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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for t

1,3-Dibutylthiourea suppliers in China

Cas:109-46-6

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality N,N-Dibutylthiourea supplier in China

Cas:109-46-6

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Hangzhou Dingyan Chem Co., Ltd

Items Standard Result Assay (Ursolic acid) 98%min 98.22% ----------------------------------------------------------------

High purity 109-46-6 N,N′-Dibutylthiourea

Cas:109-46-6

Min.Order:1 Gram

FOB Price: $100.0 / 500.0

Type:Trading Company

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Wuhan Fortuna Chemical Co.,Ltd

Unique advantages for 1,3-Dibutyl-2-thiourea Cas 109-46-6 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White Crystal powder Storage:Store below +30°C Package:25kg/bag A

Factory best price 1,3-Dibutyl-2-thiourea Cas 109-46-6 with high quality and fast delivery

Cas:109-46-6

Min.Order:100 Kilogram

FOB Price: $4.8 / 5.0

Type:Trading Company

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 1,3-dibutyl-2-thiourea

Cas:109-46-6

Min.Order:1

Negotiable

Type:Other

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

N,N'-Dibutyl-2-thiourea

Cas:109-46-6

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

109-46-6 1,3-Dibutyl-2-thiourea

Cas:109-46-6

Min.Order:1 Kilogram

FOB Price: $1000.0

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con

1 3-Dibutyl-2-Thiourea CAS 109-46-6 Manufacturer

Cas:109-46-6

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 109-46-6 with best quality

Cas:109-46-6

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

1,3-Dibutyl-2-thiourea/Rubber Accelerator DBTU

Cas:109-46-6

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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Hangzhou Sartort Biopharma Co., Ltd

Appearance:White to Light yellow powder Storage:room temperature Package:25kg/drum Application:chemicals Transportation:Express/Sea/Air Port:any port in china

1,3-Dibutylthiourea factory price

Cas:109-46-6

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Lab/Research institutions

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

1,3-Dibutylthiourea 109-46-6

Cas:109-46-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Leader Biochemical Group

Overview of Our Factories Our Factories production lines Our Factories R&D ability Our Factories warehouse Our Factorie

China Biggest Factory & Manufacturer supply 1,3-Dibutyl-2-thiourea/DBTU CAS:675-66-7

Cas:109-46-6

Min.Order:1 Kilogram

FOB Price: $30.0 / 35.0

Type:Lab/Research institutions

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Shanghai Minstar Chemical Co., Ltd

Product Name: 1,3-Dibutyl-2-thiourea CAS: 109-46-6 MF: C9H20N2S MW: 188.33 EINECS: 203-674-6 Mol File: 109-46-6.mol 1,3-Dibutyl-2-thiourea Structure 1,3-Dibutyl-2-thiourea Chemical Properties Melting point 63-65 °C(lit.) B

1,3-Dibutyl-2-thiourea

Cas:109-46-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

1,3-Dibutylthiourea

Cas:109-46-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

1,3-Dibutyl-2-thiourea

Cas:109-46-6

Min.Order:1 Kilogram

FOB Price: $30.0 / 50.0

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

1,3-Dibutylthiourea

Cas:109-46-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

N,N-Dibutylthiourea

Cas:109-46-6

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

superior quality Appearance:powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:auxiliaries Transportation:as per your request Port:Shanghai, N

Thiourea, N,N'-dibutyl-? price

Cas:109-46-6

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Hubei Jiutian Bio-medical Technology Co., Ltd

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie

CAS 109-46-6 1,3-Dibutyl-2-thiourea

Cas:109-46-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Rubber Accelerator DBTU

Cas:109-46-6

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

1,3-Dibutylthiourea

Cas:109-46-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Lingrui Chemical Co.,Ltd.

our strengths: 1: Fast and guaranteed shipment (TNT;EMS;FEDEX;DHL;UPS;EUB, special line) 2: Various payment items accepted (Btc; MoneyGram; WU) 3: Valued package (Paraffin coating; Double aluminum foil bag; Vacuum packaging) 4: Efficient delivery

1,3-Dibutyl-2-thiourea with high purity

Cas:109-46-6

Min.Order:1 Gram

Negotiable

Type:Other

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EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

TIANFUCHEM--High purity 109-46-6 1,3-Dibutyl-2-thiourea

Cas:109-46-6

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

TIANFUCHEM--High purity 109-46-6 1,3-Dibutyl-2-thiourea

Cas:109-46-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Huarong Pharm Co., Ltd.

Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu

1,3-Dibutylthiourea

Cas:109-46-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

TIANFUCHEM--High purity 109-46-6 1,3-Dibutyl-2-thiourea

Cas:109-46-6

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

Rubber Accelerator DBTU

Cas:109-46-6

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Hebei Mojin Biotechnology Co.,Ltd

1, High quality with competitive price:2, Fast and safe delivery3.Excellent pre-sales and after-sales service4. Well-trained and professional technologist and sales with rich experience in the field for 5-10 yearsAppearance:see detailed specification

1,3-Dibutyl-2-thiourea

Cas:109-46-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

N,N'-Di-n-butylthiourea

Cas:109-46-6

Min.Order:0

Negotiable

Type:Other

inquiry

Synthetic route

sodium trithiocarbonate
534-18-9

sodium trithiocarbonate

N-butylamine
109-73-9

N-butylamine

A

1-methyl-2-pyridinethione
2044-27-1

1-methyl-2-pyridinethione

B

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

Conditions
ConditionsYield
With 2-chloro-1-methyl-pyridinium iodide In dichloromethane for 5h; Heating;A 90%
B 98%
N-butylamine
109-73-9

N-butylamine

thiourea
17356-08-0

thiourea

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

Conditions
ConditionsYield
With PEG-400 In water for 0.00833333h; microwave irradiation;96%
carbon disulfide
75-15-0

carbon disulfide

N-butylamine
109-73-9

N-butylamine

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

Conditions
ConditionsYield
In water at 20℃; for 0.833333h; Solvent; Time; Green chemistry;96%
In water at 20℃; for 0.833333h; Solvent; Green chemistry;96%
With carbon tetrabromide In N,N-dimethyl-formamide at 20℃; for 0.3h; Cooling with ice;91%
With cholin hydroxide at 20℃; Cooling with ice; Ionic liquid;76%
at 100℃; for 12h; Ionic liquid; Green chemistry;75%
Ziram

Ziram

N-butylamine
109-73-9

N-butylamine

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

Conditions
ConditionsYield
With triethanolamine; triethylamine In N,N-dimethyl-formamide for 2h; Heating;78%
O-isopropyl butylammonium dithiocarbonate
80094-32-2

O-isopropyl butylammonium dithiocarbonate

N-butylamine
109-73-9

N-butylamine

A

O-isopropyl butylthiocarbamate
61613-08-9

O-isopropyl butylthiocarbamate

B

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

Conditions
ConditionsYield
In benzene at 40℃; for 12h;A 0.58 g
B 59.8%
In benzene at 40℃; for 12h; Mechanism; Product distribution; Kinetics; thermal effects, ΔH;A 0.58 g
B 59.8%
N-butylamine
109-73-9

N-butylamine

N-phenyl-1,2,3,4,5,7-pentathioazocane
419532-33-5

N-phenyl-1,2,3,4,5,7-pentathioazocane

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

Conditions
ConditionsYield
In benzene for 6h; Reflux;41%
carbon disulfide
75-15-0

carbon disulfide

trimethyl(butyl-amino)silane
5577-66-2

trimethyl(butyl-amino)silane

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

Conditions
ConditionsYield
In ethyl acetate
N-butylamine
109-73-9

N-butylamine

butyl isothiocyanate
592-82-5

butyl isothiocyanate

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

Conditions
ConditionsYield
In ethanol
In dichloromethane at 0 - 25℃; for 1h;
In ethanol at 20℃;
carbon disulfide
75-15-0

carbon disulfide

N-butylamine
109-73-9

N-butylamine

diethylazodicarboxylate
1972-28-7

diethylazodicarboxylate

A

diethyl 1-[(butylcarbamothioyl)sulfanyl]hydrazine-1,2-dicarboxylate

diethyl 1-[(butylcarbamothioyl)sulfanyl]hydrazine-1,2-dicarboxylate

B

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

C

butyl isothiocyanate
592-82-5

butyl isothiocyanate

Conditions
ConditionsYield
Stage #1: carbon disulfide; N-butylamine In water for 0.166667h;
Stage #2: diethylazodicarboxylate In water at 20℃; for 0.5h; Solvent;
(3-glycidyloxypropyl)triethoxysilane
2602-34-8

(3-glycidyloxypropyl)triethoxysilane

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

N,N'-di-n-butyl-N,N'-bis({2-hydroxy-3-[3-(triethoxysilyl)propyloxy]propyl})thiourea

N,N'-di-n-butyl-N,N'-bis({2-hydroxy-3-[3-(triethoxysilyl)propyloxy]propyl})thiourea

Conditions
ConditionsYield
at 85 - 90℃; for 2.5h;97.2%
nickel(II) chloride hexahydrate

nickel(II) chloride hexahydrate

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

trans-dichlorotetrakis(N,N'-di-n-butylthiourea)nickel(II)
104419-49-0, 24616-63-5

trans-dichlorotetrakis(N,N'-di-n-butylthiourea)nickel(II)

Conditions
ConditionsYield
In ethanol refluxing of the Ni salt with the thiourea (mole ratio 1:2) in EtOH for at least 1 h; recrystn. from EtOH and drying (vac.); elem anal.;94%
1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

N-(4'-methylphenylsulfonyl)aziridino[2'3':1,2][60]fullerene
175970-03-3

N-(4'-methylphenylsulfonyl)aziridino[2'3':1,2][60]fullerene

C69H18N2S

C69H18N2S

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane In chlorobenzene at 80℃; for 1h; chemoselective reaction;94%
1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

N,N'-di(n-butyl)formamidine
2303-94-8

N,N'-di(n-butyl)formamidine

Conditions
ConditionsYield
With sodium tetrahydroborate; nickel dichloride In methanol at 20℃; for 0.5h;91%
Multi-step reaction with 2 steps
1: aq. H2O2 / methanol
2: acetic acid / Heating
View Scheme
2-iodophenylamine
615-43-0

2-iodophenylamine

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

N‐Butylbenzo[d]thiazol‐2‐amine
24622-31-9

N‐Butylbenzo[d]thiazol‐2‐amine

Conditions
ConditionsYield
bis(triethylphosphine)nickel(II) chloride; sodium cyanoborohydride In N,N-dimethyl-formamide at 60℃; for 60h;85%
1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

N,N'-Dibutyl-guanidine

N,N'-Dibutyl-guanidine

Conditions
ConditionsYield
With copper sulphate-silica gel; sodium amide In tetrahydrofuran for 0.833333h; Ambient temperature;80%
phenylborondichloride
873-51-8

phenylborondichloride

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

1,3,5-Tri-n-butyl-2,6-diphenyl-1,3,5-triaza-2,6-dibora-cyclohexanthion-4
81233-36-5

1,3,5-Tri-n-butyl-2,6-diphenyl-1,3,5-triaza-2,6-dibora-cyclohexanthion-4

Conditions
ConditionsYield
In tetrachloromethane byproducts: HCl; edducts in 1:1 ratio, reflux under N2 for 24 h; evapd. in vac., distd. in vac., elem. anal.;79%
dibromomethylborane
17933-16-3

dibromomethylborane

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

A

4-n-Butyl-3,5-dimethyl-1,2,4,3,5-dithiazadiborolidin

4-n-Butyl-3,5-dimethyl-1,2,4,3,5-dithiazadiborolidin

B

3,5-Di-n-butyl-2,3,5,6-tetrahydro-2,6-dimethyl-4H-1,3,5,2,6-thiadiazadiborin-4-thion
84185-20-6

3,5-Di-n-butyl-2,3,5,6-tetrahydro-2,6-dimethyl-4H-1,3,5,2,6-thiadiazadiborin-4-thion

Conditions
ConditionsYield
With n-butyllithium In hexane; Petroleum ether byproducts: butane, LiBr; the urea in petroleum ether was refluxed under N2 with n-BuLi in hexanefor 48 h; the solvents were removed in vac., the residue was fractional distd.; elem. anal.;A n/a
B 78%
1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

N,N'-di-n-butylcarbodiimide
693-64-1

N,N'-di-n-butylcarbodiimide

Conditions
ConditionsYield
With di-2-pyridyl sulfite In dichloromethane for 0.166667h; Ambient temperature;76%
With diethyl ether; mercury(II) oxide
With lead(II) oxide In acetone
bis(diethylamino)dimethylsilane
4669-59-4

bis(diethylamino)dimethylsilane

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

A

1,3,5-Tri-n-butyl-2,2,4,4-tetramethyl-1,3,5-triaza-2,4-disilacyclohexan-6-thion

1,3,5-Tri-n-butyl-2,2,4,4-tetramethyl-1,3,5-triaza-2,4-disilacyclohexan-6-thion

B

butyl isothiocyanate
592-82-5

butyl isothiocyanate

Conditions
ConditionsYield
In xylene for 12h; Heating;A 76%
B 1.8 g
C18H8ClNO5

C18H8ClNO5

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

9-benzoyl-1,3-dibutyl-6-(5-chloro-2-hydroxyphenyl)-8-hydroxy-2-thioxo-1,3,6-triazaspiro[4.4]non-8-ene-4,7-dione

9-benzoyl-1,3-dibutyl-6-(5-chloro-2-hydroxyphenyl)-8-hydroxy-2-thioxo-1,3,6-triazaspiro[4.4]non-8-ene-4,7-dione

Conditions
ConditionsYield
In 1,4-dioxane Reflux;76%
8-(4-chlorobenzoyl)-3,4-dihydro-1H-pyrrolo[2,1-c][1,4]oxazine-1,6,7-trione

8-(4-chlorobenzoyl)-3,4-dihydro-1H-pyrrolo[2,1-c][1,4]oxazine-1,6,7-trione

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

1,3-dibutyl-9-(4-chlorobenzoyl)-8-hydroxy-6-(2-hydroxyethyl)-2-thioxo-1,3,6-triazaspiro[4.4]non-8-ene-4,7-dione

1,3-dibutyl-9-(4-chlorobenzoyl)-8-hydroxy-6-(2-hydroxyethyl)-2-thioxo-1,3,6-triazaspiro[4.4]non-8-ene-4,7-dione

Conditions
ConditionsYield
In 1,4-dioxane Reflux;76%
1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

diethyl malonate
105-53-3

diethyl malonate

N,N'-dibutyl-2-thiobarbituric acid
54443-89-9

N,N'-dibutyl-2-thiobarbituric acid

Conditions
ConditionsYield
With sodium ethanolate for 72h;75%
With hydrogenchloride; water; sodium In ethanol for 48h; Inert atmosphere; Reflux;40%
1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

3-benzoylpyrrolo[2,1-c][1,4]benzoxazine-1,2,4-trione
142071-82-7

3-benzoylpyrrolo[2,1-c][1,4]benzoxazine-1,2,4-trione

9-benzoyl-1,3-dibutyl-8-hydroxy-6-(2-hydroxyphenyl)-2-thioxo-1,3,6-triazaspiro[4.4]non-8-ene-4,7-dione

9-benzoyl-1,3-dibutyl-8-hydroxy-6-(2-hydroxyphenyl)-2-thioxo-1,3,6-triazaspiro[4.4]non-8-ene-4,7-dione

Conditions
ConditionsYield
In 1,4-dioxane Reflux;75%
di-tert-butyl dicarbonate
24424-99-5

di-tert-butyl dicarbonate

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

N-tert-butoxycarbonyl-N,N'-dibutylthiourea
641611-19-0

N-tert-butoxycarbonyl-N,N'-dibutylthiourea

Conditions
ConditionsYield
With dmap In ethyl acetate at 70℃; for 0.25h; Temperature;73%
Stage #1: 1,3-dibutylthiourea With sodium hydride In tetrahydrofuran at 0℃; for 0.166667h;
Stage #2: di-tert-butyl dicarbonate In tetrahydrofuran at 20℃; for 12h;
57%
1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

α-bromoacetophenone
70-11-1

α-bromoacetophenone

N-butyl-N-(3-butyl-4-phenyl-2,3-dihydro-1,3-thiazol-2-yliden)amine hydrobromide

N-butyl-N-(3-butyl-4-phenyl-2,3-dihydro-1,3-thiazol-2-yliden)amine hydrobromide

Conditions
ConditionsYield
In ethanol for 2h; Heating;72%
diethyl 3-(phenyl)oxirane-2,2-dicarboxylate
58070-00-1

diethyl 3-(phenyl)oxirane-2,2-dicarboxylate

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

ethyl 1,3-dibutyl-2,4-dioxo-trans-6-phenylhexahydropyrimidine-5-carboxylate

ethyl 1,3-dibutyl-2,4-dioxo-trans-6-phenylhexahydropyrimidine-5-carboxylate

Conditions
ConditionsYield
With ytterbium(III) triflate In 1,4-dioxane at 90℃; for 65h; Inert atmosphere; Schlenk technique; Sealed tube;72%
1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

acetophenone
98-86-2

acetophenone

N-butyl-N-(3-butyl-4-phenyl-2,3-dihydro-1,3-thiazol-2-yliden)amine hydrobromide

N-butyl-N-(3-butyl-4-phenyl-2,3-dihydro-1,3-thiazol-2-yliden)amine hydrobromide

Conditions
ConditionsYield
Stage #1: acetophenone With p-dioxane dibromide In ethanol at 70℃; for 0.0833333h;
Stage #2: 1,3-dibutylthiourea In ethanol Heating;
68%
1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

(4-nitrophenyl)ethanone
100-19-6

(4-nitrophenyl)ethanone

N-butyl-N-[3-butyl-4-(4-nitrophenyl)-2,3-dihydro-1,3-thiazol-2-yliden]amine hydrobromide

N-butyl-N-[3-butyl-4-(4-nitrophenyl)-2,3-dihydro-1,3-thiazol-2-yliden]amine hydrobromide

Conditions
ConditionsYield
Stage #1: (4-nitrophenyl)ethanone With p-dioxane dibromide In ethanol at 70℃; for 0.0833333h;
Stage #2: 1,3-dibutylthiourea In ethanol Heating;
66%
Cyclohexyl isocyanide
931-53-3

Cyclohexyl isocyanide

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

N2,3-dibutyl-N4,N5-dicyclohexylthiazolidine-2,4,5-triimine

N2,3-dibutyl-N4,N5-dicyclohexylthiazolidine-2,4,5-triimine

Conditions
ConditionsYield
With bis(acetylacetonate)nickel(II) In acetone at 50℃; for 4h;65%
1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

chloroacetic acid
79-11-8

chloroacetic acid

3-n-butyl-2-(n-butylimino)-1,3-thiazolidine-4-one
537660-16-5

3-n-butyl-2-(n-butylimino)-1,3-thiazolidine-4-one

Conditions
ConditionsYield
In water at 100℃; for 7.5h; Green chemistry;64.9%
Reflux; Green chemistry;
dimethylboron bromide
5158-50-9

dimethylboron bromide

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

A

1,3,5-Tri-n-butyl-6-methyl-1,3,5-triaza-2-bora-cyclohexandithion-4,6

1,3,5-Tri-n-butyl-6-methyl-1,3,5-triaza-2-bora-cyclohexandithion-4,6

B

1,3,5-Tri-n-butyl-2,6-dimethyl-1,3,5-triaza-2,6-dibora-cyclohexanthion-4

1,3,5-Tri-n-butyl-2,6-dimethyl-1,3,5-triaza-2,6-dibora-cyclohexanthion-4

Conditions
ConditionsYield
In tetrachloromethane byproducts: HBr; edducts in 1:1 ratio, reflux under N2 for 24 h; cooled to 0°C, evapd. in vac., sublimation (110°C/2E-3 mbar for other product, 145°C/2E-3 mbar), elem. anal.;A 53%
B 64%
4,4-dichlorobut-3-en-2-one
5780-61-0

4,4-dichlorobut-3-en-2-one

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

3-Butyl-2-[(Z)-butylimino]-4-methyl-2,3-dihydro-[1,3]thiazine-6-thione
97309-91-6

3-Butyl-2-[(Z)-butylimino]-4-methyl-2,3-dihydro-[1,3]thiazine-6-thione

Conditions
ConditionsYield
for 0.5h; Heating;63%
butyl-dichloro-borane
14090-22-3

butyl-dichloro-borane

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

2,4-Di-n-butyl-5-n-butyl-6-n-butylimino-1-thia-3,5-diaza-2,4-dibora-cyclohexan

2,4-Di-n-butyl-5-n-butyl-6-n-butylimino-1-thia-3,5-diaza-2,4-dibora-cyclohexan

Conditions
ConditionsYield
In chlorobenzene byproducts: HCl; reflux under N2 for 24 h; evapd. in vac., sublimation (100°C/2E-3 mbar), elem. anal.;63%
sodium tetraphenyl borate
143-66-8

sodium tetraphenyl borate

1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

1,2-bis-(diphenylphosphino)ethane
1663-45-2

1,2-bis-(diphenylphosphino)ethane

(1,2-bis(diphenylphosphinoethane))Ni(nBuNC(S)NHnBu)(BPh4)
1279624-75-7

(1,2-bis(diphenylphosphinoethane))Ni(nBuNC(S)NHnBu)(BPh4)

Conditions
ConditionsYield
With NEt3 In methanol mixt. of Ni acetate and dppe in MeOH; stirred, gently warmed for 5 min; thiourea deriv. added; aq. NEt3 added, mixt. warmed briefly to ca. 60°C; NaBPh4 added to filtrate; allowed to cool to room temp.; ppt. filtered, washed with cold MeOH, dried under vac.; elem. anal.;63%
1,3-dibutylthiourea
109-46-6

1,3-dibutylthiourea

1-(4-methoxyphenyl)ethanone
100-06-1

1-(4-methoxyphenyl)ethanone

N-butyl-N-[3-butyl-4-(4-methoxyphenyl)-2,3-dihydro-1,3-thiazol-2-yliden]amine hydrobromide

N-butyl-N-[3-butyl-4-(4-methoxyphenyl)-2,3-dihydro-1,3-thiazol-2-yliden]amine hydrobromide

Conditions
ConditionsYield
Stage #1: 1-(4-methoxyphenyl)ethanone With p-dioxane dibromide In ethanol at 70℃; for 0.0833333h;
Stage #2: 1,3-dibutylthiourea In ethanol Heating;
62%
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