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inquiryzirconium(IV) chloride
isopropyl alcohol
zirconium(IV) tetraisopropoxide 2-propanol
Conditions | Yield |
---|---|
In not given N2 atmosphere; |
Conditions | Yield |
---|---|
In isopropyl alcohol according Shreider, Turevskaya, Kozlova, Turova; Izv. Akad. Nauk SSR. Ser. Khim., No.8, 1687-1692 (1981);; recrystd. in i-PrOH;;; | |
In not given Electrolysis; Zr anode, Zr cathode, Ar-atmosphere, stirring, 110 V/0.23 A, 15 h; soln.contg. various salts (Bu4NBr, Bu4NBF4, NaBr or other); crystn. on cooling; elem. anal.; | |
With Bu4NBr In neat (no solvent) byproducts: H2; Electrochem. Process; Ar, at 110 V for 15 h; recrystd. from alcohol; elem. anal.; | |
With LiCl In isopropyl alcohol Electrochem. Process; anodic dissoln. in anhyd. alcohol (supporting electrolyte LiCl), according to: V. A. Shreider, E. P. Turevskaya, N. I. Kozlova, N. Ya. Turova, Inorg. Chim. Acta 53 (1981) 73; recrystn. (isopropanol); |
2-Hydroxymethylpyridine
zirconium(IV) tetraisopropoxide 2-propanol
C18H26N2O4Zr
Conditions | Yield |
---|---|
In cyclohexane at 20℃; Schlenk technique; Inert atmosphere; | 100% |
zirconium(IV) tetraisopropoxide 2-propanol
tris(tert-butoxy)silanol
[Zr(O-i-Pr)3(OSi(O-t-Bu)3)]
Conditions | Yield |
---|---|
In benzene soln. (HOSi(O-t-Bu)3) in benzene was added to soln.(Zr(O-i-Pr)4*i-PrOH) in benzene (1:1), refluxed for 4 h; react. mixt. was concd. in vacuo; elem. anal.; | 99% |
zirconium(IV) tetraisopropoxide 2-propanol
tris(tert-butoxy)silanol
[Zr(O-i-Pr)2(OSi(O-t-Bu)3)2]
Conditions | Yield |
---|---|
In benzene soln. (HOSi(O-t-Bu)3) in benzene was added to soln.(Zr(O-i-Pr)4*i-PrOH) in benzene (2:1), refluxed for 8 h; react. mixt. was concd. in vacuo; elem. anal.; | 99% |
zirconium(IV) tetraisopropoxide 2-propanol
C34H55NO2
C40H67NO4Zr
Conditions | Yield |
---|---|
In diethyl ether at -35 - 20℃; for 2h; Inert atmosphere; Schlenk technique; Glovebox; | 99% |
zirconium(IV) tetraisopropoxide 2-propanol
C33H53NO2
C42H74NO5Zr
Conditions | Yield |
---|---|
In diethyl ether at -35 - 0℃; for 2h; Inert atmosphere; Glovebox; Schlenk technique; | 99% |
zirconium(IV) tetraisopropoxide 2-propanol
Hf(OiPr)4·HOiPr
C42H74HfNO5
Conditions | Yield |
---|---|
In diethyl ether at -35 - 0℃; for 4h; Inert atmosphere; Glovebox; Schlenk technique; | 99% |
zirconium(IV) tetraisopropoxide 2-propanol
triethanolamine
zirconium bis(triethanolaminate)
Conditions | Yield |
---|---|
In benzene byproducts: i-PrOH; 2 equiv. of triethanolamine was added to C6H6 soln. of Zr-complex, reflux for 12 h with recovering of i-PrOH as azeotrope; mixt. was allowed to stand to room temp., volatiles were removed in vac., elem. anal.; | 97% |
zirconium(IV) tetraisopropoxide 2-propanol
furan-2-carboxylic acid
Conditions | Yield |
---|---|
In benzene byproducts: iPrOH; to soln. of Zr compd. ligand added (1:3), refluxed for 8 h; stood, washed with EtOH, dried (E-2 torr, 4 h); elem. anal.; | 96% |
zirconium(IV) tetraisopropoxide 2-propanol
furan-2-carboxylic acid
Conditions | Yield |
---|---|
In benzene byproducts: iPrOH; to soln. of Zr compd. ligand added (1:1), refluxed for 6 h; stood, washed with EtOH, dried (E-2 torr, 4 h); elem. anal.; | 96% |
indole-3-acetic acid
zirconium(IV) tetraisopropoxide 2-propanol
Conditions | Yield |
---|---|
In benzene byproducts: iPrOH; to soln. of Zr compd. ligand added (1:2), refluxed for 6 h; stood, washed with EtOH, dried (E-2 torr, 4 h); elem. anal.; | 94% |
zirconium(IV) tetraisopropoxide 2-propanol
4-Methylbenzyl alcohol
[Zr(O-CH2-4-MeC6H4)4]2
Conditions | Yield |
---|---|
In toluene byproducts: isopropanol; Schlenk techniques or glovebox used under Ar, soln. of Zr(O-iPr)4(HO-iPr) (0.26 mmol) in toluene added to soln. of 4-MeC6H4CH2OH (1.03 mmol) in toluene at -25 °C, allowed to reach ambient temp., stirred for 24h; solvent removed under vac., crystd. from toluene at -25 °C, filtrated, dried in vac.; elem. anal.; | 93% |
zirconium(IV) tetraisopropoxide 2-propanol
Conditions | Yield |
---|---|
In toluene at 20℃; for 24h; Inert atmosphere; | 93% |
zirconium(IV) tetraisopropoxide 2-propanol
2-[(2,6-diisopropylphenyl)imino]methyl-4,6-dibromophenole
Conditions | Yield |
---|---|
In toluene at -25 - 20℃; for 30h; Glovebox; Inert atmosphere; | 92% |
Pentachlorophenol
zirconium(IV) tetraisopropoxide 2-propanol
[Zr(O-C6Cl5)4(HO-iPr)]2
Conditions | Yield |
---|---|
In toluene byproducts: isopropanol; Schlenk techniques or glovebox used under Ar, soln. of Zr(O-iPr)4(HO-iPr) (0.26 mmol) in toluene added to soln. of C6Cl5OH (1.03 mmol) in toluene at -25 °C, allowed to reach ambient temp., stirred for 24 h; solvent removed under vac., crystd. from toluene at -25 °C, filtrated, dried in vac.; elem. anal.; | 91% |
zirconium(IV) tetraisopropoxide 2-propanol
4-Iodophenol
[Zr(O-4-IC6H4)4(HO-iPr)]2
Conditions | Yield |
---|---|
In toluene byproducts: isopropanol; Schlenk techniques or glovebox used under Ar, soln. of Zr(O-iPr)4(HO-iPr) (0.26 mmol) in toluene added to soln. of 4-IC6H4OH (1.03 mmol) in toluene at -25 °C, allowed to reach ambient temp., stirred for 24 h; solvent removed under vac., crystd. from toluene at -25 °C, filtrated, dried in vac.; elem. anal.; | 91% |
zirconium(IV) tetraisopropoxide 2-propanol
furan-2-carboxylic acid
Conditions | Yield |
---|---|
In benzene byproducts: iPrOH; to soln. of Zr compd. ligand added (1:2), refluxed for 6 h; stood, washed with EtOH, dried (E-2 torr, 4 h); elem. anal.; | 90% |
indole-3-acetic acid
zirconium(IV) tetraisopropoxide 2-propanol
Conditions | Yield |
---|---|
In benzene byproducts: iPrOH; to soln. of Zr compd. ligand added (1:3), refluxed for 8 h; stood, washed with EtOH, dried (E-2 torr, 4 h); elem. anal.; | 90% |
zirconium(IV) tetraisopropoxide 2-propanol
4-indol-3-yl-butyric acid
Conditions | Yield |
---|---|
In benzene byproducts: iPrOH; to soln. of Zr compd. ligand added (1:3), refluxed for 10 H; stood, washed with EtOH, dried (E-2 torr, 4 h); elem. anal.; | 90% |
4-Fluorophenol
zirconium(IV) tetraisopropoxide 2-propanol
[Zr(O-4-FC6H4)4(HO-iPr)]2
Conditions | Yield |
---|---|
In toluene byproducts: isopropanol; Schlenk techniques or glovebox used under Ar, soln. of Zr(O-iPr)4(HO-iPr) (0.26 mmol) in toluene added to soln. of 4-FC6H4OH (1.03 mmol) in toluene at -25 °C, allowed to reach ambient temp., stirred for 24 h; solvent removed under vac., crystd. from toluene at -25 °C, filtrated, dried in vac.; elem. anal.; | 90% |
zirconium(IV) tetraisopropoxide 2-propanol
2-fluorophenol
[Zr(O-2-FC6H4)4(HO-iPr)]2
Conditions | Yield |
---|---|
In toluene byproducts: isopropanol; Schlenk techniques or glovebox used under Ar, soln. of Zr(O-iPr)4(HO-iPr) (0.26 mmol) in toluene added to soln. of 2-FC6H4OH (1.03 mmol) in toluene at -25 °C, allowed to reach ambient temp., stirred for 24 h; solvent removed under vac., crystd. from toluene at -25 °C, filtrated, dried in vac.; elem. anal., XRD; | 90% |
zirconium(IV) tetraisopropoxide 2-propanol
Conditions | Yield |
---|---|
In toluene at 20℃; for 24h; Inert atmosphere; | 90% |
zirconium(IV) tetraisopropoxide 2-propanol
para-tert-butylphenol
[Zr(O-4-tBuC6H4)4]2
Conditions | Yield |
---|---|
In toluene byproducts: isopropanol; Schlenk techniques or glovebox used under Ar, soln. of Zr(O-iPr)4(HO-iPr) (0.26 mmol) in toluene added to soln. of 4-tBuC6H4OH (1.03 mmol) in toluene at -25 °C, allowed to reach ambient temp., stirred for 24 h; solvent removed under vac., crystd. from toluene at -25 °C, filtrated, dried in vac.; elem. anal.; | 89% |
Conditions | Yield |
---|---|
In toluene byproducts: isopropanol; Schlenk techniques or glovebox used under Ar, soln. of Zr(O-iPr)4(HO-iPr) (0.26 mmol) in toluene added to soln. of 4-MeC6H4OH (1.03 mmol) in toluene at -25 °C, allowed to reach ambient temp., stirred for 24 h; solvent removed under vac., crystd. from toluene at -25 °C, filtrated, dried in vac.; elem. anal.; | 89% |
zirconium(IV) tetraisopropoxide 2-propanol
4-indol-3-yl-butyric acid
Conditions | Yield |
---|---|
In benzene byproducts: iPrOH; to soln. of Zr compd. ligand added (1:1), refluxed for 8 h; stood, washed with EtOH, dried (E-2 torr, 4 h); elem. anal.; | 88% |
zirconium(IV) tetraisopropoxide 2-propanol
4-Methoxybenzyl alcohol
[Zr(O-CH2-4-OMeC6H4)4]2
Conditions | Yield |
---|---|
In toluene byproducts: isopropanol; Schlenk techniques or glovebox used under Ar, soln. of Zr(O-iPr)4(HO-iPr) (0.26 mmol) in toluene added to soln. of 4-MeOC6H4CH2OH (1.03 mmol) intoluene at -25 °C, allowed to reach ambient temp., stirred for 2 4 h; solvent removed under vac., crystd. from toluene at -25 °C, filtrated, dried in vac.; elem. anal.; | 88% |
zirconium(IV) tetraisopropoxide 2-propanol
3-Trifluoromethylphenol
[Zr(O-3-CF3C6H4)4(HO-iPr)]2
Conditions | Yield |
---|---|
In toluene byproducts: isopropanol; Schlenk techniques or glovebox used under Ar, soln. of Zr(O-iPr)4(HO-iPr) (0.26 mmol) in toluene added to soln. of 3-CF3C6H4OH (1.03 mmol) in toluene at -25 °C, allowed to reach ambient temp., stirred for 24 h; solvent removed under vac., crystd. from toluene at -25 °C, filtrated, dried in vac.; elem. anal.; | 88% |
zirconium(IV) tetraisopropoxide 2-propanol
2-monochlorophenol
[Zr(O-2-ClC6H4)4(HO-iPr)]2
Conditions | Yield |
---|---|
In toluene byproducts: isopropanol; Schlenk techniques or glovebox used under Ar, soln. of Zr(O-iPr)4(HO-iPr) (0.26 mmol) in toluene added to soln. of 2-ClC6H4OH (1.03 mmol) in toluene at -25 °C, allowed to reach ambient temp., stirred for 24 h; solvent removed under vac., crystd. from toluene at -25 °C, filtrated, dried in vac.; elem. anal., XRD; | 88% |
zirconium(IV) tetraisopropoxide 2-propanol
(2Z)-2-Amino-3-{[(1E)-(2-hydroxyphenyl)methylidene]-amino}but-2-enedinitrile
Conditions | Yield |
---|---|
In toluene at 20℃; for 24h; Inert atmosphere; | 88% |
zirconium(IV) tetraisopropoxide 2-propanol
2-(((3,5-di-tert-butyl-2-hydroxybenzyl)(2-hydroxyethyl)amino)methyl)-4,6-di-tert-butylphenol
toluene
Conditions | Yield |
---|---|
for 12h; Glovebox; Schlenk technique; Inert atmosphere; | 87.5% |
2,5-dimethyl-2,5-hexanediol
zirconium(IV) tetraisopropoxide 2-propanol
Conditions | Yield |
---|---|
In benzene byproducts: isopropyl alcohol; to a benzene soln. of Zr(OPr-i)4 was added a soln. of glycol in benzene,the mixt. was refluxed for 12 h, cooled to room temp.; isopropanol was sepd. during the reaction azeotropically, the volatiles were removed at room temp. under reduced pressure, recrystd. from toluene-hexane at -20°C; elem. anal.; | 87% |
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