Molecular weight: 152.15 CAS: 100-15-2 Packaging: According to customer requirements Storage method: Store in a cool and dry place. Nintedanib intermediate yellow powder Appearance:yellow powder Storage:keep sealed and keep from direct li
Cas:100-15-2
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inquiryHigh quality. Factory supply. In stock. Best price. 1.Quick response within 24 hours. 2.Best quality in your requirement. 3.We pay more attention on delivery time, and usually ship on time. 4.Free samples will be provided. 5.Ensure specifications an
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inquiryProduct Description Product Name N-Methyl-4-nitroaniline CAS No. 100-15-2 Appearance Yellow crystalline Assay ≥99% Capaci
Cas:100-15-2
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inquiryN-Methyl-4-nitroaniline CAS No.:100-15-2 Name: N-Methyl-4-nitroaniline Synonyms: 4-Nitro-N-methylaniline Molecular Structure Molecular Formula: C7H8N2O2 Molecular Weight: 152.15
Cas:100-15-2
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Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap
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inquiryHunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
Cas:100-15-2
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inquiry1. made in GMP plant, commerially 2. Normal Stock: 500kgs 3. Audit accepted. Related documents are available to offer and audited by many clients, such as Lupin, MSN, Dr reddy etc 4. Chromatographic Purity (HPLC): not less than 99.0% 5. Chi
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DayangChem exported this product to many countries and regions at best price in China. If you are looking for the product’s supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product specifica
Cas:100-15-2
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Cas:100-15-2
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inquiryN-Methyl-4-nitroaniline 100-15-2 Items Standard Result Appearance Orange yellow crystalline powder Complies
Cas:100-15-2
Min.Order:1 Gram
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inquiryNow we would like to update our product list for you, kindly check the below information: 1. Catalyst series ( such as Noble Metal Catalyst, Phosphorous ligand, etc ) 2. Pharmaceutical Intermediate ( such as diabtes series, Anti
Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryAppearance:Brownish-yellow crystalline powder Storage:R T Package:25kg/Barrel Application:Used in organic synthesis, dye intermediates. Transportation:Express/Sea/Air Port:Any port in China
Cas:100-15-2
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inquiryProduct Name: N-Methyl-4-nitroaniline CAS: 100-15-2 MF: C7H8N2O2 MW: 152.15 EINECS: 202-823-2 Melting point 149-151 °C(lit.) Boiling point 294.61°C (rough estimate) density 1.2010 vapor density 5.25 (vs air) r
Cas:100-15-2
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryN-Methyl-4-nitroaniline CAS:100-15-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic int
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Min.Order:1 Gram
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Min.Order:25 Gram
FOB Price: $90.0 / 100.0
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Cas:100-15-2
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inquiryAppearance:off-white solid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for Synthesis API and Research Transportation:As customer request Port:Qingdao/Shangha
Cas:100-15-2
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inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures
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Cas:100-15-2
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryp-Nitrophenyl-N-methyl-carbamidsaeure-methylester
N-methyl(p-nitroaniline)
Conditions | Yield |
---|---|
With tert-butylamine In methanol for 14h; Heating; | 100% |
With sodium hydroxide; cetyltrimethylammonim bromide In methanol; water at 68.5℃; Rate constant; |
Conditions | Yield |
---|---|
With potassium hydroxide | 100% |
at 130℃; for 11h; | 74% |
Conditions | Yield |
---|---|
With copper In water at 100℃; for 12h; Ullmann reaction; | 96.4% |
With copper(l) iodide; 6,7-dihydro-5H-quinolin-8-one oxime; potassium hydroxide In water at 25℃; for 24h; Inert atmosphere; | 85% |
Conditions | Yield |
---|---|
With C24H52B20Cl2Rh2Se2 In toluene at 20℃; for 2h; | 95% |
In methanol for 10h; Heating; | 41.1% |
With methanol at 95℃; |
(Z)-N-methyl-N-(4-nitrophenyl)-N'-<1-(phenylthio)-3,3-dimethylbut-1-en-2-yl>acetamidine
A
3,3-dimethyl-1-(phenylthio)butan-2-one
B
N-methyl(p-nitroaniline)
Conditions | Yield |
---|---|
With hydrogenchloride In 1,4-dioxane for 6h; Heating; | A 95% B n/a |
tert-butyl N-methyl-N-(4-nitrophenyl)carbamate
N-methyl(p-nitroaniline)
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane at 25℃; | 95% |
With tert-butylamine In methanol for 24h; Heating; | 7% |
Conditions | Yield |
---|---|
With copper In water at 100℃; for 12h; Ullmann reaction; | 93.4% |
at 20℃; for 16h; Heating; Sealed tube; | 4.5 g |
In water at 90℃; for 16h; Sealed tube; | 2.4 g |
Conditions | Yield |
---|---|
In water for 16h; Pressure bomb; | 93% |
With copper In water at 100℃; for 24h; Ullmann reaction; | 91.5% |
With 1:1 complex of Cl- with methylamine In ethanol at 150℃; sealed tube; | 84% |
In ethanol at 130℃; for 6h; | 79% |
With ethanol at 160℃; |
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 70℃; Inert atmosphere; | 93% |
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 70℃; Inert atmosphere; | 93% |
N-methyl-N-nosyl-p-nitroaniline
mercaptoacetic acid
A
2-(4-nitrophenylthio)acetic acid
B
N-methyl(p-nitroaniline)
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 20℃; | A n/a B 92% |
Conditions | Yield |
---|---|
With C19H37IrN4(2+)*2I(1-); potassium carbonate at 120℃; for 17h; Inert atmosphere; Schlenk technique; Sealed tube; | 92% |
With C12H16IrN4O2(1+)*BF4(1-); potassium hydroxide at 120℃; for 5h; Irradiation; Inert atmosphere; Sealed tube; | 60% |
With [(N,N′-bis(diisopropylphosphino)-2,6-diaminopyridine)Mn(CO)3][Br]; potassium tert-butylate In toluene at 120℃; for 24h; Inert atmosphere; Glovebox; Schlenk technique; | 59% |
N-(4-(dimethylamino)benzyl)-N-methyl-4-nitroaniline
N-methyl(p-nitroaniline)
Conditions | Yield |
---|---|
With water; trifluoroacetic acid In acetonitrile at 80℃; for 5h; Sealed tube; | 91% |
N-((1H-benzo[d][1,2,3]triazol-1-yl)methyl)-4-nitroaniline
N-methyl(p-nitroaniline)
Conditions | Yield |
---|---|
With sodium tetrahydroborate In tetrahydrofuran for 0.333333h; Heating; | 89% |
Conditions | Yield |
---|---|
With potassium hydroxide In neat (no solvent) at 100℃; for 24h; Sealed tube; | 89% |
N-methyl(p-nitroaniline)
Conditions | Yield |
---|---|
With tert-butylamine In methanol for 24h; Heating; | 86% |
ethyl N-methyl-N-4-nitrophenylcarbamate
N-methyl(p-nitroaniline)
Conditions | Yield |
---|---|
With tert-butylamine In methanol for 56h; Heating; | 86% |
N-methyl-4-nitro-N-(phenylthio)benzenamine
A
N-methyl-2-(phenylthio)-4-nitroaniline
B
N-methyl(p-nitroaniline)
C
diphenyldisulfane
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In acetonitrile for 0.166667h; Mechanism; Product distribution; Ambient temperature; various solvents, Lewis acids, and N-methylbenzenesulfenanilide; | A 7% B 65% C 84% |
In benzene at 85℃; for 144h; | A 83% B 15% C 14% |
With boron trifluoride diethyl etherate In benzene for 0.166667h; Ambient temperature; | A 26% B 36% C 63% |
p-nitro-N-(p-tolylthiomethyl)aniline
N-methyl(p-nitroaniline)
Conditions | Yield |
---|---|
With sodium tetrahydroborate In 1,2-dimethoxyethane for 0.5h; Heating; | 84% |
1-(p-nitrophenyl)-3-cyano-1-methyltriazene
N-methyl(p-nitroaniline)
Conditions | Yield |
---|---|
With sodium hydroxide In methanol for 0.5h; Heating; | 83% |
Conditions | Yield |
---|---|
With N-methyl-N-nitroso-4-nitroaniline for 3.5h; Irradiation; | A 81% B 87 % Turnov. |
N-methyl-N-nitroso-4-nitroaniline
A
methyl nitrite
B
N-methyl(p-nitroaniline)
Conditions | Yield |
---|---|
With methanol for 3.5h; Irradiation; | A 81% B 87 % Turnov. |
N-methyl-N-(4-nitrophenyl)-N'-<1-(phenylthio)pent-1-en-2-yl>acetamidine
A
1-(phenylthio)pentan-2-one
B
N-methyl(p-nitroaniline)
Conditions | Yield |
---|---|
With hydrogenchloride In 1,4-dioxane for 0.5h; Heating; Yields of byproduct given; | A 80% B n/a |
N-methyl-N-(4-nitrophenyl)-N-<1-phenyl-2-(phenylthio)vinyl>acetamidine
A
1-phenyl-2-(phenylthio)ethanone
B
N-methyl(p-nitroaniline)
Conditions | Yield |
---|---|
With hydrogenchloride In 1,4-dioxane for 0.5h; Heating; Yields of byproduct given; | A 80% B n/a |
N-methyl-N-(4-nitrophenyl)-N'-<1-(phenylthio)hex-1-en-2-yl>acetamidine
A
1-(Phenylthio)hexan-2-one
B
N-methyl(p-nitroaniline)
Conditions | Yield |
---|---|
With hydrogenchloride In 1,4-dioxane for 0.5h; Heating; Yields of byproduct given; | A 80% B n/a |
N,N-Dimethyl-4-nitroaniline
A
N-methyl-N-nitrosoaniline
B
nitrobenzene
C
N-methyl(p-nitroaniline)
D
N-methyl-N-nitroso-4-nitroaniline
Conditions | Yield |
---|---|
With n-Butyl nitrite; ammonium chloride; water for 2h; Heating; | A 2% B 1% C 4% D 80% |
4-nitro-aniline
2-(2-Methoxyethoxy)ethyl methyl carbonate
A
N-methyl(p-nitroaniline)
B
N,N-Dimethyl-4-nitroaniline
Conditions | Yield |
---|---|
With NaY at 160℃; for 4.16667h; | A 80% B n/a |
N-methyl(p-nitroaniline)
Conditions | Yield |
---|---|
With methanol; sodium methylate | 80% |
N-(4-nitrophenyl)-1H-imidazole-1-carboxamide
N-methyl(p-nitroaniline)
Conditions | Yield |
---|---|
With sodium tetrahydroborate; iodine In tetrahydrofuran at 20 - 66℃; for 6h; | 80% |
furan
N-methyl-4-nitro-N-(phenylthio)benzenamine
A
2-phenylthiofuran
B
N-methyl-2-(phenylthio)-4-nitroaniline
C
N-methyl(p-nitroaniline)
D
diphenyldisulfane
Conditions | Yield |
---|---|
at 85℃; for 144h; | A 40% B 4% C 79% D 25% |
Conditions | Yield |
---|---|
With hydrogen In ethyl acetate under 1551.44 Torr; | 100% |
With Zr12(μ3-O)5[(μ3-O)CoCl]8[(μ2-O)2(μ3-O)CoCl]3Li3(triphenyldicarboxylate)9; hydrogen; sodium triethylborohydride In toluene at 110℃; under 30003 Torr; for 42h; Catalytic behavior; Inert atmosphere; Schlenk technique; | 100% |
Stage #1: N-methyl(p-nitroaniline) With palladium 10% on activated carbon In tetrahydrofuran at 60℃; for 1.5h; Stage #2: With ammonium formate In tetrahydrofuran for 1.5h; | 94% |
Conditions | Yield |
---|---|
With N-Bromosuccinimide In acetonitrile for 0.5h; Cooling with ice; | 100% |
Stage #1: N-methyl(p-nitroaniline) With bromine; acetic acid In chloroform at 5 - 10℃; for 1h; Stage #2: With sodium hydrogencarbonate In chloroform; water | 99% |
With bromine; acetic acid In chloroform at 5 - 10℃; for 1h; | 99% |
With bromine; acetic acid |
di-tert-butyl dicarbonate
N-methyl(p-nitroaniline)
tert-butyl N-methyl-N-(4-nitrophenyl)carbamate
Conditions | Yield |
---|---|
With dmap In tetrahydrofuran at 20℃; for 2h; Reflux; Inert atmosphere; | 100% |
With dmap In tetrahydrofuran at 0 - 20℃; Inert atmosphere; | 90% |
Stage #1: N-methyl(p-nitroaniline) With dmap In tetrahydrofuran at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: di-tert-butyl dicarbonate With triethylamine In tetrahydrofuran at 20℃; for 12h; Inert atmosphere; | 60% |
N-methyl(p-nitroaniline)
Conditions | Yield |
---|---|
With bromine In chloroform; acetic acid | 99% |
Conditions | Yield |
---|---|
With porous-polymer-supported ruthenium(II)-phenyloxazoline complex catalyst In dichloromethane at 20℃; for 0.25h; Inert atmosphere; | 99% |
With [2-(4-hydroxymethyl)phenyl-4,4-(dimethyloxazole)Ru(CH3CN)4]PF6 In diethyl ether; water at 20℃; for 3h; | 75% |
methyl isocyanate
N-methyl(p-nitroaniline)
1,3-Dimethyl-1-(4-nitro-phenyl)-urea
Conditions | Yield |
---|---|
In toluene at 80℃; for 72h; | 98% |
N-methyl(p-nitroaniline)
3-(propa-1,2-dienyl)oxazolidin-2-one
(E)-3-(3-(methyl(4-nitrophenyl)amino)prop-1-en-1-yl)oxazolidin-2-one
Conditions | Yield |
---|---|
With (triphenylphosphine)gold(I) chloride; silver trifluoromethanesulfonate In dichloromethane at 20℃; for 1h; stereoselective reaction; | 98% |
With ethyldiphenylphosphine-functionalized MCM-41-anchored AuNTf2 In dichloromethane at 20℃; for 4h; | 96% |
2-bromo-N-(tert-butyl)cyclopropanecarboxamide
N-methyl(p-nitroaniline)
Conditions | Yield |
---|---|
With 18-crown-6 ether; potassium hydroxide In tetrahydrofuran at 55℃; for 12h; Inert atmosphere; diastereoselective reaction; | 98% |
1,4-dithiino<2,3-c;6,5-c'>diisothiazole-3,7-dicarbonyl chloride
N-methyl(p-nitroaniline)
N,N'-Bis(4-nitrophenyl)-N,N'-dimethyl-1,4-dithiino<2,3-c;6,5-c'>diisothiazol-3,7-dicarboxamid
Conditions | Yield |
---|---|
In 1,2-dichloro-ethane for 2h; Heating; | 96% |
(acetylamino)acetaldehyde dimethyl acetal
N-methyl(p-nitroaniline)
N-(2-(methyl(4-nitrophenyl)amino)ethyl)acetamide
Conditions | Yield |
---|---|
With triethylsilane; trifluoroacetic acid In dichloromethane at 20℃; for 2h; Inert atmosphere; chemoselective reaction; | 96% |
naphthalene-2-boronic acid
N-methyl(p-nitroaniline)
Conditions | Yield |
---|---|
With copper diacetate; triethylamine In dichloromethane at 0 - 5℃; for 4h; Sonication; Green chemistry; | 96% |
N-methyl(p-nitroaniline)
N-methyl-4-nitro-N-(trifluoromethyl)aniline
Conditions | Yield |
---|---|
Stage #1: N-methyl(p-nitroaniline); tetramethylammonium trifluoromethanethiolate In dichloromethane at 20℃; Stage #2: With silver fluoride In dichloromethane at 20℃; for 4h; Sonication; | 96% |
Conditions | Yield |
---|---|
With titanium(IV) isopropylate; palladium diacetate; triphenylphosphine In toluene at 115℃; for 5h; Inert atmosphere; | 96% |
chloroacetyl chloride
N-methyl(p-nitroaniline)
2-chloro-N-methyl-N-(4-nitrophenyl)acetamide
Conditions | Yield |
---|---|
In toluene at 100℃; for 2h; | 93% |
In ethyl acetate at 70℃; for 1h; | 90% |
In ethyl acetate at 70℃; for 1h; | 90% |
Methoxyacetyl chloride
N-methyl(p-nitroaniline)
N-methoxyacetyl-N-methyl-4-amino-nitrobenzene
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran for 20h; | 93% |
4-trifluoromethylphenylboronic acid
N-methyl(p-nitroaniline)
Conditions | Yield |
---|---|
With copper diacetate; triethylamine In dichloromethane at 0 - 5℃; for 4h; Sonication; Green chemistry; | 93% |
Conditions | Yield |
---|---|
With hydrogenchloride; 1-butyl-3-methylimidazolium nitrite In water at 5 - 25℃; for 0.533333h; | 92% |
With oxygen; nitrogen(II) oxide In 1,2-dichloro-ethane for 24h; Ambient temperature; | 90% |
Stage #1: N-methyl(p-nitroaniline) With hydrogenchloride In water at 0℃; Stage #2: With 1-(4-(nitrosooxy)butyl)-3-methylimidazolium chloride at 0 - 25℃; for 1.5h; | 90% |
Conditions | Yield |
---|---|
Stage #1: 4-chloro-1H-pyrrolo[2,3-d]pyrimidine; N-methyl(p-nitroaniline) With hydrogenchloride In 1,4-dioxane at 130℃; Stage #2: With triethylamine In methanol | 91.5% |
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