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inquiry3-(2,6-Dichlorophenyl)-5-methylisoxazole-4-carbonyl chloride CAS:4462-55-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, s
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inquiryProduct Name: 3-(2,6-Dichlorophenyl)-5-methylisoxazole-4-carbonyl chloride Synonyms: 3-(2,6-DICHLOROPHENYL)-5-METHYLISOXAZOLE;3-(2,6-Dichlorophenyl)-5-methyl-4-isoxazolecarboxylic acid chloride;3-(2,6-Dichlorophenyl)-5-methylisoxazole-4-carboxyl
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inquiryProduct name: 3-(2,6-Dichlorophenyl)-5-Methyl-1,2-Oxazole-4-Carbonyl Chloride CAS No.: 4462-55-9 Molecule Formula:C11H6Cl3NO2 Molecule Weight:290.53 Purity: 99.0% Package: 25kg/drum Description:White to buff colored powder Manufacture
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inquiryProduct Name: 3-(2,6-Dichlorophenyl)-5-methylisoxazole-4-carbonyl chloride CAS No.: 4462-55-9 EINECS: 224-723-8 Molecular Formula: C11H6Cl3NO2 Molecular Weight: 290.53 Grade Standard: Pharmaceutical Intermediates Pu
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inquiry3-(2,6-dichloro-phenyl)-5-methyl-isoxazole-4-carboxylic acid
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
Conditions | Yield |
---|---|
With thionyl chloride; N,N-dimethyl-formamide at 60℃; | 94% |
With phosphorus pentachloride at 45℃; for 1h; | 84% |
With thionyl chloride |
2,6-dichlorobenzaldehyde
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: (i) NH2OH, (ii) Cl2, CHCl3, (iii) /BRN= 506727/, MeOH 2: aq. KOH / ethanol 3: SOCl2 View Scheme | |
Multi-step reaction with 5 steps 1.1: hydroxylamine sulfate / methanol / 0.5 h 1.2: 0.5 h / pH 8 - 9 / Reflux 2.1: chlorine / methanol / 0 - 5 °C 3.1: sodium hydroxide / methanol / 0.5 h / 0 - 5 °C / pH 10 3.2: 2 h / 0 - 20 °C / pH 9 4.1: water; sodium hydroxide / methanol / 1 h / pH 11 - 13 / Reflux 5.1: phosphorus pentachloride / 1 h / 45 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: hydroxylamine sulfate / methanol / 1 h / 20 - 40 °C 1.2: 24 h / 0 - 20 °C / pH ~ 9.5 / Inert atmosphere 1.3: pH ~ 7 - 7.5 2.1: phosphorus pentachloride / toluene View Scheme | |
Multi-step reaction with 5 steps 1: hydroxylamine hydrochloride; sodium hydroxide / water; ethanol / 0 - 90 °C 2: N-chloro-succinimide / N,N-dimethyl-formamide / 2 h / 20 °C 3: triethylamine / dichloromethane / 0 - 20 °C 4: lithium hydroxide monohydrate; water / ethanol / 50 °C 5: thionyl chloride; N,N-dimethyl-formamide / 60 °C View Scheme |
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. KOH / ethanol 2: SOCl2 View Scheme | |
Multi-step reaction with 2 steps 1: water; sodium hydroxide / methanol / 1 h / pH 11 - 13 / Reflux 2: phosphorus pentachloride / 1 h / 45 °C View Scheme | |
Multi-step reaction with 2 steps 1: sodium hydroxide / water; methanol / 3 h 2: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 40 °C View Scheme |
2,6-dichlorobenzohydroximoyl chloride
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: sodium hydroxide / methanol / 0.5 h / 0 - 5 °C / pH 10 1.2: 2 h / 0 - 20 °C / pH 9 2.1: water; sodium hydroxide / methanol / 1 h / pH 11 - 13 / Reflux 3.1: phosphorus pentachloride / 1 h / 45 °C View Scheme | |
Multi-step reaction with 3 steps 1: triethylamine / dichloromethane / 0 - 20 °C 2: lithium hydroxide monohydrate; water / ethanol / 50 °C 3: thionyl chloride; N,N-dimethyl-formamide / 60 °C View Scheme |
2,6-dichlorobenzaldoxime
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: chlorine / methanol / 0 - 5 °C 2.1: sodium hydroxide / methanol / 0.5 h / 0 - 5 °C / pH 10 2.2: 2 h / 0 - 20 °C / pH 9 3.1: water; sodium hydroxide / methanol / 1 h / pH 11 - 13 / Reflux 4.1: phosphorus pentachloride / 1 h / 45 °C View Scheme | |
Multi-step reaction with 4 steps 1: N-chloro-succinimide / N,N-dimethyl-formamide / 2 h / 20 °C 2: triethylamine / dichloromethane / 0 - 20 °C 3: lithium hydroxide monohydrate; water / ethanol / 50 °C 4: thionyl chloride; N,N-dimethyl-formamide / 60 °C View Scheme |
ethyl 3-(2,6-dichlorophenyl)-5-methyl-1,2-oxazole-4-carboxylate
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: lithium hydroxide monohydrate; water / ethanol / 50 °C 2: thionyl chloride; N,N-dimethyl-formamide / 60 °C View Scheme |
6-Aminopenicillanic Acid
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
sodium dicloxacillin
Conditions | Yield |
---|---|
Stage #1: 6-Aminopenicillanic Acid With sodium hydroxide In water at 0 - 5℃; for 0.333333h; Stage #2: 3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride In acetone at 5℃; for 1h; pH=7; Stage #3: With sodium 2-ethylhexanoic acid In isopropyl alcohol at 30℃; for 0.5h; Temperature; Solvent; | 80.21% |
With ammonium hydroxide In ethyl acetate pH=2 - 8; |
propargyl alcohol
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
prop-2-ynyl 3-(2,6-dichlorophenyl)-5-methylisoxazole-4-carboxylate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 2h; | 79% |
3,4-dihydro-6-t-butyl-2H-1,4-benzoxazine
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
Conditions | Yield |
---|---|
With potassium carbonate In toluene at 40℃; for 0.416667h; Microwave irradiation; | 70% |
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
3,4-dihydro-7-methyl-2H-1,4-benzoxazine
Conditions | Yield |
---|---|
With potassium carbonate In toluene at 40℃; for 0.416667h; Microwave irradiation; | 60% |
6-bromo-3, 4-dihydro-2H-benzo[β][1, 4]oxazine
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
Conditions | Yield |
---|---|
With potassium carbonate In toluene at 40℃; for 0.416667h; Microwave irradiation; | 55% |
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
6-chloro-3,4-dihydro-2H-benzo[b][1,4]oxazine
Conditions | Yield |
---|---|
With potassium carbonate In toluene at 40℃; for 0.416667h; Microwave irradiation; | 54% |
Conditions | Yield |
---|---|
With potassium carbonate In toluene at 40℃; for 0.416667h; Microwave irradiation; | 53% |
2-amino-6-ethylbenzo[d]thiazole
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane; N,N-dimethyl-formamide at 0 - 60℃; for 18.5h; Inert atmosphere; | 51% |
anthranilic acid allyl ester
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
2-{[3-(2,6-Dichloro-phenyl)-5-methyl-isoxazole-4-carbonyl]-amino}-benzoic acid allyl ester
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In tetrahydrofuran at 20℃; | 49% |
With sodium hydrogencarbonate In tetrahydrofuran; water at 20℃; |
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
(1R,3S,5S)-tert-butyl 3-hydroxy-8-azabicyclo[3.2.1]octane-8-carboxylate
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 0 - 30℃; | 41% |
2-amino-6-(methylsulfonyl)benzothiazole
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane; N,N-dimethyl-formamide at 40 - 45℃; for 24h; Inert atmosphere; | 37% |
Conditions | Yield |
---|---|
With crithmene; potassium ethyl xanthogenate; sodium phosphate In dichloromethane at 60℃; for 24h; Giese Free Radical Synthesis; Irradiation; | 35% |
9b-amino-4b-hydroxy-7-isopropyl-4b,9b-dihydro-10H-indeno[1,2-b]benzofuran-10-one
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
3-(2,6-dichlorophenyl)-N-(4b-hydroxy-7-isopropyl-10-oxo-9b,10-dihydro-4bH-benzo[d]indeno[1,2-b]furan-9b-yl)-5-methylisooxazole-4-carboxamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; | 19% |
3-methyl-6-nitro-1H-indazole
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
1-[3-(2,6-dichloro-phenyl)-5-methyl-isoxazole-4-carbonyl]-3-methyl-6-nitro-1H-indazole
Conditions | Yield |
---|---|
With triethylamine In benzene |
aniline
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
3-(2,6-dichloro-phenyl)-5-methyl-isoxazole-4-carboxylic acid anilide
Conditions | Yield |
---|---|
In acetone |
chlorhydrate de (β-aminoethyl)-4 benzenesulfonamide
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
3-(2,6-dichloro-phenyl)-5-methyl-isoxazole-4-carboxylic acid 4-sulfamoyl-phenethylamide
Conditions | Yield |
---|---|
In pyridine |
2,4-dichlorobenzamidoxime
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 25℃; for 24h; Acylation; |
(2R,3R)-3-amino-1-(1'-methoxycarbonyl-2'-methylpropenyl)-4-oxoazetidine-2-sulfonic acid tetrabutylammonium salt
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 2.16667h; Condensation; |
(2R,3S)-3-amino-1-(1'-methoxycarbonyl-2'-methylpropenyl)-4-oxoazetidine2-sulfonic acid
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 2.16667h; Condensation; |
dimethyl amine
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
3-(2,6-Dichlorophenyl)-N,N,5-trimethylisoxazole-4-carboxamide
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; |
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
2-{[3-(2,6-Dichloro-phenyl)-5-methyl-isoxazole-4-carbonyl]-amino }-benzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 49 percent / NaHCO3 / tetrahydrofuran / 20 °C 2: 100 percent / Pd(PPh3)4; morpholine / CH2Cl2 / 20 °C View Scheme |
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 49 percent / NaHCO3 / tetrahydrofuran / 20 °C 2: 100 percent / Pd(PPh3)4; morpholine / CH2Cl2 / 20 °C 3: TBTU; DIPEA / dimethylformamide / 20 °C View Scheme |
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 49 percent / NaHCO3 / tetrahydrofuran / 20 °C 2: 100 percent / Pd(PPh3)4; morpholine / CH2Cl2 / 20 °C 3: TBTU; DIPEA / dimethylformamide / 20 °C View Scheme |
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 49 percent / NaHCO3 / tetrahydrofuran / 20 °C 2: 100 percent / Pd(PPh3)4; morpholine / CH2Cl2 / 20 °C 3: TBTU; DIPEA / dimethylformamide / 20 °C View Scheme |
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 49 percent / NaHCO3 / tetrahydrofuran / 20 °C 2: 100 percent / Pd(PPh3)4; morpholine / CH2Cl2 / 20 °C 3: TBTU; DIPEA / dimethylformamide / 20 °C View Scheme |
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 49 percent / NaHCO3 / tetrahydrofuran / 20 °C 2: 100 percent / Pd(PPh3)4; morpholine / CH2Cl2 / 20 °C 3: TBTU; DIPEA / dimethylformamide / 20 °C View Scheme |
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
(4-{2-[3-(2,6-dichloro-phenyl)-5-methyl-isoxazole-4-carbonylamino]-ethyl}-benzenesulfonyl)-carbamic acid methyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: pyridine 2: 1,2-dimethoxy-ethane View Scheme |
3-(2,6-dichlorophenyl)-5-methyl-4-isoxazolylcarbonyl chloride
3-(2,6-dichloro-phenyl)-5-methyl-isoxazole-4-carboxylic acid 4-(azepan-1-ylcarbamoyl-sulfamoyl)-phenethylamide
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: pyridine 2: 1,2-dimethoxy-ethane 3: 1,2-dimethoxy-ethane View Scheme |
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