DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:106-22-9
Min.Order:1 Kilogram
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:106-22-9
Min.Order:0 Metric Ton
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inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:106-22-9
Min.Order:1 Gram
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Type:Manufacturers
inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
Cas:106-22-9
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Manufacturers
inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.
Cas:106-22-9
Min.Order:1 Kilogram
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:106-22-9
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developmen
Cas:106-22-9
Min.Order:1 Kilogram
FOB Price: $2.0 / 6.0
Type:Trading Company
inquiryProduct Name Citronellol CAS 106-22-9 EINECS 203-375-0 Appearance Colorless to light yellow clear liquid Purity 95
1. Best prices with satisfied quality; 2. It's clients' right to choose the package's Courier (EMS, DHL, FedEx, UPS); 3.It's clients' right to choose the packing way for his produccts from many recent effective packing ways;
Appearance:Clear almost colorless liquid Storage:room temperature Package:200kg/Drum Application:Perfumery, flavoring agent. Transportation:Express/Sea/Air Port:Any port in China
Cas:106-22-9
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:106-22-9
Min.Order:1 Kilogram
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inquiryWe are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery
Cas:106-22-9
Min.Order:10 Gram
FOB Price: $3.5
Type:Trading Company
inquiryEmpagliflozin CAS:106-22-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates
Cas:106-22-9
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:106-22-9
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquirySuperiority We can customize and synthesize products that other suppliers may not be able to provide. Advantage cof, mof ligand manufacturer best service, company and transport
Cas:106-22-9
Min.Order:100 Kilogram
Negotiable
Type:Trading Company
inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:106-22-9
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryAbout Product Details
Cas:106-22-9
Min.Order:500 Kilogram
FOB Price: $1.0 / 2.0
Type:Lab/Research institutions
inquiryWe have overseas warehouses in California, Nuevo Laredo, Mexico, Vancouver, Canada, Amsterdam, The Netherlands and Melbourne, Australia. Overseas warehouses can provide some of the best selling products. We look forward to cooperating with strong loc
Cas:106-22-9
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:106-22-9
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryPacking: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Appearance:Colorless liquid / Refer to COA Storage:2-8°C P
Cas:106-22-9
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:106-22-9
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:106-22-9
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:colourless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediat
Cas:106-22-9
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
3,7-dimethyl-oct-6-enal
Citronellol
Conditions | Yield |
---|---|
With Zn(BH4)2(Ph3P)2 In tetrahydrofuran at 20℃; Reduction; | 100% |
With hydrogen; aluminum oxide; copper In isopropyl alcohol at 90℃; for 0.75h; | 100% |
With trimethylamine-N-oxide; sodium formate; C34H44FeN4O4(2+)*2I(1-) In water at 80℃; for 24h; Inert atmosphere; Schlenk technique; | 99% |
Conditions | Yield |
---|---|
With hydrogen; aluminum oxide; copper In isopropyl alcohol at 90℃; for 12h; | 100% |
With hydrogen; polymer-supported rhodium catalyst In dichloromethane under 1551.49 Torr; for 10h; Hydrogenation; | 96% |
With 1,1'-bis(diphenylphosphino)ferrocene; [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; Butane-1,4-diol; potassium tert-butylate at 110℃; for 24h; Inert atmosphere; | 71% |
Conditions | Yield |
---|---|
With hydrogen; aluminum oxide; copper In isopropyl alcohol at 90℃; for 12h; | 100% |
With dichloro(η3:η2:η3-dodeca-2,6,10-triene-1,12-diyl)ruthenium(IV); caesium carbonate; isopropyl alcohol at 82℃; for 23h; Inert atmosphere; chemoselective reaction; | 95 %Chromat. |
1-(benzyloxy)-3,7-dimethyloct-6-ene
Citronellol
Conditions | Yield |
---|---|
With hydrogen; benzyl bromide; Pd<*>MCM-48 In methanol under 760.051 Torr; for 0.5h; | 99% |
With aluminium trichloride; N,N-dimethyl-aniline In dichloromethane for 1.5h; Ambient temperature; | 98% |
With naphthalene; lithium In tetrahydrofuran; methanol at -78℃; for 40h; | 89% |
Conditions | Yield |
---|---|
With [RuCl2((E)-N-(2-(diphenylphosphino)benzyl)-1-(6-((diphenylphosphino)methyl)pyridin-2-yl)methanimine)]; hydrogen; sodium ethanolate at 80℃; under 37503.8 Torr; for 5h; Autoclave; | 98% |
With lithium aluminium tetrahydride Yield given; |
Citronellol
Conditions | Yield |
---|---|
With ammonium cerium(IV) nitrate In water; acetonitrile at 0℃; for 0.5h; Product distribution; | 98% |
2-(3,7-dimethyloct-6-enyloxy)-tetrahydro-2H-pyran
Citronellol
Conditions | Yield |
---|---|
With SA-3 silica-alumina gel In methanol at 120℃; for 2.16667h; | 98% |
With SA-3 silica-alumina gel In methanol at 120℃; for 2.16667h; Product distribution; other ethers, var. silica-alumina gels, temp. and time; | 98% |
With copper dichloride In methanol at 20℃; Hydrolysis; | 90% |
With CuCl2*2H2O In methanol at 20℃; for 1.25h; | 90% |
With boron trifluoride diethyl etherate; sodium cyanoborohydride In tetrahydrofuran for 3h; Ambient temperature; | 80% |
Citronellol
Conditions | Yield |
---|---|
With SA-3 silica-alumina gel In methanol at 120℃; for 1.33333h; | 98% |
Citronellol
Conditions | Yield |
---|---|
With dibromotriphenylphosphorane In dichloromethane at -50℃; for 2h; | 97% |
(3,7-dimethyloct-6-enyloxy)trimethylsilane
Citronellol
Conditions | Yield |
---|---|
With SA-3 silica-alumina gel In methanol for 1.16667h; Ambient temperature; | 97% |
With 18-crown-6 ether In ethanol; water at 45℃; for 3h; Green chemistry; | 91% |
Citronellol
Conditions | Yield |
---|---|
With SA-2 silica-alumina gel In methanol for 3.16667h; Ambient temperature; | 97% |
cis-3,7-dimethyl-2,6-octadienal
A
Citronellol
B
3,7-dimethyl-oct-6-enal
Conditions | Yield |
---|---|
With acetylacetonato(1,5-cyclooctadiene)rhodium(I); hydrogen; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In toluene at 25℃; under 750.075 Torr; for 0.5h; Catalytic behavior; Temperature; Pressure; Autoclave; chemoselective reaction; | A 3% B 97% |
With acetylacetonatodicarbonylrhodium(l); hydrogen; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In neat (no solvent) at 60℃; under 30003 Torr; for 10h; Temperature; Pressure; Autoclave; | A 88 %Spectr. B 12 %Spectr. |
Citronellol
Conditions | Yield |
---|---|
With cerium(III) chloride In acetonitrile for 1h; Heating; | 96% |
Conditions | Yield |
---|---|
With LaNi5 hydride In tetrahydrofuran; methanol for 12h; Ambient temperature; | 95% |
With LaNi5 hydride In tetrahydrofuran; methanol 1) 0 deg C, 6 h, 2) r.t., 12 h; | 95% |
With hydrido(triphenylphosphine)copper(I) hexamer In tetrahydrofuran for 24h; Ambient temperature; | 90% |
(E/Z)-3,7-dimethyl-2,6-octadienal
A
Citronellol
B
3,7-dimethyl-oct-6-enal
Conditions | Yield |
---|---|
With hydrogen; Ni0.88Cr0.12 In cyclohexane at 79.9℃; under 7575.6 Torr; Product distribution; other catalysts, hydrogenation rates, selectivity of catalysts; | A n/a B 92% |
With hydrogen; Ni-Gr2 In methanol at 45℃; under 22800 Torr; for 18h; | A 68% B 26% |
With hydrogen; sodium carbonate; chromium(III) oxide; nickel In water; isopropyl alcohol at 120℃; under 30400 Torr; Product distribution; other temperature, other solvent, other pressure, other catalysts; | A 0.6 % Chromat. B 97.5 % Chromat. |
tert-butyl((3,7-dimethyloct-6-en-1-yl)oxy)dimethylsilane
Citronellol
Conditions | Yield |
---|---|
With 2,5-bis(perfluorobutyl)-1,4-benzoquinone In water; acetonitrile at 20℃; for 6h; | 92% |
With oxone In methanol at 20℃; for 15h; | 80% |
With bismuth(III) chloride; sodium iodide In acetonitrile at 20℃; for 1.5h; | 76% |
3,7-dimethyl-oct-6-enal
aniline
A
Citronellol
B
N-(3,7-dimethyloct-6-en-1-yl)aniline
Conditions | Yield |
---|---|
Stage #1: 3,7-dimethyl-oct-6-enal; aniline at 25℃; for 0.166667h; Stage #2: With sodium tetrahydroborate; boric acid at 25℃; for 0.333333h; | A n/a B 92% |
Citronellol
Conditions | Yield |
---|---|
In methanol; dichloromethane desilylation; Photolysis; | 91% |
Citronellol
Conditions | Yield |
---|---|
With 18-crown-6 ether In ethanol; water at 45℃; for 2.5h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Green chemistry; | 91% |
Citronellol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran at -20℃; | 90% |
Conditions | Yield |
---|---|
With Ba(BH2S3)2 In tetrahydrofuran at 20℃; for 2.5h; | 90% |
With hydrogen In isopropyl alcohol at 70℃; under 56255.6 Torr; for 2h; Reagent/catalyst; Autoclave; Glovebox; |
(E/Z)-3,7-dimethyl-2,6-octadienal
A
Citronellol
B
tetrahydrogeraniol
menthol
Conditions | Yield |
---|---|
With hydrogen In tert-butyl alcohol at 80℃; under 1500.15 - 15001.5 Torr; for 8h; Autoclave; diastereoselective reaction; | A n/a B n/a C 89% |
Conditions | Yield |
---|---|
With hydrogen; silver In tetrahydrofuran at 150℃; under 11251.1 Torr; for 72h; | A 10% B 88% |
With sodium cyanoborohydride at 20℃; for 0.05h; | A 46% B 54% |
With (triphenylphosphine)copper(I) hydride hexamer; hydrogen; Dimethyl(phenyl)phosphine In tert-butyl alcohol; benzene at 20℃; under 25857.4 Torr; for 15h; Hydrogenation; Title compound not separated from byproducts; |
Conditions | Yield |
---|---|
With chlorine[2-(4,5-dihydro-1H-imidazol-2-yl)-6-methoxypyridine](pentamethylcyclopentadienyl)iridium(III) chloride; sodium formate In water at 80℃; for 0.5h; Schlenk technique; chemoselective reaction; | A 88% B n/a |
Citronellol
Conditions | Yield |
---|---|
With samarium diiodide; water; isopropylamine In tetrahydrofuran at 20℃; for 0.0833333h; | 87% |
With naphthalene; lithium In tetrahydrofuran; methanol at -78℃; for 40h; | 86% |
(E/Z)-3,7-dimethyl-2,6-octadienal
A
Citronellol
B
tetrahydrogeraniol
menthol
Conditions | Yield |
---|---|
With hydrogen In tert-butyl alcohol at 80℃; under 7500.75 Torr; for 8h; Autoclave; diastereoselective reaction; | A n/a B n/a C 87% D n/a |
(+/-)-citronellyl tosylate
Citronellol
Conditions | Yield |
---|---|
With tetraethylammonium perchlorate; triethylamine In dimethyl sulfoxide at 20℃; for 10h; Electrolysis; Green chemistry; | 87% |
3,7-dimethyl-1-acetoxy-6-p-toluenesulfonyloxy octane
A
Citronellol
B
tetrahydrogeraniol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran 1.) -10 deg C 2.) RT; | A 6% B 82% |
3,7-dimethyl-oct-6-enal
A
Citronellol
B
(3,7-dimethyloctyl)amine
C
3,7-dimethyl-6-octenylamine
D
3,3',7,7'-tetramethyldi-6-octenylamine
Conditions | Yield |
---|---|
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; hydrogen; ammonium hydroxide; 1-methyl-3-decylimidazolium bromide In toluene at 130℃; under 45004.5 Torr; for 6h; Reagent/catalyst; Autoclave; | A 8% B 1% C 81% D n/a E n/a F 8% |
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; hydrogen; ammonium hydroxide; 1-octyl-3-methyl-imidazolium bromide In toluene at 130℃; under 45004.5 Torr; for 6h; Autoclave; | A 20% B 2% C 41% D n/a E n/a F 21% |
Citronellol
Conditions | Yield |
---|---|
With palladium diacetate; sodium azide; trisodium tris(3-sulfophenyl)phosphine In water; acetonitrile at 25℃; for 1h; | 80% |
Conditions | Yield |
---|---|
With carbon tetrabromide; triphenylphosphine In dichloromethane at 0℃; for 2h; | 100% |
With 1H-imidazole; iodine In dichloromethane at 20℃; for 0.75h; | 93% |
With pyridine; bromine; triphenylphosphine In tetrachloromethane; N,N-dimethyl-formamide at 45℃; | 89% |
Conditions | Yield |
---|---|
Stage #1: Citronellol With sodium hydride In tetrahydrofuran at 0℃; for 0.5h; Stage #2: benzyl bromide With sodium iodide In tetrahydrofuran for 5h; Heating; | 100% |
Stage #1: Citronellol With sodium hydride In tetrahydrofuran; hexane for 2h; Heating; Stage #2: benzyl bromide With tetra-(n-butyl)ammonium iodide In tetrahydrofuran; hexane for 18h; Heating; Further stages.; | 58% |
With sodium hydride 1.) dimethoxyethane, room temperature, 2 h, 2.) room temperature, 40 h; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With pyridine at 0 - 5℃; for 1h; | 100% |
With potassium hydroxide; potassium carbonate for 0.05h; | 93% |
With pyridine In chloroform for 0.5h; sonication; | 92% |
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 20℃; | 100% |
With C12H8N2*2CH4O3S at 60℃; for 3h; | 99% |
With iodine at 25℃; for 0.0166667h; | 98% |
Citronellol
tert-butyldimethylsilyl chloride
tert-butyl((3,7-dimethyloct-6-en-1-yl)oxy)dimethylsilane
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 24h; | 100% |
With dmap; triethylamine | 96% |
With 1H-imidazole In dichloromethane at 0 - 20℃; for 16h; | 90% |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 5h; Inert atmosphere; | 100% |
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 22h; Inert atmosphere; | 88% |
Conditions | Yield |
---|---|
With Candida antarctica lipase B at 50℃; for 4h; Molecular sieve; Ionic liquid; Green chemistry; Enzymatic reaction; | 99.9% |
In n-heptane at 40℃; for 24h; lipozyme IM 20 (immobilized Mucor miehi lipase); | 94.66% |
In water at 30℃; for 18h; lipase from Aspergillus niger; Yield given; |
Conditions | Yield |
---|---|
With Candida antarctica lipase B at 50℃; for 4h; Molecular sieve; Ionic liquid; Green chemistry; Enzymatic reaction; | 99.9% |
In water at 30℃; for 18h; lipase from Aspergillus niger; Yield given; |
Conditions | Yield |
---|---|
With Candida antarctica lipase B at 50℃; for 4h; Molecular sieve; Ionic liquid; Green chemistry; Enzymatic reaction; | 99.9% |
In water at 30℃; for 18h; lipase from Aspergillus niger; Yield given; |
Conditions | Yield |
---|---|
With Candida antarctica lipase B at 50℃; for 4h; Molecular sieve; Ionic liquid; Green chemistry; Enzymatic reaction; | 99.9% |
With cetyltrimethylammonium chloride; potassium hexacyanoferrate(III) at 80℃; for 1h; | 90% |
With molecular sieve at 120℃; for 8h; |
Conditions | Yield |
---|---|
With triethylamine at 20℃; | 99.5% |
With triethylamine In dichloromethane at 0℃; for 3h; Inert atmosphere; | 64% |
Citronellol
tetrahydrogeraniol
Conditions | Yield |
---|---|
With hydrogen; platinum(IV) oxide In ethyl acetate | 99% |
With hydrogen; palladium on activated charcoal In ethyl acetate at 80℃; under 2585.81 Torr; for 0.0833333h; microwave irradiation; | 99% |
With hydrogen; palladium on activated charcoal In methanol at 20℃; for 50h; | 93% |
Citronellol
3,7-dimethyl-oct-6-enal
Conditions | Yield |
---|---|
With pyridine chromium peroxide In dichloromethane for 1.25h; Product distribution; Ambient temperature; effect of various chromium(VI) based oxidants; | 99% |
With pyridine chromium peroxide In dichloromethane for 1.25h; Ambient temperature; | 99% |
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 3-[4'-(diacetoxyiodo)phenoxy]-1-propyl-N,N,N-trimethylammonium 4-methylbenzenesulfonate In dichloromethane at 20℃; for 2h; | 99% |
Citronellol
methanesulfonyl chloride
(±)-3,7-dimethyloct-6-en-1-yl methanesulfonate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; for 3h; Inert atmosphere; | 99% |
With triethylamine In dichloromethane at 0 - 20℃; for 24.3h; | 97% |
With triethylamine In dichloromethane at 0 - 20℃; for 16h; Inert atmosphere; | 94% |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid In dichloromethane Epoxidation; | 98% |
With oxygen; cobalt(II) acetate; isobutyraldehyde In dichloromethane at 20℃; for 5h; | 98% |
With (NMe4)(Co-ortho-phenylenebis(N'-methyloxamidate)*2H2O*CH3CN; oxygen; pivalaldehyde In fluorobenzene for 2.5h; Ambient temperature; | 95% |
Conditions | Yield |
---|---|
With potassium fluoride on basic alumina In toluene for 1h; | 98% |
Citronellol
1,2-dibromomethane
5-(2,2-dimethylcyclopropyl)-3-methylpentan-1-ol
Conditions | Yield |
---|---|
Stage #1: Citronellol; 1,2-dibromomethane With triisobutylaluminum at 10 - 20℃; for 0.25h; Stage #2: With iron(III) chloride; triisobutylaluminum at 25℃; for 3h; regioselective reaction; | 98% |
chloro-trimethyl-silane
Citronellol
(3,7-dimethyloct-6-enyloxy)trimethylsilane
Conditions | Yield |
---|---|
With 1,1,1,3,3,3-hexamethyl-disilazane at 25℃; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; Inert atmosphere; | 98% |
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