selectride in THF at temperature from -100 to -90°C; product contained other unidentified PF2-containing species;	A 0% B n/a C n/a

...Expand

: phosphorous

: 7782-41-4
fluorine

A: 7647-19-0, 874483-74-6
phosphorus pentafluoride

B: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
with excess of P PF3 developing;

...Expand

: 12185-10-3
phosphorus

: 13465-66-2, 271781-78-3
selenium(IV) fluoride

A: 7782-49-2
selenium

B: 7783-55-3
trifluorophosphane

...Expand

: 7783-55-3
trifluorophosphane

: 13454-99-4
phosphorus dichloride trifluoride

Conditions

Conditions	Yield
With chlorine In neat (no solvent) react. at ambient temp. in the gas phase; light sensitive;;	99%
With Cl2 In neat (no solvent) react. at ambient temp. in the gas phase; light sensitive;;	99%
With chlorine In neat (no solvent) heating; volume contraction;;
With Cl2 In neat (no solvent) heating; volume contraction;;

: η5-indenylbis(ethylene)rhodium(I)

: 7783-55-3
trifluorophosphane

: 70620-83-6
η5-indenylbis(trifluorophosphine)rhodium(I)

Conditions

Conditions	Yield
In neat (no solvent) byproducts: CH2CH2; N2 atmosphere; heating in evacuated ampoule from -196°C to room temp.; fractionation;	99%

: (η-cyclopentadienyl)2(μ-carbonyl)(μ-η2-CF3C2CF3)dirhodium

: 7783-55-3
trifluorophosphane

: [(C5H5)Rh(CO)(PF3)(CF3CCCF3)Rh(C5H5)]

Conditions

Conditions	Yield
In pentane PF3 bubbled through soln. of Rh complex in pentane for 2-4 min; concd., chromd. (SiO2, hexane/CH2Cl2 5/3); elem. anal.;	97%

: 149613-54-7
IrH(η(2)-C6H4P(t)Bu2)(Cl)P(t)Bu2Ph

: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
In dichloromethane at 20℃; for 0.5h; Inert atmosphere; Schlenk technique;	96%

: borane carbonyl

: 7783-55-3
trifluorophosphane

A: 14931-39-6
P(BH3)F3

B: 201230-82-2
carbon monoxide

Conditions

Conditions	Yield
In neat (no solvent) 3.0mmol (OC)BH3, 2.5mmol, F2PX, -78°C, 2-3d;; very pure product;;	A 95% B n/a
In neat (no solvent) 3.0mmol (OC)BH3, 2.5mmol, F2PX, -78°C, 2-3d;; very pure product;;	A 95% B n/a

...Expand

: {(η3-C3H5)3WCl}2

: 7783-55-3
trifluorophosphane

: (η3-C3H5)3W(PF3)Cl

Conditions

Conditions	Yield
In diethyl ether PF3 passed over soln. of ((C3H5)3WCl)2 in ether (under Ar, -50°C);	95%

: 311819-28-0, 25087-75-6, 55354-87-5
RuH(OAc)(PPh3)3

: 7783-55-3
trifluorophosphane

: 67840-34-0
tris(trifluorophosphine)bis(triphenylphosphine)ruthenium(0)

Conditions

Conditions	Yield
In dichloromethane byproducts: CH3COOH; a mixt. of Ru-complex, ligand and CH2Cl2 was sealed off in an ampoule and warmed from -196°C to room temp., the mixt. was shaken overnight; evapd., washed with hexane, crystd. from CH2Cl2/hexane; elem. anal.;	93.6%

: 7440-44-0
pyrographite

: 7783-55-3
trifluorophosphane

A: 116-14-3
polytetrafluoroethylene

B: 75-73-0
carbon tetrafluoride

Conditions

Conditions	Yield
In neat (no solvent) react. of C with PF3 in a Ni-tube at 1100°C;;	A 90% B 9%

...Expand

: 3((C6H5)3P)2IrH2(1+)*PW12O40(3-)={((C6H5)3P)2IrH2}3PW12O40

: 7783-55-3
trifluorophosphane

: 115805-07-7
IrH2(P(C6H5)3)2(PF3)(1+)

Conditions

Conditions	Yield
In neat (no solvent) 300 mm of PF3, 16 h, room temp.;	90%

: 1449195-56-5
dimethyl(7-phenylnorbornadiene)platinum(II)

: 7783-55-3
trifluorophosphane

: 1262969-68-5, 1263030-29-0
cis-dimethylbis(trifluorophosphane)platinum(II)

Conditions

Conditions	Yield
In Dimethyl ether at -196 - 20℃; for 1h; Glovebox;	89%

: 7783-55-3
trifluorophosphane

Conditions

Conditions	Yield
In hexane Irradiation (UV/VIS); 90 min; recrystn. from hexane at -20°C, elem. anal.;	86%

: 93842-30-9
chlorobis[[(diphenylphosphino)ethyl]dimethylsilyl]iridium(III)

: 7783-55-3
trifluorophosphane

: 93842-42-3
[Ir((C6H5)2PCH2CH2Si(CH3)2)2(Cl)(PF3)]

Conditions

Conditions	Yield
In tetrahydrofuran PF3 was bubbled through a soln. of complex; solvent was removed, hexane was added; elem.anal.;	81%

: 7783-55-3
trifluorophosphane

: gold(I) chloride

: 141845-34-3
trifluorophosphine gold(I) chloride

Conditions

Conditions	Yield
In benzene N2-atmosphere; addn. of phosphine to AuCl suspn.; pptn. on pentane addn., filtration, washing (pentane), drying (vac.);	80%
In toluene (N2; Ar); PF3 condensed into suspension of AuCl in toluene; cooled at -65 °C for 2 days; filtrated; pentane added; crystals precipitated at 6°C;

: 1333-74-0
hydrogen

: 7783-55-3
trifluorophosphane

dihydride tetrakis(trifluorophosphine)ruthenium (II): dihydride tetrakis(trifluorophosphine)ruthenium (II)

Conditions

Conditions	Yield
In tetradecane at 150℃; under 7.60051 - 760.051 Torr; for 6.5h; Inert atmosphere;	78%

...Expand

: trans-[iron(II) hydride (η2-dihydrogen)bis[1,2-bis(diphenylphosphanyl)ethane]] tetrafluoroborate

: 7783-55-3
trifluorophosphane

: 823786-32-9
trans-[iron(II) hydride (PF3) bis[1,2-bis(diphenylphosphanyl)ethane]] tetrafluoroborate

Conditions

Conditions	Yield
In dichloromethane (H2), Fe complex in CH2Cl2 treated with PF3 gas for 10 min, stirred at room temp. for 2 h; concd., pptd.(Et2O), dried (vac.), recrystd.(CH2Cl2/Et2O) for several d;	75%

: trans-[ruthenium(II) hydride (η2-dihydrogen)bis[1,2-bis(diphenylphosphanyl)ethane]] tetrafluoroborate

: 7783-55-3
trifluorophosphane

: 823786-36-3
trans-[ruthenium(II) hydride (PF3) bis[1,2-bis(diphenylphosphanyl)ethane]] tetrafluoroborate

Conditions

Conditions	Yield
In dichloromethane (H2), Ru complex in CH2Cl2 treated with PF3 gas for 10 min, stirred at room temp. for 2 h; concd., pptd.(Et2O), dried (vac.), recrystd.(CH2Cl2/Et2O) for several d;	73%

: (triisopropylstibine)(η5-cyclopentadienyl)diphenylcarbenerhodium(I)

: 7783-55-3
trifluorophosphane

: (trifluorophosphine)(η5-cyclopentadienyl)diphenylcarbenerhodium(I)

Conditions

Conditions	Yield
In benzene Ar, a slow stream PF3 passed through the soln. at room temp. for 20 min,stirred for 20 min at room temp.; solvent removed (vac.), recrysttd. (acetone, -78°C), crysts. separated, dried (vac.); elem. anal.;	72%

: 17742-04-0
trifluoromethylsulfenyl fluoride

: 7783-55-3
trifluorophosphane

: 66604-83-9
trifluoromethylsulfanyltetrafluorophosphorane

Conditions

Conditions	Yield
-30°C, in vac. apparatus of nickel or stainless steel;	70%
-30°C, in vac. apparatus of nickel or stainless steel;	70%

: Au2Cl6

: 7783-55-3
trifluorophosphane

: 141845-34-3
trifluorophosphine gold(I) chloride

Conditions

Conditions	Yield
In thionyl chloride PF3 condensed onto Au2Cl6 in SOCl2, stirred overnight at room temp. without light or treated 2.5 h with ultrasonics; soln. cooled to -20. - -80°C, filtered, crystals washed with SOCl2;	70%

: 1,4-dicarbomethoxybenzenechromium tricarbonyl

: 7783-55-3
trifluorophosphane

: C6H4(OCOCH3)2Cr(CO)2PF3

Conditions

Conditions	Yield
With C4H8O In tetrahydrofuran Irradiation (UV/VIS); (N2); soln. of Cr complex was irradiated for 1 h, then PF3 was bubbled through the soln. for 10 min; solvent was removed in vac., residue chromd. (silicagel, hexane); identified by MAS;	70%

: trans-[ruthenium(II) hydride (η2-dihydrogen)bis[1,2-bis(diphenylphosphanyl)methane]] tetrafluoroborate

: 7783-55-3
trifluorophosphane

: 823786-34-1
trans-[ruthenium(II) hydride (PF3) bis[1,2-bis(diphenylphosphanyl)methane]] tetrafluoroborate

Conditions

Conditions	Yield
In dichloromethane (H2), Ru complex in CH2Cl2 treated with PF3 gas for 10 min, stirred at room temp. for 2 h; concd., pptd.(Et2O), dried (vac.), recrystd.(CH2Cl2/Et2O) for several d;	69%

: trans-chlorobis(triisopropylstibine)diphenylcarbenerhodium(I)

: 7783-55-3
trifluorophosphane

: 342573-38-0
trans-chlorobis(triisopropylstibine)(trifluorophosphine)rhodium(I)

Conditions

Conditions	Yield
In benzene Ar, a slow stream of PF3 passed through the soln. for 20 min at room temp.; solvent removed (vac.); elem. anal.;	68%

: trans-chlorobis(triisopropylphosphine)diphenylcarbenerhodium(I)

: 7783-55-3
trifluorophosphane

: 342573-37-9
trans-chlorobis(triisopropylphosphine)(trifluorophosphine)rhodium(I)

Conditions

Conditions	Yield
In benzene Ar, a slow stream of PF3 passed through the soln. for 20 min at room temp.; solvent removed (vac.), recrystd. (acetone, -60°C), solid separate, dried (vac.); elem. anal.;	68%

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