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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

5-Chloro-2-nitrobenzoic acid Manufacturer/High quality/Best price/In stock

Cas:2516-95-2

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Wuhan Fortuna Chemical Co.,Ltd

Manufacturer supply 5-Chloro-2-nitrobenzoic acid CAS 2516-95-2 with good quality Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates

Manufacturer supply 5-Chloro-2-nitrobenzoic acid CAS 2516-95-2 with good quality

Cas:2516-95-2

Min.Order:10 Kilogram

FOB Price: $10.0

Type:Trading Company

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 5-chloro-2-nitrobenzoic acid

Cas:2516-95-2

Min.Order:1

Negotiable

Type:Other

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COLORCOM LTD.

Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on

5-Chloro-2-Nitrobenzoic Acid

Cas:2516-95-2

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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ANQING CHICO PHARMACEUTICAL CO.,LTD.

High quality. Factory supply. In stock. Best price.1.Quick response within 24 hours;2.Best quality in your requirement;?3.We pay more attention on delivery time, and usually ship on time;4.Under the premise of safety and effectiveness, we can produce

5-Chloro-2-nitrobenzoic acid

Cas:2516-95-2

Min.Order:0

Negotiable

Type:Trading Company

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

5-Chloro-2-nitrobenzoic acid

Cas:2516-95-2

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Hebei yanxi chemical co.,LTD.

Hebei yanxi chemical co. LTD. has expanded a compositive entity from initially only as a small manufacturer. The company dedicated to the development, production and marketing of chemicals. After many years of efforts, we have established stable

5-Chloro-2-nitrobenzoic acid

Cas:2516-95-2

Min.Order:1 Metric Ton

FOB Price: $1.0 / 2.0

Type:Trading Company

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Henan Tianfu Chemical Co., Ltd.

5-Chloro-2-nitrobenzoic acid Basic information Product Name: 5-Chloro-2-nitrobenzoic acid Synonyms: RARECHEM AL BO 1106;TIMTEC-BB SBB009922;5-chloro-2-nitro-benzoicaci;Benzoic acid, 5-ch

TIANFU-CHEM CAS:2516-95-2 5-Chloro-2-nitrobenzoic acid

Cas:2516-95-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

5-Chloro-2-nitrobenzoic acid

Cas:2516-95-2

Min.Order:1 Kilogram

FOB Price: $3.0 / 10.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 2516-95-2 with best quality

Cas:2516-95-2

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

5-Chloro-2-nitrobenzoic acid 2516-95-2

Cas:2516-95-2

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Product Name 5-Chloro-2-nitrobenzoic acid Synonyms 5-Chloro-2-nitrobenzoic acid;2-Nitro-5-chlorobenzoic acid CAS: 2516-95-2 MF: - MW: -

2-Nitro-5-Chlorobenzoic acid

Cas:2516-95-2

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

5-Chloro-2-nitrobenzoic acid 2516-95-2

Cas:2516-95-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Shanghai Minstar Chemical Co., Ltd

Product Name: 5-Chloro-2-nitrobenzoic acid CAS: 2516-95-2 MF: C7H4ClNO4 MW: 201.56 EINECS: 219-738-1 Mol File: 2516-95-2.mol 5-Chloro-2-nitrobenzoic acid Structure 5-Chloro-2-nitrobenzoic acid Chemical Properties Melting point

5-chloro-2-nitrobenzoic acid

Cas:2516-95-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Qingdao Beluga Import and Export Co., LTD

5-Chloro-2-nitrobenzoic acid CAS:2516-95-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organ

5-Chloro-2-nitrobenzoic acid CAS:2516-95-2

Cas:2516-95-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

5-Chloro-2-nitrobenzoic acid

Cas:2516-95-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:2516-95-2

Cas:2516-95-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hebei Mojin Biotechnology Co.,Ltd

Hebei Mojin Biotechnology Co., Ltd, Our company is a professional in chemical raw materials and chemical reagents research and development production enterprises. Our business covers more than 30 countries, most of the big customers come from Europe,

5-Chloro-2-nitrobenzoic acid cas 2516-95-2 2-nitro-5-chlorobenzoic acid

Cas:2516-95-2

Min.Order:1 Kilogram

FOB Price: $80.0 / 100.0

Type:Trading Company

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Shanghai Terui OP New Material Technology Co., Ltd.

We have overseas warehouses in California, Nuevo Laredo, Mexico, Vancouver, Canada, Amsterdam, The Netherlands and Melbourne, Australia. Overseas warehouses can provide some of the best selling products. We look forward to cooperating with strong loc

High purity 5-Chloro-2-nitrobenzoic acid cas 2516-95-2 DDP

Cas:2516-95-2

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

5-Chloro-2-Nitrobenzoic Acid

Cas:2516-95-2

Min.Order:0

Negotiable

Type:Manufacturers

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Triumph International Development Limilted

Lorcaserin(856681-05-5)is an orally administered agent and a selective 5-HT2C receptor agonist for the treatment of obesity. It had been approved for marketing in US by FDA on 27 June in 2012. In clinical studies, lorcaserin h

5-Chloro-2-nitrobenzoic acid ? ? 2516-95-2

Cas:2516-95-2

Min.Order:100 Metric Ton

Negotiable

Type:Lab/Research institutions

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

5-Chloro-2-nitrobenzoic acid

Cas:2516-95-2

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

5-Chloro-2-nitrobenzoic acid

Cas:2516-95-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

5-Chloro-2-nitrobenzoic acid

Cas:2516-95-2

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

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Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

5-Chloro-2-nitrobenzoic acid

Cas:2516-95-2

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 5-Chloro-2-Nitrobenzoic Acid

Cas:2516-95-2

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

5-Chloro-2-nitrobenzoic acid

Cas:2516-95-2

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

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HANGZHOU YUNUO CHEMICAL CO.,LTD

superior quality moderate price & quick delivery Appearance:light yellow to yellowish-green crystalline powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your req

5-Chloro-2-nitrobenzoic acid

Cas:2516-95-2

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Siwei Development Group Ltd.

Product name: 5-Chloro-2-Nitrobenzoic Acid CAS No.:2516-95-2 Molecule Formula:C7H4ClNO4 Molecule Weight:201.56 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS

High Quality 5-Chloro-2-Nitrobenzoic Acid on stock

Cas:2516-95-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

5-Chloro-2-nitrobenzoic acid

Cas:2516-95-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

5-chloro-2-nitrobenzyl alcohol
73033-58-6

5-chloro-2-nitrobenzyl alcohol

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

Conditions
ConditionsYield
With Iron(III) nitrate nonahydrate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium chloride; oxygen In 1,2-dichloro-ethane at 25℃; for 48h; Schlenk technique;87%
5-chloro-2-nitrobenzyl alcohol
73033-58-6

5-chloro-2-nitrobenzyl alcohol

A

5-chloro-2-nitrobenzaldehyde
6628-86-0

5-chloro-2-nitrobenzaldehyde

B

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

Conditions
ConditionsYield
With Iron(III) nitrate nonahydrate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium chloride; oxygen In 1,2-dichloro-ethane at 25℃; for 48h; Schlenk technique;A 22%
B 60%
5-chloro-2-nitrobenzaldehyde
6628-86-0

5-chloro-2-nitrobenzaldehyde

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

Conditions
ConditionsYield
With potassium permanganate
5-chloro-2-nitrotoluene
5367-28-2

5-chloro-2-nitrotoluene

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

Conditions
ConditionsYield
With potassium permanganate
With potassium permanganate; tetrabutylammomium bromide
3-chlorobenzoate
535-80-8

3-chlorobenzoate

A

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

B

3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

Conditions
ConditionsYield
With nitric acid
With nitric acid das Gemisch wird in Wasser von 50grad gegossen;
beim Nitrieren;
ethyl 2-(5-chloro-2-nitrophenyl)-2-cyanoacetate
62567-91-3

ethyl 2-(5-chloro-2-nitrophenyl)-2-cyanoacetate

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

Conditions
ConditionsYield
With potassium permanganate; potassium carbonate
diethyl 2-(5-chloro-2-nitrophenyl)propanedioate
62567-90-2

diethyl 2-(5-chloro-2-nitrophenyl)propanedioate

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

Conditions
ConditionsYield
With potassium permanganate; potassium carbonate
nitric acid
7697-37-2

nitric acid

3-chlorobenzoate
535-80-8

3-chlorobenzoate

A

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

B

3-chloro-2-nitro-benzoic acid
4771-47-5

3-chloro-2-nitro-benzoic acid

5-chloro-2-nitrotoluene
5367-28-2

5-chloro-2-nitrotoluene

neutral potassium permanganate solution

neutral potassium permanganate solution

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

2,4-dinitrotoluene
121-14-2

2,4-dinitrotoluene

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: acetic acid; sodium acetate / bei der elektrolytischen Reduktion
2: hydrochloric acid
3: Verkochen des Diazoniumsulfatsmit Alkohol.Diazotization
4: potassium permanganate
View Scheme
4-hydroxylamino-2-nitrotoluene
43192-03-6

4-hydroxylamino-2-nitrotoluene

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: hydrochloric acid
2: Verkochen des Diazoniumsulfatsmit Alkohol.Diazotization
3: potassium permanganate
View Scheme
2-chloro-4-methyl-5-nitro-aniline

2-chloro-4-methyl-5-nitro-aniline

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Verkochen des Diazoniumsulfatsmit Alkohol.Diazotization
2: potassium permanganate
View Scheme
2,4-dichloronitrobenzene
611-06-3

2,4-dichloronitrobenzene

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: (i) NaOEt, DMSO, (ii) /BRN= 1451655/
2: KMnO4, aq. K2CO3
View Scheme
Multi-step reaction with 2 steps
1: (i) NaOEt, DMSO, (ii) /BRN= 1451655/
2: KMnO4, aq. K2CO3
View Scheme
3-chlorobenzoate
535-80-8

3-chlorobenzoate

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

Conditions
ConditionsYield
With sulfuric acid; nitric acid at -5 - 0℃; for 1h;
With nitric acid; acetic anhydride at 20℃;
5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

5-chloro-2-nitrobenzoyl chloride
41994-44-9

5-chloro-2-nitrobenzoyl chloride

Conditions
ConditionsYield
With thionyl chloride100%
With thionyl chloride Heating / reflux;98%
With thionyl chloride In dichloromethane for 4h; Reflux;66%
5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

5-chloroanthranilic acid
635-21-2

5-chloroanthranilic acid

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal In methanol under 735.5 Torr; for 2h; Ambient temperature;100%
With hydrogen; nickel In ethanol at 20℃;96%
Reduction;85%
5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

5-chloro-2-nitrobenzyl alcohol
73033-58-6

5-chloro-2-nitrobenzyl alcohol

Conditions
ConditionsYield
With dimethylsulfide borane complex In tetrahydrofuran at 80℃; for 3h; Inert atmosphere;100%
With borane-THF In tetrahydrofuran at 50℃; for 96h;91%
With dimethylsulfide borane complex In tetrahydrofuran at 80℃; for 3h; Inert atmosphere;90%
5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

anthranilic acid
118-92-3

anthranilic acid

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal In methanol under 735.5 Torr; for 80h;100%
5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

dimethyl sulfate
77-78-1

dimethyl sulfate

methyl 5-chloro-2-nitrobenzoate
51282-49-6

methyl 5-chloro-2-nitrobenzoate

Conditions
ConditionsYield
With potassium carbonate In acetone for 0.5h; Esterification; Heating;100%
With sodium carbonate In acetone for 3h; Heating;78%
With potassium carbonate In acetone Reflux;
With potassium carbonate In [(2)H6]acetone for 0.5h; Reflux;534 g
morpholine
110-91-8

morpholine

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

2-nitro-5-(morpholin-4-yl)benzoic acid
153437-51-5

2-nitro-5-(morpholin-4-yl)benzoic acid

Conditions
ConditionsYield
Stage #1: morpholine; 5-chloro-2-nitrobenzoic acid at 110℃; for 2h; Neat (no solvent);
Stage #2: pH=Ca. 3; Acidic aq. solution;
100%
at 120℃; for 6h;
5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

dimethyl amine
124-40-3

dimethyl amine

5-dimethylamino-2-nitrobenzoic acid
62876-66-8

5-dimethylamino-2-nitrobenzoic acid

Conditions
ConditionsYield
In water at 60℃; for 23h;99%
In water at 0 - 60℃; for 23h;99%
In water at 70℃; for 25h; Autoclave;99%
In water at 100℃; for 6h;
5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

5-hydroxy-2-nitrobenzoic acid
610-37-7

5-hydroxy-2-nitrobenzoic acid

Conditions
ConditionsYield
With sodium hydroxide for 72h; Inert atmosphere; Reflux;99%
With sodium hydroxide In water for 72h; Inert atmosphere;96.5%
With potassium hydroxide In water for 24h; Reflux;90%
methanol
67-56-1

methanol

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

methyl 5-chloro-2-nitrobenzoate
51282-49-6

methyl 5-chloro-2-nitrobenzoate

Conditions
ConditionsYield
With thionyl chloride at 80℃; for 4h; Cooling with ice; Reflux;98.2%
With thionyl chloride at 0℃; for 15h; Heating / reflux;92%
With sulfuric acid for 20h; Reflux; Inert atmosphere;89%
ethanol
64-17-5

ethanol

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

ethyl-5-chloro-2-nitrobenzoate
51282-56-5

ethyl-5-chloro-2-nitrobenzoate

Conditions
ConditionsYield
With thionyl chloride at 0℃; for 48h; Heating / reflux;97%
With sulfuric acid for 24h; Reflux;85%
pyrrolidine
123-75-1

pyrrolidine

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

2-nitro-5-(pyrrolidin-1-yl)benzoic acid

2-nitro-5-(pyrrolidin-1-yl)benzoic acid

Conditions
ConditionsYield
Stage #1: pyrrolidine; 5-chloro-2-nitrobenzoic acid at 110℃; for 2h; Neat (no solvent);
Stage #2: pH=Ca. 3; Acidic aq. solution;
95.66%
piperidine
110-89-4

piperidine

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

2-nitro-5-(piperidin-N-yl)-benzoic acid
118159-39-0

2-nitro-5-(piperidin-N-yl)-benzoic acid

Conditions
ConditionsYield
Stage #1: piperidine; 5-chloro-2-nitrobenzoic acid at 110℃; for 2h; Neat (no solvent);
Stage #2: pH=Ca. 3; Acidic aq. solution;
95.04%
5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

4-chloro-2-deuteronitrobenzene

4-chloro-2-deuteronitrobenzene

Conditions
ConditionsYield
With water-d2; silver carbonate In dimethyl sulfoxide at 120℃; for 16h;95%
5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

5-dimethylamino-2-nitrobenzoic acid
62876-66-8

5-dimethylamino-2-nitrobenzoic acid

Conditions
ConditionsYield
With dimethyl amine In water at 80℃; for 4h;94%
5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

2,4-dichloronitrobenzene
611-06-3

2,4-dichloronitrobenzene

Conditions
ConditionsYield
With copper(l) iodide; oxygen; copper(l) chloride In dimethyl sulfoxide at 160℃; under 760.051 Torr; for 30h; Schlenk technique; Sealed tube;93%
With oxygen; silver carbonate; potassium hydroxide; copper dichloride In dimethyl sulfoxide; N,N-dimethyl-formamide at 130 - 140℃;80%
With 2.9-dimethyl-1,10-phenanthroline; oxygen; copper (I) acetate; silver sulfate; sodium chloride In dimethyl sulfoxide at 160℃; for 24h; Schlenk technique;66%
With 2.9-dimethyl-1,10-phenanthroline; oxygen; copper diacetate; silver sulfate; sodium chloride In dimethyl sulfoxide at 160℃; under 760.051 Torr; for 20h; Schlenk technique;64%
5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

methyl iodide
74-88-4

methyl iodide

methyl 5-chloro-2-nitrobenzoate
51282-49-6

methyl 5-chloro-2-nitrobenzoate

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 40℃; for 1h;92%
With potassium carbonate In N,N-dimethyl-formamide at 0 - 40℃; for 1h;92%
5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

1-iodo-5-chloro-2-nitrobenzene
160938-18-1

1-iodo-5-chloro-2-nitrobenzene

Conditions
ConditionsYield
With copper(l) iodide; oxygen In dimethyl sulfoxide at 160℃; under 760.051 Torr; for 30h; Schlenk technique; Sealed tube;92%
With 2.9-dimethyl-1,10-phenanthroline; oxygen; copper diacetate; silver sulfate; sodium iodide In dimethyl sulfoxide at 160℃; under 760.051 Torr; for 20h; Schlenk technique;76%
iodobenzene
591-50-4

iodobenzene

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

5-chloro-2-nitro-1,1'-biphenyl
29547-09-9

5-chloro-2-nitro-1,1'-biphenyl

Conditions
ConditionsYield
With triphenylphosphine; silver carbonate; palladium dichloride In dimethyl sulfoxide; N,N-dimethyl-formamide at 130℃; for 30h; Inert atmosphere;92%
5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

A

5-chloro-2-nitrobenzyl alcohol
73033-58-6

5-chloro-2-nitrobenzyl alcohol

B

5-(piperidin-1-yl)-2-nitrobenzaldehyde
113259-79-3

5-(piperidin-1-yl)-2-nitrobenzaldehyde

Conditions
ConditionsYield
With hydrogenchloride In tetrahydrofuranA 91%
B n/a
5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

dimethyl sulfate
77-78-1

dimethyl sulfate

5-methylthio-2-nitrobenzoic acid
68701-32-6

5-methylthio-2-nitrobenzoic acid

Conditions
ConditionsYield
Stage #1: 5-chloro-2-nitrobenzoic acid With sodium sulfide nonahydrate; sodium hydroxide In water at 60℃; for 2.5h;
Stage #2: dimethyl sulfate at 100℃; for 1h;
90%
With sodium sulfide; sodium hydroxide 1) water, 50-55 deg C, 2,5 h 2) reflux 1 h; Yield given. Multistep reaction;
Stage #1: 5-chloro-2-nitrobenzoic acid With sodium sulfide; sodium hydroxide at 60℃;
Stage #2: dimethyl sulfate Heating;
Stage #1: 5-chloro-2-nitrobenzoic acid With sodium sulfide; sodium hydroxide In water at 60℃; for 2.5h;
Stage #2: dimethyl sulfate With sodium hydroxide In water for 1h; Heating / reflux;
Stage #3: With hydrogenchloride In water
5-chloro-2-pyridylamine
1072-98-6

5-chloro-2-pyridylamine

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

N-(5-chloropyridin-2-yl)-5-chloro-2-nitrobenzamide
280771-82-6

N-(5-chloropyridin-2-yl)-5-chloro-2-nitrobenzamide

Conditions
ConditionsYield
With pyridine; trichlorophosphate In acetonitrile at 0 - 30℃; for 1h; Inert atmosphere;90%
With pyridine; trichlorophosphate at 20℃; for 0.0833333h;
5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

4-chlorobenzonitrile
100-00-5

4-chlorobenzonitrile

Conditions
ConditionsYield
With copper(l) iodide; triethylamine In dimethyl sulfoxide at 120℃; under 760.051 Torr; for 20h; Inert atmosphere; Schlenk technique;88%
With 2.9-dimethyl-1,10-phenanthroline; oxygen; copper (I) acetate; silver sulfate; sodium iodide In dimethyl sulfoxide at 160℃; for 24h; Schlenk technique;76%
With copper(I) oxide at 120℃; for 24h; Ionic liquid;
5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

1,1'-carbonyldiimidazole
530-62-1

1,1'-carbonyldiimidazole

C10H6ClN3O3

C10H6ClN3O3

Conditions
ConditionsYield
In tetrahydrofuran for 1h; Reflux;86%
5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

5,5'-dichloro-2,2'-dinitro-1,1'-biphenyl
19036-42-1

5,5'-dichloro-2,2'-dinitro-1,1'-biphenyl

Conditions
ConditionsYield
With triphenylphosphine; silver carbonate; palladium dichloride In dimethyl sulfoxide at 130℃; for 6h; Inert atmosphere;85%
With copper(l) iodide In dimethyl sulfoxide at 140℃; for 20h; Inert atmosphere; Molecular sieve;72%
morpholine
110-91-8

morpholine

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

N-<5-chloro-2-nitrobenzoyl>morpholide
142439-67-6

N-<5-chloro-2-nitrobenzoyl>morpholide

Conditions
ConditionsYield
In thionyl chloride; acetone84%
In acetone at 0℃; for 0.25h;
Cyclohexyl isocyanide
931-53-3

Cyclohexyl isocyanide

phenylglyoxal hydrate
1074-12-0

phenylglyoxal hydrate

5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

3-bromopropylamine hydrochloride
5003-71-4

3-bromopropylamine hydrochloride

2-benzoyl-1-(5-chloro-2-nitrobenzoyl)-N-cyclohexylpyrrolidine-2-carboxamide

2-benzoyl-1-(5-chloro-2-nitrobenzoyl)-N-cyclohexylpyrrolidine-2-carboxamide

Conditions
ConditionsYield
Stage #1: Cyclohexyl isocyanide; phenylglyoxal hydrate; 5-chloro-2-nitrobenzoic acid; 3-bromopropylamine hydrochloride With sodium hydroxide In methanol at 20℃; for 24h;
Stage #2: With caesium carbonate In methanol at 20℃; for 1h;
84%
5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

potassium 5-chloro-2-nitrobenzoate

potassium 5-chloro-2-nitrobenzoate

Conditions
ConditionsYield
With potassium tert-butylate In ethanol at 20℃;83%
5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

2,6-difluorobenzoic acid
385-00-2

2,6-difluorobenzoic acid

A

2,2',6,6'-tetrafluoro-1,1'-biphenyl
781-16-8

2,2',6,6'-tetrafluoro-1,1'-biphenyl

B

5-chloro-2',6'-difluoro-2-nitro-1,1'-biphenyl
1352638-58-4

5-chloro-2',6'-difluoro-2-nitro-1,1'-biphenyl

C

5,5'-dichloro-2,2'-dinitro-1,1'-biphenyl
19036-42-1

5,5'-dichloro-2,2'-dinitro-1,1'-biphenyl

Conditions
ConditionsYield
With triphenylphosphine; silver carbonate; palladium dichloride In dimethyl sulfoxide at 130℃; for 6h; Inert atmosphere;A 11 %Chromat.
B 79%
C 21%
5-chloro-2-nitrobenzoic acid
2516-95-2

5-chloro-2-nitrobenzoic acid

3-Amino-5-chloro-2-nitrobenzoic acid
193481-78-6

3-Amino-5-chloro-2-nitrobenzoic acid

Conditions
ConditionsYield
With O-Methylhydroxylamin; potassium tert-butylate; copper diacetate In 1,2-dimethoxyethane at 20℃; Substitution; Amination;78%
With potassium tert-butylate; N-methoxylamine hydrochloride; copper diacetate In N,N-dimethyl-formamide at 0℃; for 3h;60.5%
With potassium tert-butylate; N-methoxylamine hydrochloride; copper diacetate In N,N-dimethyl-formamide for 3h;32%

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