Puyang Huicheng Electronic Material Co., Ltd was founded in 2002, which is focus on high complex new type intermediates and fine chemical custom synthesis, LED&OLED materials and related intermediates, catalyst design and synthesis.
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inquiryDayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
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inquiryProduct Description Product Name 9-Phenyl-9H,9'H-[3,3']bicarbazolyl CAS No. 1060735-14-9 Assay ≥99% Capacity 50mt/year Min.packing 100gram Application OLED/p
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inquiryT he company has advanced technology, as well as a large number of excellent R & D team, to provide customers from the grams to one hundred kilograms and tons of high-quality products, competitive prices and quality service Appearance:White
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryAbout Product Details Item Specification Test Results Appearance White crystalline powder Conform
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inquiry9-Phenyl-9H,9'H-[3,3']bicarbazolyl Basic information Product Name: 9-Phenyl-9H,9'H-[3,3']bicarbazolyl Synonyms: 9-Phenyl-9H,9'H-[3,3']bicarbazolyl;3-(9-Phenyl-9H-
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiryName: Phenyl-3,3'-Bi-9H-carbazole Synonyms: 9-Phenyl-9H,9'H-[3,3']bicarbazolyl CAS:1060735-14-9 MF: C30H20N2 Appearance:White powder Storage:Store in cool and dry place, away from sun light. Package:25kg/drum Application: OLED
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiry1.High quality : the purity is 99% min . through multiple producing procedures. 2.Competitive price : low price because of our skilled production technolpgy ,save the production cost at most , and give big profit room to our customers 3.Safe a
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inquiryBeluga chemical professional supply 9-phenyl-9H,9'H-3,3'-bicarbazole CAS 1060735-14-9urer 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and research capabilities
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryAppearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:By
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryChemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryOur advantages: 1, High quality with competitive price: 1) Standard:BP/USP/EP/Enterprise standard 2) All Purity≥99% 3) We are manufacturer and can provide high quality products with factory price. 2, Fast and safe delivery 1) Parcel can be
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:1060735-14-9
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryWe're in good position to supply OLED intermediates . We supply 9-Phenyl-9H,9'H-[3,3']bicarbazolyl CAS# 1060735-14-9 at best price in China, Our 9-Phenyl-9H,9'H-[3,3']bicarbazolyl CAS# 1060735-14-9 has been exported to many
Cas:1060735-14-9
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inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
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inquiryProduct Name: 9-Phenyl-9H,9'H-[3,3']bicarbazolyl Synonyms: 9-Phenyl-9H,9'H-[3,3']bicarbazolyl;3-(9-Phenyl-9H-carbazol-3-yl)-9H-carbazole;9-phenyl-9H,9'H-3,3'-bicarbazole;3-(9-phenyl-carbazol-3-yl)-9H-carbazole;N-Phenyl-3
Cas:1060735-14-9
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryWe Huarong Pharm can provide Customized Synthesis & Process R&D & APIs and intermediates Production & Quality Research & Registration Application, especially our GMP validation service which complies with SFDA, FDA, WHO and EU EMPA. O
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inquiryHigh quality, competitive price, fast delivery and first-class service we possesses have won the trust and praise of customers. Standard: BP/USP/EP The purity is equal or greater than 99%. As a supplier, we can provide high-quality products. Cle
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
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inquiryN-phenyl-9H-carbazol-3-boronic acid
3-bromo-9H-carbazole
9-phenyl-3,3'-bicarbazole
Conditions | Yield |
---|---|
Stage #1: N-phenyl-9H-carbazol-3-boronic acid; 3-bromo-9H-carbazole With potassium carbonate In ethanol; water; toluene for 0.5h; Inert atmosphere; Stage #2: With tris-(dibenzylideneacetone)dipalladium(0); triphenylphosphine In ethanol; water; toluene for 2h; Reflux; | 97% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In water; toluene for 12h; Inert atmosphere; Reflux; | 90% |
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sodium carbonate In 1,4-dioxane; water for 4h; Inert atmosphere; Reflux; | 86% |
3-bromo-9-phenyl-9H-carbazole
9-phenyl-3,3'-bicarbazole
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In water; toluene for 12h; Reflux; | 90% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran at 65℃; for 18h; | 73% |
3-bromo-9H-carbazole
9-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)-9H-carbazole
9-phenyl-3,3'-bicarbazole
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0) In water; toluene for 5h; Inert atmosphere; Reflux; | 87% |
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate In 1,4-dioxane for 4h; Inert atmosphere; Reflux; | 80% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 80℃; for 24h; Inert atmosphere; | 77% |
N-phenyl-9H-carbazol-3-boronic acid
3-iodocarbazole
9-phenyl-3,3'-bicarbazole
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In water; toluene at 80℃; for 7h; Inert atmosphere; | 84% |
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In water; toluene at 80℃; for 7h; Inert atmosphere; | 2.43 g |
3-bromo-9-phenyl-9H-carbazole
3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole
9-phenyl-3,3'-bicarbazole
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); tetrabutylammomium bromide; sodium hydroxide In water; toluene at 80℃; for 12h; Inert atmosphere; | 75% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In water; toluene for 12h; Reflux; | 61% |
3-iodocarbazole
9-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)-9H-carbazole
9-phenyl-3,3'-bicarbazole
Conditions | Yield |
---|---|
With potassium phosphate; tetrakis(triphenylphosphine) palladium(0) In 1,4-dioxane at 85℃; for 48h; Inert atmosphere; | 74% |
With potassium phosphate; tetrakis(triphenylphosphine) palladium(0) In 1,4-dioxane at 85℃; for 48h; Suzuki coupling; Inert atmosphere; | 74% |
9H-carbazole
9-phenyl-3,3'-bicarbazole
Conditions | Yield |
---|---|
With N-Bromosuccinimide In methanol; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; N,N-dimethyl-formamide | |
Multi-step reaction with 4 steps 1: potassium carbonate; 18-crown-6 ether; tri-tert-butyl phosphine / tris-(dibenzylideneacetone)dipalladium(0) / toluene; xylene / 18 h / Inert atmosphere; Reflux 2: N-Bromosuccinimide / N,N-dimethyl-formamide / 0 °C 3: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 6 h / 80 °C / Inert atmosphere 4: potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / tris-(dibenzylideneacetone)dipalladium(0) / toluene; water / 5 h / Inert atmosphere; Reflux View Scheme | |
Multi-step reaction with 2 steps 1: N-Bromosuccinimide / N,N-dimethyl-formamide / 0 °C 2: potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / tris-(dibenzylideneacetone)dipalladium(0) / toluene; water / 5 h / Inert atmosphere; Reflux View Scheme |
bromobenzene
9-phenyl-3,3'-bicarbazole
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: potassium carbonate; 18-crown-6 ether; tri-tert-butyl phosphine / tris-(dibenzylideneacetone)dipalladium(0) / toluene; xylene / 18 h / Inert atmosphere; Reflux 2: N-Bromosuccinimide / N,N-dimethyl-formamide / 0 °C 3: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 6 h / 80 °C / Inert atmosphere 4: potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / tris-(dibenzylideneacetone)dipalladium(0) / toluene; water / 5 h / Inert atmosphere; Reflux View Scheme | |
Multi-step reaction with 2 steps 1: potassium acetate; dibenzo-18-crown-6; copper / N,N-dimethyl-formamide / 4 h / 120 °C 2: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / tetrahydrofuran / 18 h / 65 °C View Scheme |
3-bromo-9-phenyl-9H-carbazole
9-phenyl-3,3'-bicarbazole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 6 h / 80 °C / Inert atmosphere 2: potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / tris-(dibenzylideneacetone)dipalladium(0) / toluene; water / 5 h / Inert atmosphere; Reflux View Scheme | |
Multi-step reaction with 2 steps 1.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C 1.2: 8 h / 20 °C 2.1: potassium phosphate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / 48 h / 85 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C 1.2: 12 h / 20 °C 2.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / toluene; ethanol / 5 h / Reflux View Scheme | |
Multi-step reaction with 2 steps 1.1: n-butyllithium / diethyl ether; hexane / 0.5 h / -78 °C 1.2: -78 - 20 °C 2.1: tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran; water / 80 - 90 °C / Alkaline conditions View Scheme | |
Multi-step reaction with 2 steps 1.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere 1.2: -78 °C / Inert atmosphere 1.3: 0.5 h / Inert atmosphere 2.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / tetrahydrofuran; water / 8 h / Reflux; Inert atmosphere View Scheme |
N-phenylcarbazole
9-phenyl-3,3'-bicarbazole
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: N-Bromosuccinimide / N,N-dimethyl-formamide / 0 °C 2: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 6 h / 80 °C / Inert atmosphere 3: potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / tris-(dibenzylideneacetone)dipalladium(0) / toluene; water / 5 h / Inert atmosphere; Reflux View Scheme | |
Multi-step reaction with 4 steps 1.1: sulfuric acid; potassium iodate; potassium iodide / ethanol / 2 h / 75 °C 2.1: n-butyllithium / toluene; diethyl ether; hexane / 1 h / -45 - -5 °C / Inert atmosphere 2.2: 2 h / -45 °C / Inert atmosphere 3.1: hydrogenchloride / water; toluene; diethyl ether; hexane / 20 °C / Inert atmosphere 4.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; toluene / 7 h / 80 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: N-Bromosuccinimide / N,N-dimethyl-formamide / 12 h / 20 °C 2: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; water / 12 h / Reflux View Scheme |
N-phenyl-9H-carbazol-3-boronic acid
3-bromo-9H-carbazole
tris-(o-tolyl)phosphine
9-phenyl-3,3'-bicarbazole
Conditions | Yield |
---|---|
With potassium carbonate; palladium diacetate In 1,2-dimethoxyethane; toluene |
9-phenyl-3,3'-bicarbazole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrogenchloride / water; toluene; diethyl ether; hexane / 20 °C / Inert atmosphere 2: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; toluene / 7 h / 80 °C / Inert atmosphere View Scheme |
3-iodo-9-phenyl-9H-carbazole
9-phenyl-3,3'-bicarbazole
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: n-butyllithium / toluene; diethyl ether; hexane / 1 h / -45 - -5 °C / Inert atmosphere 1.2: 2 h / -45 °C / Inert atmosphere 2.1: hydrogenchloride / water; toluene; diethyl ether; hexane / 20 °C / Inert atmosphere 3.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; toluene / 7 h / 80 °C / Inert atmosphere View Scheme |
3-bromo-9H-carbazole
9-phenyl-3,3'-bicarbazole
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; tri-tert-butyl phosphine / toluene / 100 °C 2.1: n-butyllithium / diethyl ether; hexane / 0.5 h / -78 °C 2.2: -78 - 20 °C 3.1: tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran; water / 80 - 90 °C / Alkaline conditions View Scheme | |
Multi-step reaction with 2 steps 1: potassium acetate; dibenzo-18-crown-6; copper / N,N-dimethyl-formamide / 4 h / 120 °C 2: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / tetrahydrofuran / 18 h / 65 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: sodium hydride / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere 1.2: Inert atmosphere 2.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / toluene; water / 12 h / 95 °C / Inert atmosphere 3.1: tetrabutyl ammonium fluoride / tetrahydrofuran; dichloromethane / 2 h / 20 °C View Scheme |
iodobenzene
9-phenyl-3,3'-bicarbazole
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; tri-tert-butyl phosphine / toluene / 100 °C 2.1: n-butyllithium / diethyl ether; hexane / 0.5 h / -78 °C 2.2: -78 - 20 °C 3.1: tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran; water / 80 - 90 °C / Alkaline conditions View Scheme | |
Multi-step reaction with 3 steps 1: potassium phosphate; copper(l) iodide / toluene / 12 h / Reflux 2: N-Bromosuccinimide / N,N-dimethyl-formamide / 12 h / 20 °C 3: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; water / 12 h / Reflux View Scheme |
Conditions | Yield |
---|---|
With copper; potassium carbonate In nitrobenzene at 180℃; for 4h; Inert atmosphere; | 5.59 g |
9-phenyl-3,3'-bicarbazole
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran; dichloromethane at 20℃; for 2h; | 7.5 g |
Conditions | Yield |
---|---|
With caesium carbonate In 1-methyl-pyrrolidin-2-one at 170℃; for 24h; Inert atmosphere; | 99% |
9-phenyl-3,3'-bicarbazole
1-chlorobenzofuro[2,3-c]pyridine
C41H25N3O
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0) In xylene for 14h; Inert atmosphere; Reflux; | 98% |
9-phenyl-3,3'-bicarbazole
1,4-bromoiodobenzene
9-(4-bromophenyl)-9'-phenyl-9H,9'H-[3,3']bicarbazole
Conditions | Yield |
---|---|
With copper; potassium carbonate; sodium hydrogensulfite In 1,2-dichloro-benzene at 170℃; for 19.5h; Inert atmosphere; | 97% |
With potassium phosphate; copper(l) iodide; ethylenediamine In toluene for 24h; Reflux; | 80.1% |
With potassium phosphate; ethylenediamine; copper(l) iodide In toluene for 24h; Reflux; | 80.1% |
9-phenyl-3,3'-bicarbazole
2-(2,4-difluorophenyl)pyridine
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl acetamide at 190℃; for 23h; Sealed tube; Microwave irradiation; | 96% |
2,3-dichloroquinoxaline
9-phenyl-3,3'-bicarbazole
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; for 1h; | 95% |
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; for 2.5h; | 59% |
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; for 2.5h; | 59% |
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; for 1h; | 54% |
9-phenyl-3,3'-bicarbazole
(3-bromophenyl)(3-(dibenzo[b,d]furan-4-yl)phenyl)diphenylsilane
C66H44N2OSi
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0) In xylene Reflux; Inert atmosphere; | 94% |
bromobenzene
9-phenyl-3,3'-bicarbazole
9,9′-diphenyl-9H,9′H-3,3′-bicarbazole
Conditions | Yield |
---|---|
Stage #1: bromobenzene; 9-phenyl-3,3'-bicarbazole With potassium tert-butylate In toluene for 0.5h; Inert atmosphere; Stage #2: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; XPhos In toluene for 7h; Reflux; | 93% |
With tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In toluene for 12h; Reflux; Inert atmosphere; | 90% |
9-phenyl-3,3'-bicarbazole
2-(4-fluorophenyl)-3-phenylquinoxaline
9-phenyl-9'-[4-(3-phenylquinoxalin-2-yl)phenyl]-3,3'-bi(9H-carbazol)
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium t-butanolate In toluene at 80℃; for 6h; | 92% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium t-butanolate In toluene at 80℃; for 6h; | 91% |
9-phenyl-3,3'-bicarbazole
4-(3-bromophenyl)dibenzo[b,d]thiophene
C48H30N2S
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 60℃; for 12h; | 90% |
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In toluene for 4h; Reflux; | 89% |
9-phenyl-3,3'-bicarbazole
Conditions | Yield |
---|---|
With potassium phosphate In 1-methyl-pyrrolidin-2-one at 160℃; for 22h; Inert atmosphere; | 89% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 60℃; for 12h; Inert atmosphere; | 88% |
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene; toluene for 15h; Inert atmosphere; Reflux; | 73% |
With tris-(dibenzylideneacetone)dipalladium(0); trineopentyl phosphine; sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene; toluene for 15h; Inert atmosphere; Reflux; | 73% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene for 12h; Inert atmosphere; Reflux; | 88% |
9-phenyl-3,3'-bicarbazole
2,4-bis(4-fluorophenyl)-6-phenyl-1,3,5-triazine
Conditions | Yield |
---|---|
Stage #1: 2,4-bis(p-fluorophenyl)-6-phenyl-1,3,5-triazine With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.166667h; Inert atmosphere; Stage #2: 9-phenyl-3,3'-bicarbazole In N,N-dimethyl-formamide at 20℃; for 1h; | 87% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium t-butanolate In toluene at 80℃; for 6h; | 87% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 100℃; | 86% |
9-phenyl-3,3'-bicarbazole
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 100℃; | 86% |
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene Inert atmosphere; Reflux; | 86% |
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; rac-diaminocyclohexane In 1,4-dioxane for 12h; Inert atmosphere; Reflux; | 86% |
2-bromodibenzothiophene
9-phenyl-3,3'-bicarbazole
9-(dibenzo[b,d]thiophen-2-yl)-9'-phenyl-9H,9'H-3,3'-bicarbazole
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; trans-1,2-Diaminocyclohexane In 1,4-dioxane for 24h; Reflux; | 85% |
With potassium phosphate; copper(l) iodide; (S,S)-1,2-diaminocyclohexane In 1,4-dioxane for 24h; Reflux; | 85% |
With potassium phosphate; copper(l) iodide; (S,S)-1,2-diaminocyclohexane In 1,4-dioxane for 24h; Reflux; | 85% |
Conditions | Yield |
---|---|
With bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene for 6h; Inert atmosphere; Heating; | 85% |
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; trans-1,2-Diaminocyclohexane In 1,4-dioxane for 24h; Reflux; | 85% |
With potassium phosphate; copper(l) iodide; (S,S)-1,2-diaminocyclohexane In 1,4-dioxane for 24h; Reflux; | 85% |
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; trans-1,2-Diaminocyclohexane In 1,4-dioxane Reflux; | 85% |
With potassium phosphate; copper(l) iodide; (S,S)-1,2-diaminocyclohexane In 1,4-dioxane for 24h; Reflux; | 85% |
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; trans-1,2-Diaminocyclohexane In 1,4-dioxane for 24h; Reflux; | 85% |
With potassium phosphate; copper(l) iodide; trans-1,2-cyclohexanediamine In 1,4-dioxane for 24h; Reflux; | 85% |
With potassium phosphate; copper(l) iodide; (S,S)-1,2-diaminocyclohexane In 1,4-dioxane for 24h; Reflux; | 85% |
With potassium phosphate; copper(l) iodide; (S,S)-1,2-diaminocyclohexane In 1,4-dioxane for 24h; Reflux; | 85% |
With potassium phosphate; copper(l) iodide; trans-1,2-Diaminocyclohexane In 1,4-dioxane for 24h; Reflux; | 85% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium t-butanolate In toluene at 80℃; for 6h; | 85% |
9-phenyl-3,3'-bicarbazole
2-bromobenzo[9,10]phenanthrene
C48H30N2
Conditions | Yield |
---|---|
With 18-crown-6 ether; copper; potassium carbonate In 1,2-dichloro-benzene at 150℃; for 24h; Inert atmosphere; | 85% |
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