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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

3-Chloro-2-nitrobenzoic acid Manufacturer/High quality/Best price/In stock

Cas:4771-47-5

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 3-Chloro-2-Nitrobenzoic Acid

Cas:4771-47-5

Min.Order:1

Negotiable

Type:Other

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Large Stock 99.0% 3-Chloro-2-nitrobenzoic acid 4771-47-5 Producer

Cas:4771-47-5

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

inquiry

Enke Pharma-tech Co.,Ltd. (Cangzhou, China )

Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap

3-Chloro-2-nitrobenzoic acid

Cas:4771-47-5

Min.Order:1 Kilogram

FOB Price: $5.0

Type:Manufacturers

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COLORCOM LTD.

Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on

3-Chloro-2-Nitrobenzoic Acid

Cas:4771-47-5

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

3-Chloro-2-nitrobenzoic acid

Cas:4771-47-5

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Hebei yanxi chemical co.,LTD.

Hebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car

3-chloro-2-nitrobenzoic Acid

Cas:4771-47-5

Min.Order:1 Metric Ton

FOB Price: $1.0 / 2.0

Type:Trading Company

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Jinan Finer Chemical Co., Ltd

Product Description Product website: http://www.finerchem.com/pro01en/id/1171.html Product Name 3-Chloro-2-nitrobenzoic acid CAS No. 4771-4

3-Chloro-2-nitrobenzoic acid

Cas:4771-47-5

Min.Order:1 Gram

FOB Price: $11.0

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

Our advantage:Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scient

TIANFU-CHEM 3-Chloro-2-nitrobenzoic acid

Cas:4771-47-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 4771-47-5 with best quality

Cas:4771-47-5

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W

3-Chloro-2-nitrobenzoic acid CAS4771-47-5

Cas:4771-47-5

Min.Order:1 Kilogram

FOB Price: $289.0 / 499.0

Type:Trading Company

inquiry

Henan Sinotech Import&Export Corporation

3-Chloro-2-nitrobenzoic acid Basic information Product Name: 3-Chloro-2-nitrobenzoic acid Synonyms: Benzoic acid, 3-chloro-2-nitro-;3-CHLORO-2-NITROBENZOIC ACID 99%;3-Chloro-2-nitrobenzoic ac

3-Chloro-2-nitrobenzoic acid CAS: 4771-47-5

Cas:4771-47-5

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Benzoicacid, 3-chloro-2-nitro- 4771-47-5

Cas:4771-47-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

3-Chloro-2-nitrobenzoic acid CAS:4771-47-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organ

3-Chloro-2-nitrobenzoic acid CAS:4771-47-5

Cas:4771-47-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Benzoicacid, 3-chloro-2-nitro-

Cas:4771-47-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Mojin Biotechnology Co.,Ltd

Product quality: Our company have high quality product , and also the product we have good manufacture . First of all, this product is of fine quality. Every finish should be checked by quality inspection system.And every one should be also tried

high quality 3-Chloro-2-nitrobenzoic acid CAS: 4771-47-5

Cas:4771-47-5

Min.Order:1 Kilogram

FOB Price: $20.0 / 30.0

Type:Trading Company

inquiry

Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

3-Chloro-2-nitrobenzoic acid

Cas:4771-47-5

Min.Order:1 Kilogram

FOB Price: $40.0 / 50.0

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Benzoicacid, 3-chloro-2-nitro-

Cas:4771-47-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

3-Chloro-2-nitrobenzoic acid

Cas:4771-47-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

3-Chloro-2-nitrobenzoic acid

Cas:4771-47-5

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

3-Chloro-2-nitrobenzoic acid

Cas:4771-47-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

3-Chloro-2-nitrobenzoic acid

Cas:4771-47-5

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

3-Chloro-2-nitrobenzoic acid

Cas:4771-47-5

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediates Tr

Benzoicacid, 3-chloro-2-nitro-

Cas:4771-47-5

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Siwei Development Group Ltd.

Product name: 3-Chloro-2-Nitrobenzoic Acid CAS No.:4771-47-5 Molecule Formula:C7H3ClNO4 Molecule Weight:200.56 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS

High Quality 3-Chloro-2-Nitrobenzoic Acid on stock

Cas:4771-47-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

3-Chloro-2-nitrobenzoic acid

Cas:4771-47-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Minstar Chemical Co., Ltd

Product Name: 3-Chloro-2-nitrobenzoic acid Synonyms: 3-CHLORO-2-NITROBENZOIC ACID;3-chloro-2-nitrobenzoicacidt;3-CHOLORO-2-NITROBNZOIC ACID;2-NITRO-3-CHLOROBENZOICACID;3-chloro-2-nitrobenzoate;Benzoic acid, 3-chloro-2-nitro-;3-Chloro-2-nitroben

3-Chloro-2-nitrobenzoic acid 4771-47-5 C7H4ClNO4

Cas:4771-47-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

3-Chloro-2-nitrobenzoic acid

Cas:4771-47-5

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

3-Chloro-2-nitrobenzoic acid

Cas:4771-47-5

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

3-Chloro-2-nitrobenzoic acid

Cas:4771-47-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

2-amino-3-chlorobenzoic acid
6388-47-2

2-amino-3-chlorobenzoic acid

3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

Conditions
ConditionsYield
With sodium perborate; titanium(IV) hydroxide; acetic acid at 85 - 90℃; for 1h; Temperature; Inert atmosphere;84.9%
3-chloro-2-nitrotoluene
5367-26-0

3-chloro-2-nitrotoluene

3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

Conditions
ConditionsYield
With potassium permanganate; water; magnesium sulfate
With potassium permanganate; tetrabutylammomium bromide
3-chlorobenzoate
535-80-8

3-chlorobenzoate

A

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

B

3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

Conditions
ConditionsYield
With nitric acid
With nitric acid das Gemisch wird in Wasser von 50grad gegossen;
beim Nitrieren;
2-Nitroso-3-chlor-toluol
23082-43-1

2-Nitroso-3-chlor-toluol

3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

Conditions
ConditionsYield
With potassium dichromate
3-Chloro-2-nitroso-benzoic acid

3-Chloro-2-nitroso-benzoic acid

3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

Conditions
ConditionsYield
With nitric acid
nitric acid
7697-37-2

nitric acid

3-chlorobenzoate
535-80-8

3-chlorobenzoate

A

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

B

3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

3-chloro-2-nitrotoluene
5367-26-0

3-chloro-2-nitrotoluene

magnesium sulfate
7487-88-9

magnesium sulfate

KMnO4

KMnO4

3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

2,4-dinitrotoluene
121-14-2

2,4-dinitrotoluene

3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: acetic acid; sodium acetate / bei der elektrolytischen Reduktion
2: hydrochloric acid
3: Verkochen des Diazoniumsulfats mit Alkohol.Diazotization
4: KMnO4; water; MgSO4
View Scheme
2,6-dinitrotoluene
606-20-2

2,6-dinitrotoluene

3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: bei der elektrolytischen Reduktion
2: concentrated hydrochloric acid
3: sulfuric acid / Diazotization.Verkochen der Loesung mit Alkohol
4: KMnO4; water; MgSO4
View Scheme
4-hydroxylamino-2-nitrotoluene
43192-03-6

4-hydroxylamino-2-nitrotoluene

3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: hydrochloric acid
2: Verkochen des Diazoniumsulfats mit Alkohol.Diazotization
3: KMnO4; water; MgSO4
View Scheme
2-hydroxylamino-6-nitrotoluene
5805-95-8

2-hydroxylamino-6-nitrotoluene

3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: concentrated hydrochloric acid
2: sulfuric acid / Diazotization.Verkochen der Loesung mit Alkohol
3: KMnO4; water; MgSO4
View Scheme
2-chloro-4-methyl-3-nitro-aniline
39053-44-6

2-chloro-4-methyl-3-nitro-aniline

3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Verkochen des Diazoniumsulfats mit Alkohol.Diazotization
2: KMnO4; water; MgSO4
View Scheme
4-chloro-2-methyl-3-nitro-aniline
219312-08-0

4-chloro-2-methyl-3-nitro-aniline

3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sulfuric acid / Diazotization.Verkochen der Loesung mit Alkohol
2: KMnO4; water; MgSO4
View Scheme
2-chloro-6-methylaniline
87-63-8

2-chloro-6-methylaniline

3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: K2S2O8, H2SO4
2: aq. K2Cr2O7
View Scheme
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

3-hydroxy-2-nitrobenzoic acid
602-00-6

3-hydroxy-2-nitrobenzoic acid

Conditions
ConditionsYield
With potassium hydroxide; water for 12h; Heating / reflux;100%
With water; potassium hydroxide Reflux;100%
With potassium hydroxide In water at 110℃; for 12h;99%
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

3-chloro-2-nitrobenzamide
59772-47-3

3-chloro-2-nitrobenzamide

Conditions
ConditionsYield
Stage #1: 3-chloro-2-nitro-benzoic acid With thionyl chloride at 80℃; for 1h;
Stage #2: With ammonia In dichloromethane; water at 0℃; for 0.416667h;
100%
Multi-step reaction with 2 steps
1: 51.1 g / thionyl chloride / toluene / 3 h / Heating
2: 96 percent / 28percent aq. NH3 / 0.33 h
View Scheme
Multi-step reaction with 2 steps
1: PCl5 / benzene / 3 h / Heating
2: conc. NH4OH
View Scheme
Stage #1: 3-chloro-2-nitro-benzoic acid With thionyl chloride In toluene at 80℃; for 4h;
Stage #2: With ammonium hydroxide at 20℃; for 1h;
With thionyl chloride; aqueous NH3 In dichloromethane
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

3-chloro-2,6-dinitrobenzoic acid
150272-17-6

3-chloro-2,6-dinitrobenzoic acid

Conditions
ConditionsYield
With sulfuric acid; nitric acid at 20℃; for 2h; Heating / reflux;99%
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

methyl iodide
74-88-4

methyl iodide

3-chloro-2-nitro-benzoic acid methyl ester
42087-81-0

3-chloro-2-nitro-benzoic acid methyl ester

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 40℃; for 1h;99%
With potassium carbonate In acetone at 40℃; for 1h;99%
With potassium carbonate In N,N-dimethyl-formamide at 40℃; for 4.5h; Inert atmosphere;97%
With potassium carbonate In N,N-dimethyl-formamide at 40℃; for 1h;94%
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

3-chloro-2-nitro-benzoic acid methyl ester
42087-81-0

3-chloro-2-nitro-benzoic acid methyl ester

Conditions
ConditionsYield
In diethyl ether Inert atmosphere;99%
morpholine
110-91-8

morpholine

3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

3-morpholino-2-nitrobenzoic acid

3-morpholino-2-nitrobenzoic acid

Conditions
ConditionsYield
at 130℃; for 48h;98%
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

1-chloro-4-iodo-2-nitrobenzene
41252-95-3

1-chloro-4-iodo-2-nitrobenzene

Conditions
ConditionsYield
With copper(I) oxide; potassium phosphate; bismuth (III) nitrate pentahydrate; palladium(II) trifluoroacetate; oxygen; sodium iodide In dimethyl sulfoxide at 170℃; for 20h; Schlenk technique;96%
With copper(I) oxide; potassium phosphate; bismuth (III) nitrate pentahydrate; palladium(II) trifluoroacetate; oxygen; sodium iodide In dimethyl sulfoxide at 170℃; for 10h; Catalytic behavior; Schlenk technique; Green chemistry; regioselective reaction;93%
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

3-chloro-2-nitrobenzoyl chloride
19088-99-4

3-chloro-2-nitrobenzoyl chloride

Conditions
ConditionsYield
With thionyl chloride; N,N-dimethyl-formamide In dichloromethane for 2h; Reflux; Inert atmosphere;94%
With phosphorus pentachloride In benzene for 3h; Heating;
With thionyl chloride In toluene for 3h; Heating;51.1 g
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

dimethyl sulfate
77-78-1

dimethyl sulfate

3-chloro-2-nitro-benzoic acid methyl ester
42087-81-0

3-chloro-2-nitro-benzoic acid methyl ester

Conditions
ConditionsYield
With potassium carbonate In acetone for 0.5h; Esterification; Heating;89%
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

(3-chloro-2-nitrophenyl)methanol
77158-86-2

(3-chloro-2-nitrophenyl)methanol

Conditions
ConditionsYield
With diborane In tetrahydrofuran for 2h; Ambient temperature;88%
Multi-step reaction with 2 steps
1: thionyl chloride; DMF / tetrahydrofuran / Heating
2: sodium borohydride / dimethylformamide; tetrahydrofuran / 20 °C
View Scheme
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

2-amino-3-chlorobenzoic acid
6388-47-2

2-amino-3-chlorobenzoic acid

Conditions
ConditionsYield
With sodium tetrahydroborate; nickel dichloride In methanol; water for 1h; Ambient temperature;85%
With hydrogenchloride; tin72%
With ammonium hydroxide; sodium dithionite In water at 20℃; for 1h;70%
selenium
7782-49-2

selenium

iodobenzene
591-50-4

iodobenzene

3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

3-chloro-2-nitrophenyl phenyl selenoether

3-chloro-2-nitrophenyl phenyl selenoether

Conditions
ConditionsYield
With 1,10-Phenanthroline; oxygen; copper diacetate; potassium carbonate In toluene at 100℃; for 24h;80%
diphenyl diselenide
1666-13-3

diphenyl diselenide

3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

3-chloro-2-nitrophenyl phenyl selenoether

3-chloro-2-nitrophenyl phenyl selenoether

Conditions
ConditionsYield
With 1,10-Phenanthroline; oxygen; copper diacetate; potassium carbonate In toluene at 150℃; for 24h;80%
With 1,10-Phenanthroline; oxygen; copper diacetate; potassium carbonate In toluene at 150℃; under 760.051 Torr; for 24h; Schlenk technique; Sealed tube;67%
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

diazomethyl-trimethyl-silane
18107-18-1

diazomethyl-trimethyl-silane

3-chloro-2-nitro-benzoic acid methyl ester
42087-81-0

3-chloro-2-nitro-benzoic acid methyl ester

Conditions
ConditionsYield
In methanol; hexanes; acetonitrile at 0℃; for 0.5h;74%
In methanol; hexanes; acetonitrile at 0℃; for 0.5h;74%
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

phenylacetylene
536-74-3

phenylacetylene

A

1,4-diphenyl-1,3-butadiyne
886-66-8

1,4-diphenyl-1,3-butadiyne

B

1-chloro-2-nitro-3-(phenylethynyl)benzene

1-chloro-2-nitro-3-(phenylethynyl)benzene

Conditions
ConditionsYield
With 1,10-Phenanthroline; oxygen; sodium hydrogencarbonate; copper(II) sulfate In N,N-dimethyl-formamide; toluene at 150℃; for 24h; Molecular sieve; Schlenk technique;A 65%
B 63%
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

1-hydroxy-1H-benzo[d][1,2,3]triazole-7-carboxylic acid

1-hydroxy-1H-benzo[d][1,2,3]triazole-7-carboxylic acid

Conditions
ConditionsYield
With hydrazine hydrate In ethanol for 18h; Heating;62%
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

1-chloro-2-nitro-3-tosylbenzene
873970-95-7

1-chloro-2-nitro-3-tosylbenzene

Conditions
ConditionsYield
With 1,10-Phenanthroline; silver carbonate at 160℃; for 18h; Schlenk technique; Sealed tube;62%
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

2-amino-3-hydrothiobenzoic acid

2-amino-3-hydrothiobenzoic acid

Conditions
ConditionsYield
With sodiumsulfide nonahydrate In water Reflux;59%
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

2-6-dimethoxybenzoic acid
1466-76-8

2-6-dimethoxybenzoic acid

A

3-chloro-2',6'-dimethoxy-2-nitro-1,1'-biphenyl
1352638-56-2

3-chloro-2',6'-dimethoxy-2-nitro-1,1'-biphenyl

B

C12H6Cl2N2O4
1352638-64-2

C12H6Cl2N2O4

Conditions
ConditionsYield
With triphenylphosphine; silver carbonate; palladium dichloride In dimethyl sulfoxide at 130℃; for 6h; Inert atmosphere;A 57%
B 22%
3,5-dimethylphenyl iodide
22445-41-6

3,5-dimethylphenyl iodide

3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

4-chloro-3-nitro-3',5'-dimethyl-1,1'-biphenyl
1344681-48-6

4-chloro-3-nitro-3',5'-dimethyl-1,1'-biphenyl

Conditions
ConditionsYield
Stage #1: 3,5-dimethylphenyl iodide; 3-chloro-2-nitro-benzoic acid With palladium diacetate; acetic acid; silver carbonate at 130℃; for 16h;
Stage #2: With silver carbonate In dimethyl sulfoxide at 130℃; for 3h; regioselective reaction;
56%
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

thiophenol
108-98-5

thiophenol

(3-chloro-2-nitrophenyl)(phenyl)sulfane

(3-chloro-2-nitrophenyl)(phenyl)sulfane

Conditions
ConditionsYield
With copper(l) iodide; 1,10-Phenanthroline; oxygen; potassium carbonate In dimethyl sulfoxide at 140℃; for 24h; Molecular sieve;56%
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

4-bromo-1-chloro-2-nitrobenzene
16588-24-2

4-bromo-1-chloro-2-nitrobenzene

Conditions
ConditionsYield
With copper(I) oxide; potassium phosphate; tetrakis(triphenylphosphine) palladium(0); bismuth (III) nitrate pentahydrate; oxygen; sodium bromide In dimethyl sulfoxide at 170℃; for 10h; Schlenk technique; Green chemistry; regioselective reaction;56%
oxalyl dichloride
79-37-8

oxalyl dichloride

N-(5-amino-2-methylphenyl)-4-diethylaminomethylbenzamide
250681-65-3

N-(5-amino-2-methylphenyl)-4-diethylaminomethylbenzamide

N-[2-methyl-5-(3-morpholino-2-nitrobenzamido)phenyl]-4-diethylaminomethylbenzamide
250682-02-1

N-[2-methyl-5-(3-morpholino-2-nitrobenzamido)phenyl]-4-diethylaminomethylbenzamide

3-chloro-2-nitrobenzoyl chloride
19088-99-4

3-chloro-2-nitrobenzoyl chloride

3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

N-[5-(3-chloro-2-nitrobenzamido)-2-methylphenyl]-4-diethylaminomethylbenzamide
1431463-84-1

N-[5-(3-chloro-2-nitrobenzamido)-2-methylphenyl]-4-diethylaminomethylbenzamide

Conditions
ConditionsYield
55%
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

3-chloro-2-nitro-aniline
59483-54-4

3-chloro-2-nitro-aniline

Conditions
ConditionsYield
With diphenyl phosphoryl azide; triethylamine In N,N-dimethyl-formamide at 20℃; for 3h;53.4%
(i) NaN3, SO3/H2SO4, (ii) H2O; Multistep reaction;
Multi-step reaction with 4 steps
1: SOCl2 / 3 h / Heating
2: NaN3 / acetone; H2O / 0.5 h / Ambient temperature
3: benzene / Heating
4: 5 N aq. NaOH / benzene / 1 h / Ambient temperature
View Scheme
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

ethyl 1,2,3,4-tetrahydro-β-carboline-3-carboxylate
84518-77-4

ethyl 1,2,3,4-tetrahydro-β-carboline-3-carboxylate

A

2-Cyclohexyl-1-[(E)-cyclohexylimino]-1,2,3a,4,9,10-hexahydro-2,9,10a-triaza-cyclopenta[b]fluoren-3-one
130472-83-2

2-Cyclohexyl-1-[(E)-cyclohexylimino]-1,2,3a,4,9,10-hexahydro-2,9,10a-triaza-cyclopenta[b]fluoren-3-one

B

2-(3-Chloro-2-nitro-benzoyl)-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid ethyl ester
130472-82-1

2-(3-Chloro-2-nitro-benzoyl)-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid ethyl ester

Conditions
ConditionsYield
With dicyclohexyl-carbodiimide In dichloromethane for 3h; Ambient temperature;A 20%
B 51%
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

methyl(([1,2,4]triazolo-[4,3-a]pyridin-3-yl)methyl)amine hydrochloride

methyl(([1,2,4]triazolo-[4,3-a]pyridin-3-yl)methyl)amine hydrochloride

3-chloro-N-methyl-2-nitro-N-(([1,2,4]triazolo[4,3-a]pyridin-3-yl)methyl)benzamide

3-chloro-N-methyl-2-nitro-N-(([1,2,4]triazolo[4,3-a]pyridin-3-yl)methyl)benzamide

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 2h;40%
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

1-(4-fluorophenylmethyl)piperazine
70931-28-1

1-(4-fluorophenylmethyl)piperazine

1-[4-(4-fluorobenzyl)piperazin-1-yl]-(3-chloro-2-nitrophenyl)methanone

1-[4-(4-fluorobenzyl)piperazin-1-yl]-(3-chloro-2-nitrophenyl)methanone

Conditions
ConditionsYield
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine In N,N-dimethyl-formamide at 50℃; for 0.166667h; Microwave irradiation;34%
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

phenylmagnesium bromide
100-58-3

phenylmagnesium bromide

(3-chloro-2-nitrophenyl)(phenyl)methanone
78940-48-4

(3-chloro-2-nitrophenyl)(phenyl)methanone

Conditions
ConditionsYield
Stage #1: 3-chloro-2-nitro-benzoic acid With thionyl chloride at 80℃; for 2h;
Stage #2: phenylmagnesium bromide In tetrahydrofuran at -15 - 20℃;
31%
3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

methylamine
74-89-5

methylamine

3-(methylamino)-2-nitrobenzoic acid
124341-37-3

3-(methylamino)-2-nitrobenzoic acid

Conditions
ConditionsYield
In water at 100℃; for 96h;26%
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