2-Chloro-6-methylaniline CAS No.: 87-63-8 Customization Sythesis Company Profile: Synchem is dedicated to custom synthesis and manufacturing services for small molecules. We serve the needs of customers in the pharmaceutical, agrochemical, and
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryProduct description: Product name 2-Chloro-6-methylaniline CAS number 87-63-8 Assay ≥99% Appearance Colorless to red liquid Capacity 100mt/year Application Pharmaceutical/pes
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inquiryHebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiryProduct Name: 2-Chloro-6-methylaniline Synonyms: 6COT;6-CHLORO-2-METHYLANILINE;6-CHLORO-2-TOLUIDINE;6-CHLORO-O-TOLUIDINE;3-CHLORO-2-AMINOTOLUENE;1-AMINO-2-CHLORO-6-METHYLBENZENE;2-METHYL-6-CHLORO ANILINE;2-
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiryProduct name 2-Chloro-6-methylaniline CAS 87-63-8 Molecular Formula C7H8ClN Molecular Weight 141.6 Melting Point 1
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inquiry2-Chloro-6-methylaniline Basic information Product Name: 2-Chloro-6-methylaniline Synonyms: benzenamine,2-chloro-6-methyl-;benzenamine,2-chloro-6-methyl-(6-cot);o-Toluidine, 6-chloro-;2-chloro-6-methylbenzenamine;2-Chloro-6-methyl-phenylamine;2
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
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inquiry2-Chloro-6-methylaniline CAS:87-63-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic int
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
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inquiry2-chloro-6-methylaniline
Conditions | Yield |
---|---|
Stage #1: 3-chloro-5-methyl-4-nitroaniline With sulfuric acid; sodium nitrite In water at 0℃; for 0.5h; Stage #2: With hypophosphorous acid In water at 0℃; for 3h; Stage #3: With iron In water at 90℃; for 4h; Reagent/catalyst; | 82.5% |
2-bromo-1-chloro-3-methylbenzene
2-chloro-6-methylaniline
Conditions | Yield |
---|---|
With ammonium hydroxide; L-2-O-methyl-chiro-inositol; copper(II) acetate monohydrate In 1-methyl-pyrrolidin-2-one at 110℃; for 12h; | 82% |
Conditions | Yield |
---|---|
With N-chloro-succinimide; 1-(3,5-bis(trifluoromethyl)phenyl)-3-((1S,2S)-2-(mesitylselanyl)-2,3-dihydro-1H-inden-1-yl)thiourea In chloroform-d1 at 0℃; for 12h; regioselective reaction; | 65% |
N-(2-chloro-6-methylphenyl)acetamide
2-chloro-6-methylaniline
Conditions | Yield |
---|---|
With hydrogenchloride In water at 50 - 55℃; for 7h; Time; | 61.7% |
2-chloro-6-methylaniline
Conditions | Yield |
---|---|
With hydrogenchloride In sulfolane; water at 120℃; for 26h; | 60% |
1-azido-2-methyl-benzene
2-chloro-6-methylaniline
Conditions | Yield |
---|---|
With hydrogenchloride |
Conditions | Yield |
---|---|
With sulfuric acid at 165℃; | |
With sulfuric acid at 150 - 160℃; |
Conditions | Yield |
---|---|
With hydrogenchloride |
N-(2-chloro-6-methylphenyl)pivalamide
2-chloro-6-methylaniline
Conditions | Yield |
---|---|
With hydrogen bromide for 4.5h; Heating; Yield given; |
N-(o-tolyl)hydroxylamine
A
4-amino-3-methylphenol
B
o-toluidine
C
2-chloro-6-methylaniline
D
4-chloro-2-methylbenzeneamine
Conditions | Yield |
---|---|
With perchloric acid; sodium perchlorate; sodium chloride In water; acetonitrile at 25℃; Rate constant; |
hydrogenchloride
N-(o-tolyl)hydroxylamine
A
N,N'-Di-o-tolyl-diazene N-oxide
B
2-chloro-6-methylaniline
C
5-chloro-2-methyl-benzenamine
D
4-chloro-2-methylbenzeneamine
hydrogenchloride
1-azido-2-methyl-benzene
A
2-chloro-6-methylaniline
B
4-chloro-2-methylbenzeneamine
Conditions | Yield |
---|---|
Aufbewahren an einem kuehlen dunklen Ort; |
hydrogenchloride
ethanol
1-methyl-2-nitrobenzene
A
o-toluidine
B
2-chloro-6-methylaniline
C
4-chloro-2-methylbenzeneamine
hydrogenchloride
ethanol
1-methyl-2-nitrobenzene
A
o-toluidine
B
2-chloro-6-methylaniline
C
4-chloro-2-methylbenzeneamine
sulfuric acid
6-amino-5-chloro-toluene-3-sulfonic acid
2-chloro-6-methylaniline
Conditions | Yield |
---|---|
at 150 - 160℃; |
N-(2-chlorophenyl)-2,2,2-trimethylacetamide
2-chloro-6-methylaniline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 72.1 percent / TMEDA, n-BuLi / various solvent(s); hexane / 1.) -12 to -20 deg C, 50min, 2.) -20 deg C, 2 h 2: conc. aq. HBr / 4.5 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1: TMEDA, BuLi / various solvent(s); hexane / 1.) 65min, 2.) 1 h 2: conc. aq. HBr / 4.5 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 25 percent aq. NaOH / various solvent(s) 2: 72.1 percent / TMEDA, n-BuLi / various solvent(s); hexane / 1.) -12 to -20 deg C, 50min, 2.) -20 deg C, 2 h 3: conc. aq. HBr / 4.5 h / Heating View Scheme | |
Multi-step reaction with 3 steps 1: 25 percent aq. NaOH / various solvent(s) 2: TMEDA, BuLi / various solvent(s); hexane / 1.) 65min, 2.) 1 h 3: conc. aq. HBr / 4.5 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: sodium hydroxide / water / 2 h / 50 °C 2: acetic acid; hydrogenchloride; dihydrogen peroxide / water / 40 - 50 °C 3: hydrogenchloride / water; sulfolane / 26 h / 120 °C View Scheme |
Conditions | Yield |
---|---|
With hydrogen In ethanol at 80℃; under 15001.5 Torr; for 2.5h; Catalytic behavior; chemoselective reaction; |
Conditions | Yield |
---|---|
With N-chloro-succinimide In chloroform-d1 at 0℃; for 12h; |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: chloroform / 12 h / Reflux 2.1: palladium 10% on activated carbon; hydrogen / methanol / 1 h / 40 °C / 1800.18 - 3000.3 Torr / Inert atmosphere; Autoclave 3.1: sodium nitrite; hydrogenchloride / water / 0.5 h / -3 - 3 °C 3.2: 5.5 h / -3 - 3 °C 4.1: hydrogenchloride / water / 7 h / 50 - 55 °C View Scheme |
N-(2-methyl-6-nitrophenyl)acetamide
2-chloro-6-methylaniline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: palladium 10% on activated carbon; hydrogen / methanol / 1 h / 40 °C / 1800.18 - 3000.3 Torr / Inert atmosphere; Autoclave 2.1: sodium nitrite; hydrogenchloride / water / 0.5 h / -3 - 3 °C 2.2: 5.5 h / -3 - 3 °C 3.1: hydrogenchloride / water / 7 h / 50 - 55 °C View Scheme |
2-chloro-6-methylaniline
4-bromo-2-chloro-6-methylphenylamine hydrobromide salt
Conditions | Yield |
---|---|
With bromine; acetic acid In methanol at 0℃; | 99% |
Conditions | Yield |
---|---|
With hafnium tetrakis(trifluoromethanesulfonate) In dichloromethane at 20℃; for 0.5h; Friedel Crafts alkylation; | 99% |
In dichloromethane for 72h; Inert atmosphere; Reflux; | 51% |
(E)-1,3-diphenyl-2-propen-1-ol
2-chloro-6-methylaniline
Conditions | Yield |
---|---|
With 1,3-bis(carboxymethyl)imidazolium iodide In neat (no solvent) at 80℃; for 6h; regioselective reaction; | 99% |
chloroacetyl chloride
2-chloro-6-methylaniline
2-chloro-N-(2-chloro-6-methylphenyl)acetamide
Conditions | Yield |
---|---|
Stage #1: 2-chloro-6-methylaniline With pyridine In dichloromethane at -10℃; for 0.166667h; Stage #2: chloroacetyl chloride In dichloromethane at -10 - 20℃; for 2h; | 98% |
at 0 - 25℃; for 2.5h; | 87.6% |
With sodium acetate In water; acetone at 20 - 50℃; for 16h; | 71% |
2-chloro-6-methylaniline
2,6-dichloroimidazo[1,5-a]pyrido[3,2-e]pyrazine
2-Chloro-N-(2-chloro-6-methylphenyl)imidazo[1,5-a]pyrido[3,2-e]pyrazin-6-amine
Conditions | Yield |
---|---|
Stage #1: 2-chloro-6-methylaniline With sodium hexamethyldisilazane In tetrahydrofuran for 0.5h; Heating; Stage #2: 2,6-dichloroimidazo[1,5-a]pyrido[3,2-e]pyrazine In tetrahydrofuran for 0.5h; Heating; | 98% |
3-oxo-propionic acid ethyl ester
2-chloro-6-methylaniline
C10H10ClNO2
Conditions | Yield |
---|---|
Stage #1: 3-oxo-propionic acid ethyl ester With sodium methylate In tetrahydrofuran at 20℃; for 10h; Stage #2: 2-chloro-6-methylaniline In tetrahydrofuran for 1h; Solvent; Reflux; | 97.3% |
acetylacetone
2-chloro-6-methylaniline
(Z)-4-(2-chloro-6-methylphenylamino)pent-3-en-2-one
Conditions | Yield |
---|---|
With iron(III) trifluoromethanesulfonate In neat (no solvent) at 20℃; for 0.1h; Green chemistry; | 97% |
With zinc trifluoromethanesulfonate In neat (no solvent) at 20℃; for 0.2h; stereoselective reaction; | 96% |
2-[[6-[4-(2-acetoxyethyl)-1-piperazinyl]-2-methyl-4-pyrimidinyl]amino]-5-thiazolecarboxylic acid
2-chloro-6-methylaniline
N-(2-chloro-6-methylphenyl)-2-[[6-[4-(2-acetoxyethyl)-1-piperazinyl]-2-methyl- 4-pyrimidinyl]amino]-5-thiazolecarboxamide
Conditions | Yield |
---|---|
Stage #1: 2-[[6-[4-(2-acetoxyethyl)-1-piperazinyl]-2-methyl-4-pyrimidinyl]amino]-5-thiazolecarboxylic acid With thionyl chloride; sodium hydroxide In water; 1,2-dichloro-ethane at 55 - 60℃; for 4h; Stage #2: 2-chloro-6-methylaniline With triethylamine In 1,2-dichloro-ethane at 40 - 45℃; for 1h; Solvent; Reagent/catalyst; Temperature; | 95.6% |
With O-phenyl phosphorodichloridate; triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere; | 71.7% |
With O-phenyl phosphorodichloridate; triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere; | 71.7% |
2-methyl-4,6-dichloroaniline
o-toluidine
2-chloro-6-methylaniline
4-chloro-2-methylbenzeneamine
Conditions | Yield |
---|---|
With carbon disulfide In acetone | 95.5% |
2-chloro-6-methylaniline
2-[(tert-butoxycarbonyl)amino]-1,3-thiazole-5-carboxylic acid
[5-(2-chloro-6-methylphenylcarbamoyl)thiazol-2-yl]-carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With Dichlorophenylphosphine; N-ethyl-N,N-diisopropylamine In dichloromethane at -5 - 20℃; for 14h; | 95% |
Stage #1: 2-[(tert-butoxycarbonyl)amino]-1,3-thiazole-5-carboxylic acid With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20℃; for 4h; Stage #2: 2-chloro-6-methylaniline With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 24h; | 48% |
ethyl acetoacetate
2-chloro-6-methylaniline
(Z)-ethyl 3-(2-chloro-6-methylphenylamino)but-2-enoate
Conditions | Yield |
---|---|
With zinc trifluoromethanesulfonate In neat (no solvent) at 20℃; for 0.25h; stereoselective reaction; | 94% |
With iron(III) trifluoromethanesulfonate In neat (no solvent) at 20℃; for 0.133333h; Green chemistry; | 93% |
2-chloro-6-methylaniline
2-chloro-6-methylbenzenediazonium tetrafluoroborate
Conditions | Yield |
---|---|
With tetrafluoroboric acid; sodium nitrite In ethanol; water at 0℃; | 94% |
3-oxo-propionic acid ethyl ester
thiourea
2-chloro-6-methylaniline
2-amino-N-(2-chloro-6-methylphenyl)-1,3-thiazole-5-carboxamide
Conditions | Yield |
---|---|
Stage #1: 3-oxo-propionic acid ethyl ester With sodium methylate In tetrahydrofuran at 20℃; for 0.166667h; Stage #2: 2-chloro-6-methylaniline In tetrahydrofuran for 0.75h; Reflux; Stage #3: thiourea Solvent; Further stages; | 92.31% |
Stage #1: 3-oxo-propionic acid ethyl ester; 2-chloro-6-methylaniline With sodium methylate In tetrahydrofuran for 0.75h; Reflux; Stage #2: With copper(ll) bromide In tetrahydrofuran for 1h; Reflux; Stage #3: thiourea In tetrahydrofuran at 20 - 25℃; for 0.25h; Reagent/catalyst; | 90.94% |
Conditions | Yield |
---|---|
Stage #1: 3-oxo-propionic acid ethyl ester With sodium methylate In tetrahydrofuran at 20℃; for 0.166667h; Stage #2: 2-chloro-6-methylaniline In tetrahydrofuran for 1h; Reflux; Stage #3: With copper(ll) bromide In tetrahydrofuran for 2h; Reagent/catalyst; Solvent; Reflux; | 91.6% |
Stage #1: 3-oxo-propionic acid ethyl ester With sodium methylate In tetrahydrofuran at 20℃; for 0.166667h; Stage #2: 2-chloro-6-methylaniline In tetrahydrofuran for 1h; Reflux; Stage #3: With copper(I) bromide In tetrahydrofuran for 2h; Reagent/catalyst; Solvent; Reflux; | 91.6% |
Stage #1: 3-oxo-propionic acid ethyl ester; 2-chloro-6-methylaniline With sodium methylate In tetrahydrofuran for 1h; Reflux; Stage #2: With copper(I) bromide In tetrahydrofuran for 2h; Solvent; Reflux; | 91.6% |
Conditions | Yield |
---|---|
With palladium diacetate; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate In toluene at 160℃; for 3h; microwave irradiation; | 91.5% |
4-oxo-5-{[(trifluoromethyl)sulfonyl]oxy}-4H-pyran-2-carboxylic acid
2-chloro-6-methylaniline
6-(2-chloro-6-methylphenylcarbamoyl)-4oxo-4H-pyran-3-yl trifluoromethanesulfonate
Conditions | Yield |
---|---|
With O-phenyl phosphorodichloridate; triethylamine In dichloromethane at 0℃; Inert atmosphere; | 90% |
(Z)-but-2-ene-1,4-diyl dimethanesulfonate
2-chloro-6-methylaniline
1-(2-Chloro-6-methyl-phenyl)-2,5-dihydro-1H-pyrrole
Conditions | Yield |
---|---|
In dichloromethane Ambient temperature; | 89% |
para-bromotoluene
2-chloro-6-methylaniline
N-(2'-chloro-6'-methylphenyl)-4-methylaniline
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; sodium t-butanolate; bis(dibenzylideneacetone)-palladium(0) In toluene at 60 - 90℃; Buchwald-Hartwig coupling; | 89% |
carbon disulfide
allyl bromide
2-chloro-6-methylaniline
S-allyl-N-(2-chloro-6-methylphenyl)dithiocarbamate
Conditions | Yield |
---|---|
With tin(II) chloride dihdyrate at 20℃; neat (no solvent); | 89% |
Conditions | Yield |
---|---|
With palladium diacetate; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate In toluene at 160℃; for 3h; microwave irradiation; | 88% |
2-chloro-4-morpholinothieno[3,2-d]pyrimidine-6-carboxylic acid
2-chloro-6-methylaniline
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide In ethyl acetate at 80℃; for 0.5h; | 86.8% |
2-chloro-4-morpholinothieno[3,2-d]pyrimidine-6-carbaldehyde
2-chloro-6-methylaniline
Conditions | Yield |
---|---|
With acetic acid In ethanol at 80℃; for 3h; | 86.5% |
benzoyl chloride
2-chloro-6-methylaniline
N-(2-chloro-6-methylphenyl)benzamide
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 0℃; for 3h; Inert atmosphere; | 86% |
With triethylamine In toluene Heating; | 70% |
With triethylamine In dichloromethane at 20℃; | 52% |
Schotten-Baumann reaction; | |
With triethylamine |
Benzoyl isothiocyanate
2-chloro-6-methylaniline
1-Benzoyl-3-(2-chloro-6-methyl-phenyl)-thiourea
Conditions | Yield |
---|---|
In benzene | 86% |
In acetone at 20℃; for 2h; |
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