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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

4-Iodo-2-methylaniline

Cas:13194-68-8

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Henan Tianfu Chemical Co., Ltd.

Product Name: 4-IODO-2-METHYLANILINE Synonyms: Aniline, 4-iodo-2-methyl-;Benzenamine, 4-iodo-2-methyl-;BUTTPARK 24\04-61;AURORA 1126;AKOS BBS-00007953;4-IODO-2-METHYLANILINE;4-IODO-2-METHYLBENZENAMINE;2-AMINO-5-IODOTOLUENE CAS: 1

13194-68-8 4-IODO-2-METHYLANILINE

Cas:13194-68-8

Min.Order:1 Kilogram

FOB Price: $8900.0

Type:Lab/Research institutions

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 13194-68-8 with competitive price

Cas:13194-68-8

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Benzenamine,4-iodo-2-methyl- 13194-68-8

Cas:13194-68-8

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Minstar Chemical Co., Ltd

Product Name: 4-IODO-2-METHYLANILINE CAS: 13194-68-8 MF: C7H8IN MW: 233.05 EINECS: 236-154-2 Mol File: 13194-68-8.mol 4-IODO-2-METHYLANILINE Structure 4-IODO-2-METHYLANILINE Chemical Properties Melting point 86-89 °C (lit.

4-IODO-2-METHYLANILINE

Cas:13194-68-8

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

4-Iodo-2-Methylbenzenamine

Cas:13194-68-8

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present

4-Iodo-2-methylaniline

Cas:13194-68-8

Min.Order:1 Gram

FOB Price: $1454.0

Type:Trading Company

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

2-Amino-5-iodotoluene

Cas:13194-68-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providing h

Factory Supply 4-iodo-2-methylaniline

Cas:13194-68-8

Min.Order:0

Negotiable

Type:Other

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Henan Wentao Chemical Product Co., Ltd.

We are leading fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...)

4-IODO-2-METHYLANILINECAS NO.: 13194-68-8

Cas:13194-68-8

Min.Order:1 Kilogram

FOB Price: $5.0

Type:Lab/Research institutions

inquiry

Enke Pharma-tech Co.,Ltd. (Cangzhou, China )

Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, intermediat

4-Iodo-2-methylaniline

Cas:13194-68-8

Min.Order:1 Metric Ton

FOB Price: $5.0 / 15.0

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:Grey to purple crystals Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:as per your request Application:Used as Pharmaceutical Intermediates,ect. T

4-IODO-2-METHYLANILINE

Cas:13194-68-8

Min.Order:10 Gram

Negotiable

Type:Trading Company

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

4-Iodo-2-Methylaniline cas no. 13194-68-8 98%

Cas:13194-68-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

4-Iodo-2-methylaniline

Cas:13194-68-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

4-iodo-2-methylaniline

Cas:13194-68-8

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

4-Iodo-2-Methylaniline

Cas:13194-68-8

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

4-Iodo-2-Methylaniline

Cas:13194-68-8

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

4-Iodo-2-Methylbenzenamine

Cas:13194-68-8

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Xi`an Eastling Biotech Co., Ltd.

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou

4-IODO-2-METHYLANILINE

Cas:13194-68-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hubei Taiho Chemical Co.,LTD

TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp

4-iodo-2-methylaniline

Cas:13194-68-8

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as

4-Iodo-2-methylaniline

Cas:13194-68-8

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Nanjing Fred Technology Co.,Ltd.

Fredchem focus on CRO/CMO business and its own R&D of API/Intermediates Package:Grams, Kilograms Application:Pharmaceutical field Transportation:According to customer request Port:Shanghai

4-Iodo-2-methylaniline

Cas:13194-68-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Antimex Chemical Limied

4-IODO-2-METHYLANILINEAppearance:Grey to purple crystals Storage:Protected from light, stored hermetically and in a dry place Package:25 kgs/drum Application:Pharmaceutical Intermediate Transportation:By sea or air

4-IODO-2-METHYLANILINE

Cas:13194-68-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Sartort Biopharma Co., Ltd

Best quality with low priceAppearance:Grey to purple crystals Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai

4-Iodo-2-methylaniline

Cas:13194-68-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Fandachem Co.,Ltd

2-Amino-5-iodotoluene cas 13194-68-8Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

2-Amino-5-iodotoluene cas 13194-68-8

Cas:13194-68-8

Min.Order:0

Negotiable

Type:Other

inquiry

Hunan Russell Chemicals Technology Co.,Ltd

low price and high purityAppearance:solid or liquid Storage:in sealed air resistant place Package:As customer require Application:Pharma;Industry;Agricultural Transportation:by sea or by airplane Port:any port in China

4-Iodo-2-methylaniline, 98% 13194-68-8

Cas:13194-68-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shanghai Yuanye Bio-Technology Co., Ltd.

Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers.Appearance:White powder Storage:keep sealed and keep from direct light Package:According client's requirements Application:pharmaceutica

4-Iodo-2-Methylaniline manufacturer

Cas:13194-68-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shenzhen Foris Technology Co. LTD

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

4-Iodo-2-methylaniline 13194-68-8

Cas:13194-68-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

4-IODO-2-METHYLANILINE

Cas:13194-68-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Beantown Chemical

in stock Application:13194-68-8

4-Iodo-2-methylaniline, 98%

Cas:13194-68-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

o-toluidine
95-53-4

o-toluidine

4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

Conditions
ConditionsYield
With N-iodo-succinimide In acetonitrile at 25 - 30℃; for 0.333333h; regioselective reaction;94.5%
With 1,4-dibenzyl-1,4-diazoniabicyclo[2.2.2]octane dichloroiodate In neat (no solvent) at 20℃; for 0.166667h; regioselective reaction;93%
With N,N,N-trimethylbenzenemethanaminium dichloroiodate; calcium carbonate In methanol; dichloromethane for 2h; Ambient temperature;92%
4-Bromo-2-methylaniline
583-75-5

4-Bromo-2-methylaniline

4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

Conditions
ConditionsYield
With copper(l) iodide; sodium iodide; N,N`-dimethylethylenediamine In 1,4-dioxane at 110℃; for 18h; Finkelstein Reaction; Inert atmosphere; Schlenk technique;90%
With iodine; sodium iodide In acetonitrile at 20℃; for 36h; Inert atmosphere; UV-irradiation; Green chemistry;75%
N-(2-methylphenyl)acetamide
120-66-1

N-(2-methylphenyl)acetamide

4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

Conditions
ConditionsYield
With Iodine monochloride Verseifung des entstandenen 5-Jod-2-acetamino-toluols;
With Iodine monochloride; acetic acid Verseifung des entstandenen 5-Jod-2-acetamino-toluols mit alkoholischer Salzsaeure;
4-iodo-2-methyl-1-nitro-benzene
52415-00-6

4-iodo-2-methyl-1-nitro-benzene

4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

Conditions
ConditionsYield
With ammonia; water; iron(II) sulfate at 60 - 70℃;
2-iodo-5,5-dimethyl-2-nitro-cyclohexane-1,3-dione
100377-05-7

2-iodo-5,5-dimethyl-2-nitro-cyclohexane-1,3-dione

o-toluidine
95-53-4

o-toluidine

4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

Conditions
ConditionsYield
With benzene
diethyl ether
60-29-7

diethyl ether

water
7732-18-5

water

iodine
7553-56-2

iodine

o-toluidine
95-53-4

o-toluidine

CaCO3

CaCO3

4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

Conditions
ConditionsYield
at 100℃;
sulfuric acid
7664-93-9

sulfuric acid

(4-amino-3-methyl-phenyl)-arsonic acid
860526-66-5

(4-amino-3-methyl-phenyl)-arsonic acid

potassium iodide

potassium iodide

4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

sulfuric acid
7664-93-9

sulfuric acid

bis-(4-amino-3-methyl-phenyl)-arsinic acid
860753-20-4

bis-(4-amino-3-methyl-phenyl)-arsinic acid

potassium iodide

potassium iodide

4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

o-toluidine
95-53-4

o-toluidine

A

2-iodo-6-methylbenzenamine

2-iodo-6-methylbenzenamine

B

4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

Conditions
ConditionsYield
With ammonium iodide; dihydrogen peroxide In acetic acid at 20℃; for 8h;
With dihydrogen peroxide; acetic acid; potassium iodide In water at 20℃; for 6h;
With N-iodo-succinimide; acetic acid In benzene at 20℃; for 72h; regioselective reaction;
4-nitro-3-methylaniline
611-05-2

4-nitro-3-methylaniline

4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 40 °C / Diazotization.man giesst die Diazoniumsulfatloesung in eine waessr. Loesung von KI
2: NH3; water; FeSO4 / 60 - 70 °C
View Scheme
formaldehyd
50-00-0

formaldehyd

4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

N-(4-iodo-2-methylphenyl)formamide
791594-20-2

N-(4-iodo-2-methylphenyl)formamide

Conditions
ConditionsYield
With acetic anhydride In tetrahydrofuran; toluene at 20℃;100%
4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

m-phenylenediamine
108-45-2

m-phenylenediamine

(E)-4-(2-(4-iodo-2-methylphenyl)diazenyl)benzene-1,3-diamine

(E)-4-(2-(4-iodo-2-methylphenyl)diazenyl)benzene-1,3-diamine

Conditions
ConditionsYield
Stage #1: 4-iodo-2-methylaniline With hydrogenchloride; sodium nitrite In water at 0℃; for 0.666667h;
Stage #2: m-phenylenediamine With hydrogenchloride In water at 0℃; for 0.5h;
100%
4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

4-azido-2-methylbenzeneamine

4-azido-2-methylbenzeneamine

Conditions
ConditionsYield
With copper(l) iodide; sodium azide; sodium L-ascorbate; (1S,2S)-N,N'-dimethyl-1,2-diaminocyclohexane In ethanol for 0.833333h; Heating;99%
4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

5-iodo-1H-indazole
55919-82-9

5-iodo-1H-indazole

Conditions
ConditionsYield
With acetic acid; sodium nitrite In water for 6h;99%
Stage #1: 4-iodo-2-methylaniline With tetrafluoroboric acid; sodium nitrite In water at 0℃;
Stage #2: With 18-crown-6 ether; potassium acetate In chloroform at 20℃; Further stages.;
With acetic acid; sodium nitrite In water at 10 - 20℃; for 6h;
Multi-step reaction with 2 steps
1.1: chloroform / 5 - 20 °C
1.2: 20 h / 70 °C
2.1: potassium hydroxide; water / tetrahydrofuran / 0.25 h
View Scheme
di-tert-butyl dicarbonate
24424-99-5

di-tert-butyl dicarbonate

4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

(4-iodo-2-methyl-phenyl)-carbamic acid tert-butyl ester
666746-27-6

(4-iodo-2-methyl-phenyl)-carbamic acid tert-butyl ester

Conditions
ConditionsYield
In toluene at 80℃; for 16h;99%
In toluene for 2h; Heating / reflux;
4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

N-(4-iodo-2-methylphenyl)iminodiacetic acid diethyl ester
1190892-36-4

N-(4-iodo-2-methylphenyl)iminodiacetic acid diethyl ester

Conditions
ConditionsYield
99%
4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

diethyl 2-ethoxymethylenemalonate
87-13-8

diethyl 2-ethoxymethylenemalonate

diethyl 2-(((4-iodo-2-methylphenyl)amino)methylene)malonate
951006-38-5

diethyl 2-(((4-iodo-2-methylphenyl)amino)methylene)malonate

Conditions
ConditionsYield
at 100℃; for 1h;98%
at 90 - 95℃; for 0.75h;
4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

methylamine
74-89-5

methylamine

3-methyl-4-amino-N-methyl aniline

3-methyl-4-amino-N-methyl aniline

Conditions
ConditionsYield
With copper(l) iodide; 6,7-dihydro-5H-quinolin-8-one oxime; potassium hydroxide In water at 25℃; for 24h; Inert atmosphere;95%
4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

2,2,2-Trichloroethyl chloroformate
17341-93-4

2,2,2-Trichloroethyl chloroformate

C10H9Cl3INO2

C10H9Cl3INO2

Conditions
ConditionsYield
With sodium hydroxide In water; ethyl acetate at 0 - 20℃; for 1h;95%
4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

phenylboronic acid
98-80-6

phenylboronic acid

3-methylbiphenyl-4-amine
63019-98-7

3-methylbiphenyl-4-amine

Conditions
ConditionsYield
With potassium carbonate In water at 90℃; for 8h; Suzuki coupling;92%
4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

3,5-diiodosalicylic acid
133-91-5

3,5-diiodosalicylic acid

2-Hydroxy-3,5-diiodo-N-(4-iodo-2-methyl-phenyl)-benzamide
90426-00-9

2-Hydroxy-3,5-diiodo-N-(4-iodo-2-methyl-phenyl)-benzamide

Conditions
ConditionsYield
With phosphorus trichloride In xylene at 140℃; for 4h;91%
4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

tris-iso-propylsilyl acetylene
89343-06-6

tris-iso-propylsilyl acetylene

2-methyl-4-[tris(1-methylethyl)silylethynyl]aniline

2-methyl-4-[tris(1-methylethyl)silylethynyl]aniline

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; for 20h; Sonogashira Cross-Coupling; Inert atmosphere;91%
4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

2,3,4,-trifluorobenzoic acid
61079-72-9

2,3,4,-trifluorobenzoic acid

PD 0169842
212628-45-0

PD 0169842

Conditions
ConditionsYield
With lithium hexamethyldisilazane In tetrahydrofuran at -78 - 20℃;90%
Stage #1: 2,3,4,-trifluorobenzoic acid With lithium hexamethyldisilazane In tetrahydrofuran at -78℃;
Stage #2: 4-iodo-2-methylaniline With lithium hexamethyldisilazane In tetrahydrofuran at -78 - 20℃;
88%
4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

3-bromo-4,5,6-trifluorobenzoic acid
212631-85-1

3-bromo-4,5,6-trifluorobenzoic acid

5-bromo-3,4-difluoro-2-(4-iodo-2-methyl-phenylamino)-benzoic acid
212628-46-1

5-bromo-3,4-difluoro-2-(4-iodo-2-methyl-phenylamino)-benzoic acid

Conditions
ConditionsYield
Stage #1: 5-bromo-2,3,4-trifluorobenzoic acid With lithium hexamethyldisilazane In tetrahydrofuran at -78℃;
Stage #2: 4-iodo-2-methylaniline With lithium hexamethyldisilazane In tetrahydrofuran at -78 - 20℃;
89%
With hydrogenchloride; lithium diisopropyl amide In tetrahydrofuran; n-heptane
With hydrogenchloride; lithium diisopropyl amide In tetrahydrofuran; n-heptane
4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

1-azido-4-iodo-2-methyl-benzene

1-azido-4-iodo-2-methyl-benzene

Conditions
ConditionsYield
Stage #1: 4-iodo-2-methylaniline With trifluoroacetic acid; sodium nitrite In water at 0℃; for 0.166667h;
Stage #2: With sodium azide In water at 20℃; for 2h; Further stages.;
89%
thiophosgene
463-71-8

thiophosgene

4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

4-iodo-1-isothiocyanato-2-methylbenzene
143014-18-0

4-iodo-1-isothiocyanato-2-methylbenzene

Conditions
ConditionsYield
In dichloromethane; water89%
With potassium carbonate In chloroform; water
With triethylamine In tetrahydrofuran at 0 - 20℃; for 2.5h; Inert atmosphere;
4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

C14H14INO2S
349090-50-2

C14H14INO2S

Conditions
ConditionsYield
In water at 20℃; for 0.416667h;89%
4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

methanesulfonyl chloride
124-63-0

methanesulfonyl chloride

N-(4-iodo-2-methylphenyl)methanesulfonamide
349090-90-0

N-(4-iodo-2-methylphenyl)methanesulfonamide

Conditions
ConditionsYield
In water at 20℃; for 0.583333h;87%
With pyridine In dichloromethane at 0℃; Reflux;55%
4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

benzyl bromide
100-39-0

benzyl bromide

4-benzylsulfanyl-2-methyl-phenylamine

4-benzylsulfanyl-2-methyl-phenylamine

Conditions
ConditionsYield
Stage #1: 4-iodo-2-methylaniline With tert.-butyl lithium; isopropylmagnesium chloride In tetrahydrofuran; diethyl ether; pentane at -78℃; for 0.5h;
Stage #2: With sulfur In tetrahydrofuran; diethyl ether; pentane at -78 - 20℃; for 0.5h;
Stage #3: benzyl bromide In tetrahydrofuran; diethyl ether; pentane at 0 - 20℃;
86%
pyrrolidine
123-75-1

pyrrolidine

4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

1-[2-(4-iodo-2-methylphenyl)diazen-1-yl]pyrrolidine
1394130-76-7

1-[2-(4-iodo-2-methylphenyl)diazen-1-yl]pyrrolidine

Conditions
ConditionsYield
Stage #1: 4-iodo-2-methylaniline With hydrogenchloride; sodium nitrite In water at 0℃; for 0.5h;
Stage #2: pyrrolidine With potassium carbonate In water; acetonitrile at 0 - 20℃; for 0.5h;
86%
4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

methyl ethynyl ketone
1423-60-5

methyl ethynyl ketone

(3Z)-4-[(4-iodo-2-methylphenyl)amino]but-3-en-2-one

(3Z)-4-[(4-iodo-2-methylphenyl)amino]but-3-en-2-one

Conditions
ConditionsYield
In ethanol at 20℃; for 5h;85%
N-(tert-butoxycarbonyl)-4-aminobutanoic acid
57294-38-9

N-(tert-butoxycarbonyl)-4-aminobutanoic acid

4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

4-(4-iodo-2-methylphenylamino)-4-oxobutylcarbamic acid tert-butyl ester

4-(4-iodo-2-methylphenylamino)-4-oxobutylcarbamic acid tert-butyl ester

Conditions
ConditionsYield
With 2-(1H-9-azabenzotriazol-1-yl)-1,1,3,3-tetramethyluroniumhexafluorophosphate; potassium carbonate In acetonitrile at 20℃; for 3h;84.2%
4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

4-iodo-2-methylbenzenediazonium tetrafluoroborate

4-iodo-2-methylbenzenediazonium tetrafluoroborate

Conditions
ConditionsYield
Stage #1: 4-iodo-2-methylaniline With tetrafluoroboric acid at 0℃;
Stage #2: With sodium nitrite at 0 - 20℃; for 3h; Further stages.;
84%
N-(1,1-dimethyl-2-methylthioethyl)-6-iodophthalic acid isoimide
866639-18-1

N-(1,1-dimethyl-2-methylthioethyl)-6-iodophthalic acid isoimide

4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

N2-(1,1-dimethyl-2-methylthioethyl)-3-iodo-N1-(4-iodo-2-methylphenyl)phthalamide
474557-91-0

N2-(1,1-dimethyl-2-methylthioethyl)-3-iodo-N1-(4-iodo-2-methylphenyl)phthalamide

Conditions
ConditionsYield
In acetonitrile for 0.166667h;84%
2-Picolinic acid
98-98-6

2-Picolinic acid

4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

N-(4-iodo-2-methylphenyl)picolinamide

N-(4-iodo-2-methylphenyl)picolinamide

Conditions
ConditionsYield
With triethylamine; trichlorophosphate In dichloromethane at 0℃; for 2h;84%
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

N-(4-iodo-2-methylphenyl)-3-methylbut-2-enamide

N-(4-iodo-2-methylphenyl)-3-methylbut-2-enamide

Conditions
ConditionsYield
With pyridine In dichloromethane at 20℃; for 6h;84%
4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

methyl vinyl ketone
78-94-4

methyl vinyl ketone

6-iodo-8,4-dimethylquinoline

6-iodo-8,4-dimethylquinoline

Conditions
ConditionsYield
With indium(III) chloride; silica gel for 0.166667h; Cycloaddition; Irradiation;83%
With indium(III) chloride; silica gel for 0.166667h; microwave irradiation;83%
4-iodo-2-methylaniline
13194-68-8

4-iodo-2-methylaniline

6-hydroxy-2-methyl-4H-benzo[d][1,3]oxazin-4-one

6-hydroxy-2-methyl-4H-benzo[d][1,3]oxazin-4-one

6-hydroxy-3-(4-iodo-2-methylphenyl)-2-methylquinazolin-4(3H)-one
1214739-68-0

6-hydroxy-3-(4-iodo-2-methylphenyl)-2-methylquinazolin-4(3H)-one

Conditions
ConditionsYield
With acetic acid at 120℃; for 12h;80%

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