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inquiryProduct Description Product website: http://www.finerchem.com Product Name 2-Chloro-5-nitrobenzoic acid CAS No.
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inquiry2-Chloro-5-nitrobenzoic acid Basic information Product Name: 2-Chloro-5-nitrobenzoic acid Synonyms: RARECHEM AL BO 0234;2-CHLORO-5-NITROBENZOIC ACID;5-NITRO-2-CHLOROBENZOIC ACID;LABOTEST
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
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inquiry2-Chloro-5-nitrobenzoic acid Molecular formula: C7H4ClNO4 CAS NO.: 2516-96-3 Appearance: Light yellow crystalline powder Content: 99%-101% Appearance:Light yellow crystalline powder Storage:Store
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inquiry2-Chloro-5-nitrobenzoic acid CAS:2516-96-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality orga
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Min.Order:1 Gram
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryProduct name: 2-Chloro-5-Nitrobenzoic Acid CAS No.:2516-96-3 Molecule Formula:C7H3ClNO4 Molecule Weight:200.56 Purity: 99.0% Package: 25kg/drum Description:Light yellow powder Manufacture Standards:Enterprise Standard
Cas:2516-96-3
Min.Order:1 Kilogram
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inquiryProduct Name: 2-Chloro-5-nitrobenzoic acid Synonyms: RARECHEM AL BO 0234;2-CHLORO-5-NITROBENZOIC ACID;LABOTEST-BB LT00847209;2-chloro-5-nitro-benzoicaci;6-Chloro-3-nitrobenzoic acid;Benzoic acid, 2-chloro-5-nitro-;5-NITRO-2-CHLOROBENZOIC ACID;2
Cas:2516-96-3
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
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inquiryGOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
Superior quality, moderate price & quick delivery. Appearance:light yellow to light yellow-green crystalline Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:as per your request Application:Used as Pharmaceutic
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inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiryStock products, own laboratoryAppearance:Off-white to light yellow crystal powde Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiryConditions | Yield |
---|---|
With sulfuric acid; nitric acid at -5 - 20℃; for 2h; Large scale; | 95.4% |
With sulfuric acid; nitric acid at -5 - 5℃; for 2h; | 95.8% |
With sulfuric acid; potassium nitrate at 25℃; for 3h; | 90.2% |
Conditions | Yield |
---|---|
With sulfuric acid In water at 65 - 95℃; for 3h; Temperature; | 95% |
2-chloro-5-nitro-benzamide
2-chloro-5-nitrobenzoic acid
Conditions | Yield |
---|---|
With hydrogenchloride | |
With sulfuric acid; sodium nitrite |
1-chloro-2-methyl-4-nitrobenzene
2-chloro-5-nitrobenzoic acid
Conditions | Yield |
---|---|
With nitric acid at 140 - 150℃; |
Conditions | Yield |
---|---|
With phosphorus pentachloride |
Conditions | Yield |
---|---|
With permanganate(VII) ion |
ortho-chlorobenzoic acid
A
2-chloro-5-nitrobenzoic acid
B
2-chloro-3-nitrobezoic acid
Conditions | Yield |
---|---|
With nitric acid | |
With sulfuric acid; nitric acid |
2-chloro-N-(4-chlorophenyl)-5-nitrobenzamide
2-chloro-5-nitrobenzoic acid
Conditions | Yield |
---|---|
With sodium hydroxide |
hydrogenchloride
6-nitro-3-phenylbenzo[d][1,2,3]triazin-4(3H)-one
A
2-chloro-5-nitrobenzoic acid
B
aniline
Conditions | Yield |
---|---|
at 120 - 130℃; |
hydrogenchloride
6-nitrobenzo[d][1,2,3]triazin-4(3H)-one
A
2-chloro-5-nitrobenzoic acid
B
ammonia
Conditions | Yield |
---|---|
at 120 - 130℃; |
Conditions | Yield |
---|---|
at 120 - 130℃; |
sulfuric acid
nitric acid
ortho-chlorobenzoic acid
2-chloro-5-nitrobenzoic acid
nitric acid
ortho-chlorobenzoic acid
A
2-chloro-5-nitrobenzoic acid
B
2-chloro-3-nitrobezoic acid
Conditions | Yield |
---|---|
at -30 - 0℃; |
5-nitro-2-sulfo-benzoic acid
phosphorus pentachloride
2-chloro-5-nitrobenzoic acid
Conditions | Yield |
---|---|
at 180℃; |
2-chloro-5-nitrobenzoic acid
Conditions | Yield |
---|---|
With permanganate(VII) ion |
2-chloro-5-nitrobenzoic acid
Conditions | Yield |
---|---|
With copper(I) chloride |
2'-chloro-5'-nitroacetophenone
2-chloro-5-nitrobenzoic acid
(2-chloro-5-nitro-phenyl)-methanesulfonic acid
2-chloro-5-nitrobenzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diluted sulfuric acid 2: nitric acid View Scheme |
4-chloro-3-cyanonitrobenzene
2-chloro-5-nitrobenzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. NaOH solution; aqueous hydrogen peroxide 2: aqueous sulfuric acid; sodium nitrite View Scheme | |
Multi-step reaction with 2 steps 1: concentrated sulfuric acid 2: concentrated aqueous hydrochloric acid View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: hydrochloric acid; sodium nitrite / die Loesung mit Wasserdampf destillieren 2: diluted sulfuric acid 3: nitric acid View Scheme | |
Multi-step reaction with 3 steps 1: Diazotization.Behandlung der Diazoloesung mit Kaliumkupfercyanuerloesung 2: diluted sulfuric acid 3: nitric acid View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sulfuric acid; sodium nitrate / 0 - 5 °C 2: permanganate; alkali View Scheme |
2-chloro-5-nitrobenzoylchloride
2-chloro-5-nitrobenzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: aq. NaOH View Scheme |
2-chloro-5-nitrobenzaldehyde
A
2-chloro-5-nitrobenzoic acid
B
2-chloro-5-nitrobenzyl alcohol
Conditions | Yield |
---|---|
With sodium borohydrid In methanol; water | |
With sodium borohydrid In methanol; water | |
With sodium borohydrid In methanol; water |
2-chloro-5-nitrobenzoic acid
2-chloro-5-nitrobenzoylchloride
Conditions | Yield |
---|---|
With thionyl chloride | 100% |
In toluene | 95% |
With phosphorus pentachloride In benzene for 3h; Heating; | 93.1% |
2-chloro-5-nitrobenzoic acid
3-amino-4-hydroxytoluene
2-(2-amino-4-methylphenoxy)-5-nitrobenzoic acid
Conditions | Yield |
---|---|
With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydride 1.)ice-bath cooling, 1.5 h 2.)r.t., overnight; | 100% |
Conditions | Yield |
---|---|
With silver carbonate In dimethyl sulfoxide; N,N-dimethyl-formamide at 110℃; for 16h; Inert atmosphere; | 100% |
With silver carbonate In dimethyl sulfoxide at 120℃; for 16h; | 90% |
With silver(I) acetate; potassium carbonate In 1-methyl-pyrrolidin-2-one at 120℃; for 16h; Inert atmosphere; | 85% |
2-chloro-5-nitrobenzoic acid
cyclohexylamine
2-(cyclohexylamino)-5-nitrobenzoic acid
Conditions | Yield |
---|---|
at 120℃; for 0.0833333h; microwave irradiation; | 99% |
Stage #1: 2-chloro-5-nitrobenzoic acid; cyclohexylamine at 120℃; for 0.1h; Microwave heating; Stage #2: With sodium hydroxide In dichloromethane; water Stage #3: With hydrogenchloride In water Acidic aqueous solution; | 31% |
With water; sodium carbonate at 140℃; |
pyrrolidine
2-chloro-5-nitrobenzoic acid
2-tetrahydropyrrolyl-5-nitrobenzoic acid
Conditions | Yield |
---|---|
at 80℃; for 0.0833333h; microwave irradiation; | 99% |
With copper; potassium carbonate In N,N-dimethyl-formamide at 25℃; for 0.25h; Ullmann condensation; ultrasonic irradiation; | 92% |
In ethanol for 7h; Heating; | 89% |
2-chloro-5-nitrobenzoic acid
2-chloro-5-nitrobenzyl alcohol
Conditions | Yield |
---|---|
With sodium tetrahydroborate; boron trifluoride diethyl etherate In tetrahydrofuran at 0 - 20℃; for 1h; | 99% |
With sodium tetrahydroborate; boron trifluoride diethyl etherate In tetrahydrofuran at 0 - 20℃; | 90% |
With phenylsilane; C34H30CoO6; potassium In tetrahydrofuran at 20℃; for 20h; Inert atmosphere; Schlenk technique; Glovebox; | 71% |
With sodium tetrahydroborate; boron trifluoride diethyl etherate In tetrahydrofuran at 0 - 20℃; for 1h; |
2-chloro-5-nitrobenzoic acid
Cyclopentamine
2-(cyclopentylamino)-5-nitrobenzoic acid
Conditions | Yield |
---|---|
at 120℃; for 0.0833333h; microwave irradiation; | 99% |
Conditions | Yield |
---|---|
at 100℃; for 0.0833333h; microwave irradiation; | 99% |
With copper; potassium carbonate In N,N-dimethyl-formamide at 25℃; for 0.333333h; Ullmann condensation; ultrasonic irradiation; | 79% |
2-chloro-5-nitrobenzoic acid
dibutylamine
2-Dibutylamino-5-nitro-benzoic acid
Conditions | Yield |
---|---|
for 3h; Heating; | 98% |
Conditions | Yield |
---|---|
With 25 wtpercent H3PO4/ZrO2-TiO2 at 140℃; for 0.75h; Neat (no solvent); chemoselective reaction; | 98% |
1-Decanol
2-chloro-5-nitrobenzoic acid
decyl 2-chloro-5-nitrobenzoate
Conditions | Yield |
---|---|
With 25 wtpercent H3PO4/ZrO2-TiO2 at 160℃; for 0.5h; Neat (no solvent); chemoselective reaction; | 98% |
methanol
2-chloro-5-nitrobenzoic acid
2-chloro-5-nitro-benzoic acid methyl ester
Conditions | Yield |
---|---|
sulfuric acid for 24h; Heating / reflux; | 97.9% |
With sulfuric acid for 24h; Reflux; | 96% |
With sulfuric acid at 80℃; for 24h; | 96% |
Conditions | Yield |
---|---|
With hydrogen; platinum | 97% |
With hydrogen; platinum(IV) oxide In ethanol Ambient temperature; | 95% |
With iron; ammonium chloride In ethanol; water at 78 - 80℃; for 5h; | 95.1% |
Conditions | Yield |
---|---|
With pyridine; water; potassium carbonate; copper for 0.25h; sonication; | 97% |
With water; potassium hydroxide for 6h; Heating; Large scale; | 97% |
Stage #1: 2-chloro-5-nitrobenzoic acid With potassium hydroxide In water at 25 - 30℃; under 1875.19 Torr; for 0.333333h; Industrial scale; Stage #2: In water at 125 - 130℃; for 5h; Industrial scale; | 96% |
2-chloro-5-nitrobenzoic acid
glycine
2-[(carboxymethyl)amino]-5-nitrobenzoic acid
Conditions | Yield |
---|---|
With copper; potassium carbonate In N,N-dimethyl-formamide at 25℃; for 0.416667h; Ullmann condensation; ultrasonic irradiation; | 97% |
With copper; potassium carbonate In N,N-dimethyl-formamide for 2h; Heating; | 97% |
With copper; sodium carbonate In water for 2h; Reflux; | 50% |
With water; copper; sodium carbonate |
2-chloro-5-nitrobenzoic acid
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 12h; | 97% |
n-heptan1ol
2-chloro-5-nitrobenzoic acid
heptyl 2-chloro-5-nitrobenzoate
Conditions | Yield |
---|---|
With 25 wtpercent H3PO4/ZrO2-TiO2 at 130℃; for 0.75h; Neat (no solvent); chemoselective reaction; | 97% |
Conditions | Yield |
---|---|
Stage #1: N-methylcyclohexylamine With iodine; triphenylphosphine In dichloromethane at 0℃; for 0.166667h; Stage #2: 2-chloro-5-nitrobenzoic acid In dichloromethane at 25℃; | 96% |
2-chloro-5-nitrobenzoic acid
triethylamine
2-chloro-5-nitro-N,N-diethylbenzamide
Conditions | Yield |
---|---|
Stage #1: triethylamine With iodine; triphenylphosphine In dichloromethane at 0℃; for 0.166667h; Stage #2: 2-chloro-5-nitrobenzoic acid In dichloromethane at 25℃; Reagent/catalyst; | 95% |
With iodine; triphenylphosphine In dichloromethane at 0 - 20℃; | 75% |
disulfiram
2-chloro-5-nitrobenzoic acid
2-chloro-5-nitro-N,N-diethylbenzamide
Conditions | Yield |
---|---|
With di-tert-butyl peroxide; copper(I) bromide In ethyl acetate at 120℃; | 95% |
Conditions | Yield |
---|---|
at 20℃; | 95% |
2-chloro-5-nitrobenzoic acid
p-toluidine
2-chloro-5-nitro-N-(p-tolyl)benzamide
Conditions | Yield |
---|---|
With EDC-polymer In tetrahydrofuran at 20℃; for 4h; | 94% |
Conditions | Yield |
---|---|
Stage #1: tribenzylamine With iodine; triphenylphosphine In dichloromethane at 0℃; for 0.166667h; Stage #2: 2-chloro-5-nitrobenzoic acid In dichloromethane at 25℃; | 94% |
Conditions | Yield |
---|---|
Stage #1: 2-chloro-5-nitrobenzoic acid With N-Bromosuccinimide; triphenylphosphine In dichloromethane at 0℃; for 0.25h; Stage #2: N,O-dimethylhydroxylamine*hydrochloride With triethylamine In dichloromethane at 20℃; for 1h; chemoselective reaction; | 94% |
Conditions | Yield |
---|---|
With copper diacetate; potassium carbonate at 185℃; for 2h; Ullmann Condensation; Inert atmosphere; | 93% |
With potassium carbonate In water at 150℃; for 2h; Temperature; Time; | 90% |
With sodium carbonate In N,N-dimethyl-formamide for 4h; Ullmann Condensation; Reflux; | 90% |
azonane
2-chloro-5-nitrobenzoic acid
5-nitro-2-octamethyleneimino-benzoic acid
Conditions | Yield |
---|---|
With sodium carbonate In ethanol for 4h; Heating; | 93% |
2-chloro-5-nitrobenzoic acid
hexan-1-ol
hexyl 2-chloro-5-nitrobenzoate
Conditions | Yield |
---|---|
With 25 wtpercent H3PO4/ZrO2-TiO2 at 120℃; for 1.66667h; Neat (no solvent); chemoselective reaction; | 93% |
2-chloro-5-nitrobenzoic acid
Conditions | Yield |
---|---|
With potassium tert-butylate In ethanol at 20℃; for 1h; Inert atmosphere; | 93% |
With potassium tert-butylate In ethanol at 20℃; |
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