CAS No.78-83-1,2-Methyl-1-propanol Suppliers,MSDS download

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EAST CHEMSOURCES LIMITED

2-Methyl-1-propanol English name: 2-Methyl-1-propanol CAS RN: 78-83-1 Molecular formula: C4H10O Molecular weight: 74.12 Structural formula:

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Hebei Mojin Biotechnology Co.,Ltd

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Triumph International Development Limilted

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Aecochem Corp.

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Synthetic route

: 558-30-5
2-methyl-1,2-epoxypropane

A: 78-83-1
2-methyl-propan-1-ol

B: 78-84-2
isobutyraldehyde

Conditions

Conditions	Yield
With hydrogen; chromium(III) oxide; copper at 140℃; under 26252.1 Torr; for 0.666667h;	A 98.1% B 1.9%

: 18269-50-6
isobutoxytrimethylsilane

: 78-83-1
2-methyl-propan-1-ol

Conditions

Conditions	Yield
With methanol; 1,3-disulfonic acid imidazolium hydrogen sulfate at 20℃; for 0.0666667h; Green chemistry;	97%

: 75-65-0
tert-butyl alcohol

A: 78-83-1
2-methyl-propan-1-ol

B: 7732-18-5
water

C: 115-11-7
isobutene

Conditions

Conditions	Yield
aluminum oxide at 315.546℃; under 11103.3 Torr;	A 1.4% B 1.1% C 96.4%

...Expand

: 71412-40-3
N,N'-(4-methyl-m-phenylene)-bis-carbamic acid diisobutyl ester

A: 78-83-1
2-methyl-propan-1-ol

B: 584-84-9
2,4-Toluene diisocyanate

Conditions

Conditions	Yield
In 1,2,4-Trichlorobenzene at 120 - 350℃; under 7500.75 Torr; Product distribution / selectivity; Industry scale;	A n/a B 92.9%

: 97-72-3
2-Methylpropionic anhydride

: 78-83-1
2-methyl-propan-1-ol

Conditions

Conditions	Yield
With [Zn(BH4)2(py)] In tetrahydrofuran for 2.5h; Heating;	92%

: 78-84-2
isobutyraldehyde

: 78-83-1
2-methyl-propan-1-ol

Conditions

Conditions	Yield
With sodium tetrahydroborate; Dowex1-x8 In tetrahydrofuran at 20℃; for 0.3h;	90%
gadolinium(III) isopropoxide In isopropyl alcohol at 30℃; for 2h;	74%
With PEG-bound sodium benzoyloxyborohydride In toluene at 21 - 23℃; for 2h;	66%

: 187737-37-7
propene

: 201230-82-2
carbon monoxide

A: 78-83-1
2-methyl-propan-1-ol

B: 71-36-3
butan-1-ol

Conditions

Conditions	Yield
Stage #1: propene; carbon monoxide With hydrogen; triphenylphosphine; acetylacetonatodicarbonyl triphenylphosphine Rhodium (ROPAC) at 89℃; for 240h; Inert atmosphere; Stage #2: With hydrogen; Raney-nickel at 110℃; under 18751.9 Torr; for 90h; Product distribution / selectivity; Inert atmosphere;	A 8.6% B 87.1%
Stage #1: propene; carbon monoxide With carbonyl-2,4-pentanedionato(triphenylphosphine)rhodium(I); hydrogen; triphenylphosphine at 89℃; under 11251.1 - 13501.4 Torr; for 240h; Industrial scale; Stage #2: With hydrogen at 110℃; under 18751.9 Torr; for 90h; Industrial scale;	A 8.6% B 87.1%
Stage #1: propene; carbon monoxide With (acetylacetonato)dicarbonylrhodium (l); tris(triphenylphosphine)ruthenium(II) chloride; hydrogen; triphenylphosphine In toluene at 19.84 - 49.84℃; under 23289.8 Torr; for 4h; Autoclave; Stage #2: With hydrogen In toluene at 49.84 - 99.84℃; under 25877.6 Torr; for 4h; Autoclave;

...Expand

: 73198-21-7
Isobutylmethyl(p-nitrophenyl)sulfonium perchlorate

A: 67-56-1
methanol

B: 78-83-1
2-methyl-propan-1-ol

C: 701-57-5
1-methylthio-4-nitro-benzene

D: Isobutyl p-nitrophenyl sulfide

Conditions

Conditions	Yield
With water Mechanism; Product distribution;	A n/a B n/a C 15% D 85%

...Expand

: 79-31-2
isobutyric Acid

: 78-83-1
2-methyl-propan-1-ol

Conditions

Conditions	Yield
With lithium aluminium tetrahydride In diethyl ether at 0℃; for 6h;	80%
With diphenylamine borane In dichloromethane 1.) 0 deg C, 1 h, 2.) 20 deg C, 1 h;	72%
With hydrogen In n-heptane at 123℃; under 41372.9 Torr; for 4h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Time; Pressure; Autoclave;
With hydrogen In hexane at 130℃; under 15001.5 Torr; for 18h; Molecular sieve; chemoselective reaction;	83 %Chromat.
With methanol; CuO on mesoporous silica at 360℃; Reagent/catalyst;

: 84110-40-7
Dihydroxy-isobutyl-boran

: acetonitrile complex of hypofluorous acid

: 78-83-1
2-methyl-propan-1-ol

Conditions

Conditions	Yield
In dichloromethane at 20℃;	80%

: 1679-47-6
3-methyltetrahydro-2-furanone

A: 2938-98-9
2-methyl-1,4-butandiol

B: 78-83-1
2-methyl-propan-1-ol

C: 71-36-3
butan-1-ol

Conditions

Conditions	Yield
With 5 wt% ruthenium/carbon; hydrogen In water at 100℃; under 105011 Torr; for 6.3h; Reagent/catalyst; Temperature;	A 80% B n/a C n/a

...Expand

: 6283-77-8
2-methylpropane-1,1-diyl diacetate

: 78-83-1
2-methyl-propan-1-ol

Conditions

Conditions	Yield
With sodium tetrahydroborate; nickel(II) chloride hexahydrate In methanol at 20℃; for 3.5h; chemoselective reaction;	80%

: 558-30-5
2-methyl-1,2-epoxypropane

A: 78-83-1
2-methyl-propan-1-ol

B: 115-11-7
isobutene

C: 75-65-0
tert-butyl alcohol

Conditions

Conditions	Yield
With hydrogen; chromium(III) oxide; nickel at 90℃; under 26252.1 Torr; for 0.666667h; 100 - 170 degC, Al Ni Ti as a catalyst;	A 75.4% B 0.62% C 24.3%

...Expand

: 20266-12-0
1-butoxy-1-isobutoxy butane

A: 78-83-1
2-methyl-propan-1-ol

B: 109-21-7
butyl butyrate

C: 539-90-2
isobutyl n-butyrate

D: 79-31-2
isobutyric Acid

E: 107-92-6
butyric acid

F: 71-36-3
butan-1-ol

Conditions

Conditions	Yield
With oxygen; cobalt(II) acetate at 90℃; under 750.06 Torr; Mechanism; Rate constant; other oxygen pressure;	A 5.5% B 3% C 3.5% D 5% E 73.5% F 7%

...Expand

: 67-56-1
methanol

: 64-17-5
ethanol

: 78-83-1
2-methyl-propan-1-ol

Conditions

Conditions	Yield
With trans-RuCl2(dppm)2; sodium hydroxide at 180℃; for 2h; Catalytic behavior; Reagent/catalyst; Time; Guerbet Reaction; Autoclave; Inert atmosphere; Sealed tube;	71%
With Mn(CO)((C6H5)2PCH2P(C6H5)2)2Br; sodium methylate at 180℃; for 90h; Catalytic behavior; Reagent/catalyst; Guerbet Reaction;	14.4%
With chloro(hexamethylbenzene)(1-hydroxy-2-diphenylphosphino-3-methylphosphacyclohexa-3,5-diene) ruthenium(II) hexafluorophosphate; sodium methylate at 180℃; for 2h; Glovebox; Autoclave; Inert atmosphere;	11.1%

: 201230-82-2
carbon monoxide

A: 67-56-1
methanol

B: 71-23-8
propan-1-ol

C: 64-17-5
ethanol

D: 78-83-1
2-methyl-propan-1-ol

Conditions

Conditions	Yield
With hydrogen at 400℃; under 75007.5 Torr; Catalytic behavior; Reagent/catalyst;	A 65.2% B 1% C 3.6% D 27%
With hydrogen at 370℃; under 76005.1 Torr;

...Expand

: 187737-37-7
propene

A: 74-98-6
propane

B: 78-83-1
2-methyl-propan-1-ol

C: 71-36-3
butan-1-ol

Conditions

Conditions	Yield
With carbon monoxide; hydrogen; decacarbonylditechnetium; bithionol In hexane at 235℃; under 150012 Torr; for 6h; Product distribution; also Tc2(CO)10-catalyst;	A 62% B 3% C 35%

...Expand

: 124-38-9
carbon dioxide

: 201230-82-2
carbon monoxide

A: 67-56-1
methanol

B: 71-23-8
propan-1-ol

C: 57-55-6
propylene glycol

D: 626-95-9
1,4-Pentanediol

E: 111-29-5
1 ,5-pentanediol

F: 110-63-4
Butane-1,4-diol

G: 60-29-7
diethyl ether

H: 34557-54-5
methane

I: 64-17-5
ethanol

J: 6032-29-7
(+/-)-2-pentanol

K: 18826-95-4, 107-88-0
1.3-butanediol

L: 5343-92-0
1,2-pentanediol

M: 74-84-0
ethane

N: 74-98-6
propane

O: 115-10-6
Dimethyl ether

P: 540-67-0
ethyl methyl ether

Q: 78-83-1
2-methyl-propan-1-ol

R: 584-02-1
2-pentanol

S: 71-41-0
pentan-1-ol

T: 3174-67-2
1,3-pentanediol

U: 79-20-9
acetic acid methyl ester

V: 67-63-0
isopropyl alcohol

W: 78-92-2, 15892-23-6
iso-butanol

X: 75-65-0
tert-butyl alcohol

Y: 71-36-3
butan-1-ol

Z: 584-03-2
1,2-dihydroxybutane

Conditions

Conditions	Yield
With hydrogen; Cu/Co/Al at 260 - 320℃; under 45004.5 - 75007.5 Torr; Conversion of starting material;	A 57.5% B n/a C n/a D n/a E n/a F n/a G n/a H n/a I 28.5% J n/a K n/a L n/a M n/a N n/a O n/a P n/a Q n/a R n/a S n/a T n/a U n/a V n/a W n/a X n/a Y n/a Z n/a
With hydrogen; Cu/ZnO/Al2O3 at 285 - 300℃; under 45004.5 - 67506.8 Torr; Conversion of starting material;	A 57.5% B n/a C n/a D n/a E n/a F n/a G n/a H n/a I 28.5% J n/a K n/a L n/a M n/a N n/a O n/a P n/a Q n/a R n/a S n/a T n/a U n/a V n/a W n/a X n/a Y n/a Z n/a

...Expand

: 124-38-9
carbon dioxide

: 201230-82-2
carbon monoxide

A: 67-56-1
methanol

B: 71-23-8
propan-1-ol

C: 57-55-6
propylene glycol

D: 626-95-9
1,4-Pentanediol

E: 111-29-5
1 ,5-pentanediol

F: 110-63-4
Butane-1,4-diol

G: 60-29-7
diethyl ether

H: 64-17-5
ethanol

I: 6032-29-7
(+/-)-2-pentanol

J: 18826-95-4, 107-88-0
1.3-butanediol

K: 5343-92-0
1,2-pentanediol

L: 115-10-6
Dimethyl ether

M: 540-67-0
ethyl methyl ether

N: 78-83-1
2-methyl-propan-1-ol

O: 584-02-1
2-pentanol

P: 71-41-0
pentan-1-ol

Q: 3174-67-2
1,3-pentanediol

R: 79-20-9
acetic acid methyl ester

S: 67-63-0
isopropyl alcohol

T: 78-92-2, 15892-23-6
iso-butanol

U: 75-65-0
tert-butyl alcohol

V: 71-36-3
butan-1-ol

W: 584-03-2
1,2-dihydroxybutane

Conditions

Conditions	Yield
With hydrogen; Zn/Cr/K at 350 - 420℃; under 75007.5 - 135014 Torr; Conversion of starting material;	A 57.5% B n/a C n/a D n/a E n/a F n/a G n/a H 28.5% I n/a J n/a K n/a L n/a M n/a N n/a O n/a P n/a Q n/a R n/a S n/a T n/a U n/a V n/a W n/a

...Expand

: lithium 2-lithioethoxide

: 78-84-2
isobutyraldehyde

A: 78-83-1
2-methyl-propan-1-ol

B: 54876-99-2
4-methylpentane-1,3-diol

Conditions

Conditions	Yield
In tetrahydrofuran at -95℃;	A n/a B 55%

...Expand

: 492-62-6
alpha-D-glucopyranose

: 78-83-1
2-methyl-propan-1-ol

Conditions

Conditions	Yield
With glucose dehydrogenase; 2-keto acid decarboxylase; 2-keto-3-desoxygluconate aldolase; acetolactate synthase; dihydroxy acid dehydratase; ketol acid reductoisomerase; NAD; thiamine diphosphate; magnesium chloride; alcohol dehydrogenase In aq. buffer at 50℃; for 23h; pH=7; Enzymatic reaction;	53%

: 513-42-8
3-hydroxy-2-methyl-1-propene

A: 78-83-1
2-methyl-propan-1-ol

B: 79-31-2
isobutyric Acid

Conditions

Conditions	Yield
Stage #1: 3-hydroxy-2-methyl-1-propene With Pd/SiO2; [Rh(trop2NH)(PPh3)]OTf; water; sodium hydroxide at 20℃; for 12h; Inert atmosphere; Stage #2: With hydrogenchloride In water Inert atmosphere;	A 40% B 50%

: 78-85-3
2-methylpropenal

: 78-83-1
2-methyl-propan-1-ol

Conditions

Conditions	Yield
With aluminum tri-n-butoxide at 60℃; for 5h; Time; Meerwein-Ponndorf-Verley Reduction;	44.54%

: 20266-11-9
1-(1-Isobutoxy-2-methyl-propoxy)-butane

A: 97-85-8
isobutyl isobutanoate

B: 78-83-1
2-methyl-propan-1-ol

C: 97-87-0
n-butyl isobutyrate

D: 79-31-2
isobutyric Acid

E: 107-92-6
butyric acid

F: 71-36-3
butan-1-ol

Conditions

Conditions	Yield
With oxygen; cobalt(II) acetate at 90℃; under 750.06 Torr; Mechanism; Rate constant; other oxygen pressure;	A 6% B 12% C 6% D 26% E 33% F 14%

...Expand

: 187737-37-7
propene

: 201230-82-2
carbon monoxide

A: 78-83-1
2-methyl-propan-1-ol

B: 123-72-8
butyraldehyde

C: 78-84-2
isobutyraldehyde

D: 71-36-3
butan-1-ol

Conditions

Conditions	Yield
With (acetylacetonato)dicarbonylrhodium (l); hydrogen; triethylphosphine In ethanol at 140℃; under 37503.8 Torr; Pressure; Inert atmosphere; Autoclave;	A n/a B n/a C 30.8% D 11%
With dicobalt octacarbonyl; water; 1,2-bis-(diphenylphosphino)ethane In 1,4-dioxane Product distribution; var. CO pressure, var. temperatures, var. propene concentration, var. times;
With hydrogen; heteronuclear Pd-Co complex on silica at 100℃; under 2280 Torr; for 1h; Product distribution; var. of catalyst, temp.;

...Expand

: 67-56-1
methanol

: 64-17-5
ethanol

A: 71-23-8
propan-1-ol

B: 78-83-1
2-methyl-propan-1-ol

Conditions

Conditions	Yield
With trans, cis-[RuCl2(1-amino-2-diphenylphosphinoethane-N,P)2]; sodium hydroxide at 180℃; for 2h; Catalytic behavior; Reagent/catalyst; Guerbet Reaction; Autoclave; Sealed tube; Inert atmosphere;	A 8.6% B 28%
With (bis[(2-diisopropylphosphino)ethyl]amine)Mn(CO)2Br; sodium methylate at 180℃; for 24h; Catalytic behavior; Reagent/catalyst;	A 10.5% B 27%
With Ru(Ph2PCH2CH2NMe2)2Cl2; sodium methylate at 180℃; for 20h; Catalytic behavior; Reagent/catalyst; Autoclave; Inert atmosphere;
With C42H48Cl2P4RuSi2; sodium methylate at 180℃; for 2h; Temperature; Inert atmosphere; Schlenk technique; Autoclave;	A 5.3 %Chromat. B 38.1 %Chromat.

...Expand

: 201230-82-2
carbon monoxide

: 67-63-0
isopropyl alcohol

A: 123-51-3
i-Amyl alcohol

B: 78-83-1
2-methyl-propan-1-ol

C: 108-20-3
di-isopropyl ether

D: 78448-33-6
1-isopropoxy-2-methyl-propane

Conditions

Conditions	Yield
With hydrogen; Cobalt rhodium; iodine at 200℃; under 315025 Torr; for 2h; Product distribution; other promoter, other pressure;	A n/a B 22% C 12% D 9%

...Expand

: 13262-24-3
2-methyl-1,1-bis(2-methylpropoxy)propane

A: 97-85-8
isobutyl isobutanoate

B: 78-83-1
2-methyl-propan-1-ol

C: 79-31-2
isobutyric Acid

Conditions

Conditions	Yield
With oxygen; cobalt(II) acetate at 90℃; under 750.06 Torr; Mechanism; Rate constant; other oxygen pressure;	A 5% B 11% C 15%

...Expand

: 13002-16-9
n-butyraldehyde diisobutyl acetal

A: 78-83-1
2-methyl-propan-1-ol

B: 539-90-2
isobutyl n-butyrate

Conditions

Conditions	Yield
With oxygen; cobalt(II) acetate at 90℃; under 750.06 Torr; Mechanism; Rate constant; other oxygen pressure;	A 14% B 8%

: 765-69-5
2-Methylcyclopentane-1,3-dione

: 78-83-1
2-methyl-propan-1-ol

: 22117-97-1
3-isobutoxy-2-methyl-2-cyclopenten-1-one

Conditions

Conditions	Yield
With toluene-4-sulfonic acid In benzene for 16h; Heating;	100%
With toluene-4-sulfonic acid	100%
With toluene-4-sulfonic acid In benzene for 8h; Heating;	99%

: 78-83-1
2-methyl-propan-1-ol

: 327-92-4
1,5-difluoro-2,4-dinitrobenzene

: 100876-90-2
1,5-diisobutoxy-2,4-dinitrobenzene

Conditions

Conditions	Yield
In triethylamine at 20℃; for 12h; Inert atmosphere;	100%
With triethylamine In chloroform for 5h;	91.6%
With potassium fluoride
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 120h;

: 78-83-1
2-methyl-propan-1-ol

: 79-31-2
isobutyric Acid

Conditions

Conditions	Yield
With 2,2,6,6-tetramethyl-piperidine-N-oxyl; trichloroisocyanuric acid; sodium hydrogencarbonate; sodium bromide In water; acetone at 20℃; for 3h;	100%
With tert.-butylhydroperoxide; copper(ll) bromide In water; dimethyl sulfoxide at 20℃; for 1.2h; Inert atmosphere;	88%
With aluminium trichloride; silver bromate In acetonitrile for 0.65h; Heating;	83%

: 78-83-1
2-methyl-propan-1-ol

: 98-59-9
p-toluenesulfonyl chloride

: 4873-56-7
isobutyl p-toluenesulfonate

Conditions

Conditions	Yield
With tetrabutylammomium bromide; sodium hydroxide In water; toluene at 40 - 50℃; for 1h;	100%
With dmap; triethylamine In dichloromethane at 0 - 25℃; Inert atmosphere;	86%
With pyridine In chloroform at 0 - 25℃; for 12h; Inert atmosphere;	81%

: 78-83-1
2-methyl-propan-1-ol

: 122706-30-3
6-methyl-6,7-dihydro-7-hydroxy-5H-pyrrolo<3,4-b>pyridin-5-one

: 135128-35-7
7-Isobutoxy-6-methyl-6,7-dihydro-pyrrolo[3,4-b]pyridin-5-one

Conditions

Conditions	Yield
With toluene-4-sulfonic acid at 108℃; for 3h;	100%

: 78-83-1
2-methyl-propan-1-ol

: sodium-O,O-(CH2CH(CH3)2)2-dithiophosphate

Conditions

Conditions	Yield
With diphosphorus pentasulfide In tetrahydrofuran for 2h; Ambient temperature;	100%

: 72-18-4
L-valine

: 78-83-1
2-methyl-propan-1-ol

: 104-15-4
toluene-4-sulfonic acid

: 13018-45-6
(S)-1-isobutoxy-3-methyl-1-oxobutan-2-aminium 4-methylbenzenesulfonate

Conditions

Conditions	Yield
In water; toluene for 24h; Reflux; Dean-Stark;	100%
In benzene Heating;	84%
In benzene Heating;

...Expand

: 78-83-1
2-methyl-propan-1-ol

: 4753-07-5, 5160-10-1, 14206-57-6, 14227-66-8, 14257-35-3, 42385-75-1, 67650-37-7, 68682-05-3, 69308-57-2, 69349-74-2, 70223-96-0, 70223-97-1, 71276-38-5, 85248-99-3, 118493-15-5, 120575-76-0
2,3,6,2',3',4',6'-hepta-O-acetyl-α-D-maltosyl bromide

: 3,6-di-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranose 1,2-(i-butyl orthoacetate)

Conditions

Conditions	Yield
With 2,4,6-trimethyl-pyridine; 4 A molecular sieve; mercury dibromide In nitromethane; chloroform; benzene for 22h; Ambient temperature;	100%

: 78-83-1
2-methyl-propan-1-ol

: 4753-07-5
2,3,6,2',3',4',6'-hepta-O-acetyl-lactosyl bromide

: 3,6-di-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-glucopyranose 1,2-(i-butyl orthoacetate)

Conditions

Conditions	Yield
With 2,4,6-trimethyl-pyridine; 4 A molecular sieve; mercury dibromide In nitromethane; chloroform; benzene for 22h; Ambient temperature;	100%

: 78-83-1
2-methyl-propan-1-ol

: 6645-46-1
L-carnitine chloride

: R-carnitine isobutyl ester

Conditions

Conditions	Yield
With hydrogenchloride for 3h; Heating;	100%

: 78-83-1
2-methyl-propan-1-ol

: 126-81-8
dimedone

: 5,5-dimethyl-3-(2-methylpropoxy)cyclohex-2-en-1-one

Conditions

Conditions	Yield
With toluene-4-sulfonic acid In benzene Heating;	100%

: 328-50-7
α-ketoglutaric acid

: 78-83-1
2-methyl-propan-1-ol

: 105553-43-3
di-i-butyl 2-oxoglutarate

Conditions

Conditions	Yield
With Novozym 435 lipase B from Candida antarctica at 30℃;	100%

: 916913-52-5
N-(3-[tert-butyl(dimethyl)silyl]oxy-2-naphthyl)-5-methylfuran-2-sulfonamide

: 78-83-1
2-methyl-propan-1-ol

: 916913-53-6
N-(3-[tert-butyl(dimethyl)silyl]oxy-2-naphthyl)-N-isobutyl-5-methylfuran-2-sulfonamide

Conditions

Conditions	Yield
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran; toluene at 20℃; Mitsunobu reaction;	100%

: 909896-93-1
methyl 4-{[2-[(pyridin-3-ylsulfonyl)amino]-5-(trifluoromethyl)phenoxy]methyl}benzoate

: 78-83-1
2-methyl-propan-1-ol

: 909897-17-2
methyl 4-{[2-[isobutyl(pyridin-3-ylsulfonyl)amino]-5-(trifluoromethyl)phenoxy]methyl}benzoate

Conditions

Conditions	Yield
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 20℃; for 1h;	100%

: 909897-11-6
methyl 4-{[2-[(1H-imidazol-2-ylsulfonyl)amino]-5-(trifluoromethyl)phenoxy]methyl}benzoate

: 78-83-1
2-methyl-propan-1-ol

: 909897-26-3
methyl 4-{[2-{isobutyl[(1H-imidazol-2-yl)sulfonyl]amino}-5-(trifluoromethyl)phenoxy]methyl}benzoate

Conditions

Conditions	Yield
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 20℃;	100%

: 909897-09-2
methyl 4-{[2-{[(1-methyl-1H-pyrrol-3-yl)sulfonyl]amino}-5-(trifluoromethyl)phenoxy]methyl}benzoate

: 78-83-1
2-methyl-propan-1-ol

: 909897-25-2
methyl 4-{[2-{isobutyl[(1-methyl-1H-pyrrol-3-yl)sulfonyl]amino}-5-(trifluoromethyl)phenoxy]methyl}benzoate

Conditions

Conditions	Yield
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 20℃;	100%

: 909896-95-3
methyl 4-{[2-{[(1-methyl-1H-pyrrol-2-yl)sulfonyl]amino}-5-(trifluoromethyl)phenoxy]methyl}benzoate

: 78-83-1
2-methyl-propan-1-ol

: 909897-18-3
methyl 4-{[2-{isobutyl[(1-methyl-1H-pyrrol-2-yl)sulfonyl]amino}-5-(trifluoromethyl)phenoxy]methyl}benzoate

Conditions

Conditions	Yield
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 20℃;	100%

: 909897-07-0
methyl 4-{[2-[(1H-pyrrol-3-ylsulfonyl)amino]-5-(trifluoromethyl)phenoxy]methyl}benzoate

: 78-83-1
2-methyl-propan-1-ol

: 909897-24-1
methyl 4-{[2-{isobutyl[(1H-pyrrol-3-yl)sulfonyl]amino}-5-(trifluoromethyl)phenoxy]methyl}benzoate

Conditions

Conditions	Yield
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 20℃;	100%

: 78-83-1
2-methyl-propan-1-ol

: 10175-01-6
bis(2-methoxycarbonylethyl)tin dichloride

: 66896-27-3
di(2-iso-butoxycarbonylethyl)tin dichloride

Conditions

Conditions	Yield
In further solvent(s) addn. of Sn compd. to iso-butanol, reflux, acid or base catalysis;	100%

: 78-83-1
2-methyl-propan-1-ol

: 72063-81-1
2,4-diisobutylamino-6-chloro-pyrimidine

: 1067679-81-5
4-isobutoxy-2,6-diisobutylamino-pyrimidine

Conditions

Conditions	Yield
Stage #1: 2-methyl-propan-1-ol With sodium hydride In mineral oil at 20℃; Inert atmosphere; Stage #2: 2,4-diisobutylamino-6-chloro-pyrimidine In mineral oil at 125℃; for 72h; Inert atmosphere;	100%

: 78-83-1
2-methyl-propan-1-ol

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 1187923-23-4
1-methoxy-4-[1-(2-methylpropan-1-yloxy)ethyl]benzene

Conditions

Conditions	Yield
Stage #1: 2-methyl-propan-1-ol; 1-(4-methoxyphenyl)ethanone With sodium tetrahydroborate at 20℃; Stage #2: With hydrogenchloride In water at 60℃; for 5h;	100%
With hydrogen In n-heptane at 80℃; under 760.051 Torr; for 2.5h;

: 78-83-1
2-methyl-propan-1-ol

: 3282-30-2
pivaloyl chloride

: 5129-38-4
isobutyl pivalate

Conditions

Conditions	Yield
at 20℃; for 0.0833333h; Neat (no solvent);	100%

: 78-83-1
2-methyl-propan-1-ol

: 1633-82-5
3-chloro-n-propanesulfonyl chloride

: C7H15ClO3S

Conditions

Conditions	Yield
With triethylamine In toluene at 3 - 8℃; for 4h; Inert atmosphere;	100%

: 78-83-1
2-methyl-propan-1-ol

: 35213-00-4
2,6-dinitrobenzonitrile

: 1093204-61-5
2-isobutoxy-6-nitrobenzonitrile

Conditions

Conditions	Yield
Stage #1: 2-methyl-propan-1-ol With sodium hydride In tetrahydrofuran; mineral oil at 0 - 20℃; for 0.5h; Inert atmosphere; Stage #2: 2,6-dinitrobenzonitrile In tetrahydrofuran; mineral oil at -70 - 20℃; Inert atmosphere;	100%

: 3095-95-2
diethylphosphonoacetic acid

: 78-83-1
2-methyl-propan-1-ol

: 75412-64-5
diethyl <(iso-butoxycarbonyl)methyl>phosphonate

Conditions

Conditions	Yield
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; ethyl acetate; toluene at 20℃; for 4h; Inert atmosphere;	100%
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In toluene at 20℃; for 4h; Inert atmosphere;	95%

: 78-83-1
2-methyl-propan-1-ol

: 20632-12-6
1-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)propan-1-one

: 6-[1-(2-methylpropan-1-yloxy)propyl]-2,3-dihydro-1,4-benzodioxine

Conditions

Conditions	Yield
Stage #1: 2-methyl-propan-1-ol; 1-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)propan-1-one With sodium tetrahydroborate at 20℃; Stage #2: With hydrogenchloride In water at 60℃; for 4h;	100%

: 78-83-1
2-methyl-propan-1-ol

: 18212-83-4
1-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-2-phenylethanone

: 6-[1-(2-methylpropan-1-yloxy)-2-phenylethyl]-2,3-dihydro-1,4-benzodioxine

Conditions

Conditions	Yield
Stage #1: 2-methyl-propan-1-ol; 1-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-2-phenylethanone With sodium tetrahydroborate at 20℃; Stage #2: With hydrogenchloride In water at 60℃; for 5h;	100%

: 78-83-1
2-methyl-propan-1-ol

: 100-47-0
benzonitrile

: isobutyl benzimidate

Conditions

Conditions	Yield
With acetyl chloride at 0 - 20℃; for 24.5h;	100%
With acetyl chloride at 0 - 20℃; for 24h;	58%
With acetyl chloride at 0 - 25℃; Schlenk technique;

: 78-83-1
2-methyl-propan-1-ol

: C31H40N4O7

: C36H50N4O7

Conditions

Conditions	Yield
Stage #1: C31H40N4O7 With dmap; 2,4,6-trichlorobenzoyl chloride; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide In dichloromethane for 0.0833333h; Stage #2: 2-methyl-propan-1-ol In dichloromethane at 20℃; for 1h;	100%

: 78-83-1
2-methyl-propan-1-ol

: 79-31-2
isobutyric Acid

: 97-85-8
isobutyl isobutanoate

Conditions

Conditions	Yield
With 1-butyl-3-methylimidazolium hydrogen sulfate at 80℃; under 760.051 Torr; for 3h; Reagent/catalyst; Temperature;	99.8%
With sulfuric acid
With titanium(IV) oxide at 235℃;

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