CAS No.930-28-9,Cyclopentyl chloride Suppliers,MSDS download

: 287-92-3
Cyclopentane

: 930-28-9
cyclopentyl chloride

Conditions

Conditions	Yield
With potassium chloride; tetrabutyl-ammonium chloride; acetic acid In water at 20℃; for 6.5h; Reagent/catalyst;	96%
With sodium hypochlorite In water; acetone at 20℃; for 2h; Inert atmosphere;	95%
With hydrogenchloride; potassium chloride; tetrabutyl-ammonium chloride In water at 20℃; Irradiation; Green chemistry;	94%

: cyclopentyl o-(N-methylcarbamoyl)phenyl sulphoxide

A: 2527-66-4
2-methyl-1,2-benzisothiazole-3(2H)-one

B: 930-28-9
cyclopentyl chloride

C: 2-chlorocyclopentyl o-(N-methylcarbamoyl)phenyl sulphide

Conditions

Conditions	Yield
With thionyl chloride In dichloromethane for 1h; Heating;	A 53% B 83% C 10%

...Expand

: 96-41-3
Cyclopentanol

A: 930-28-9
cyclopentyl chloride

B: 142-29-0
cyclopentene

Conditions

Conditions	Yield
With 1-chloro-1-(dimethylamino)-2-methyl-1-propene In dichloromethane 1.) 0 deg C; 2.) rt., 3h;	A 80% B n/a
With 1-chloro-1-(dimethylamino)-2-methyl-1-propene In dichloromethane 1.) 0 deg C; 2.)rt., 3h;
With bismuth(III) chloride In tetrachloromethane for 1.5h; Heating;

: 142-29-0
cyclopentene

A: 96-41-3
Cyclopentanol

B: 930-28-9
cyclopentyl chloride

Conditions

Conditions	Yield
With tetrachloromethane; copper(II) choride dihydrate; chromium(III) acetylacetonate; water at 130℃; for 12h; Sealed tube;	A 80% B 20%

: 120-92-3
cyclopentanone

: 930-28-9
cyclopentyl chloride

Conditions

Conditions	Yield
With dichloromethylsilane; iron(III) chloride In 1,2-dimethoxyethane for 6h; Heating;	75%

: 96-41-3
Cyclopentanol

: 930-28-9
cyclopentyl chloride

Conditions

Conditions	Yield
With tertiary butyl chloride; n-pentylmethylimidazolium bromide at 60℃; for 3.75h;	72%
With pyridine; p-toluenesulfonyl chloride at 100℃;	40%
With phosphorus trichloride

: 50715-28-1
cyclopentyl chloroformate

: 109-63-7
trifluoroborane diethyl ether

A: 930-28-9
cyclopentyl chloride

B: 142-29-0
cyclopentene

...Expand

: 50715-28-1
cyclopentyl chloroformate

: 930-28-9
cyclopentyl chloride

Conditions

Conditions	Yield
With boron fluoride ether; pentane
With hexane; boron fluoride ether

: 56-23-5
tetrachloromethane

: 142-29-0
cyclopentene

A: 930-28-9
cyclopentyl chloride

B: 14916-75-7
1,2-dichlorocyclopentane

C: 7582-02-7
1-chloro-2-(trichloromethyl)cyclopentane

D: 2690-18-8
3,3'-bicyclopentenyl

Conditions

Conditions	Yield
Irradiation; Further byproducts given;

...Expand

: 56-23-5
tetrachloromethane

: 142-29-0
cyclopentene

A: 930-28-9
cyclopentyl chloride

B: 14916-75-7
1,2-dichlorocyclopentane

C: 7582-01-6
Trichlormethyl-cyclopentan

Conditions

Conditions	Yield
Irradiation; Further byproducts given;

...Expand

: 75-09-2
dichloromethane

: 142-29-0
cyclopentene

A: 930-28-9
cyclopentyl chloride

B: 13988-39-1
chloromethylcyclopentane

C: 2690-18-8
3,3'-bicyclopentenyl

Conditions

Conditions	Yield
(radiolysis);

...Expand

: 142-29-0
cyclopentene

A: 930-28-9
cyclopentyl chloride

B: 14916-75-7
1,2-dichlorocyclopentane

C: 7582-02-7
1-chloro-2-(trichloromethyl)cyclopentane

Conditions

Conditions	Yield
With tetrachloromethane Irradiation; Further byproducts given;

...Expand

: 56-23-5
tetrachloromethane

: 110-05-4
di-tert-butyl peroxide

: 287-92-3
Cyclopentane

A: 67-66-3
chloroform

B: 67-72-1
hexachloroethane

C: 930-28-9
cyclopentyl chloride

D: 75-65-0
tert-butyl alcohol

Conditions

Conditions	Yield
Product distribution; Irradiation;

...Expand

: 96449-49-9
cyclopentyldiphenylbismutane

A: 930-28-9
cyclopentyl chloride

B: 108-90-7
chlorobenzene

Conditions

Conditions	Yield
With sulfuryl dichloride In dichloromethane -70 deg C to r.t.;	A 43 % Chromat. B 2 % Chromat.

: 75-71-8
Dichlorodifluoromethane

: 142-29-0
cyclopentene

A: 930-28-9
cyclopentyl chloride

B: 77116-58-6
(Chloro-difluoro-methyl)-cyclopentane

C: 77116-57-5
3-(Chloro-difluoro-methyl)-cyclopentene

: 77116-59-7
(3aS,4R,7R,7aS)-5-(Chloro-difluoro-methyl)-octahydro-4,7-methano-indene

Conditions

Conditions	Yield
at 200℃; Further byproducts given. Title compound not separated from byproducts;

...Expand

: 142-29-0
cyclopentene

: 930-28-9
cyclopentyl chloride

Conditions

Conditions	Yield
With nitrogen trichloride; borane 1.) CH2Cl2, 0 deg C, 2.) CH2Cl2, 30 h, 25 deg C; Yield given. Multistep reaction;

: 287-92-3
Cyclopentane

: 7782-50-5
chlorine

: 930-28-9
cyclopentyl chloride

: 287-92-3
Cyclopentane

: 7782-50-5
chlorine

: 78-00-2
tetraethyllead(IV)

: 930-28-9
cyclopentyl chloride

Conditions

Conditions	Yield
at 155℃;
at 155℃;

...Expand

: 67-66-3
chloroform

: 96-41-3
Cyclopentanol

: 10026-13-8, 874483-75-7
phosphorus pentachloride

calcium carbonate: calcium carbonate

A: 930-28-9
cyclopentyl chloride

B trans-1,2-dichloro-cyclopentane: trans-1,2-dichloro-cyclopentane

...Expand

: 287-92-3
Cyclopentane

A: 96-41-3
Cyclopentanol

B: 930-28-9
cyclopentyl chloride

C: 120-92-3
cyclopentanone

Conditions

Conditions	Yield
With oxygen In acetonitrile at 13℃; under 760 Torr; Product distribution; Further Variations:; Reagents; Irradiation;

...Expand

: 56-23-5
tetrachloromethane

: 142-29-0
cyclopentene

A: 930-28-9
cyclopentyl chloride

: trans-1-chloro-2-(trichloromethyl)cyclopentane

Conditions

Conditions	Yield
With chromium(III) acetylacetonate; water at 140℃; for 6h; Autoclave;

...Expand

: C5H9ClO2S

: 930-28-9
cyclopentyl chloride

Conditions

Conditions	Yield
With titanium tetrachloride In dichloromethane at 0℃; for 1h; Inert atmosphere;

: 621-59-0
isovanillin

: 930-28-9
cyclopentyl chloride

: 67387-76-2
3-cyclopentyloxy-4-methoxybenzylaldehyde

Conditions

Conditions	Yield
With potassium carbonate In N,N-dimethyl-formamide at 125℃; for 2h;	100%
With potassium carbonate In N-methyl-acetamide
With potassium carbonate

: 930-28-9
cyclopentyl chloride

: tricyclo[8.2.1.02,9]trideca-5,11-diene-13-one

: anti-tricyclo[8.2.1.02,9]trideca-5,11-diene-13-ol

Conditions

Conditions	Yield
Stage #1: cyclopentyl chloride With magnesium In tetrahydrofuran at 50℃; for 1h; Stage #2: tricyclo[8.2.1.02,9]trideca-5,11-diene-13-one In tetrahydrofuran at 40℃; for 0.166667h;	100%

: 930-28-9
cyclopentyl chloride

: 100-58-3
phenylmagnesium bromide

: 700-88-9
cyclopentylbenzene

Conditions

Conditions	Yield
With iron(III) chloride; N,N′-bis(2,6-diisopropylphenyl)imidazol-2-ylidene hydrochloride In tetrahydrofuran at 0 - 40℃; for 1.66667h;	99%
With copper(l) iodide In 2-methyltetrahydrofuran; toluene at 80℃; for 18h; Inert atmosphere; Schlenk technique; Sealed tube;	71%
With copper(l) iodide In 2-methyltetrahydrofuran; hexane at 80℃; for 14h; Schlenk technique; Inert atmosphere;	70%
With iron(III) chloride; N,N′-bis(2,6-diisopropylphenyl)imidazol-2-ylidene hydrochloride In tetrahydrofuran at 0 - 40℃; for 1.66667h;

: 930-28-9
cyclopentyl chloride

: 16643-09-7
trimethylstannyl sodium

: 15095-84-8
Trimethylstannyl-cyclopentan

Conditions

Conditions	Yield
In tetrahydrofuran 25°C in N2-atmosphere; various yields for various conditions;	98%
In further solvent(s) byproducts: NaCl; under argon, equimolar amounts, at 0°C in tetraglyme; GLC;	92%

: 930-28-9
cyclopentyl chloride

: 205672-25-9
4-amino-5-bromo-2-chloropyrimidine

: 733039-20-8
5-bromo-2-chloro-N-cyclopentylaminopyrimidine-4-amine

Conditions

Conditions	Yield
With triethylamine In methanol at 20℃;	92.74%
With copper diacetate; sodium hydroxide In dichloromethane at 80℃; for 10h;	77%

: 930-28-9
cyclopentyl chloride

: N,N‐dimethyl-2‐{[5‐(4-tert-butoxycarbonylpiperazin‐1‐yl)pyridin‐2‐yl]amino}‐7H‐pyrrolo[2,3‐d]pyrimidine‐6‐ carboxamide

: 1374639-78-7
N,N‐dimethyl‐7‐cyclopentyl‐2‐{[5‐(4-tert-butoxycarbonylpiperazin‐1‐yl)pyridin‐2‐yl]amino}‐7H‐pyrrolo[2,3‐d]pyrimidine‐6‐carboxamide

Conditions

Conditions	Yield
With potassium carbonate In acetonitrile at 55℃; for 5h;	90.6%

: 930-28-9
cyclopentyl chloride

: C19H23N7O2

: 6-acetyl-8-cyclopentyl-5-methyl-2-[[5-(1-piperazinyl)-2-pyridinyl]amino]-5,6-dihydropyrido[2,3-d]pyrimidyl-7(8H)-one

Conditions

Conditions	Yield
With 1,10-Phenanthroline; potassium carbonate; copper(I) bromide In N,N-dimethyl-formamide at 90℃; for 2h; Temperature; Reagent/catalyst;	90.5%

: 14159-55-8
2-cyclohex-1-enyl-pyridine

: 930-28-9
cyclopentyl chloride

: 2-(2-cyclopentylcyclohex-1-en-1-yl)pyridine

Conditions

Conditions	Yield
With N,N,N,N,-tetramethylethylenediamine; neopentylmagnesium bromide; cobalt(II) bromide; 1,3-diisopropyl-1H-benzo[d]imidazol-3-ium bromide In tetrahydrofuran at 0 - 20℃; for 12h; Schlenk technique;	90%

: 930-28-9
cyclopentyl chloride

: 874-90-8
4-methoxybenzonitrile

: 346720-43-2
N-cyclopentyl-4-methoxybenzamide

Conditions

Conditions	Yield
With zinc perchlorate In neat (no solvent) at 80℃; for 3h; Ritter Amidation;	90%
With iron(II) chloride tetrahydrate In neat (no solvent) at 80℃; for 4h; Ritter Amidation;	90%

: 930-28-9
cyclopentyl chloride

: 2-chloro-6-bromo-5-methyl-8H-pyrido[2,3-d]pyrimidin-7-one

: 2-chloro-6-bromo-8-cyclopentyl-5-methyl-8H-pyrido[2,3-d]pyrimidin-7-one

Conditions

Conditions	Yield
With sodium acetate In ethanol at 20℃; for 7h;	88%

: 930-28-9
cyclopentyl chloride

: 4,4,5,5-tetramethyl-2-(2-phenylhexan-2-yl)-1,3,2-dioxaborolane

: (2-cyclopentylhexan-2-yl)benzene

Conditions

Conditions	Yield
With potassium tert-butylate In 1,4-dioxane at 100℃; for 3h; Inert atmosphere; Sealed tube;	88%

: 930-28-9
cyclopentyl chloride

: (2,6-dibutylbenzo[1,2-b:5,4-b']difuran-3,5-diyl)bis((4-hydroxyphenyl)methanone)

: (2,6-dibutylbenzo[1,2-b:5,4-b']difuran-3,5-diyl)bis((4-(cyclopentyloxy)phenyl)methylketone)

Conditions

Conditions	Yield
Stage #1: (2,6-dibutylbenzo[1,2-b:5,4-b']difuran-3,5-diyl)bis((4-hydroxyphenyl)methanone) With potassium carbonate In toluene at 25 - 30℃; for 0.5h; Stage #2: cyclopentyl chloride In toluene at 25 - 30℃; for 5h;	87.8%

: 17771-33-4
7-hydroxy-2,2-dimethyl-chroman-4-one

: 930-28-9
cyclopentyl chloride

: 120046-18-6
7-(cyclopentyloxy)-2,2-dimethyl-2,3-dihydro-4H-chromen-4-one

Conditions

Conditions	Yield
With potassium carbonate; potassium iodide In N,N-dimethyl-formamide at 80℃; for 22h;	85%

: (E)-1-([1,1'-biphenyl]-4-yl)-N-(4-methoxyphenyl)ethan-1-imine

: 930-28-9
cyclopentyl chloride

: 1443686-20-1
1-(3-cyclopentyl-[1,1'-biphenyl]-4-yl)ethanone

Conditions

Conditions	Yield
Stage #1: (E)-1-([1,1'-biphenyl]-4-yl)-N-(4-methoxyphenyl)ethan-1-imine; cyclopentyl chloride With neopentylmagnesium bromide; cobalt(II) bromide; 1,3-Diisopropyl-4,5-dihydro-3H-imidazol-1-ium tetrafluoroborate In tetrahydrofuran at 0 - 20℃; for 29h; Schlenk technique; Inert atmosphere; Stage #2: With hydrogenchloride; water In tetrahydrofuran Inert atmosphere; Schlenk technique;	85%
With 1,3-diisopropylimidazolium tetrafluoroborate; neopentylmagnesium bromide; cobalt(II) bromide In tetrahydrofuran at 20℃; for 24h; Schlenk technique;	85%

: 930-28-9
cyclopentyl chloride

: 4294-57-9
para-methylphenylmagnesium bromide

: 827-55-4
p-cyclopentyltoluene

Conditions

Conditions	Yield
Stage #1: cyclopentyl chloride With [1,3-bis(3,5-di-tert-butyl-2-hydroxybenzyl)benzimidazolium][FeCl4] In diethyl ether at 0℃; for 0.0333333h; Schlenk technique; Inert atmosphere; Stage #2: para-methylphenylmagnesium bromide In diethyl ether at 0 - 30℃; for 2h; Temperature; Schlenk technique; Inert atmosphere;	84%

: 930-28-9
cyclopentyl chloride

: (Bicyclo<2.2.1>hept-5-en-2-yl)trimethoxysilan

: C14H24O2Si

Conditions

Conditions	Yield
Stage #1: cyclopentyl chloride With iodine; magnesium In tert-butyl methyl ether Inert atmosphere; Reflux; Stage #2: (Bicyclo<2.2.1>hept-5-en-2-yl)trimethoxysilan In tert-butyl methyl ether Inert atmosphere; Reflux;	84%

: 930-28-9
cyclopentyl chloride

: 143-33-9
sodium cyanide

: 4254-02-8
cyclopentanecarbonitrile

Conditions

Conditions	Yield
With tetrakis[tris(dimethylamino)phosphoranylideneamino]phosphonium chloride; tris phosphate In octane at 110℃; for 6h;	82%

: 930-28-9
cyclopentyl chloride

: 1481-36-3
fluorocyclopentane

Conditions

Conditions	Yield
With potassium fluoride; tetrakis[tris(dimethylamino)phosphoranylideneamino]phosphonium chloride; tris phosphate In DMF (N,N-dimethyl-formamide) at 110℃; for 6h;	80%
With potassium fluoride; tetrakis[tris(dimethylamino)phosphoranylideneamino]phosphonium chloride In DMF (N,N-dimethyl-formamide) at 110℃; for 6h;	68%

: 230-27-3
7,8-benzoquinoline

: 930-28-9
cyclopentyl chloride

: 10-cyclopentylbenzo[h]quinoline

Conditions

Conditions	Yield
With 1,3-diisopropylimidazolium tetrafluoroborate; neopentylmagnesium bromide; cobalt(II) bromide In tetrahydrofuran at 20℃; for 24h; Schlenk technique;	80%
With iron(II) triflate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; lithium hexamethyldisilazane at 140℃; for 12h; regioselective reaction;	76%

: 1945-84-2
2-ethynylpyridine

: 930-28-9
cyclopentyl chloride

: 865173-44-0
2-(cyclopentylethynyl)pyridine

Conditions

Conditions	Yield
With copper(l) iodide; C21H23ClNiP2S; caesium carbonate; sodium iodide In dimethyl sulfoxide at 50℃; for 12h; Sonogashira Cross-Coupling; Schlenk technique; Inert atmosphere;	80%

: 873-73-4
4-n-chlorophenylacetylene

: 930-28-9
cyclopentyl chloride

: 1-chloro-4-(cyclopentylethynyl)benzene

Conditions

Conditions	Yield
With copper(l) iodide; C21H23ClNiP2S; caesium carbonate; sodium iodide In dimethyl sulfoxide at 50℃; for 12h; Sonogashira Cross-Coupling; Schlenk technique; Inert atmosphere;	79%

: 930-28-9
cyclopentyl chloride

: 3839-31-4
dimethyl(phenyl)silyllithium

: cyclopentyldimethyl(phenyl)silane

Conditions

Conditions	Yield
In tetrahydrofuran at 0 - 20℃; for 12h; Schlenk technique; Sealed tube; Inert atmosphere;	74%

: 930-28-9
cyclopentyl chloride

: 768-60-5
4-methoxyphenylacetylen

: 1-(cyclopentylethynyl)-4-methoxybenzene

Conditions

Conditions	Yield
With copper(l) iodide; C21H23ClNiP2S; caesium carbonate; sodium iodide In dimethyl sulfoxide at 50℃; for 12h; Sonogashira Cross-Coupling; Schlenk technique; Inert atmosphere;	74%

: 930-28-9
cyclopentyl chloride

: 1079-66-9
chloro-diphenylphosphine

: 7650-81-9
cyclopentyl(diphenyl)phosphane

Conditions

Conditions	Yield
With magnesium In diethyl ether at 20℃; Inert atmosphere;	72%

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