The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Cas:130-61-0
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inquiryDayangChem exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product s
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inquiry130-61-0 Thioridazine hydrochloride 1.Large qty in stock 2.High quality 3.Lowest price 4.Best service Our Advantage 1. Risk-free guarantee,15days refund 2. Most of the products in stock,can ship within 7days after the order 3. S
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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Cas:130-61-0
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inquiryThioridazine hydrochloride CAS:130-61-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryProduct Detail Minimum Order Qty. 10 Gram
Cas:130-61-0
Min.Order:10 Gram
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inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:130-61-0
Min.Order:10 Gram
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inquirySuperior quality, moderate price & quick delivery. Appearance:white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:10g/bag,or as your request Application:Used as Pharmaceutical Intermediates Transporta
Cas:130-61-0
Min.Order:1 Gram
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Type:Trading Company
inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
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inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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Min.Order:1 Metric Ton
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
1.A strong technical force and advanced processing equipments. The quality of the products has been strictly inspected and all kinds of index have reached or exceeded domestic and international standards.2. Now we have established long-term stable re
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
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inquiryWhy is SINOWAY:1) Specialized in pharmaceutical and healthcare industrial since 19872) ISO 9001:2015 & SGS audited supplier . 3) Accept various payment terms : T.T 30-60 days.4) We have warehouse in USA with quickly shipment . Application:API
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou
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inquirythioridazine Hydrochloride
Conditions | Yield |
---|---|
Stage #1: (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-{2-[2-(methylthio)-10H-phenothiazin-10-yl]ethyl}piperidine-1-carboxylate With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 50℃; for 18h; Inert atmosphere; Stage #2: With hydrogenchloride In ethanol; water | 100% |
Multi-step reaction with 2 steps 1: lithium aluminium tetrahydride / tetrahydrofuran / 18 h / 0 - 50 °C / Inert atmosphere 2: hydrogenchloride / ethanol; water View Scheme |
thioridazine
thioridazine Hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol; water | 100% |
Conditions | Yield |
---|---|
With dihydrogen peroxide In water for 72h; Ambient temperature; | 93% |
carbonochloridic acid 1-chloro-ethyl ester
thioridazine Hydrochloride
Conditions | Yield |
---|---|
Stage #1: thioridazine Hydrochloride With triethylamine In 1,2-dichloro-ethane at 20℃; for 0.333333h; Inert atmosphere; Stage #2: carbonochloridic acid 1-chloro-ethyl ester In 1,2-dichloro-ethane for 12h; Inert atmosphere; Reflux; | 84% |
1-methyl-1-propanethiol
thioridazine Hydrochloride
2-(sec-butylthio)-10-(2-(1-methylpiperidin-2-yl)ethyl)-10H-phenothiazine
Conditions | Yield |
---|---|
With Singacycle A1; lithium hexamethyldisilazane In o-xylene at 160℃; for 12h; Glovebox; Sealed tube; | 71% |
Conditions | Yield |
---|---|
With Singacycle A1; lithium hexamethyldisilazane In o-xylene at 160℃; for 12h; Glovebox; Sealed tube; | 62% |
1-Adamantanethiol
thioridazine Hydrochloride
Conditions | Yield |
---|---|
With Singacycle A1; lithium hexamethyldisilazane In o-xylene at 160℃; for 12h; Glovebox; Sealed tube; | 61% |
thioridazine Hydrochloride
phenylmethanethiol
2-(benzylthio)-10-(2-(1-methylpiperidin-2-yl)ethyl)-10H-phenothiazine
Conditions | Yield |
---|---|
With Singacycle A1; lithium hexamethyldisilazane In o-xylene at 160℃; for 12h; Glovebox; Sealed tube; | 56% |
Conditions | Yield |
---|---|
In acetonitrile for 24h; Reflux; Inert atmosphere; | 51% |
Conditions | Yield |
---|---|
With Singacycle A1; lithium hexamethyldisilazane In o-xylene at 160℃; for 12h; Glovebox; Sealed tube; | 49% |
thioridazine Hydrochloride
Conditions | Yield |
---|---|
In methanol slow addn. of soln. of ZnCl2 to soln. of ligand (room temp.), stirring (1 h), conctg. (reduced pressure), storing (overnight at 4°C); decanting viscous liq., redissolving in methanol with stirring at 60°C, suction filtn., washing (2-3 times, cold methanol), drying (air),drying (vac.), recrystn. (hot methanol), elem. anal.; | 48.5% |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 18h; | A 43% B 38% |
Conditions | Yield |
---|---|
In methanol slow addn. of soln. of ZnCl2 to soln. of ligand (room temp.), refluxing (60°C, 1.5-2 h), cooling (overnight to 4°C); decanting oily product, redissolving in methanol with stirring at 60°C, suction filtn., washing (2-3 times, cold methanol), drying (air),drying (vac.), recrystn. (hot methanol), elem. anal.; | 35.1% |
Conditions | Yield |
---|---|
In methanol dissolving ligand in methanol, slow addn. with stirring to conctd. methanolic soln. of PdCl2 contg. HCl (room temp.), stirring (1 h), cooling (overnight to 4°C); suction filtn., washing (several times, cold water, cold methanol), air drying, drying in vac. over anhydrous CaSO4, recrystn. from hot methanol, elem. anal.; | 30% |
thioridazine Hydrochloride
Conditions | Yield |
---|---|
With potassium metaperiodate; phosphoric acid; sulfuric acid In water |
Conditions | Yield |
---|---|
With potassium dichromate In water at 25℃; for 1h; |
thioridazine Hydrochloride
Conditions | Yield |
---|---|
With iron(III) chloride In water at 25℃; Product distribution; Further Variations:; Temperatures; Reagents; |
potassium tetrachloroplatinate(II)
thioridazine Hydrochloride
Pt(C6H4SN(CH2CH2C5H9NH(CH3))C6H3SCH3)Cl3
Conditions | Yield |
---|---|
In water byproducts: KCl; aq. soln. of ligand mixed with Pt complex; filtered off, washed with H2O, dried in vac. at 100 °C; elem. anal.; |
potassium tetrachloropalladate(II)
thioridazine Hydrochloride
Pd(C6H4SN(CH2CH2C5H9NH(CH3))C6H3SCH3)Cl3
Conditions | Yield |
---|---|
In water byproducts: KCl; aq. soln. of ligand mixed with Pd complex; filtered off, washed with H2O, dried in vac. at 100 °C; elem. anal.; |
thioridazine Hydrochloride
Northioridazine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: triethylamine / 1,2-dichloro-ethane / 0.33 h / 20 °C / Inert atmosphere 1.2: 12 h / Inert atmosphere; Reflux 2.1: water / methanol / 12 h / Reflux; Inert atmosphere View Scheme |
thioridazine Hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: triethylamine / 1,2-dichloro-ethane / 0.33 h / 20 °C / Inert atmosphere 1.2: 12 h / Inert atmosphere; Reflux 2.1: water / methanol / 12 h / Reflux; Inert atmosphere 3.1: tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere 3.2: 24 h / 20 °C / Inert atmosphere View Scheme |
thioridazine Hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: triethylamine / 1,2-dichloro-ethane / 0.33 h / 20 °C / Inert atmosphere 1.2: 12 h / Inert atmosphere; Reflux 2.1: water / methanol / 12 h / Reflux; Inert atmosphere 3.1: tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere 3.2: 24 h / 20 °C / Inert atmosphere View Scheme |
thioridazine Hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: triethylamine / 1,2-dichloro-ethane / 0.33 h / 20 °C / Inert atmosphere 1.2: 12 h / Inert atmosphere; Reflux 2.1: water / methanol / 12 h / Reflux; Inert atmosphere 3.1: tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere 3.2: 24 h / 20 °C / Inert atmosphere View Scheme |
thioridazine Hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C 2: lithium aluminium tetrahydride / tetrahydrofuran / 8 h / 20 °C / Reflux; Inert atmosphere View Scheme |
thioridazine Hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C 2: lithium aluminium tetrahydride / tetrahydrofuran / 8 h / 20 °C / Reflux; Inert atmosphere View Scheme |
thioridazine Hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 8 h / 20 °C / Reflux; Inert atmosphere 3.1: carbonochloridic acid 1-chloro-ethyl ester; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere 3.2: 4 h / Reflux; Inert atmosphere View Scheme |
thioridazine Hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C 2: chlorotriisopropylsilane; trifluoroacetic acid / water / 72 h / 110 °C / Sealed tube 3: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 8 h / 20 °C / Reflux; Inert atmosphere 3.1: carbonochloridic acid 1-chloro-ethyl ester; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere 3.2: 4 h / Reflux; Inert atmosphere 4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C / Inert atmosphere View Scheme |
thioridazine Hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C 2.1: chlorotriisopropylsilane; trifluoroacetic acid / water / 72 h / 110 °C / Sealed tube 3.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere 3.2: 16 h / 20 °C 4.1: water; tert-butyl alcohol / 20 °C 4.2: 33 °C View Scheme | |
Multi-step reaction with 5 steps 1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 8 h / 20 °C / Reflux; Inert atmosphere 3.1: carbonochloridic acid 1-chloro-ethyl ester; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere 3.2: 4 h / Reflux; Inert atmosphere 4.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere 4.2: 16 h / 20 °C 5.1: water; tert-butyl alcohol / 20 °C 5.2: 33 °C View Scheme |
thioridazine Hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C 2.1: chlorotriisopropylsilane; trifluoroacetic acid / water / 72 h / 110 °C / Sealed tube 3.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere 3.2: 16 h / 20 °C 4.1: water; tert-butyl alcohol / 20 °C 4.2: 58 h / 33 °C View Scheme | |
Multi-step reaction with 5 steps 1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 8 h / 20 °C / Reflux; Inert atmosphere 3.1: carbonochloridic acid 1-chloro-ethyl ester; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere 3.2: 4 h / Reflux; Inert atmosphere 4.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere 4.2: 16 h / 20 °C 5.1: water; tert-butyl alcohol / 20 °C 5.2: 58 h / 33 °C View Scheme |
thioridazine Hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C 2.1: chlorotriisopropylsilane; trifluoroacetic acid / water / 72 h / 110 °C / Sealed tube 3.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere 3.2: 16 h / 20 °C 4.1: water; tert-butyl alcohol / 20 °C 4.2: 58 h / 33 °C View Scheme | |
Multi-step reaction with 5 steps 1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 8 h / 20 °C / Reflux; Inert atmosphere 3.1: carbonochloridic acid 1-chloro-ethyl ester; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere 3.2: 4 h / Reflux; Inert atmosphere 4.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere 4.2: 16 h / 20 °C 5.1: water; tert-butyl alcohol / 20 °C 5.2: 58 h / 33 °C View Scheme |
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