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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

2-Chloro-5-nitrobenzoic acid

Cas:2516-96-3

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Jinan Finer Chemical Co., Ltd

Product Description Product website: http://www.finerchem.com Product Name 2-Chloro-5-nitrobenzoic acid CAS No.

2-Chloro-5-nitrobenzoic acid

Cas:2516-96-3

Min.Order:1 Gram

FOB Price: $8.0

Type:Lab/Research institutions

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 2-chloro-5-nitrobenzoic acid

Cas:2516-96-3

Min.Order:1

Negotiable

Type:Other

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COLORCOM LTD.

Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on

2-Chloro-5-Nitrobenzoic Acid

Cas:2516-96-3

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

2-Chloro-5-nitrobenzoic acid

Cas:2516-96-3

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

2-Chloro-5-nitrobenzoic acid Basic information Product Name: 2-Chloro-5-nitrobenzoic acid Synonyms: RARECHEM AL BO 0234;2-CHLORO-5-NITROBENZOIC ACID;5-NITRO-2-CHLOROBENZOIC ACID;LABOTEST

2-Chloro-5-nitrobenzoic acid 2516-96-3

Cas:2516-96-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

2-Chloro-5-nitrobenzoic acid

Cas:2516-96-3

Min.Order:1 Gram

FOB Price: $1000.0 / 1300.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 2516-96-3 with best quality

Cas:2516-96-3

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

2-Chloro-5-nitrobenzoic acid Molecular formula: C7H4ClNO4 CAS NO.: 2516-96-3 Appearance: Light yellow crystalline powder Content: 99%-101% Appearance:Light yellow crystalline powder Storage:Store

2-Chloro-5-nitrobenzoic acid CAS:2516-96-3

Cas:2516-96-3

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

2-Chloro-5-nitrobenzoic acid 2516-96-3

Cas:2516-96-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

2-Chloro-5-nitrobenzoic acid CAS:2516-96-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality orga

2-Chloro-5-nitrobenzoic acid CAS:2516-96-3

Cas:2516-96-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

2-Chloro-5-nitrobenzoic acid

Cas:2516-96-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:2516-96-3

Cas:2516-96-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Factory Supply High Quality CAS 2516-96-3 ,2-Chloro-5-nitrobenzoic acid

Cas:2516-96-3

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

2-Chloro-5-Nitrobenzoic Acid

Cas:2516-96-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

2-Chloro-5-nitrobenzoic acid

Cas:2516-96-3

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

2-Chloro-5-nitrobenzoic acid

Cas:2516-96-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 2-Chloro-5-Nitrobenzoic Acid

Cas:2516-96-3

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

2-Chloro-5-nitrobenzoic acid

Cas:2516-96-3

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

Siwei Development Group Ltd.

Product name: 2-Chloro-5-Nitrobenzoic Acid CAS No.:2516-96-3 Molecule Formula:C7H3ClNO4 Molecule Weight:200.56 Purity: 99.0% Package: 25kg/drum Description:Light yellow powder Manufacture Standards:Enterprise Standard

Best Quality 2-Chloro-5-Nitrobenzoic Acid with good supplier

Cas:2516-96-3

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Shanghai Minstar Chemical Co., Ltd

Product Name: 2-Chloro-5-nitrobenzoic acid Synonyms: RARECHEM AL BO 0234;2-CHLORO-5-NITROBENZOIC ACID;LABOTEST-BB LT00847209;2-chloro-5-nitro-benzoicaci;6-Chloro-3-nitrobenzoic acid;Benzoic acid, 2-chloro-5-nitro-;5-NITRO-2-CHLOROBENZOIC ACID;2

2-Chloro-5-nitrobenzoic acid 2516-96-3 C7H4ClNO4

Cas:2516-96-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

2-Chloro-5-nitrobenzoic acid

Cas:2516-96-3

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

2-Chloro-5-nitrobenzoic acid

Cas:2516-96-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

2-Chloro-5-nitrobenzoic acid

Cas:2516-96-3

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

2-Chloro-5-nitrobenzoic acid

Cas:2516-96-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

2-Chloro-5-nitrobenzoic acid

Cas:2516-96-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Golden Pharma Co., Limited

GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation

2-Chloro-5-nitrobenzoic acid

Cas:2516-96-3

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:light yellow to light yellow-green crystalline Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:as per your request Application:Used as Pharmaceutic

2-Chloro-5-nitrobenzoic acid

Cas:2516-96-3

Min.Order:10 Gram

Negotiable

Type:Trading Company

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

2-Chloro-5-nitrobenzoic acid

Cas:2516-96-3

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratoryAppearance:Off-white to light yellow crystal powde Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

2-Chloro-5-nitrobenzoic acid cas no. 2516-96-3 98%

Cas:2516-96-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

ortho-chlorobenzoic acid
118-91-2

ortho-chlorobenzoic acid

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

Conditions
ConditionsYield
With sulfuric acid; nitric acid at -5 - 20℃; for 2h; Large scale;95.4%
With sulfuric acid; nitric acid at -5 - 5℃; for 2h;95.8%
With sulfuric acid; potassium nitrate at 25℃; for 3h;90.2%
1-chloro-4-nitro-2-(trichloromethyl)benzene
831-50-5

1-chloro-4-nitro-2-(trichloromethyl)benzene

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

Conditions
ConditionsYield
With sulfuric acid In water at 65 - 95℃; for 3h; Temperature;95%
2-chloro-5-nitro-benzamide
16588-15-1

2-chloro-5-nitro-benzamide

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

Conditions
ConditionsYield
With hydrogenchloride
With sulfuric acid; sodium nitrite
1-chloro-2-methyl-4-nitrobenzene
13290-74-9

1-chloro-2-methyl-4-nitrobenzene

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

Conditions
ConditionsYield
With nitric acid at 140 - 150℃;
5-nitrosalicylic acid
96-97-9

5-nitrosalicylic acid

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

Conditions
ConditionsYield
With phosphorus pentachloride
2-chloro-5-nitrobenzaldehyde
6361-21-3

2-chloro-5-nitrobenzaldehyde

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

Conditions
ConditionsYield
With permanganate(VII) ion
ortho-chlorobenzoic acid
118-91-2

ortho-chlorobenzoic acid

A

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

B

2-chloro-3-nitrobezoic acid
3970-35-2

2-chloro-3-nitrobezoic acid

Conditions
ConditionsYield
With nitric acid
With sulfuric acid; nitric acid
2-chloro-N-(4-chlorophenyl)-5-nitrobenzamide
54253-05-3

2-chloro-N-(4-chlorophenyl)-5-nitrobenzamide

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

Conditions
ConditionsYield
With sodium hydroxide
hydrogenchloride
7647-01-0

hydrogenchloride

6-nitro-3-phenylbenzo[d][1,2,3]triazin-4(3H)-one
60041-99-8

6-nitro-3-phenylbenzo[d][1,2,3]triazin-4(3H)-one

A

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

B

aniline
62-53-3

aniline

Conditions
ConditionsYield
at 120 - 130℃;
hydrogenchloride
7647-01-0

hydrogenchloride

6-nitrobenzo[d][1,2,3]triazin-4(3H)-one
91532-29-5

6-nitrobenzo[d][1,2,3]triazin-4(3H)-one

A

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

B

ammonia
7664-41-7

ammonia

C

nitrogen

nitrogen

Conditions
ConditionsYield
at 120 - 130℃;
hydrogenchloride
7647-01-0

hydrogenchloride

3-methyl-6-nitro-3H-benzo[d][1,2,3]triazin-4-one

3-methyl-6-nitro-3H-benzo[d][1,2,3]triazin-4-one

A

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

B

methylamine
74-89-5

methylamine

C

nitrogen

nitrogen

Conditions
ConditionsYield
at 120 - 130℃;
sulfuric acid
7664-93-9

sulfuric acid

nitric acid
7697-37-2

nitric acid

ortho-chlorobenzoic acid
118-91-2

ortho-chlorobenzoic acid

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

nitric acid
7697-37-2

nitric acid

ortho-chlorobenzoic acid
118-91-2

ortho-chlorobenzoic acid

A

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

B

2-chloro-3-nitrobezoic acid
3970-35-2

2-chloro-3-nitrobezoic acid

Conditions
ConditionsYield
at -30 - 0℃;
5-nitro-2-sulfo-benzoic acid
40567-35-9

5-nitro-2-sulfo-benzoic acid

phosphorus pentachloride
10026-13-8, 874483-75-7

phosphorus pentachloride

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

Conditions
ConditionsYield
at 180℃;
6-chloro-3-nitro-toluene-ω-sulfonic acid

6-chloro-3-nitro-toluene-ω-sulfonic acid

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

Conditions
ConditionsYield
With permanganate(VII) ion
diazotized 3-amino-5-nitro-benzoic acid

diazotized 3-amino-5-nitro-benzoic acid

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

Conditions
ConditionsYield
With copper(I) chloride
sulfuric acid
7664-93-9

sulfuric acid

4-chloro-3-(trifluoromethyl)nitrobenzene
777-37-7

4-chloro-3-(trifluoromethyl)nitrobenzene

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

2'-chloro-5'-nitroacetophenone
23082-50-0

2'-chloro-5'-nitroacetophenone

potassium permanganate

potassium permanganate

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

(2-chloro-5-nitro-phenyl)-methanesulfonic acid
749147-27-1

(2-chloro-5-nitro-phenyl)-methanesulfonic acid

permanganate

permanganate

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

2-Chlorobenzonitrile
873-32-5

2-Chlorobenzonitrile

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: diluted sulfuric acid
2: nitric acid
View Scheme
4-chloro-3-cyanonitrobenzene
16588-02-6

4-chloro-3-cyanonitrobenzene

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: aq. NaOH solution; aqueous hydrogen peroxide
2: aqueous sulfuric acid; sodium nitrite
View Scheme
Multi-step reaction with 2 steps
1: concentrated sulfuric acid
2: concentrated aqueous hydrochloric acid
View Scheme
2-Chloroaniline
95-51-2

2-Chloroaniline

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: hydrochloric acid; sodium nitrite / die Loesung mit Wasserdampf destillieren
2: diluted sulfuric acid
3: nitric acid
View Scheme
Multi-step reaction with 3 steps
1: Diazotization.Behandlung der Diazoloesung mit Kaliumkupfercyanuerloesung
2: diluted sulfuric acid
3: nitric acid
View Scheme
2-chloro-benzaldehyde
89-98-5

2-chloro-benzaldehyde

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sulfuric acid; sodium nitrate / 0 - 5 °C
2: permanganate; alkali
View Scheme
2-chloro-5-nitrobenzoylchloride
25784-91-2

2-chloro-5-nitrobenzoylchloride

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
2: aq. NaOH
View Scheme
2-chloro-5-nitrobenzaldehyde
6361-21-3

2-chloro-5-nitrobenzaldehyde

A

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

B

2-chloro-5-nitrobenzyl alcohol
80866-80-4

2-chloro-5-nitrobenzyl alcohol

Conditions
ConditionsYield
With sodium borohydrid In methanol; water
With sodium borohydrid In methanol; water
With sodium borohydrid In methanol; water
2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

2-chloro-5-nitrobenzoylchloride
25784-91-2

2-chloro-5-nitrobenzoylchloride

Conditions
ConditionsYield
With thionyl chloride100%
In toluene95%
With phosphorus pentachloride In benzene for 3h; Heating;93.1%
2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

3-amino-4-hydroxytoluene
95-84-1

3-amino-4-hydroxytoluene

2-(2-amino-4-methylphenoxy)-5-nitrobenzoic acid
78460-76-1

2-(2-amino-4-methylphenoxy)-5-nitrobenzoic acid

Conditions
ConditionsYield
With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydride 1.)ice-bath cooling, 1.5 h 2.)r.t., overnight;100%
2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

4-chlorobenzonitrile
100-00-5

4-chlorobenzonitrile

Conditions
ConditionsYield
With silver carbonate In dimethyl sulfoxide; N,N-dimethyl-formamide at 110℃; for 16h; Inert atmosphere;100%
With silver carbonate In dimethyl sulfoxide at 120℃; for 16h;90%
With silver(I) acetate; potassium carbonate In 1-methyl-pyrrolidin-2-one at 120℃; for 16h; Inert atmosphere;85%
2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

cyclohexylamine
108-91-8

cyclohexylamine

2-(cyclohexylamino)-5-nitrobenzoic acid
66380-72-1

2-(cyclohexylamino)-5-nitrobenzoic acid

Conditions
ConditionsYield
at 120℃; for 0.0833333h; microwave irradiation;99%
Stage #1: 2-chloro-5-nitrobenzoic acid; cyclohexylamine at 120℃; for 0.1h; Microwave heating;
Stage #2: With sodium hydroxide In dichloromethane; water
Stage #3: With hydrogenchloride In water Acidic aqueous solution;
31%
With water; sodium carbonate at 140℃;
pyrrolidine
123-75-1

pyrrolidine

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

2-tetrahydropyrrolyl-5-nitrobenzoic acid
19555-48-7

2-tetrahydropyrrolyl-5-nitrobenzoic acid

Conditions
ConditionsYield
at 80℃; for 0.0833333h; microwave irradiation;99%
With copper; potassium carbonate In N,N-dimethyl-formamide at 25℃; for 0.25h; Ullmann condensation; ultrasonic irradiation;92%
In ethanol for 7h; Heating;89%
2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

2-chloro-5-nitrobenzyl alcohol
80866-80-4

2-chloro-5-nitrobenzyl alcohol

Conditions
ConditionsYield
With sodium tetrahydroborate; boron trifluoride diethyl etherate In tetrahydrofuran at 0 - 20℃; for 1h;99%
With sodium tetrahydroborate; boron trifluoride diethyl etherate In tetrahydrofuran at 0 - 20℃;90%
With phenylsilane; C34H30CoO6; potassium In tetrahydrofuran at 20℃; for 20h; Inert atmosphere; Schlenk technique; Glovebox;71%
With sodium tetrahydroborate; boron trifluoride diethyl etherate In tetrahydrofuran at 0 - 20℃; for 1h;
2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

Cyclopentamine
1003-03-8

Cyclopentamine

2-(cyclopentylamino)-5-nitrobenzoic acid
247568-48-5

2-(cyclopentylamino)-5-nitrobenzoic acid

Conditions
ConditionsYield
at 120℃; for 0.0833333h; microwave irradiation;99%
2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

di-n-propylamine
142-84-7

di-n-propylamine

2-(dipropylamino)-5-nitrobenzoic acid

2-(dipropylamino)-5-nitrobenzoic acid

Conditions
ConditionsYield
at 100℃; for 0.0833333h; microwave irradiation;99%
With copper; potassium carbonate In N,N-dimethyl-formamide at 25℃; for 0.333333h; Ullmann condensation; ultrasonic irradiation;79%
2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

dibutylamine
111-92-2

dibutylamine

2-Dibutylamino-5-nitro-benzoic acid
83909-53-9

2-Dibutylamino-5-nitro-benzoic acid

Conditions
ConditionsYield
for 3h; Heating;98%
octanol
111-87-5

octanol

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

octyl 2-chloro-5-nitrobenzoate
1256568-06-5

octyl 2-chloro-5-nitrobenzoate

Conditions
ConditionsYield
With 25 wtpercent H3PO4/ZrO2-TiO2 at 140℃; for 0.75h; Neat (no solvent); chemoselective reaction;98%
1-Decanol
112-30-1

1-Decanol

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

decyl 2-chloro-5-nitrobenzoate
1256568-05-4

decyl 2-chloro-5-nitrobenzoate

Conditions
ConditionsYield
With 25 wtpercent H3PO4/ZrO2-TiO2 at 160℃; for 0.5h; Neat (no solvent); chemoselective reaction;98%
methanol
67-56-1

methanol

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

2-chloro-5-nitro-benzoic acid methyl ester
6307-82-0

2-chloro-5-nitro-benzoic acid methyl ester

Conditions
ConditionsYield
sulfuric acid for 24h; Heating / reflux;97.9%
With sulfuric acid for 24h; Reflux;96%
With sulfuric acid at 80℃; for 24h;96%
2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

2-chloro-5-aminobenzoic acid
89-54-3

2-chloro-5-aminobenzoic acid

Conditions
ConditionsYield
With hydrogen; platinum97%
With hydrogen; platinum(IV) oxide In ethanol Ambient temperature;95%
With iron; ammonium chloride In ethanol; water at 78 - 80℃; for 5h;95.1%
2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

5-nitrosalicylic acid
96-97-9

5-nitrosalicylic acid

Conditions
ConditionsYield
With pyridine; water; potassium carbonate; copper for 0.25h; sonication;97%
With water; potassium hydroxide for 6h; Heating; Large scale;97%
Stage #1: 2-chloro-5-nitrobenzoic acid With potassium hydroxide In water at 25 - 30℃; under 1875.19 Torr; for 0.333333h; Industrial scale;
Stage #2: In water at 125 - 130℃; for 5h; Industrial scale;
96%
2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

glycine
56-40-6

glycine

2-[(carboxymethyl)amino]-5-nitrobenzoic acid
26491-02-1

2-[(carboxymethyl)amino]-5-nitrobenzoic acid

Conditions
ConditionsYield
With copper; potassium carbonate In N,N-dimethyl-formamide at 25℃; for 0.416667h; Ullmann condensation; ultrasonic irradiation;97%
With copper; potassium carbonate In N,N-dimethyl-formamide for 2h; Heating;97%
With copper; sodium carbonate In water for 2h; Reflux;50%
With water; copper; sodium carbonate
2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

3-(2-hydroxyethyl)-1-methyl-1H-imidazol-3-ium tetrafluoroborate

3-(2-hydroxyethyl)-1-methyl-1H-imidazol-3-ium tetrafluoroborate

BF4(1-)*C13H13ClN3O4(1+)

BF4(1-)*C13H13ClN3O4(1+)

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 12h;97%
n-heptan1ol
111-70-6

n-heptan1ol

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

heptyl 2-chloro-5-nitrobenzoate
1256568-07-6

heptyl 2-chloro-5-nitrobenzoate

Conditions
ConditionsYield
With 25 wtpercent H3PO4/ZrO2-TiO2 at 130℃; for 0.75h; Neat (no solvent); chemoselective reaction;97%
N-methylcyclohexylamine
626-67-5

N-methylcyclohexylamine

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

(2-chloro-5-nitrophenyl)(piperidin-1-yl)methanone

(2-chloro-5-nitrophenyl)(piperidin-1-yl)methanone

Conditions
ConditionsYield
Stage #1: N-methylcyclohexylamine With iodine; triphenylphosphine In dichloromethane at 0℃; for 0.166667h;
Stage #2: 2-chloro-5-nitrobenzoic acid In dichloromethane at 25℃;
96%
2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

triethylamine
121-44-8

triethylamine

2-chloro-5-nitro-N,N-diethylbenzamide
67272-98-4

2-chloro-5-nitro-N,N-diethylbenzamide

Conditions
ConditionsYield
Stage #1: triethylamine With iodine; triphenylphosphine In dichloromethane at 0℃; for 0.166667h;
Stage #2: 2-chloro-5-nitrobenzoic acid In dichloromethane at 25℃; Reagent/catalyst;
95%
With iodine; triphenylphosphine In dichloromethane at 0 - 20℃;75%
disulfiram
97-77-8

disulfiram

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

2-chloro-5-nitro-N,N-diethylbenzamide
67272-98-4

2-chloro-5-nitro-N,N-diethylbenzamide

Conditions
ConditionsYield
With di-tert-butyl peroxide; copper(I) bromide In ethyl acetate at 120℃;95%
2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

ethanolamine
141-43-5

ethanolamine

acetone
67-64-1

acetone

N-(1,1-dimethyl-3-oxobutyl)monoethanolammonium 2-chloro-5-nitrobenzoate

N-(1,1-dimethyl-3-oxobutyl)monoethanolammonium 2-chloro-5-nitrobenzoate

Conditions
ConditionsYield
at 20℃;95%
2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

p-toluidine
106-49-0

p-toluidine

2-chloro-5-nitro-N-(p-tolyl)benzamide
292638-37-0

2-chloro-5-nitro-N-(p-tolyl)benzamide

Conditions
ConditionsYield
With EDC-polymer In tetrahydrofuran at 20℃; for 4h;94%
2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

tribenzylamine
620-40-6

tribenzylamine

C21H17ClN2O3

C21H17ClN2O3

Conditions
ConditionsYield
Stage #1: tribenzylamine With iodine; triphenylphosphine In dichloromethane at 0℃; for 0.166667h;
Stage #2: 2-chloro-5-nitrobenzoic acid In dichloromethane at 25℃;
94%
2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

N,O-dimethylhydroxylamine*hydrochloride
6638-79-5

N,O-dimethylhydroxylamine*hydrochloride

2-chloro-N-methoxy-N-methyl-5-nitrobenzamide

2-chloro-N-methoxy-N-methyl-5-nitrobenzamide

Conditions
ConditionsYield
Stage #1: 2-chloro-5-nitrobenzoic acid With N-Bromosuccinimide; triphenylphosphine In dichloromethane at 0℃; for 0.25h;
Stage #2: N,O-dimethylhydroxylamine*hydrochloride With triethylamine In dichloromethane at 20℃; for 1h; chemoselective reaction;
94%
2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

aniline
62-53-3

aniline

Conditions
ConditionsYield
With copper diacetate; potassium carbonate at 185℃; for 2h; Ullmann Condensation; Inert atmosphere;93%
With potassium carbonate In water at 150℃; for 2h; Temperature; Time;90%
With sodium carbonate In N,N-dimethyl-formamide for 4h; Ullmann Condensation; Reflux;90%
azonane
5661-71-2

azonane

2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

5-nitro-2-octamethyleneimino-benzoic acid
78243-43-3

5-nitro-2-octamethyleneimino-benzoic acid

Conditions
ConditionsYield
With sodium carbonate In ethanol for 4h; Heating;93%
2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

hexan-1-ol
111-27-3

hexan-1-ol

hexyl 2-chloro-5-nitrobenzoate
1256568-09-8

hexyl 2-chloro-5-nitrobenzoate

Conditions
ConditionsYield
With 25 wtpercent H3PO4/ZrO2-TiO2 at 120℃; for 1.66667h; Neat (no solvent); chemoselective reaction;93%
2-chloro-5-nitrobenzoic acid
2516-96-3

2-chloro-5-nitrobenzoic acid

potassium 2-chloro-5-nitrobenzoate

potassium 2-chloro-5-nitrobenzoate

Conditions
ConditionsYield
With potassium tert-butylate In ethanol at 20℃; for 1h; Inert atmosphere;93%
With potassium tert-butylate In ethanol at 20℃;

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