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inquiryProduct Name: BIS(HEXAMETHYLENE)TRIAMINE Synonyms: TIMTEC-BB SBB006597;BIS(6-AMINOHEXYL)AMINE;BIS(HEXAMETHYLENE)TRIAMINE;6,6'-IMINODIHEXYLAMINE;1,13-diamino-7-azatridecane;6,6’-diamino-dihexylamin
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Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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inquiryBis(hexamethylene)triamine50%;95% (Bis(6-aminohexyl)amine;7-azatridecane-1,13-diamine),CAS No.:143-23-7 from fandachem Package:as customers' requirements Application:intermediate Transportation:by air, by sea, by express Port:Shanghai, China
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8-(2-(trimethylsilyl)ethanesulfonyl)-1,8,15-triazapentadecane
1,8,15-triazapentadecane
Conditions | Yield |
---|---|
With cesium fluoride In N,N-dimethyl-formamide at 100℃; | 46% |
N1,N13-diacetyl-1,13-diamino-7-azatridecane
1,8,15-triazapentadecane
Conditions | Yield |
---|---|
With hydrogenchloride for 2h; Heating; Yield given; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 78 percent / 24 h / 100 °C 2: Raney Ni / benzene / 7 h / Heating 3: 2N HCl / 2 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 2: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr View Scheme |
mono-N-acetylhexamethylenediamine
1,8,15-triazapentadecane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Raney Ni / benzene / 7 h / Heating 2: 2N HCl / 2 h / Heating View Scheme |
6-amino-1-hexanol
A
hexamethylene imine
B
1,6-Hexanediamine
C
6-(azepan-1-yl)hexan-1-amine
D
1,8,15-triazapentadecane
Conditions | Yield |
---|---|
With ammonia; hydrogen In tert-butyl alcohol at 220℃; under 120012 Torr; for 6h; | A 33 %Chromat. B 20.7 %Chromat. C n/a D n/a |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 2: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr View Scheme |
6-amino-1-hexanol
A
hexamethylene imine
B
6-(azepan-1-yl)hexan-1-amine
C
1,8,15-triazapentadecane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 2: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 2: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 3: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr View Scheme |
6-amino-1-hexanol
A
6-(azepan-1-yl)hexan-1-amine
B
1,8,15-triazapentadecane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 2: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 3: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr View Scheme |
1,6-Hexanediamine
A
hexamethylene imine
B
6-(azepan-1-yl)hexan-1-amine
C
1,8,15-triazapentadecane
Conditions | Yield |
---|---|
With ammonia; hydrogen In tert-butyl alcohol at 220℃; under 120012 Torr; for 6h; |
hexamethylene imine
A
1,6-Hexanediamine
B
6-(azepan-1-yl)hexan-1-amine
C
1,8,15-triazapentadecane
Conditions | Yield |
---|---|
With ammonia; hydrogen In tert-butyl alcohol at 220℃; under 120012 Torr; for 6h; |
1,6-hexanediol
A
hexamethylene imine
B
1,6-Hexanediamine
C
6-(azepan-1-yl)hexan-1-amine
D
1,8,15-triazapentadecane
Conditions | Yield |
---|---|
With ammonia; hydrogen In tert-butyl alcohol at 220℃; under 120012 Torr; for 4.5h; Kinetics; Temperature; Pressure; Time; | A 31.9 %Chromat. B 38.4 %Chromat. C n/a D n/a |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrogen; ammonia; / tert-butyl alcohol / 4.5 h / 220 °C / 120012 Torr 2: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr View Scheme | |
Multi-step reaction with 2 steps 1: hydrogen; ammonia; / tert-butyl alcohol / 4.5 h / 220 °C / 120012 Torr 2: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr View Scheme | |
Multi-step reaction with 2 steps 1: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 2: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr View Scheme | |
Multi-step reaction with 3 steps 1: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 2: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 3: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr View Scheme |
1,6-hexanediol
A
hexamethylene imine
B
6-(azepan-1-yl)hexan-1-amine
C
1,8,15-triazapentadecane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrogen; ammonia; / tert-butyl alcohol / 4.5 h / 220 °C / 120012 Torr 2: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr View Scheme | |
Multi-step reaction with 2 steps 1: hydrogen; ammonia; / tert-butyl alcohol / 4.5 h / 220 °C / 120012 Torr 2: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr View Scheme | |
Multi-step reaction with 2 steps 1: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 2: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr View Scheme | |
Multi-step reaction with 2 steps 1: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 2: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr View Scheme | |
Multi-step reaction with 3 steps 1: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 2: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 3: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: hydrogen; ammonia; / tert-butyl alcohol / 4.5 h / 220 °C / 120012 Torr 2: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 3: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr View Scheme | |
Multi-step reaction with 3 steps 1: hydrogen; ammonia; / tert-butyl alcohol / 4.5 h / 220 °C / 120012 Torr 2: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 3: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr View Scheme | |
Multi-step reaction with 3 steps 1: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 2: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 3: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr View Scheme | |
Multi-step reaction with 4 steps 1: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 2: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 3: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 4: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr View Scheme |
1,6-hexanediol
A
6-(azepan-1-yl)hexan-1-amine
B
1,8,15-triazapentadecane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: hydrogen; ammonia; / tert-butyl alcohol / 4.5 h / 220 °C / 120012 Torr 2: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 3: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr View Scheme | |
Multi-step reaction with 3 steps 1: hydrogen; ammonia; / tert-butyl alcohol / 4.5 h / 220 °C / 120012 Torr 2: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 3: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr View Scheme | |
Multi-step reaction with 3 steps 1: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 2: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 3: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr View Scheme | |
Multi-step reaction with 4 steps 1: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 2: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 3: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr 4: hydrogen; ammonia; / tert-butyl alcohol / 6 h / 220 °C / 120012 Torr View Scheme |
hexanedinitrile
A
hexamethylene imine
B
1,6-Hexanediamine
D
1-amino-5-cyanopentane
E
1,8,15-triazapentadecane
Conditions | Yield |
---|---|
With 1-butyl-3-methylimidazolium hydroxide; hydrogen In ethanol at 349.84℃; under 15001.5 Torr; for 6h; Reagent/catalyst; Temperature; Pressure; Time; Flow reactor; Sealed tube; Inert atmosphere; Ionic liquid; |
1,8,15-triazapentadecane
p-toluenesulfonyl chloride
N,N',N"-tritosyl-7-aza-tridecanetriamine
Conditions | Yield |
---|---|
With potassium carbonate In water at 70℃; for 24h; | 98% |
Conditions | Yield |
---|---|
95% | |
In toluene at 80℃; for 20h; Inert atmosphere; | 80% |
In toluene at 60℃; | |
In 5,5-dimethyl-1,3-cyclohexadiene at 80℃; for 8h; Inert atmosphere; |
Conditions | Yield |
---|---|
With ((CH3)3CCO)2O In further solvent(s) heating mixt. of 1 equiv. of triamine deriv., 5 equiv. of chromium compd., 1 equiv. of cobalt compd. and 6 equiv. of pivalic anhydride in pivalic acid at 160°C for 30 h; | 92% |
Conditions | Yield |
---|---|
With ((CH3)3CCO)2O In further solvent(s) heating mixt. of 1 equiv. of triamine deriv., 5 equiv. of chromium compd., 1 equiv. of nickel compd. and 6 equiv. of pivalic anhydride in pivalic acid at 160°C for 30 h; | 92% |
di-tert-butyl dicarbonate
1,8,15-triazapentadecane
di-tert-butyl (((tert-butoxycarbonyl)azanediyl)bis(hexane-6,1-diyl))dicarbamate
Conditions | Yield |
---|---|
In methanol for 12h; | 91% |
In dichloromethane for 12h; | 82% |
7-chloro-4-bromo-quinoline
1,8,15-triazapentadecane
Conditions | Yield |
---|---|
With potassium phosphate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In 1,4-dioxane; water at 120℃; for 14h; Sealed tube; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 1h; Cooling with ice; | 86% |
Conditions | Yield |
---|---|
With 1,2,2,6,6-pentamethylpiperidine In N,N-dimethyl-formamide at 20℃; | 85% |
2,2,2-trichloro-1-(4-chloro-1H-pyrrol-2-yl)ethan-1-one
1,8,15-triazapentadecane
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 18h; Inert atmosphere; | 84% |
Conditions | Yield |
---|---|
With ((CH3)3CCO)2O In further solvent(s) heating mixt. of 1 equiv. of triamine deriv., 5 equiv. of chromium compd., 1 equiv. of manganese compd. and 6 equiv. of pivalic anhydride in pivalic acid at 160°C for 30 h; | 81% |
1,8,15-triazapentadecane
Glyoxilic acid
[6-(6-amino-hexylamino)-hexylamino]-acetic acid
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In methanol at 20℃; | 80% |
1,8,15-triazapentadecane
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran; methanol at 20℃; for 16h; | 80% |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In methanol; acetonitrile at 50℃; for 5h; | 79% |
Conditions | Yield |
---|---|
Stage #1: 1,8,15-triazapentadecane; Deoxycholic acid With benzotriazol-1-ol; triethylamine In N,N-dimethyl-formamide at 0℃; for 0.166667h; Inert atmosphere; Stage #2: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 0 - 25℃; for 24h; Inert atmosphere; | 79% |
4,5-dibromopyrrol-2-yl trichloromethyl ketone
1,8,15-triazapentadecane
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 18h; Inert atmosphere; | 78% |
In tetrahydrofuran at 19℃; for 36h; | 68% |
Conditions | Yield |
---|---|
With triethylamine In chloroform | 75% |
Conditions | Yield |
---|---|
With ((CH3)3CCO)2O In further solvent(s) heating mixt. of 1 equiv. of triamine deriv., 5 equiv. of chromium compd., 1 equiv. of zinc compd. and 6 equiv. of pivalic anhydride in pivalic acid at 160°C for 30 h; | 75% |
1,8,15-triazapentadecane
N,N'-bis-Boc-S-methyl-isothiourea
Conditions | Yield |
---|---|
In tetrahydrofuran; methanol at 50℃; for 16h; | 74% |
Conditions | Yield |
---|---|
Stage #1: 1,8,15-triazapentadecane; cholic acid With benzotriazol-1-ol; triethylamine In N,N-dimethyl-formamide at 0℃; for 0.166667h; Inert atmosphere; Stage #2: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 0 - 25℃; for 24h; Inert atmosphere; | 72% |
1,8,15-triazapentadecane
1,1‘-(azanediylbis(hexane-6,1-diyl))diguanidine
Conditions | Yield |
---|---|
In ethanol; water at 20℃; for 16h; | 71% |
With hydrogen bromide; acetic acid In ethanol; water at 20℃; for 16h; | 71% |
1,6-Hexanediamine
hexan-1-amine
1,8,15-triazapentadecane
hexamethylene imine
Conditions | Yield |
---|---|
70% |
1,8,15-triazapentadecane
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran; methanol at 20℃; for 16h; | 69% |
di-tert-butyl dicarbonate
1,8,15-triazapentadecane
N1-Boc-N6-(6-(Boc-amino)hexyl)hexane-1,6-diamine
Conditions | Yield |
---|---|
In methanol at -80℃; for 1h; | 68% |
Conditions | Yield |
---|---|
With ((CH3)3CCO)2O In further solvent(s) heating mixt. of 1 equiv. of triamine deriv., 5 equiv. of chromium compd., 1 equiv. of copper compd. and 6 equiv. of pivalic anhydride in pivalic acid at 160°C for 30 h; | 64% |
Conditions | Yield |
---|---|
Stage #1: 1,8,15-triazapentadecane; cholic acid With benzotriazol-1-ol; triethylamine In N,N-dimethyl-formamide at 0℃; for 0.166667h; Inert atmosphere; Stage #2: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 0 - 25℃; for 24h; Inert atmosphere; | 62% |
1,8,15-triazapentadecane
benzaldehyde
N1-benzyl-N6-(6-(benzylamino)hexyl)hexane-1,6-diamine
Conditions | Yield |
---|---|
Stage #1: 1,8,15-triazapentadecane; benzaldehyde In isopropyl alcohol at 0 - 20℃; for 2h; Stage #2: With hydrogen; palladium 10% on activated carbon In isopropyl alcohol under 1500.15 Torr; for 16h; | 61% |
2,6-bis-tert-butoxycarbonylamino-hexanoic acid
1,8,15-triazapentadecane
Conditions | Yield |
---|---|
Stage #1: 2,6-bis-tert-butoxycarbonylamino-hexanoic acid With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane; N,N-dimethyl-formamide at 0℃; Stage #2: 1,8,15-triazapentadecane In dichloromethane; N,N-dimethyl-formamide for 48h; | 60% |
1,8,15-triazapentadecane
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In methanol; acetonitrile at 50℃; for 5h; | 57% |
Conditions | Yield |
---|---|
In isopropyl alcohol for 16h; Heating / reflux; | 52% |
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